CN106214546A - The preparation method of full Citrullus vulgaris ferment facial film - Google Patents
The preparation method of full Citrullus vulgaris ferment facial film Download PDFInfo
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- CN106214546A CN106214546A CN201610705030.1A CN201610705030A CN106214546A CN 106214546 A CN106214546 A CN 106214546A CN 201610705030 A CN201610705030 A CN 201610705030A CN 106214546 A CN106214546 A CN 106214546A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention discloses the preparation method of a kind of full Citrullus vulgaris ferment facial film, it is characterised in that comprise the following steps: separated with flesh of Pulp Citrulli by Citrullus vulgaris peel, afterwards the white peel of Citrullus vulgaris peel is separated with green peel;Green fruit peel powder is broken into EXOCARPIUM CITRULLI powder;Flesh of Pulp Citrulli quick-freezing rear cutout becomes fruit grain, and white peel quick-freezing rear cutout is become peel granule, standby;The mixing of peel granule, EXOCARPIUM CITRULLI powder and granule stem is carried out enzyme digestion reaction;Enzymatic hydrolysate and fruit grain are mixed to prepare the second mixture;White sugar and the alternately laying of the second mixture are carried out one time fermentation and obtains one time fermentation product;One time fermentation product is filtered, it is thus achieved that filtrate and filtrate, after carrying out secondary seal fermentation after mixing with filtrate, Fructus Citri Limoniae powder and Mel after pulverizing after filtrate quick-freezing, obtain full Citrullus vulgaris ferment, apply it to soak non-woven fabrics and obtain full Citrullus vulgaris ferment facial film.The inventive method through carrying out separating treatment and repeatedly after fermentation process to the different piece of Citrullus vulgaris, it is thus achieved that the full Citrullus vulgaris ferment of pure taste.
Description
Technical field
The present invention relates to ferment facial film technical field.It is more particularly related to a kind of full Citrullus vulgaris ferment facial film
Preparation method.
Background technology
Facial film is a kind of multipurpose cosmetics integrating cleaning, skin protection and beauty treatment, and its effect is applied to face
On skin, dried through certain time, skin is formed one layer of membranoid substance, after this film is taken off or washed off, can reach clean
The purpose of skin, skin protection and beauty treatment.Due to the adsorption of facial film, the secretory activity making skin is vigorous, is peeling off or is washing away facial film
Time, the secretions of skin, scurf, dirt etc. can being removed together along with facial film, skin just seems abnormal clean, reaches satisfied
Clean skin effect;Cover at skin surface due to facial film again, the evaporation of suppression moisture, thus soften skin horny layer, expand pore
With sweat gland mouth, making skin surface temperature increase, blood circulation promoting, the active nutritional making skin effectively absorb in facial film becomes
Point, play good skin care effect;Along with the formation of facial film is with dry, produced tension force makes the tensity of skin increase, and causes
Make the skin-tightening relaxed, this wrinkle being conducive to eliminating and reduce face, thus produce cosmetic result.
But, existing facial film contains multiple alcohols, plasticizer, preservative, surfactant and other additives etc. mostly,
It is not natural whitening skin and preserving moisture composition, skin is had certain zest, it is impossible to reach the effect of real skin care.
Summary of the invention
It is an object of the invention to solve at least the above, and the advantage that at least will be described later is provided.
It is a still further object of the present invention to provide the preparation method of a kind of full Citrullus vulgaris ferment facial film, through the different portions to Citrullus vulgaris
Point carry out separating treatment and repeatedly after fermentation process, it is thus achieved that the full Citrullus vulgaris ferment of pure taste, apply Citrullus vulgaris ferment to nothing afterwards
Spin after cloth soaks, it is thus achieved that the Citrullus vulgaris ferment facial film of abnormal smells from the patient delicate fragrance.
