CN1061973C - Technology for extracting amino acid of animal and plant - Google Patents
Technology for extracting amino acid of animal and plant Download PDFInfo
- Publication number
- CN1061973C CN1061973C CN93111781A CN93111781A CN1061973C CN 1061973 C CN1061973 C CN 1061973C CN 93111781 A CN93111781 A CN 93111781A CN 93111781 A CN93111781 A CN 93111781A CN 1061973 C CN1061973 C CN 1061973C
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- silkworm chrysalis
- pollen
- amino acid
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- animal
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Abstract
The present invention belongs to a preparing technology of amino acid, which comprises a processing technology of pollen, a processing technology of silkworm pupas and a composite processing technology of a pollen extracting solution and silkworm pupas. The present invention is characterized in that the whole technology processes natural substances to ensure the pure natural property of a finished product. Besides, all procedures are carried out at a normal temperature. Compared with the original high temperature, the present invention has less damage to nutrients. Thus, the nutritive value of the finished product is improved.
Description
The present invention relates to amino acid whose preparation method.
Protein is the important composition composition of body, and amino acid is the fundamental structural unit of synthetic protein.As the pollen and the silkworm chrysalis that extract amino acid whose main raw material, quite abundant in the resource of China, because people are to pollen, the nutrition of silkworm chrysalis and drug action understanding differ, and therefore, natural pollen of China and silkworm chrysalis be not as yet by a large amount of Application and Development.
At present, when in pollen and silkworm chrysalis, extracting amino acid, normally make product separately, promptly from pollen, produce plant type amino acid respectively and from silkworm chrysalis, extract animal-type amino acid, its extracting method normally adopts biology and enzymolysis process to extract amino acid, because these method majorities are by the chemosynthesis composition, therefore, it is so-called pure natural that its inherent content just can not reach.
The objective of the invention is to design the method that a kind of interaction that utilizes treated pollen and silkworm chrysalis prepares amino acid of animal and plant.
Its main technical schemes comprises A, the treatment process of pollen: the pollen pre-treatment → silt → extraction → suction filtration sieves; B, silkworm chrysalis treatment process: silkworm chrysalis pre-treatment → degreasing deodorizing → oven dry; The composite treatment process of C, pollen extracting liquid and silkworm chrysalis:
A, wet bubble: respectively by putting into reactor with distilled water after 50% the mixed, bubble is wet under 40 ℃-45 ℃ temperature, stirs 4 hours postcooling to normal temperature with pollen extracting liquid and using baked silkworm chrysalis, and wherein distilled water accounts for 83.3%, and mixture accounts for 16.7%;
B, defibrination press filtration: chilled mixture is worn into slurry back extrusion process in the filter cake machine in colloidal mill;
C, emulsification enzymolysis, the mixture after the extruding is the high-pressure pump internal emulsification of 6000 handkerchiefs (600Kg) at pressure, adds 5% pineapple juice again in the material after emulsification, enzymolysis becomes amino acid of animal and plant;
D, extraction: the material behind the enzymolysis is extracted muddy liquid and filter cake once more in the suction filtration machine;
E, clarification layering: the giant knotweed of adding 1 ‰ is clarified in muddy liquid, makes it to be divided into significantly two-layer;
F, suction filtration concentrate: the supernatant liquid after the layering is placed in 60 ℃ of vacuum chambers under the temperature with the extraction of core vacuum machine is condensed into pale crystal;
In the silkworm chrysalis treatment process, put into 30 ℃-36 ℃ clear water after bright silkworm chrysalis gilled, add 1 ‰ giant knotweed again and mix thoroughly, carry out rinsing;
In the degreasing deodorization process of silkworm chrysalis, add 5% pure pineapple juice in the silkworm chrysalis after cleaning, degreasing deodorizing under 40 ℃-50 ℃ temperature.
