CN106215223A - A kind of chitosan and bamboo fibre are blended the preparation method of wet nonwoven fabrics medical dressing - Google Patents

A kind of chitosan and bamboo fibre are blended the preparation method of wet nonwoven fabrics medical dressing Download PDF

Info

Publication number
CN106215223A
CN106215223A CN201610602868.8A CN201610602868A CN106215223A CN 106215223 A CN106215223 A CN 106215223A CN 201610602868 A CN201610602868 A CN 201610602868A CN 106215223 A CN106215223 A CN 106215223A
Authority
CN
China
Prior art keywords
mixed liquor
chitosan
weight portion
blended
bamboo fibre
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610602868.8A
Other languages
Chinese (zh)
Inventor
胡盼
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hunan Dili Intelligent Technology Co Ltd
Original Assignee
Hunan Dili Intelligent Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hunan Dili Intelligent Technology Co Ltd filed Critical Hunan Dili Intelligent Technology Co Ltd
Priority to CN201610602868.8A priority Critical patent/CN106215223A/en
Publication of CN106215223A publication Critical patent/CN106215223A/en
Pending legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/22Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing macromolecular materials
    • A61L15/28Polysaccharides or their derivatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/22Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing macromolecular materials
    • A61L15/24Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/22Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing macromolecular materials
    • A61L15/26Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/40Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons containing ingredients of undetermined constitution or reaction products thereof, e.g. plant or animal extracts
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/42Use of materials characterised by their function or physical properties
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/42Use of materials characterised by their function or physical properties
    • A61L15/425Porous materials, e.g. foams or sponges
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/42Use of materials characterised by their function or physical properties
    • A61L15/44Medicaments
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/42Use of materials characterised by their function or physical properties
    • A61L15/46Deodorants or malodour counteractants, e.g. to inhibit the formation of ammonia or bacteria
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L15/00Chemical aspects of, or use of materials for, bandages, dressings or absorbent pads
    • A61L15/16Bandages, dressings or absorbent pads for physiological fluids such as urine or blood, e.g. sanitary towels, tampons
    • A61L15/42Use of materials characterised by their function or physical properties
    • A61L15/50Lubricants; Anti-adhesive agents
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/06Wet spinning methods
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/12Stretch-spinning methods
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2300/00Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
    • A61L2300/40Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices characterised by a specific therapeutic activity or mode of action
    • A61L2300/412Tissue-regenerating or healing or proliferative agents
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61LMETHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2300/00Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices
    • A61L2300/40Biologically active materials used in bandages, wound dressings, absorbent pads or medical devices characterised by a specific therapeutic activity or mode of action
    • A61L2300/418Agents promoting blood coagulation, blood-clotting agents, embolising agents

Abstract

nullThe invention discloses a kind of chitosan and bamboo fibre is blended wet nonwoven fabrics medical dressing and preparation method thereof,Chitosan and the bamboo fibre that weight portion is 2 10 so that weight portion is 10 20 carry out proportioning,Adding weight portion is the deionized water of 200 1000,Making beating after blended,Add the water-soluble high-molecular material that weight portion is 0.01 1,The larger particles in mixed liquor is removed after filtration,So that molding,Again by prepared mixed liquor by after spinneret orifice extrusion mixing liquid thread,Again through 85 90 DEG C of coagulating baths,This mixed liquor thread is frozen into spun filament,Spun filament is carried out drawing-off and forms composite fibre long filament,Transudate for wound surface has the strongest adsorption,Can be the most antibacterial,Antiinflammatory,Promote the healing of wound,Product is soft,Wound surface can be close to,Air permeable humidity retaining is good,Few with wound surface adhesion,Alleviate the misery changed dressings.Production method is simple, quick, with low cost.