In order to realize according to object of the present invention and further advantage, it is provided that the preparation of a kind of full Citrullus vulgaris ferment facial film
Method, it is characterised in that comprise the following steps:
Step one, Citrullus vulgaris peel is separated with flesh of Pulp Citrulli, afterwards the white peel of Citrullus vulgaris peel is separated with green peel;
Step 2, by after the green peel quick-freezing of isolated, be ground into the EXOCARPIUM CITRULLI powder that particle diameter is 40-60 mesh, standby
With;
Step 3, particle diameter is become to be less than the fruit grain of 3cm the flesh of Pulp Citrulli quick-freezing rear cutout in step one, after white peel quick-freezing
It is cut into the particle diameter peel granule less than 0.5cm, standby;
Step 4, Citrullus vulgaris stem quick-freezing is cut into length less than the granule stem of 0.6cm, standby;
Step 5, it is the ratio of 2-3:1:1 by described peel granule, described EXOCARPIUM CITRULLI powder and granule stem according to volume ratio
Mix homogeneously prepares the first mixture, afterwards, is added to cellulase, and continuously stirred enzyme digestion reaction 2-4h obtains enzymolysis and produces
Thing, saves backup at 0-4 DEG C, and wherein, the temperature of enzyme digestion reaction is 35-38 DEG C, and the addition of cellulase is 1.5-3mg/Kg
First mixture;
Step 6, enzymatic hydrolysate is heated to 70-90 DEG C, insulated and stirred 10-15min, standby;
Step 7, it is 1:2-by the fruit grain in the enzymatic hydrolysate after heat treated in step 6 and step 3 according to volume ratio
The ratio of 3 is mixed to prepare the second mixture, standby;
Step 8, laying a layer thickness less than the white sugar layer of 1.5cm at fermenter base, on white sugar layer, laying depth is
Second mixture layer of 3-5cm, afterwards, repeats to lay white sugar layer and the second mixture layer four times, in the second mixing of the superiors
Inoculation yeast bacterium in nitride layer;
Step 9, repetition step 8, until the remaining space of fermentation vessel is less than the 8% of its capacity, are 25-28 in temperature
DEG C lower seal ferments 25-30 days, it is thus achieved that one time fermentation product;
Step 10, by one time fermentation product filter, it is thus achieved that filtrate and filtrate, little by being crushed to particle diameter after filtrate quick-freezing
In 80 mesh, standby;
Step 11, will pulverize after filtrate, filtrate, Fructus Citri Limoniae powder and Mel be 10:30-45:1:6's according to volume ratio
Carry out secondary seal fermentation after ratio mixing and obtain ferment in second time product in 2-3 month;
Step 12, by ferment in second time product through filtering and cryopreservation after pasteurize, it is thus achieved that full Citrullus vulgaris ferment;
Step 13, dry non-woven fabrics mask sheet being dipped in Citrullus vulgaris ferment keep 2-3h, afterwards, pack preserves,
Wherein, the non-deposited face side of non-woven fabrics mask sheet is uniformly distributed multiple bulge-structure with cavity, described bulge-structure
Opening is towards the deposited face side of non-woven fabrics mask sheet.
Preferably, wherein, in described step 3, particle diameter is become to be less than 2cm's the flesh of Pulp Citrulli quick-freezing rear cutout in step one
Fruit grain, becomes particle diameter to be less than the peel granule of 0.3cm white peel quick-freezing rear cutout, standby.
Preferably, wherein, in described step 5, the enzyme digestion reaction time is 2.5-3h.
Preferably, wherein, in described step 5, the temperature of enzyme digestion reaction is 38 DEG C, and the addition of cellulase is
2.5mg/Kg the first mixture.
Preferably, wherein, in described step 7, enzymatic hydrolysate is 1:3 with the volume ratio of the fruit grain in step 3.
Preferably, wherein, in described step 8, in each fermentation tank, saccharomycetic inoculum concentration is 0.5-1%.
Preferably, wherein, in described step 8, it is that 27-28 DEG C of lower seal ferments 30 days in temperature, it is thus achieved that one time fermentation
Product.
Preferably, wherein, in described step 10, filtrate, filtrate, Fructus Citri Limoniae powder and Mel after pulverizing are according to volume
Carry out secondary seal fermentation after mixing than the ratio for 10:30:1:6 and within 2-3 month, obtain ferment in second time product, wherein, fermentation temperature
Degree is for 28-30 DEG C.
