CN106221341A - A kind of preparation method of weather resistant non-toxic pigment - Google Patents
A kind of preparation method of weather resistant non-toxic pigment Download PDFInfo
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- CN106221341A CN106221341A CN201610636555.4A CN201610636555A CN106221341A CN 106221341 A CN106221341 A CN 106221341A CN 201610636555 A CN201610636555 A CN 201610636555A CN 106221341 A CN106221341 A CN 106221341A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/06—Artists' paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/41—Organic pigments; Organic dyes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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Abstract
The invention discloses the preparation method of a kind of weather resistant non-toxic pigment, belong to study article synthesis field.The present invention is exposed to the sun aging under sunlight after first being cleaned by Carnis Mactrae shell, powder it is sintered into after pulverizing and sieving, react under ultrasound condition with water again and be dispersed into white homogenate, with warm water soaking after subsequently straw being prescinded, again short stalk is laid on fermenter base, after white homogenate bedding, re-lay rice paper, sealed fermenting after adding water, high-speed stirring mixes mixing homogenate again, is uniformly mixed so as to obtain base material in proportion with brown sugar and glutinous rice flour, then by itself and water, dyestuff is mixed in proportion, and obtains weather resistant non-toxic pigment after excusing from death is uniformly dispersed.Gained pigment of the present invention can stably be deposited, do not have precipitation and lamination, attachment fastness and color saturation good, safety non-toxic, after using this pigment to be depicted as picture, can long-term storage colour-fast, can large-scale promotion use.
Description
Technical field
The invention discloses the preparation method of a kind of weather resistant non-toxic pigment, belong to study article synthesis field.
Background technology
With oil painting etc., watercolor is a difference in that it has two basic features: one is that picture has penetrating regarding mostly
Feel and feel；Two is the mobility slept in painting process, has thereby resulted in watercolor and has been different from appearance style and features and the wound of other pictures kind
Making the difference of skill and technique, watercolor presents transparent, slim and graceful, beautiful and moistening is smooth, the warmest gorgeous sunlight, or deeply
Heavy vast ocean, the most bright and the most beautiful bright-colored HUAMU or the cloud of chilly haze, arouse watercolor painter's heart invariably
Color impulsion and performance desire, usually can draw fantasy magnificent picture.
And watercolors are the key factors being related to watercolor, pigment is used to powder or the slurry like material of coloring.
The media such as water, oils and fats or organic solvent do not dissolve, but can disperse in these media equably and medium can be made to colour, and
There is again certain covering power.The pigment basic demand granule of the fine arts is the finest and the smoothest more good, and color is the most bright-coloured more good, the most lasting not
Variable color is the best.
But, in traditional drawing art painting, osmosis type and the chemical instability of dyestuff used result in gained
Works have the critical defect being difficult to preserve.Dyestuff with solvent penetration in painting process, surface is the most dry when having solvent, meeting
Producing and cause the problem of variable color to picture infiltration, this is that painter is not intended to see.This phenomenon of osmosis can affect or disobey
Back of the body painter creates thought expression on works；It addition, the poor chemical stability of dyestuff, in illumination, air in oxygen, air
Under the factor effects such as humidity, understand variable color, fade, cause works to lose original artistic charm and value, preserve the life-span the most significantly
Shorten.
Summary of the invention
The technical problem that present invention mainly solves: occur during preparation and use for tradition watercolors, change
Learn poor stability, in illumination, air in oxygen, air under the factor effect such as humidity, can variable color, fade, cause works to lose former
Some artistic charms and value, the problem that the preservation life-span is also greatly shortened, it is provided that the preparation side of a kind of weather resistant non-toxic pigment
Method, the present invention is exposed to the sun aging under sunlight, is sintered into powder after pulverizing and sieving after first being cleaned by Carnis Mactrae shell, then with water ultrasonic
Under the conditions of react and be dispersed into white homogenate, with warm water soaking after being prescinded by straw subsequently, shorter stalk is laid on fermenter base,
With white homogenate bedding after, re-lay rice paper, sealed fermenting after adding water, then high-speed stirring mix mixing homogenate, with brown sugar and Oryza glutinosa
Powder is uniformly mixed so as to obtain base material in proportion, then by itself and water, dyestuff is mixed in proportion, and obtains weather resistant nontoxic after excusing from death is uniformly dispersed
Pigment.Gained pigment of the present invention can stably be deposited, and does not haves precipitation and lamination, attachment fastness and color saturation are good, peace
Atoxic, after using this pigment to be depicted as picture, can long-term storage colour-fast, can large-scale promotion use.