Advantage of the present invention be since the present invention in the treatment process of silkworm chrysalis, employing is put into clear water with silkworm chrysalis, add 1 ‰ Chinese medicine giant knotweed again and mix the mode of immersion thoroughly, allow its natural swelling, and then in colloidal mill, wear into slurry with treated pollen, and compare with original high speed pulverization mode, can keep the nutritive value of silkworm chrysalis preferably, remove raw meat, smell in the silkworm chrysalis, guaranteed the distinctive natural fragrance of natural animal-plant; Secondly, in operation of the present invention, all under low-temperature condition, extract and emulsification, compare with original high temperature (about 200 ℃), can keep natural ferment and biological enzyme activity in the plant pollen effectively, the 3rd, in technology of the present invention, used additive is natural matter, compares with the mode of original employing chemosynthesis composition, can guarantee amino acid whose pure natural degree preferably.The 4th, the present invention utilizes the organized enzyme of plant pollen that the animal silkworm chrysalis is carried out enzymolysis, this mode had both avoided need carrying out silkworm chrysalis with the chemosynthesis enzyme defective of enzymolysis in the past, realized that again Plants and Animals is amino acid whose fused, thereby broken through the water-soluble boundary that can not fuse, produced a kind of brand-new amino acid of animal and plant with liposoluble
Further describe embodiments of the invention below.Content as referred to herein is weight percentage.
One, earlier pollen is handled
1, the pre-treatment of pollen: pollen and clear water are put into reactor, and wherein pollen accounts for 16.7%, and water accounts for 83.3%, under 36 ℃-38 ℃ temperature, through the stirring of not timing in 17-18 hour.
2, the silt that sieves: pretreated pollen is removed foreign material and silt with 40 purposes sieve.
3, extract, the pollen of removing foreign material silt is infiltrated distilled water by the product standard nutritive index again, its content is pollen 16.7%, and water 83.3% carries out vacuum extraction then under 45 ℃-55 ℃ temperature.
4, suction filtration, the liquid after extracting is split suction filtration in the vacuum filtration machine again.
Two, the treatment process of silkworm chrysalis
1, the pre-treatment of silkworm chrysalis: earlier bright silkworm chrysalis is gilled, the giant knotweed of adding 1 ‰ is mixed thoroughly in 30-36 ℃ clear water then, carries out about 4 hours rinsing.
2, degreasing deodorizing: put into 5% pure pineapple juice in the silkworm chrysalis after cleaning, degreasing deodorizing under 40 ℃-50 ℃ temperature.
3, the Radix Glycyrrhizae of adding 1 ‰ in through the bright silkworm chrysalis after the degreasing deodorizing is dried in 60 ℃ dry drying room again.
Three, the composite treatment process of pollen extracting liquid and silkworm chrysalis
1, wet bubble: respectively by putting into reactor with distilled water after 50% the mixed, bubble is wet under 40 ℃-45 ℃ temperature, stirs 4 hours postcooling to normal temperature with pollen extracting liquid and using baked silkworm chrysalis, and wherein distilled water accounts for 83.3%, and mixture accounts for 16.7%.
2, the defibrination press filtration, chilled mixture is worn into slurry back extrusion process in the filter cake machine in colloidal mill.
3, the mixture after the emulsification enzymolysis extruding is that the high-pressure pump internal emulsification of 6000 handkerchiefs (600Kg) adds 5% pineapple juice again in the material after emulsification at pressure, and enzymolysis becomes amino acid of animal and plant.
4, extract: the material behind the enzymolysis is extracted muddy liquid and filter cake once more in the suction filtration machine.
5, clarification layering: the giant knotweed of adding 1 ‰ is clarified in muddy liquid, makes it to be divided into significantly two-layer.
B, suction filtration concentrate: the supernatant liquid after the layering is placed in 60 ℃ of vacuum chambers under the temperature with the extraction of core vacuum machine is condensed into pale crystal.
Required according to each level then requirement is made various ways such as liquid state or capsular with the powdery amino acid starting material.