A kind of full Citrullus vulgaris ferment applying above-mentioned preparation method to prepare.
Beneficial effects of the present invention:
The inventive method does not add allogenic water during preparing full Citrullus vulgaris ferment, but uses the water of flesh of Pulp Citrulli itself
Point, polysaccharide and fructose carry out fermentation process, maintain original local flavor of Citrullus vulgaris, by fermenting twice not only by EXOCARPIUM CITRULLI, west
Nutrient in melon stem and flesh of Pulp Citrulli fully decomposes and discharges, moreover it is possible to the nutrition in watermelon seeds fully extracted,
The full Citrullus vulgaris ferment prepared not only maintains original local flavor of Citrullus vulgaris, also has abundant nutritive value, such as: calcium, phosphorus,
Ferrum, potassium, vitamin A, vitamin C, lycopene and multiple essential amino acid, afterwards, be immersed in Citrullus vulgaris ferment by non-woven fabrics
In fully absorb Citrullus vulgaris ferment so that it is in nutritional labeling be adsorbed on non-woven fabrics and be prepared as Citrullus vulgaris ferment facial film, easily use,
Taste is fragrant and sweet, can reach relieving restlessness to a certain extent, solve summer-heat and effect of skin care, reach the effect of skin maintenance;?
Multiple bulge-structure is set, it is possible to many some full Citrullus vulgaris ferment of absorption in immersion process, afterwards, people on non-woven fabrics mask sheet
Use during, the more nutritional labeling absorbed in ferment, skin care.
The Citrullus vulgaris ferment facial film that the present invention provides is a kind of brand-new, science, ferment face pack prescription of safety, reaches to make
The vigor with safety and sanitation, increasing ferment, the pure Citrullus vulgaris fragrance keeping ferment, it is easy to accepted by general population and like
Like, beneficially marketing, reach to moisten, whitening and triple effects of driving away summer heat.
Part is embodied by the further advantage of the present invention, target and feature by description below, and part also will be by this
Invention research and practice and be understood by the person skilled in the art.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, to make those skilled in the art with reference to description
Word can be implemented according to this.
Should be appreciated that used herein such as " have ", " comprising " " including " term do not allot one or more its
Its element or the existence of a combination thereof or interpolation.
Embodiment 1
The present invention provides the preparation method of a kind of full Citrullus vulgaris ferment facial film, it is characterised in that comprise the following steps:
Step one, Citrullus vulgaris peel is separated with flesh of Pulp Citrulli, afterwards the white peel of Citrullus vulgaris peel is separated with green peel;
Step 2, by after the green peel quick-freezing of isolated, be ground into the EXOCARPIUM CITRULLI powder that particle diameter is 40 mesh, standby;
Step 3, particle diameter is become to be less than the fruit grain of 3cm the flesh of Pulp Citrulli quick-freezing rear cutout in step one, after white peel quick-freezing
It is cut into the particle diameter peel granule less than 0.5cm, standby;
Step 4, Citrullus vulgaris stem quick-freezing is cut into length less than the granule stem of 0.6cm, standby;
Step 5, described peel granule, described EXOCARPIUM CITRULLI powder and granule stem are mixed according to the ratio that volume ratio is 2:1:1
Closing and uniformly prepare the first mixture, afterwards, be added to cellulase, continuously stirred enzyme digestion reaction 2h obtains enzymatic hydrolysate,
Saving backup at 0-4 DEG C, wherein, the temperature of enzyme digestion reaction is 35-38 DEG C, and the addition of cellulase is that 1.5mg/Kg first mixes
Compound;
Step 6, enzymatic hydrolysate is heated to 70 DEG C, insulated and stirred 10min, standby;
Step 7, it is 1:2 by the fruit grain in the enzymatic hydrolysate after heat treated in step 6 and step 3 according to volume ratio
Ratio be mixed to prepare the second mixture, standby;
Step 8, laying a layer thickness less than the white sugar layer of 1.5cm at fermenter base, on white sugar layer, laying depth is
Second mixture layer of 3cm, afterwards, repeats to lay white sugar layer and the second mixture layer four times, at the second mixture of the superiors