In order to solve above-mentioned technical problem, the technical solution adopted in the present invention is:
(1) weigh 3～5kg Carnis Mactrae shells, after manually repeatedly cleaning 3～5 times with deionized water, be placed under sunlight and be exposed to the sun 5～7
My god, then pour in Universalpulverizer, cross 120～180 mesh sieves after pulverizing, collect the shell powder after sieving, proceed in Muffle furnace,
950～1100 DEG C progressively it are warming up to 8～10 DEG C/min speed, insulation calcining 15～20min, cool to room temperature with the furnace and obtain white
Powder；
(2) count by weight, weigh 100～120 parts of above-mentioned gained white powders, pour into and fill 200～300 parts of deionized waters
Beaker in, subsequently beaker is placed in sonic oscillation instrument, with 100～150W power ultrasonics dispersion 8～10min, obtain white even
Slurry；
(3) weigh 3～5kg straws, be 5～8cm short stalks with chopper cut growth, be 35～45 DEG C of deionized waters by temperature subsequently
Middle immersion 3～5h, filters, and collects the short stalk after being soaked, and it is evenly laid out in fermenter base, paving to thickness be 6～
8cm, then on short stalk, lay one layer of above-mentioned gained white homogenate, until all being covered by short for lower floor stalk, then it is homogenized table in white
4～6 layers of rice paper are laid in face, are 0.6～0.8cm above-mentioned gained white homogenate at rice paper surface-coated thick layer；
(4) treat that above-mentioned white homogenate interpolation terminates, add deionized water along fermentor walls, until the water surface exceedes white refining surfaces
25～30cm, then fermentation tank is sealed, under the conditions of 38～40 DEG C, constant-temperature enclosed standing for fermentation 25～30 days, treat fermentation ends,
Start fermenter stirrer, with 1600～1800r/min rotating speed stirrings 45～60min, end to be mixed, cross 120～180 mesh
Sieve, obtains and carefully mixes homogenate；
(5) count by weight, beaker is sequentially added into 150～180 parts of above-mentioned gained and carefully mixes homogenate, 4～6 portions of brown sugar, 5
～7 parts of glutinous rice flours, subsequently beaker is placed in magnetic stirrer, with 600～800r/min rotating speed stirring mixing 30～45min,
Obtain pigment base material；
(6) count by weight, batch mixer is sequentially added into 80～100 parts of above-mentioned gained pigment base materials, 6～8 parts of deionizations
Water, 8～12 part 2,6-sodium dichlorophenol indophenolate, under the conditions of rotating speed is 800～1000r/min, stirring mixing 15～20min, subsequently
Material is proceeded to sonic oscillation instrument, processes 20～30min with 120～160W power ultrasonics, obtain weather resistant non-toxic pigment.
The concrete application process of the present invention: take 15～20g gained weather resistant non-toxic pigments of the present invention, pour in color saucer,
Add 6～8mL deionized waters, after being uniformly mixed with paintbrush, water paper is painted, obtains artistic work, treat pigment
After natural drying, gained works are placed in natural storage at lucifuge aeration-drying, compared to the works used drawn by conventional pigment,
Preserve the life-span improve 8～10 years, during preservation, colour-fast, cracking, mouldy, can give full play to works artistic charm and
It is worth.
The invention has the beneficial effects as follows:
(1) the weather resistant non-toxic pigment product that prepared by the present invention overcomes the defect of traditional product, meets student, artist etc.
High request to art watercolour pigment；
(2) gained pigment displays of the present invention goes out outstanding quality of colour, and bright in colour bright, color is saturated strong, strong coloring force,
Compared to conventional pigment, there is the characteristics such as higher water-fast, fast light, weatherability, use the works that gained pigment of the present invention is drawn
Physical stability relatively uses Conventional dye to be enhanced.
