CN106190463A - A kind of for process stamping parts thermostable rustproof oil and preparation method - Google Patents
A kind of for process stamping parts thermostable rustproof oil and preparation method Download PDFInfo
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- CN106190463A CN106190463A CN201610529904.2A CN201610529904A CN106190463A CN 106190463 A CN106190463 A CN 106190463A CN 201610529904 A CN201610529904 A CN 201610529904A CN 106190463 A CN106190463 A CN 106190463A
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- silane coupler
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- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
- C10M169/04—Mixtures of base-materials and additives
- C10M169/044—Mixtures of base-materials and additives the additives being a mixture of non-macromolecular and macromolecular compounds
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
- C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
- C10M2203/1006—Petroleum or coal fractions, e.g. tars, solvents, bitumen used as base material
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/28—Esters
- C10M2207/283—Esters of polyhydroxy compounds
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- C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
- C10M2207/40—Fatty vegetable or animal oils
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
- C10M2215/04—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms
- C10M2215/042—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to acyclic or cycloaliphatic carbon atoms containing hydroxy groups; Alkoxylated derivatives thereof
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- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/223—Five-membered rings containing nitrogen and carbon only
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2215/22—Heterocyclic nitrogen compounds
- C10M2215/223—Five-membered rings containing nitrogen and carbon only
- C10M2215/224—Imidazoles
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- C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2217/04—Macromolecular compounds from nitrogen-containing monomers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2217/044—Polyamides
- C10M2217/0443—Polyamides used as base material
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/02—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds
- C10M2219/024—Sulfur-containing compounds obtained by sulfurisation with sulfur or sulfur-containing compounds of esters, e.g. fats
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- C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
- C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
- C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
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- C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
- C10M2229/02—Unspecified siloxanes; Silicones
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- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2229/00—Organic macromolecular compounds containing atoms of elements not provided for in groups C10M2205/00, C10M2209/00, C10M2213/00, C10M2217/00, C10M2221/00 or C10M2225/00 as ingredients in lubricant compositions
- C10M2229/04—Siloxanes with specific structure
- C10M2229/041—Siloxanes with specific structure containing aliphatic substituents
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- C10N2010/00—Metal present as such or in compounds
- C10N2010/04—Groups 2 or 12
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/10—Inhibition of oxidation, e.g. anti-oxidants
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/12—Inhibition of corrosion, e.g. anti-rust agents or anti-corrosives
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- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/24—Metal working without essential removal of material, e.g. forming, gorging, drawing, pressing, stamping, rolling or extruding; Punching metal
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- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/20—Metal working
- C10N2040/244—Metal working of specific metals
- C10N2040/246—Iron or steel
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- C10N2040/00—Specified use or application for which the lubricating composition is intended
- C10N2040/48—Slushing oils
Abstract
The invention discloses a kind of thermostable rustproof oil for processing stamping parts and preparation method, this antirust oil is grouped into by the one-tenth of following weight portion: 60 70 parts of machinery oil, high temperature resistant film former 10 20 parts, silane coupler 5 15 parts, benzotriazole 46 parts, lanoline 3 10 parts, imidazoline two thiourea 23 parts, sorbitan monooleate 4 10 parts, barium mahogany sulfonate 6 10 parts, triethanolamine 7 12 parts, auxiliary additive 10 18 parts.The film former of antirust oil of the present invention is fluorinated polyimide resin; this material chemical stability is high; decomposition temperature, more than 600 DEG C, can improve the resistance to elevated temperatures of antirust oil to a great extent as film former, and stamping parts can be protected not oxidized in hot stamping operation；Additionally, add silane coupler in formula, it can improve the polymer adhesive force to inorganic steel plate, and it has double reaction, can react with inorganic matter, with polymer reaction, can improve again adhesive force and the durability of antirust oil.
Description
Technical field
The present invention relates to the antirust field of stamping parts, be specifically related to a kind of thermostable rustproof oil for processing stamping parts and system
Preparation Method.
Background technology
Drop stamping is that depended on pressure machine and mould apply external force to sheet material, band, tubing and section bar etc., is allowed to produce plasticity and becomes
Shape or separation, thus obtain the forming and machining method of the workpiece (stamping parts) of required form and size.Prepare by this method
Parts size precision high, be widely used in auto manufacturing.
Steel plate is at high temperature oxidized easily the problem being always exist in drop stamping technique, in drop stamping technique, and steel
Plate first has to be heated to uniform temperature abundant austenitizing carried out above, and steel plate at high temperature easily produces with air contact
Oxide skin, this oxide skin not only affects the outward appearance of part, and easily comes off, it is necessary to periodically clear up, and this makes drop stamping become
Shape technique is more complicated, not only increases cost but also affects the surface quality of stamping parts.Conventional prevents stamping parts surface oxidation
Method be to smear ORC at surface of steel plate, existing ORC often also exists one in the drop stamping technique
Fixed problem, one is that heat-resisting quantity is poor, the most easily decomposes, loses non-oxidizability；Two is the associativity with steel plate
Difference, easily comes off, and must carry out shot-peening etc. and process before part carries out other process, and technique is loaded down with trivial details.Therefore one is studied
Stamping parts special thermostable rustproof oil is one and significantly works.