Inoculation yeast bacterium on layer;
Step 9, repetition step 8 are until the remaining space of fermentation vessel is less than the 8% of its capacity, at temperature is 25 DEG C
Sealing and fermenting 25 days, it is thus achieved that one time fermentation product;
Step 10, by one time fermentation product filter, it is thus achieved that filtrate and filtrate, little by being crushed to particle diameter after filtrate quick-freezing
In 80 mesh, standby;
Step 11, will pulverize after filtrate, filtrate, Fructus Citri Limoniae powder and Mel according to the ratio that volume ratio is 10:30:1:6
Carry out secondary seal fermentation after example mixing and obtain ferment in second time product in 2-3 month;And
Step 12, by ferment in second time product through filtering and cryopreservation after pasteurize, it is thus achieved that full Citrullus vulgaris ferment;
Step 13, dry non-woven fabrics mask sheet being dipped in Citrullus vulgaris ferment keep 2-3h, afterwards, pack preserves,
Wherein, the non-deposited face side of non-woven fabrics mask sheet is uniformly distributed multiple bulge-structure with cavity, described bulge-structure
Opening is towards the deposited face side of non-woven fabrics mask sheet.
Embodiment 2
The present invention provides the preparation method of a kind of full Citrullus vulgaris ferment facial film, it is characterised in that comprise the following steps:
Step one, Citrullus vulgaris peel is separated with flesh of Pulp Citrulli, afterwards the white peel of Citrullus vulgaris peel is separated with green peel;
Step 2, by after the green peel quick-freezing of isolated, be ground into the EXOCARPIUM CITRULLI powder that particle diameter is 60 mesh, standby;
Step 3, the fruit grain becoming particle diameter to be 2cm the flesh of Pulp Citrulli quick-freezing rear cutout in step one, by white peel quick-freezing rear cutout
Become the particle diameter peel granule less than 0.4cm, standby;
Step 4, Citrullus vulgaris stem quick-freezing is cut into length less than the granule stem of 0.5cm, standby;
Step 5, described peel granule, described EXOCARPIUM CITRULLI powder and granule stem are mixed according to the ratio that volume ratio is 2:1:1
Closing and uniformly prepare the first mixture, afterwards, be added to cellulase, continuously stirred enzyme digestion reaction 2-4h obtains enzymolysis and produces
Thing, saves backup at 0-4 DEG C, and wherein, the temperature of enzyme digestion reaction is 35-38 DEG C, and the addition of cellulase is 2mg/Kg first
Mixture;
Step 6, enzymatic hydrolysate is heated to 70 DEG C, insulated and stirred 15min, standby;
Step 7, it is 1:3 by the fruit grain in the enzymatic hydrolysate after heat treated in step 6 and step 3 according to volume ratio
Ratio be mixed to prepare the second mixture, standby;
Step 8, laying a layer thickness less than the white sugar layer of 1.5cm at fermenter base, on white sugar layer, laying depth is
Second mixture layer of 5cm, afterwards, repeats to lay white sugar layer and the second mixture layer four times, at the second mixture of the superiors
Inoculation yeast bacterium on layer;
Step 9, repetition step 8 are until the remaining space of fermentation vessel is less than the 8% of its capacity, at temperature is 28 DEG C
Sealing and fermenting 25 days, it is thus achieved that one time fermentation product;
Step 10, by one time fermentation product filter, it is thus achieved that filtrate and filtrate, little by being crushed to particle diameter after filtrate quick-freezing
In 80 mesh, standby;
Step 11, will pulverize after filtrate, filtrate, Fructus Citri Limoniae powder and Mel according to the ratio that volume ratio is 10:35:1:6
Carry out secondary seal fermentation after example mixing and obtain ferment in second time product in 3 months;And
Step 12, by ferment in second time product through filtering and cryopreservation after pasteurize, it is thus achieved that full Citrullus vulgaris ferment;
Step 13, dry non-woven fabrics mask sheet being dipped in Citrullus vulgaris ferment keep 2-3h, afterwards, pack preserves,
Wherein, the non-deposited face side of non-woven fabrics mask sheet is uniformly distributed multiple bulge-structure with cavity, described bulge-structure
Opening is towards the deposited face side of non-woven fabrics mask sheet.