Description

A kind of chitosan and bamboo fibre are blended the preparation method of wet nonwoven fabrics medical dressing
Technical field
The present invention relates to the preparation method of a kind of medical dressing.
Background technology
Medical aseptic dressing is mainly used in when human body suffers when epidermis, muscular tissue wound, to this must and Shi Jinhang wrapping and treatment, and currently mainly use common dressing and be unfavorable for the healing of wound, and easily produce adhesion Deng.
Bamboo fibre has the characteristics such as good breathability, moment water absorption, stronger wearability and good dyeability, tool There are natural antibacterial, antibacterial, acaricide, deodorant and anti-ultraviolet function.
Chitosan is as a kind of natural macromolecular material, without any side effects to human body, and have Antibacterial activity, Absorption and excretion heavy metal, the promotion function such as blood coagulation and wound healing, have the functional natural of immunoregulatory activity for a kind of Macromolecular material.
Summary of the invention
Because the drawbacks described above of prior art, the technical problem to be solved is to provide a kind of chitosan and bamboo The preparation method of fiber blend wet nonwoven fabrics medical dressing.
For achieving the above object, the invention provides a kind of chitosan and bamboo fibre is blended wet nonwoven fabrics medical dressing Preparation method, chitosan with weight portion as 10-20 and the weight portion bamboo fibre as 2-10 carry out proportioning, add weight portion and are The deionized water of 200-1000, blended rear making beating, add the water-soluble high-molecular material that weight portion is 0.01-1, after filtration Remove the larger particles in mixed liquor, in order to molding, then by prepared mixed liquor by after spinneret orifice extrusion mixing liquid thread, Again through 85-90 DEG C of coagulating bath, this mixed liquor thread is frozen into spun filament, spun filament is carried out drawing-off formation composite fibre long Silk.This solidification temperature is conducive to the solidification of viscose glue stock solution, forms the structure of even compact, is also beneficial to form overall orientation degree Height, crystallizes fairly perfect fiber;The too high or too low structure being all unfavorable for forming even compact of temperature (concentration).
Further, described water-soluble high-molecular material is sodium alginate, polyacrylamide, polyacrylic acid, polyvinyl pyrrole One or more in alkanone, polyvinyl alcohol, polymaleic anhydride, polyquaternium, Polyethylene Glycol and shuttle cellulose.
Further, described its speed of manufacturing paper with pulp of technique using wet-laid method to prepare non-woven fabrics is 30-40 m/min Clock.
Technique effect: the present invention can resist some antibacterials easily causing infection, it is to avoid wound suppuration, simultaneously for wound The transudate in face has the strongest adsorption, can be the most antibacterial, antiinflammatory, promotes the healing of wound, and nontoxic, aseptic, becomes This is cheap, easy to use.
Product is soft, can be close to wound surface, and air permeable humidity retaining is good, has stronger hemostasis and the energy of absorptive tissue transudate Power, can efficiently control wound infection, and wound healing is few with wound surface adhesion, alleviates the misery changed dressings, and decreases medical treatment The generation of rubbish.Product processes is simple, quick, reduces production cost, and product is easy to use.
Detailed description of the invention
Embodiment 1:
Take 12 parts of chitosans and 8 parts of bamboo fibres, add deionized water 200 parts, pull an oar 30 minutes, add sodium alginate 0.04, mistake Filter the larger particles in mixed liquor, in order to molding.After mixed liquor above is passed through spinneret orifice extrusion mixing liquid thread, Again through 85-90 DEG C of solidification, this solidification temperature is conducive to the solidification of viscose glue stock solution, forms the structure of even compact, is also beneficial to shape The integral degree of orientation is high, crystallizes fairly perfect fiber;Too high or too low being all unfavorable for of temperature (concentration) forms even compact Structure;This mixed liquor thread is frozen into spun filament.Spun filament is carried out drawing-off and forms composite fibre long filament.This method prepares Dressing, its stability is preferable, and in storing 6 months, product does not occurs outward appearance, loss on drying change and keep aseptic condition.This Bright skin glues stickiness test and shows that product can contact uniformly with wound face, and not viscous glutinous skin, and the wounded is without sense of discomfort.Owing to applying The cell adhesion of material is the highly important problem that medical dressing design needs to consider.Owing to material is incorrect and cause Dressing adhere to granulation tissue, thus cause the secondary damage that dressing brings when removing, including the adhesion to granulation, to migrate Epithelial cell, fibroblastic infringement of hypertrophy, even ratio does not uses dressing more serious.The surface of the test group of the present embodiment Cell adhesion value is the lowest, is substantially less than other three groups of matched groups, illustrates that the hydrophilic of dressing of the present invention is high, water absorbing capacity is strong, from And it being unfavorable for the adhesion of cell, such dressing will not cause tissue adhesion.
Embodiment 2:
Take 18 parts of chitosans and 2 parts of bamboo fibres, add deionized water 300 parts, pull an oar 30 minutes, add polyacrylamide 0.01, The larger particles being filtered to remove in mixed liquor, in order to molding.By mixed liquor above by spinneret orifice extrusion mixing liquid thread After, then through 85-90 DEG C of solidification, this solidification temperature is conducive to the solidification of viscose glue stock solution, forms the structure of even compact, is also beneficial to Form overall orientation degree high, crystallize fairly perfect fiber;Too high or too low being all unfavorable for of temperature (concentration) forms even compact Structure;This mixed liquor thread is frozen into spun filament.Spun filament is carried out drawing-off and forms composite fibre long filament.
Embodiment 3:
Take 10 parts of chitosans and 10 parts of bamboo fibres, add deionized water 400 parts, pull an oar 30 minutes, add polyacrylic acid 0.5 part, The larger particles being filtered to remove in mixed liquor, in order to molding.By mixed liquor above by spinneret orifice extrusion mixing liquid thread After, then through 85-90 DEG C of solidification, this solidification temperature is conducive to the solidification of viscose glue stock solution, forms the structure of even compact, is also beneficial to Form overall orientation degree high, crystallize fairly perfect fiber;Too high or too low being all unfavorable for of temperature (concentration) forms even compact Structure;This mixed liquor thread is frozen into spun filament.Spun filament is carried out drawing-off and forms composite fibre long filament.Optionally, system The dressing fibre diameter obtained is 56.34 μm, and fiber number is 563dtex, is 72.2/cm through density, and weft density is 17.4/cm. Finer and close, good water absorption, anti, each performance reaches optimal.