Detailed description of the invention
Weigh 3～5kg Carnis Mactrae shells, after manually repeatedly cleaning 3～5 times with deionized water, be placed under sunlight be exposed to the sun 5～
7 days, then pour in Universalpulverizer, cross 120～180 mesh sieves after pulverizing, collect the shell powder after sieving, proceed to Muffle furnace
In, progressively it is warming up to 950～1100 DEG C with 8～10 DEG C/min speed, insulation calcining 15～20min, cool to room temperature with the furnace and obtain
White powder；Count by weight, weigh 100～120 parts of above-mentioned gained white powders, pour into and fill 200～300 parts of deionizations
In the beaker of water, subsequently beaker is placed in sonic oscillation instrument, with 100～150W power ultrasonic dispersions 8～10min, obtains white
Homogenate；Weigh 3～5kg straws, be 5～8cm short stalks with chopper cut growth, be in 35～45 DEG C of deionized waters by temperature subsequently
Soaking 3～5h, filter, collect the short stalk after being soaked, it is evenly laid out in fermenter base, and paving to thickness is 6～8cm,
One layer of above-mentioned gained white homogenate is laid again, until all being covered by short for lower floor stalk, then white refining surfaces paving on short stalk
If 4～6 layers of rice paper, it is 0.6～0.8cm above-mentioned gained white homogenate at rice paper surface-coated thick layer；Treat above-mentioned white homogenate
Interpolation terminates, and adds deionized water along fermentor walls, until the water surface exceedes white refining surfaces 25～30cm then fermentation tank is close
Envelope, under the conditions of 38～40 DEG C, constant-temperature enclosed standing for fermentation 25～30 days, treat fermentation ends, start fermenter stirrer, with
1600～1800r/min rotating speed stirrings 45～60min, end to be mixed, cross 120～180 mesh sieves, obtain and carefully mix homogenate；By weight
Amount number meter, is sequentially added into 150～180 parts of above-mentioned gained in beaker and carefully mixes homogenate, 4～6 portions of brown sugar, 5～7 parts of Oryza glutinosa
Powder, is placed in beaker in magnetic stirrer subsequently, with 600～800r/min rotating speed stirring mixing 30～45min, obtains pigment base
Material；Count by weight, batch mixer is sequentially added into 80～100 parts of above-mentioned gained pigment base materials, 6～8 parts of deionized waters, 8
～12 part 2,6-sodium dichlorophenol indophenolate, under the conditions of rotating speed is 800～1000r/min, stirring mixing 15～20min, subsequently by thing
Material proceeds to sonic oscillation instrument, processes 20～30min with 120～160W power ultrasonics, obtains weather resistant non-toxic pigment.
Example 1
Weigh 3kg Carnis Mactrae shell, after manually repeatedly cleaning 3 times with deionized water, be placed under sunlight and be exposed to the sun 5 days, then pour ten thousand into
Pulverizer can be crossed 120 mesh sieves, collected the shell powder after sieving, proceed in Muffle furnace after pulverizing, with 8 DEG C/min speed by
Step is warming up to 950 DEG C, insulation calcining 15min, cools to room temperature with the furnace and obtains white powder；Count by weight, weigh on 100 parts
State gained white powder, pour in the beaker filling 200 parts of deionized waters, subsequently beaker is placed in sonic oscillation instrument, with
100W power ultrasonic dispersion 8min, obtains white homogenate；Weigh 3kg straw, be the short stalk of 5cm with chopper cut growth, subsequently by temperature
Degree is immersion 3h in 35 DEG C of deionized waters, filters, and collects the short stalk after being soaked, and it is evenly laid out in fermenter base,
Paving to thickness is 6cm, then lays one layer of above-mentioned gained white homogenate on short stalk, until all being covered by short for lower floor stalk, then in vain
Color refining surfaces lays 4 layers of rice paper, is the homogenate of 0.6cm above-mentioned gained white at rice paper surface-coated thick layer；Treat above-mentioned white
Homogenate interpolation terminates, and adds deionized water along fermentor walls, until the water surface exceedes white refining surfaces 25cm then fermentation tank is close
Envelope, under the conditions of 38 DEG C, constant-temperature enclosed standing for fermentation 25 days, treat fermentation ends, start fermenter stirrer, with 1600r/min
Rotating speed stirring 45min, end to be mixed, cross 120 mesh sieves, obtain and carefully mix homogenate；Count by weight, be sequentially added in beaker
150 parts of above-mentioned gained carefully mix homogenate, 4 portions of brown sugar, 5 parts of glutinous rice flours, are placed in magnetic stirrer by beaker subsequently, with 600r/
Min rotating speed stirring mixing 30min, obtains pigment base material；Count by weight, batch mixer is sequentially added into 80 parts of above-mentioned gained face
Material base material, 6 parts of deionized waters, 8 part 2,6-sodium dichlorophenol indophenolate, under the conditions of rotating speed is 800r/min, stirring mixing 15min, with
After material proceeded to sonic oscillation instrument, process 20min with 120W power ultrasonic, obtain weather resistant non-toxic pigment.
