CN106190584A - A kind of extracting method of Herba Lysimachiae foenum-graeci quintessence oil - Google Patents
A kind of extracting method of Herba Lysimachiae foenum-graeci quintessence oil Download PDFInfo
- Publication number
- CN106190584A CN106190584A CN201610731725.7A CN201610731725A CN106190584A CN 106190584 A CN106190584 A CN 106190584A CN 201610731725 A CN201610731725 A CN 201610731725A CN 106190584 A CN106190584 A CN 106190584A
- Authority
- CN
- China
- Prior art keywords
- herba lysimachiae
- lysimachiae foenum
- quintessence oil
- extracting method
- graeci
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Medicines Containing Plant Substances (AREA)
- Cosmetics (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention discloses the extracting method of a kind of Herba Lysimachiae foenum-graeci quintessence oil, comprises the steps: the Herba Lysimachiae foenum-graeci lyophilization that (1) will clean up, pulverized 100 mesh sieves；(2) powder of step (1) adds water, by ultrasonic Treatment 50～70min；(3) powder after step (2) processes is put into distillation in steam distillation apparatus and obtain Herba Lysimachiae foenum-graeci quintessence oil.Compared with the conventional steam way of distillation, the extracting method of the present invention is remarkably improved the oil yield of Herba Lysimachiae foenum-graeci quintessence oil.
Description
Technical field
The invention belongs to field of plant extraction, be specifically related to the extracting method of a kind of Herba Lysimachiae foenum-graeci quintessence oil.
Background technology
Herba Lysimachiae foenum-graeci (Lysimachia foenum-graecum Hance) is Primulaceae Lysimachia plant, has another name called smoked
Clothing grass, Rhizoma et radix valerianae etc., mainly originate in the ground such as Guangxi, Guangdong, Yunnan, be the valable starting materials of perfume industry, be largely used to height in China
Shelves cigarette, the perfuming of wine, Herba Lysimachiae foenum-graeci also has acrid in the mouth, sweet, warm characteristic, has the effects such as heat clearing away, circulation of qi promoting, pain relieving, anthelmintic, be used for treating
Flu, headache, toothache.The common extracting method of Herba Lysimachiae foenum-graeci quintessence oil has steam distillation and organic solvent extraction, due to water
Vapor distillation method equipment cost is low, simple to operate and is widely used.
Summary of the invention
It is an object of the invention to the steam distillation of existing Herba Lysimachiae foenum-graeci quintessence oil is improved, it is provided that a kind of Herba Lysimachiae foenum-graeci
The higher extracting method of quintessence oil oil yield.
In order to solve above-mentioned technical problem, the invention provides following technical scheme:
The extracting method of a kind of Herba Lysimachiae foenum-graeci quintessence oil, comprises the steps:
(1) the Herba Lysimachiae foenum-graeci lyophilization that will clean up, pulverized 100 mesh sieves；
(2) powder of step (1) adds water, by ultrasonic Treatment 50～70min；
(3) powder after step (2) processes is put into distillation in steam distillation apparatus and obtain Herba Lysimachiae foenum-graeci quintessence oil.
Detailed description of the invention
Hereinafter the preferred embodiments of the present invention are illustrated, it will be appreciated that preferred embodiment described herein is only used
In the description and interpretation present invention, it is not intended to limit the present invention.
Embodiment 1
The extracting method of a kind of Herba Lysimachiae foenum-graeci quintessence oil, comprises the steps:
(1) first Herba Lysimachiae foenum-graeci is cleaned up, more freeze-dried after, pulverized 100 mesh sieves, the powder obtained is standby；
(2) powder of step (1) is added in ultrasonic cell-break machine, add appropriate water (solid-liquid ratio be generally 1:5～
6 g/g), ultrasound wave (power 1500～1800w, ultrasonic frequency 20～25KHz) processes 50～70min, and during process, temperature should
Control less than 30 DEG C；
(3) powder after step (2) processes being put in steam distillation apparatus and distilled, after steam condensation, liquid liquid divides
From obtaining Herba Lysimachiae foenum-graeci quintessence oil, in faint yellow.
With tradition without compared with the steam distillation of ultrasonic Treatment, in distillation condition and conventional steam distillation technique
In the case of identical, the oil yield of extracting method of the present invention can improve 3～4 times relatively, and distillation time can shorten 1/2.
Finally it is noted that the foregoing is only the preferred embodiments of the present invention, it is not limited to the present invention,
Although being described in detail the present invention with reference to previous embodiment, for a person skilled in the art, it still may be used
So that the technical scheme described in foregoing embodiments to be modified, or wherein portion of techniques feature is carried out equivalent.
All within the spirit and principles in the present invention, any modification, equivalent substitution and improvement etc. made, should be included in the present invention's
Within protection domain.
Claims (1)
1. an extracting method for Herba Lysimachiae foenum-graeci quintessence oil, comprises the steps:
(1) the Herba Lysimachiae foenum-graeci lyophilization that will clean up, pulverized 100 mesh sieves；
(2) powder of step (1) adds water, by ultrasonic Treatment 50～70min；
(3) powder after step (2) processes is put into distillation in steam distillation apparatus and obtain Herba Lysimachiae foenum-graeci quintessence oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610731725.7A CN106190584A (en) | 2016-08-26 | 2016-08-26 | A kind of extracting method of Herba Lysimachiae foenum-graeci quintessence oil |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610731725.7A CN106190584A (en) | 2016-08-26 | 2016-08-26 | A kind of extracting method of Herba Lysimachiae foenum-graeci quintessence oil |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106190584A true CN106190584A (en) | 2016-12-07 |
Family
ID=57525747
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610731725.7A Pending CN106190584A (en) | 2016-08-26 | 2016-08-26 | A kind of extracting method of Herba Lysimachiae foenum-graeci quintessence oil |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106190584A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101457178A (en) * | 2008-12-10 | 2009-06-17 | 广西中烟工业有限责任公司 | Method for extracting water-soluble volatilization component from lysimachia foenum-graecum |
| CN103122277A (en) * | 2013-01-23 | 2013-05-29 | 兰州大学 | Method for extracting natural flavor with dimethyl ether |
-
2016
- 2016-08-26 CN CN201610731725.7A patent/CN106190584A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101457178A (en) * | 2008-12-10 | 2009-06-17 | 广西中烟工业有限责任公司 | Method for extracting water-soluble volatilization component from lysimachia foenum-graecum |
| CN103122277A (en) * | 2013-01-23 | 2013-05-29 | 兰州大学 | Method for extracting natural flavor with dimethyl ether |
Non-Patent Citations (1)
| Title |
|---|
| 吴晓菊等: "超声强化水蒸气蒸馏提取神香草精油的工艺", 《食品研究与开发》 * |
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| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20161207 |
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| RJ01 | Rejection of invention patent application after publication |