Embodiment 4:
Take 16 parts of chitosans and 4 parts of bamboo fibres, add deionized water 800 parts, pull an oar 30 minutes, add shuttle methylcellulose 0.4 Part, the larger particles being filtered to remove in mixed liquor, in order to molding.Mixed liquor above is thin by spinneret orifice extrusion mixing liquid After stream, then through 85-90 DEG C of solidification, this solidification temperature is conducive to the solidification of viscose glue stock solution, forms the structure of even compact, the most favorably High in forming overall orientation degree, crystallize fairly perfect fiber;Temperature (concentration) is too high or too low is all unfavorable for being formed uniformly cause Close structure;This mixed liquor thread is frozen into spun filament.Spun filament is carried out drawing-off and forms composite fibre long filament.Described adopts Its speed of manufacturing paper with pulp of technique preparing non-woven fabrics with wet-laid method is 30-40 m/min.
Embodiment 5:
Take 10 parts of chitosans and 10 parts of bamboo fibres, add deionized water 1000 parts, pull an oar 30 minutes, add polyvinyl alcohol 0.6 part, The larger particles being filtered to remove in mixed liquor, in order to molding.By mixed liquor above by spinneret orifice extrusion mixing liquid thread After, then through 85-90 DEG C of solidification, this solidification temperature is conducive to the solidification of viscose glue stock solution, forms the structure of even compact, is also beneficial to Form overall orientation degree high, crystallize fairly perfect fiber;Too high or too low being all unfavorable for of temperature (concentration) forms even compact Structure;This mixed liquor thread is frozen into spun filament.Spun filament is carried out drawing-off and forms composite fibre long filament.
Embodiment 6:
Take 16 parts of chitosans and 4 parts of bamboo fibres, add deionized water 800 parts, pull an oar 30 minutes, add Polyethylene Glycol 1 part, filter Remove the larger particles in mixed liquor, in order to molding.After mixed liquor above is passed through spinneret orifice extrusion mixing liquid thread, then Through 85-90 DEG C of solidification, this solidification temperature is conducive to the solidification of viscose glue stock solution, forms the structure of even compact, is also beneficial to be formed Overall orientation degree is high, crystallizes fairly perfect fiber;The too high or too low knot being all unfavorable for forming even compact of temperature (concentration) Structure;This mixed liquor thread is frozen into spun filament.Spun filament is carried out drawing-off and forms composite fibre long filament.
Embodiment 7:
Take 20 parts of chitosans and 4 parts of bamboo fibres, add deionized water 800 parts, pull an oar 30 minutes, add Polyethylene Glycol 0.5 part, mistake Filter the larger particles in mixed liquor, in order to molding.After mixed liquor above is passed through spinneret orifice extrusion mixing liquid thread, Again through 85-90 DEG C of solidification, this solidification temperature is conducive to the solidification of viscose glue stock solution, forms the structure of even compact, is also beneficial to shape The integral degree of orientation is high, crystallizes fairly perfect fiber;Too high or too low being all unfavorable for of temperature (concentration) forms even compact Structure;This mixed liquor thread is frozen into spun filament.Spun filament is carried out drawing-off and forms composite fibre long filament.
It is sponge loose structure that chitosan prepared by the present invention and bamboo fibre are blended wet nonwoven fabrics medical dressing, average hole Footpath is 100 microns, and mutually runs through, and is conducive to the ventilative and absorption of moisture.Other dressing in the prior art that compares, Dressing of the present invention loose porous, hole is the most intensive and hole size uniform, and pore size is moderate, of the present invention applies The water absorbing capacity of material is extremely strong, the absorbable liquid being equivalent to own wt 17 ~ 25 times.
The medical dressing that embodiment 1-7 prepares is carried out the detection of external moisture pick-up properties: weigh 8.3 g sodium chloride and The anhydrous calcium chloride of 0.277 g, is dissolved in the distilled water of 1L and is configured to the solution A that British Pharmacopoeia specifies.Testing example 4, During the pick up of dressing that 5,6 prepare, place 24 h after dressing is cut into 5 cm × 5 cm sizes respectively, make the regain of fiber Reach balance.At this moment the initial mass measuring dressing is W.Weigh the solution A than dressing weight 40 times, respectively by solution and dressing pair Should be placed in the culture dish of 2 a diameter of 9 cm, after placing 30 min at 37 DEG C, clamp one jiao of dressing at sky with tweezers In, weigh the wet quality (W1) of dressing after hanging 30s.The pick up of unit mass dressing=(W1-W)/W (g/g), unit are Pick up=4 (W1-W) g/100 cm2.Repeat above-mentioned experiment 3 times, seek its meansigma methods.
During test liquid distribution in fiber and between fiber, the dressing (quality is W1) after imbibition with gauze respectively Packing together after being placed in dewaterer dehydration 15min, measuring the quality of dressing after being dehydrated is W2, and this quality is fiber itself Dry mass and be absorbed into the summation of liquid quality of fibrous inside.Then the dressing after centrifuge dehydration in 105 DEG C of dry 4h, examination The dry mass W3 of fiber is recorded after the most permanent quality of sample.W1-W2 is to absorb liquid between the fibers, and W2-W3 is to be absorbed into fibre Liquid within Wei.(W1-W2)/W3 and (w2-w3)/w3 can calculate the dressing of every gram of dry mass respectively and absorb between fiber Liquid with fibrous inside.
Experimental result: medical dressing being centrifuged dehydration and is finding after drying, dressing itself has good water suction Property, in the moisture absorbed, most can be retained in fibrous inside, is difficult to be removed by centrifuge dehydration.
The preferred embodiment of the present invention described in detail above.Should be appreciated that those of ordinary skill in the art without Need creative work just can make many modifications and variations according to the design of the present invention.Therefore, all technology in the art Personnel are available by logical analysis, reasoning, or a limited experiment the most on the basis of existing technology Technical scheme, all should be in the protection domain being defined in the patent claims.