Take 15g gained of the present invention weather resistant non-toxic pigment, pour in color saucer, add 6mL deionized water, stir with paintbrush
After mixing mix homogeneously, water paper is painted, obtains artistic work, after pigment natural drying, gained works are placed in lucifuge
Natural storage at aeration-drying, compared to the works used drawn by conventional pigment, the preservation life-span improves 8 years, during preservation,
Colour-fast, cracking, mouldy, artistic charm and the value of works can be given full play to.
Example 2
Weigh 4kg Carnis Mactrae shell, after manually repeatedly cleaning 4 times with deionized water, be placed under sunlight and be exposed to the sun 6 days, then pour ten thousand into
Pulverizer can be crossed 160 mesh sieves, collected the shell powder after sieving, proceed in Muffle furnace after pulverizing, with 9 DEG C/min speed by
Step is warming up to 1000 DEG C, insulation calcining 18min, cools to room temperature with the furnace and obtains white powder；Count by weight, weigh 110 parts
Above-mentioned gained white powder, pours in the beaker filling 260 parts of deionized waters, is placed in by beaker subsequently in sonic oscillation instrument, with
120W power ultrasonic dispersion 9min, obtains white homogenate；Weigh 4kg straw, be the short stalk of 6cm with chopper cut growth, subsequently by temperature
Degree is immersion 4h in 40 DEG C of deionized waters, filters, and collects the short stalk after being soaked, and it is evenly laid out in fermenter base,
Paving to thickness is 7cm, then lays one layer of above-mentioned gained white homogenate on short stalk, until all being covered by short for lower floor stalk, then in vain
Color refining surfaces lays 5 layers of rice paper, is the homogenate of 0.7cm above-mentioned gained white at rice paper surface-coated thick layer；Treat above-mentioned white
Homogenate interpolation terminates, and adds deionized water along fermentor walls, until the water surface exceedes white refining surfaces 28cm then fermentation tank is close
Envelope, under the conditions of 39 DEG C, constant-temperature enclosed standing for fermentation 28 days, treat fermentation ends, start fermenter stirrer, with 1700r/min
Rotating speed stirring 50min, end to be mixed, cross 160 mesh sieves, obtain and carefully mix homogenate；Count by weight, be sequentially added in beaker
160 parts of above-mentioned gained carefully mix homogenate, 5 portions of brown sugar, 6 parts of glutinous rice flours, are placed in magnetic stirrer by beaker subsequently, with 700r/
Min rotating speed stirring mixing 40min, obtains pigment base material；Count by weight, batch mixer is sequentially added into 90 parts of above-mentioned gained face
Material 7 parts of deionized waters of base material, 10 part 2,6-sodium dichlorophenol indophenolate, under the conditions of rotating speed is 900r/min, stirring mixing 18min, with
After material proceeded to sonic oscillation instrument, process 25min with 140W power ultrasonic, obtain weather resistant non-toxic pigment.
Take 18g gained of the present invention weather resistant non-toxic pigment, pour in color saucer, add 7mL deionized water, stir with paintbrush
After mixing mix homogeneously, water paper is painted, obtains artistic work, after pigment natural drying, gained works are placed in lucifuge
Natural storage at aeration-drying, compared to the works used drawn by conventional pigment, the preservation life-span improves 9 years, during preservation,
Colour-fast, cracking, mouldy, artistic charm and the value of works can be given full play to.