Embodiment 3
The present invention provides the preparation method of a kind of full Citrullus vulgaris ferment facial film, it is characterised in that comprise the following steps:
Step one, Citrullus vulgaris peel is separated with flesh of Pulp Citrulli, afterwards the white peel of Citrullus vulgaris peel is separated with green peel;
Step 2, by after the green peel quick-freezing of isolated, be ground into the EXOCARPIUM CITRULLI powder that particle diameter is 40 mesh, standby;
Step 3, particle diameter is become to be less than the fruit grain of 3cm the flesh of Pulp Citrulli quick-freezing rear cutout in step one, after white peel quick-freezing
It is cut into the particle diameter peel granule less than 0.2cm, standby;
Step 4, Citrullus vulgaris stem quick-freezing is cut into length less than the granule stem of 0.3cm, standby;
Step 5, it is the ratio of 2-3:1:1 by described peel granule, described EXOCARPIUM CITRULLI powder and granule stem according to volume ratio
Mix homogeneously prepares the first mixture, afterwards, is added to cellulase, and continuously stirred enzyme digestion reaction 4h obtains enzymolysis and produces
Thing, saves backup at 0-4 DEG C, and wherein, the temperature of enzyme digestion reaction is 38 DEG C, and the addition of cellulase is that 3mg/Kg first mixes
Thing;
Step 6, enzymatic hydrolysate is heated to 90 DEG C, insulated and stirred 10-15min, standby;
Step 7, it is 1:2-by the fruit grain in the enzymatic hydrolysate after heat treated in step 6 and step 3 according to volume ratio
The ratio of 3 is mixed to prepare the second mixture, standby;
Step 8, laying a layer thickness less than the white sugar layer of 1.5cm at fermenter base, on white sugar layer, laying depth is
Second mixture layer of 3-5cm, afterwards, repeats to lay white sugar layer and the second mixture layer four times, in the second mixing of the superiors
Inoculation yeast bacterium in nitride layer;
Step 9, repetition step 8, until the remaining space of fermentation vessel is less than the 8% of its capacity, are 25-28 in temperature
DEG C lower seal ferments 25-30 days, it is thus achieved that one time fermentation product;
Step 10, by one time fermentation product filter, it is thus achieved that filtrate and filtrate, little by being crushed to particle diameter after filtrate quick-freezing
In 80 mesh, standby;
Step 11, will pulverize after filtrate, filtrate, Fructus Citri Limoniae powder and Mel according to the ratio that volume ratio is 10:35:1:6
Carry out secondary seal fermentation after example mixing and obtain ferment in second time product in 2-3 month;
Step 12, by ferment in second time product through filtering and cryopreservation after pasteurize, it is thus achieved that full Citrullus vulgaris ferment;
Step 13, dry non-woven fabrics mask sheet being dipped in Citrullus vulgaris ferment keep 2-3h, afterwards, pack preserves,
Wherein, the non-deposited face side of non-woven fabrics mask sheet is uniformly distributed multiple bulge-structure with cavity, described bulge-structure
Opening is towards the deposited face side of non-woven fabrics mask sheet.