Claims (3)
1, amino acid of animal and plant preparation method, the treatment process that comprises A, pollen is: the pollen pre-treatment → silt → extraction → suction filtration sieves, B, silkworm chrysalis treatment process are: silkworm chrysalis pre-treatment → degreasing deodorizing → oven dry is characterized in that this technology also comprises C: the composite treatment process of pollen extracting liquid and silkworm chrysalis:
A, wet bubble: respectively by putting into reactor with distilled water after 50% the mixed, bubble is wet under 40 ℃-45 ℃ temperature, stirs 4 hours postcooling to normal temperature with pollen extracting liquid and using baked silkworm chrysalis, and wherein distilled water accounts for 83.3%, and mixture accounts for 16.7%;
B, defibrination press filtration: chilled mixture is worn into slurry back extrusion process in the filter cake machine in colloidal mill,
C, emulsification enzymolysis: the mixture after the extruding is the high-pressure pump internal emulsification of 6000 handkerchiefs at pressure, adds 5% pineapple juice again in the material after emulsification, and enzymolysis becomes amino acid of animal and plant;
D, extraction: the material behind the enzymolysis is extracted muddy liquid and filter cake once more in the suction filtration machine;
E, clarification layering: the giant knotweed of adding 1 ‰ is clarified in muddy liquid, makes it to be divided into significantly two-layer;
F, suction filtration concentrate: the supernatant liquid after the layering is placed in 60 ℃ of vacuum chambers under the temperature with the extraction of core vacuum machine is condensed into pale crystal.
2, method according to claim 1 is characterized in that in the silkworm chrysalis pretreatment process, puts into 30 ℃-36 ℃ clear water after bright silkworm chrysalis is gilled, and adds 1 ‰ giant knotweed again and mixes thoroughly, carries out rinsing.
3, method according to claim 1 is characterized in that in the degreasing deodorizing operation of silkworm chrysalis, adds 5% pineapple juice in the silkworm chrysalis after cleaning, degreasing deodorizing under 40 ℃-50 ℃ temperature.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN93111781A CN1061973C (en) | 1993-10-27 | 1993-10-27 | Technology for extracting amino acid of animal and plant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN93111781A CN1061973C (en) | 1993-10-27 | 1993-10-27 | Technology for extracting amino acid of animal and plant |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1102181A CN1102181A (en) | 1995-05-03 |
| CN1061973C true CN1061973C (en) | 2001-02-14 |
Family
ID=4989540
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN93111781A Expired - Fee Related CN1061973C (en) | 1993-10-27 | 1993-10-27 | Technology for extracting amino acid of animal and plant |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1061973C (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN87106139A (en) * | 1987-09-03 | 1988-02-10 | 浙江省农业科学院 | Method for producing pollen essence |
| CN86108878A (en) * | 1986-12-30 | 1988-07-20 | 南宁市味精厂 | From pollen, extract the method for nutrition with enzyme |
| CN1039844A (en) * | 1988-10-14 | 1990-02-21 | 马瑞英 | From silkworm chrysalis, extract the method for amino acid composite liquid |
-
1993
- 1993-10-27 CN CN93111781A patent/CN1061973C/en not_active Expired - Fee Related
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN86108878A (en) * | 1986-12-30 | 1988-07-20 | 南宁市味精厂 | From pollen, extract the method for nutrition with enzyme |
| CN87106139A (en) * | 1987-09-03 | 1988-02-10 | 浙江省农业科学院 | Method for producing pollen essence |
| CN1039844A (en) * | 1988-10-14 | 1990-02-21 | 马瑞英 | From silkworm chrysalis, extract the method for amino acid composite liquid |
Non-Patent Citations (1)
| Title |
|---|
| 中成药1992.VOL14[7] 1992.1.1 花粉加工技术研究.陈传盈等 * |
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| Publication number | Publication date |
|---|---|
| CN1102181A (en) | 1995-05-03 |
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