Example 3
Weigh 5kg Carnis Mactrae shell, after manually repeatedly cleaning 5 times with deionized water, be placed under sunlight and be exposed to the sun 7 days, then pour ten thousand into
Pulverizer can be crossed 180 mesh sieves, collected the shell powder after sieving, proceed in Muffle furnace after pulverizing, with 10 DEG C/min speed by
Step is warming up to 1100 DEG C, insulation calcining 20min, cools to room temperature with the furnace and obtains white powder；Count by weight, weigh 120 parts
Above-mentioned gained white powder, pours in the beaker filling 300 parts of deionized waters, is placed in by beaker subsequently in sonic oscillation instrument, with
150W power ultrasonic dispersion 10min, obtains white homogenate；Weigh 5kg straw, be the short stalk of 8cm with chopper cut growth, subsequently by temperature
Degree is immersion 5h in 45 DEG C of deionized waters, filters, and collects the short stalk after being soaked, and it is evenly laid out in fermenter base,
Paving to thickness is 8cm, then lays one layer of above-mentioned gained white homogenate on short stalk, until all being covered by short for lower floor stalk, then in vain
Color refining surfaces lays 6 layers of rice paper, is the homogenate of 0.8cm above-mentioned gained white at rice paper surface-coated thick layer；Treat above-mentioned white
Homogenate interpolation terminates, and adds deionized water along fermentor walls, until the water surface exceedes white refining surfaces 30cm then fermentation tank is close
Envelope, under the conditions of 40 DEG C, constant-temperature enclosed standing for fermentation 30 days, treat fermentation ends, start fermenter stirrer, with 1800r/min
Rotating speed stirring 60min, end to be mixed, cross 180 mesh sieves, obtain and carefully mix homogenate；Count by weight, be sequentially added in beaker
180 parts of above-mentioned gained carefully mix homogenate, 6 portions of brown sugar, 7 parts of glutinous rice flours, are placed in magnetic stirrer by beaker subsequently, with 800r/
Min rotating speed stirring mixing 45min, obtains pigment base material；Count by weight, batch mixer is sequentially added into 100 parts of above-mentioned gained
Pigment base material, 8 parts of deionized waters, 12 part 2,6-sodium dichlorophenol indophenolate, under the conditions of rotating speed is 1000r/min, stirring mixing
20min, proceeds to sonic oscillation instrument subsequently by material, processes 30min with 160W power ultrasonic, obtains weather resistant non-toxic pigment.
Take 20g gained of the present invention weather resistant non-toxic pigment, pour in color saucer, add 8mL deionized water, stir with paintbrush
After mixing mix homogeneously, water paper is painted, obtains artistic work, after pigment natural drying, gained works are placed in lucifuge
Natural storage at aeration-drying, compared to the works used drawn by conventional pigment, the preservation life-span improves 10 years, preserves process
In, colour-fast, cracking, mouldy, artistic charm and the value of works can be given full play to.