Embodiment 4
The present invention provides the preparation method of a kind of full Citrullus vulgaris ferment facial film, it is characterised in that comprise the following steps:
Step one, Citrullus vulgaris peel is separated with flesh of Pulp Citrulli, afterwards the white peel of Citrullus vulgaris peel is separated with green peel;
Step 2, by after the green peel quick-freezing of isolated, be ground into the EXOCARPIUM CITRULLI powder that particle diameter is 60 mesh, standby;
Step 3, particle diameter is become to be less than the fruit grain of 3cm the flesh of Pulp Citrulli quick-freezing rear cutout in step one, after white peel quick-freezing
It is cut into the particle diameter peel granule less than 0.5cm, standby;
Step 4, Citrullus vulgaris stem quick-freezing is cut into length less than the granule stem of 0.6cm, standby;
Step 5, it is the ratio of 2-3:1:1 by described peel granule, described EXOCARPIUM CITRULLI powder and granule stem according to volume ratio
Mix homogeneously prepares the first mixture, afterwards, is added to cellulase, and continuously stirred enzyme digestion reaction 3h obtains enzymolysis and produces
Thing, saves backup at 0-4 DEG C, and wherein, the temperature of enzyme digestion reaction is 35-38 DEG C, and the addition of cellulase is 3mg/Kg first
Mixture;
Step 6, enzymatic hydrolysate is heated to 80 DEG C, insulated and stirred 15min, standby;
Step 7, it is 1:3 by the fruit grain in the enzymatic hydrolysate after heat treated in step 6 and step 3 according to volume ratio
Ratio be mixed to prepare the second mixture, standby;
Step 8, laying a layer thickness less than the white sugar layer of 1.5cm at fermenter base, on white sugar layer, laying depth is
Second mixture layer of 3-5cm, afterwards, repeats to lay white sugar layer and the second mixture layer four times, in the second mixing of the superiors
Inoculation yeast bacterium in nitride layer;
Step 9, repetition step 8, until the remaining space of fermentation vessel is less than the 8% of its capacity, are 25-28 in temperature
DEG C lower seal ferments 25-30 days, it is thus achieved that one time fermentation product;
Step 10, by one time fermentation product filter, it is thus achieved that filtrate and filtrate, little by being crushed to particle diameter after filtrate quick-freezing
In 80 mesh, standby;
Step 11, will pulverize after filtrate, filtrate, Fructus Citri Limoniae powder and Mel according to the ratio that volume ratio is 10:45:1:6
Carry out secondary seal fermentation after example mixing and obtain ferment in second time product in 2-3 month;
Step 12, by ferment in second time product through filtering and cryopreservation after pasteurize, it is thus achieved that full Citrullus vulgaris ferment;
Step 13, dry non-woven fabrics mask sheet being dipped in Citrullus vulgaris ferment keep 2-3h, afterwards, pack preserves,
Wherein, the non-deposited face side of non-woven fabrics mask sheet is uniformly distributed multiple bulge-structure with cavity, described bulge-structure
Opening is towards the deposited face side of non-woven fabrics mask sheet.
The full Citrullus vulgaris ferment prepared through said method is nutritious, and in good taste, color is beautiful, homogenizing, it is not necessary to adds and protects
Toner, is full-natural nutritive fruit ferment, extracts the most not by Exocarpium Citrulli of concern and watermelon seeds through the inventive method
In nutritional labeling, enrich fruit ferment kind.
Although embodiment of the present invention are disclosed as above, but it is not restricted in description and embodiment listed
Using, it can be applied to various applicable the field of the invention completely, for those skilled in the art, and can be easily
Realizing other amendment, therefore under the general concept limited without departing substantially from claim and equivalency range, the present invention does not limit
In specific details with shown here as the embodiment with description.