Claims (3)

1. a chitosan and bamboo fibre are blended the preparation method of wet nonwoven fabrics medical dressing, it is characterised in that: with weight portion Chitosan and the bamboo fibre that weight portion is 2-10 for 10-20 carry out proportioning, and adding weight portion is the deionized water of 200-1000, After blended, making beating, adds the water-soluble high-molecular material that weight portion is 0.01-1, and remove in mixed liquor after filtration is bigger Granule, in order to molding, then by prepared mixed liquor by after spinneret orifice extrusion mixing liquid thread, then through 85-90 DEG C of coagulating bath, This mixed liquor thread is frozen into spun filament, spun filament is carried out drawing-off and forms composite fibre long filament.
A kind of chitosan the most according to claim 1 and bamboo fibre are blended the preparation method of wet nonwoven fabrics medical dressing, It is characterized in that: described water-soluble high-molecular material be sodium alginate, polyacrylamide, polyacrylic acid, polyvinylpyrrolidone, One or more in polyvinyl alcohol, polymaleic anhydride, polyquaternium, Polyethylene Glycol and shuttle cellulose.
A kind of chitosan the most according to claim 1 and bamboo fibre are blended the preparation method of wet nonwoven fabrics medical dressing, It is characterized in that: described its speed of manufacturing paper with pulp of technique using wet-laid method to prepare non-woven fabrics is 30-40 m/min.
CN201610602868.8A 2016-07-28 2016-07-28 A kind of chitosan and bamboo fibre are blended the preparation method of wet nonwoven fabrics medical dressing Pending CN106215223A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610602868.8A CN106215223A (en) 2016-07-28 2016-07-28 A kind of chitosan and bamboo fibre are blended the preparation method of wet nonwoven fabrics medical dressing