Claims (1)
1. the preparation method of a weather resistant non-toxic pigment, it is characterised in that concrete preparation process is:
(1) weigh 3～5kg Carnis Mactrae shells, after manually repeatedly cleaning 3～5 times with deionized water, be placed under sunlight and be exposed to the sun 5～7
My god, then pour in Universalpulverizer, cross 120～180 mesh sieves after pulverizing, collect the shell powder after sieving, proceed in Muffle furnace,
950～1100 DEG C progressively it are warming up to 8～10 DEG C/min speed, insulation calcining 15～20min, cool to room temperature with the furnace and obtain white
Powder；
(2) count by weight, weigh 100～120 parts of above-mentioned gained white powders, pour into and fill 200～300 parts of deionized waters
Beaker in, subsequently beaker is placed in sonic oscillation instrument, with 100～150W power ultrasonics dispersion 8～10min, obtain white even
Slurry；
(3) weigh 3～5kg straws, be 5～8cm short stalks with chopper cut growth, be 35～45 DEG C of deionized waters by temperature subsequently
Middle immersion 3～5h, filters, and collects the short stalk after being soaked, and it is evenly laid out in fermenter base, paving to thickness be 6～
8cm, then on short stalk, lay one layer of above-mentioned gained white homogenate, until all being covered by short for lower floor stalk, then it is homogenized table in white
4～6 layers of rice paper are laid in face, are 0.6～0.8cm above-mentioned gained white homogenate at rice paper surface-coated thick layer；
(4) treat that above-mentioned white homogenate interpolation terminates, add deionized water along fermentor walls, until the water surface exceedes white refining surfaces
25～30cm, then fermentation tank is sealed, under the conditions of 38～40 DEG C, constant-temperature enclosed standing for fermentation 25～30 days, treat fermentation ends,
Start fermenter stirrer, with 1600～1800r/min rotating speed stirrings 45～60min, end to be mixed, cross 120～180 mesh
Sieve, obtains and carefully mixes homogenate；
(5) count by weight, beaker is sequentially added into 150～180 parts of above-mentioned gained and carefully mixes homogenate, 4～6 portions of brown sugar, 5
～7 parts of glutinous rice flours, subsequently beaker is placed in magnetic stirrer, with 600～800r/min rotating speed stirring mixing 30～45min,
Obtain pigment base material；
(6) count by weight, batch mixer is sequentially added into 80～100 parts of above-mentioned gained pigment base materials, 6～8 parts of deionizations
Water, 8～12 part 2,6-sodium dichlorophenol indophenolate, under the conditions of rotating speed is 800～1000r/min, stirring mixing 15～20min, subsequently
Material is proceeded to sonic oscillation instrument, processes 20～30min with 120～160W power ultrasonics, obtain weather resistant non-toxic pigment.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610636555.4A CN106221341A (en) | 2016-08-05 | 2016-08-05 | A kind of preparation method of weather resistant non-toxic pigment |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610636555.4A CN106221341A (en) | 2016-08-05 | 2016-08-05 | A kind of preparation method of weather resistant non-toxic pigment |
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| CN106221341A true CN106221341A (en) | 2016-12-14 |
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| CN201610636555.4A Pending CN106221341A (en) | 2016-08-05 | 2016-08-05 | A kind of preparation method of weather resistant non-toxic pigment |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112280354A (en) * | 2020-11-24 | 2021-01-29 | 宜春学院 | Environment-friendly odorless art painting pigment and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103554850A (en) * | 2013-10-25 | 2014-02-05 | 苏笮斌 | Environment-friendly type anti-cracking corrosion-resistant waterproof material and preparation method thereof |
| CN104341847A (en) * | 2013-07-31 | 2015-02-11 | 东莞市康博士装饰材料有限公司 | Novel glutinous rice slurry film-forming aid used for paint |
| CN104987838A (en) * | 2015-07-13 | 2015-10-21 | 舟山赛莱特海洋科技有限公司 | Preparation method of antimicrobial coating based on shell powder |
| CN105482531A (en) * | 2015-12-31 | 2016-04-13 | 苏州冰心文化用品有限公司 | Solid instant transparent watercolor and preparation method thereof |
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2016
- 2016-08-05 CN CN201610636555.4A patent/CN106221341A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104341847A (en) * | 2013-07-31 | 2015-02-11 | 东莞市康博士装饰材料有限公司 | Novel glutinous rice slurry film-forming aid used for paint |
| CN103554850A (en) * | 2013-10-25 | 2014-02-05 | 苏笮斌 | Environment-friendly type anti-cracking corrosion-resistant waterproof material and preparation method thereof |
| CN104987838A (en) * | 2015-07-13 | 2015-10-21 | 舟山赛莱特海洋科技有限公司 | Preparation method of antimicrobial coating based on shell powder |
| CN105482531A (en) * | 2015-12-31 | 2016-04-13 | 苏州冰心文化用品有限公司 | Solid instant transparent watercolor and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112280354A (en) * | 2020-11-24 | 2021-01-29 | 宜春学院 | Environment-friendly odorless art painting pigment and preparation method thereof |
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Application publication date: 20161214 |