Claims (9)
1. the preparation method of a full Citrullus vulgaris ferment facial film, it is characterised in that comprise the following steps:
Step one, Citrullus vulgaris peel is separated with flesh of Pulp Citrulli, afterwards the white peel of Citrullus vulgaris peel is separated with green peel;
Step 2, by after the green peel quick-freezing of isolated, be ground into the EXOCARPIUM CITRULLI powder that particle diameter is 40-60 mesh, standby;
Step 3, become particle diameter to be less than the fruit grain of 3cm the flesh of Pulp Citrulli quick-freezing rear cutout in step one, be cut into after white peel quick-freezing
The particle diameter peel granule less than 0.5cm, standby;
Step 4, Citrullus vulgaris stem quick-freezing is cut into length less than the granule stem of 0.6cm, standby;
Step 5, by described peel granule, described EXOCARPIUM CITRULLI powder and granule stem according to the mixing of ratio that volume ratio is 2-3:1:1
Uniformly preparing the first mixture, afterwards, be added to cellulase, continuously stirred enzyme digestion reaction 2-4h obtains enzymatic hydrolysate,
Saving backup at 0-4 DEG C, wherein, the temperature of enzyme digestion reaction is 35-38 DEG C, and the addition of cellulase is 1.5-3mg/Kg first
Mixture;
Step 6, enzymatic hydrolysate is heated to 70-90 DEG C, insulated and stirred 10-15min, standby;
Step 7, it is 1:2-3's by the fruit grain in the enzymatic hydrolysate after heat treated in step 6 and step 3 according to volume ratio
Ratio is mixed to prepare the second mixture, standby;
Step 8, laying a layer thickness less than the white sugar layer of 1.5cm at fermenter base, on white sugar layer, laying depth is 3-
Second mixture layer of 5cm, afterwards, repeats to lay white sugar layer and the second mixture layer four times, at the second mixture of the superiors
Inoculation yeast bacterium on layer;
Step 9, repetition step 8 are until the remaining space of fermentation vessel is less than the 8% of its capacity, at temperature is 25-28 DEG C
Sealing and fermenting 25-30 days, it is thus achieved that one time fermentation product;
Step 10, one time fermentation product is filtered, it is thus achieved that filtrate and filtrate, particle diameter will be crushed to after filtrate quick-freezing less than 80
Mesh, standby;
Step 11, will pulverize after filtrate, filtrate, Fructus Citri Limoniae powder and Mel be the ratio of 10:30-45:1:6 according to volume ratio
Carry out secondary seal fermentation after mixing and obtain ferment in second time product in 2-3 month;And
Step 12, by ferment in second time product through filtering and cryopreservation after pasteurize, it is thus achieved that full Citrullus vulgaris ferment;
Step 13, dry non-woven fabrics mask sheet being dipped in Citrullus vulgaris ferment keep 2-3h, afterwards, pack preserves, wherein,
It is uniformly distributed multiple bulge-structure with cavity, the opening court of described bulge-structure on the non-deposited face side of non-woven fabrics mask sheet
To the deposited face side of non-woven fabrics mask sheet.
2. the preparation method of full Citrullus vulgaris ferment facial film as claimed in claim 1, it is characterised in that in described step 3, will step
Flesh of Pulp Citrulli quick-freezing rear cutout in rapid one becomes particle diameter to be less than the fruit grain of 2cm, becomes particle diameter to be less than 0.3cm's white peel quick-freezing rear cutout
Peel granule, standby.
3. the preparation method of full Citrullus vulgaris ferment facial film as claimed in claim 1, it is characterised in that in described step 5, enzymolysis
Response time is 2.5-3h.
4. the preparation method of full Citrullus vulgaris ferment facial film as claimed in claim 1, it is characterised in that in described step 5, enzymolysis
The temperature of reaction is 38 DEG C, and the addition of cellulase is 2.5mg/Kg the first mixture.
5. the preparation method of full Citrullus vulgaris ferment facial film as claimed in claim 1, it is characterised in that in described step 7, enzymolysis
Product is 1:3 with the volume ratio of the fruit grain in step 3.
6. the preparation method of full Citrullus vulgaris ferment facial film as claimed in claim 1, it is characterised in that in described step 8, each
In fermentation tank, saccharomycetic inoculum concentration is 0.5-1%.
7. the preparation method of full Citrullus vulgaris ferment facial film as claimed in claim 1, it is characterised in that in described step 8, in temperature
Degree ferments 30 days for 27-28 DEG C of lower seal, it is thus achieved that one time fermentation product.
8. the preparation method of full Citrullus vulgaris ferment facial film as claimed in claim 1, it is characterised in that in described step 10, by powder
Filtrate, filtrate, Fructus Citri Limoniae powder and Mel after broken carries out secondary seal after mixing according to the ratio that volume ratio is 10:30:1:6 and sends out
Within ferment 2-3 month, obtaining ferment in second time product, wherein, fermentation temperature is 28-30 DEG C.
9. apply full Citrullus vulgaris ferment prepared by the preparation method as described in claim 1-8 for one kind.
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