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610602868.8A CN106215223A (en) 2016-07-28 2016-07-28 A kind of chitosan and bamboo fibre are blended the preparation method of wet nonwoven fabrics medical dressing

Publications (1)

Publication Number Publication Date
CN106215223A true CN106215223A (en) 2016-12-14

Family

ID=57534557

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610602868.8A Pending CN106215223A (en) 2016-07-28 2016-07-28 A kind of chitosan and bamboo fibre are blended the preparation method of wet nonwoven fabrics medical dressing

Country Status (1)

Country Link
CN (1) CN106215223A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112095225A (en) * 2020-09-16 2020-12-18 宿州衣尔雅无纺布有限公司 Breathable dry non-woven fabric and production method thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101049515A (en) * 2007-05-15 2007-10-10 浙江理工大学 Method for preparing medical use dressing of non-woven fabrics in wet-process cross blent from chitosan and silk fibrino
CN103726117A (en) * 2012-02-26 2014-04-16 昆山华阳复合材料科技有限公司 Medical fiber membrane for safety protection
CN104324412A (en) * 2014-10-24 2015-02-04 浙江奥林医疗用品有限公司 Bamboo chitosan functional dressing

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101049515A (en) * 2007-05-15 2007-10-10 浙江理工大学 Method for preparing medical use dressing of non-woven fabrics in wet-process cross blent from chitosan and silk fibrino
CN103726117A (en) * 2012-02-26 2014-04-16 昆山华阳复合材料科技有限公司 Medical fiber membrane for safety protection
CN104324412A (en) * 2014-10-24 2015-02-04 浙江奥林医疗用品有限公司 Bamboo chitosan functional dressing

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
冯孝中: "《高分子材料》", 28 February 2007, 哈尔滨工业大学出版社 *
马传勋: "天然纤维增强医用复合材料的研究现状", 《现代医药卫生》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112095225A (en) * 2020-09-16 2020-12-18 宿州衣尔雅无纺布有限公司 Breathable dry non-woven fabric and production method thereof

Similar Documents

Publication Publication Date Title
JP4499669B2 (en) Trauma bandage
CN107376000B (en) Microfibre state hemostatic material and preparation method thereof and hemostatic article
CN103550817B (en) A kind of Bacterial cellulose/shitosan composite sponge dressing and preparation method thereof
CN107237005B (en) Alginic acid and chitosan double-component fiber and preparation method thereof
CN107737368B (en) Hemostatic material and its preparation method and application
CN107693835A (en) A kind of polyvinyl alcohol/collagen/n-trimethyl chitosan chloride electrospun composite fibers film and preparation method thereof
WO1996010106A1 (en) Fibres
CN107823693B (en) Stanch fibre film and preparation method thereof and hemostatic article
WO2014101458A1 (en) Chemically modified sea silk fiber, wound dressing made therefrom and preparation method thereof
CN109224116A (en) A kind of the antibacterial anti hemorrhagic medical dressing and preparation method of high-absorbable
CN109731121A (en) A kind of preparation method of the cellulose containing mesoporous silicon oxide and chitosan combine dressing
CN113018502B (en) Medical multifunctional hemostatic dressing and preparation method thereof
CN105544002A (en) Superabsorbent composite fiber and preparation method thereof
WO2015103988A1 (en) Medical dressing hydrogel composite fabric, and preparation method therefor and uses thereof
WO2018056937A2 (en) Nanofibrous adhesion barrier
CN108653794A (en) A kind of preparation method of based composite dressing for medical use
CN102921035A (en) Antiseptic dressing for deep infected wounds
CN106215223A (en) A kind of chitosan and bamboo fibre are blended the preparation method of wet nonwoven fabrics medical dressing
CA3012973C (en) Carboxymethlated cellulose sheet for covering a wound
CN102284080A (en) Method for preparing chitosan compound acetalized polyvinyl alcohol medical dressing
CN110025815B (en) Silver ion dressing used after anorectal operation and gynecological operation and preparation method thereof
CN106110372A (en) A kind of collagen sponge dressing containing medical base fabric
CN108714240A (en) A kind of preparation method of biomass styptic sponge
CN111481731A (en) Collagen-chitosan electrostatic spinning membrane composite alginate anti-seawater soaking application and preparation method thereof
RU2806364C1 (en) Method of obtaining hemostatic agent based on chitosan

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20161214

RJ01 Rejection of invention patent application after publication