Summary of the invention
The invention provides a kind of thermostable rustproof oil for processing stamping parts and preparation method, it is possible to effectively prevent steel
Plate is oxidized in drop stamping technique, and good without carrying out other process with the stickiness of steel plate.
For realizing object above, the present invention is practiced by the following technical programs:
A kind of thermostable rustproof oil for processing stamping parts, is grouped into by the one-tenth of following weight portion: machinery oil 60-70
Part, high temperature resistant film former 10-20 part, silane coupler 5-15 part, benzotriazole 4-6 part, lanoline 3-10 part, imidazoline two
Thiourea 2-3 part, sorbitan monooleate 4-10 part, barium mahogany sulfonate 6-10 part, triethanolamine 7-12 part, auxiliary additive
10-18 part.
Preferably, the described thermostable rustproof oil for processing stamping parts, the one-tenth of following weight portion it is grouped into: machinery oil
63-67 part, high temperature resistant film former 13-16 part, silane coupler 8-13 part, benzotriazole 4-5 part, lanoline 3-6 part, imidazoles
Quinoline two thiourea 2-3 part, sorbitan monooleate 5-7 part, barium mahogany sulfonate 7-9 part, triethanolamine 8-10 part, auxiliary is added
Agent 14-16.
Preferably, the described thermostable rustproof oil for processing stamping parts, the one-tenth of following weight portion it is grouped into: machinery oil
64 parts, high temperature resistant film former 15 parts, silane coupler 10 parts, benzotriazole 5 parts, lanoline 4 parts, imidazoline two thiourea 2 parts,
Sorbitan monooleate 6 parts, barium mahogany sulfonate 8 parts, triethanolamine 9 parts, auxiliary additive 15 parts.
Preferably, described high temperature resistant film former is fluorinated polyimide resin.
Preferably, described auxiliary additive is the mixture of dimethicone and sulfonated castor oil.
For processing the preparation method of the thermostable rustproof oil of stamping parts, comprise the following steps:
(1) machinery oil is joined in container, thermal dehydration；
(2) machinery oil after dehydration adds high temperature resistant film former, is warming up to 110-130 DEG C when stirring,
Add silane coupler, react 1-2h；
(3) compounding substances that step (2) obtains is cooled to 70-80 DEG C, adds lanoline, imidazoline two thiourea, benzene a pair of horses going side by side
Triazole, barium mahogany sulfonate, stir, to be dissolved after continue to be cooled to 55-65 DEG C, add sorbitan monooleate,
Triethanolamine, dimethicone, sulfonated castor oil, continue to be uniformly mixed；
(4) the mixture stirring after mix homogeneously in step (3) is cooled to 35-40 DEG C, crosses and filter to remove impurity,
To antirust oil.
The film former that the method have the benefit that antirust oil of the present invention is fluorinated polyimide resin, this material chemically stable
Property high, decomposition temperature, more than 600 DEG C, can improve the resistance to elevated temperatures of antirust oil to a great extent as film former, permissible
Protection stamping parts is not oxidized in hot stamping operation；Additionally, add silane coupler in formula, it can improve polymer
Adhesive force to inorganic steel plate, it has double reaction, can react with inorganic matter, can improve with polymer reaction again
The adhesive force of antirust oil and durability.
Detailed description of the invention
For making the purpose of the embodiment of the present invention, technical scheme and advantage clearer, below in conjunction with the embodiment of the present invention,
Technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is the present invention one
Divide embodiment rather than whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art are not making
The every other embodiment obtained under creative work premise, broadly falls into the scope of protection of the invention.
Embodiment 1:
A kind of thermostable rustproof oil for processing stamping parts, is grouped into by the one-tenth of following weight portion: 60 parts of machinery oil, contains
Fluorine polyimide resin 10 parts, silane coupler 5 parts, benzotriazole 4 parts, lanoline 3 parts, imidazoline two thiourea 2 parts, dehydration
Sorbitol monooleate 4 parts, barium mahogany sulfonate 6 parts, triethanolamine 7 parts, dimethicone 5 parts, sulfonated castor oil 5 parts.
For processing the preparation method of the thermostable rustproof oil of stamping parts, comprise the following steps:
(1) machinery oil is joined in container, thermal dehydration；
(2) machinery oil after dehydration adds high temperature resistant film former, is warming up to 110-130 DEG C when stirring,
Add silane coupler, react 1-2h；
(3) compounding substances that step (2) obtains is cooled to 70-80 DEG C, adds lanoline, imidazoline two thiourea, benzene a pair of horses going side by side
Triazole, barium mahogany sulfonate, stir, to be dissolved after continue to be cooled to 55-65 DEG C, add sorbitan monooleate,
Triethanolamine, dimethicone, sulfonated castor oil, continue to be uniformly mixed；
(4) the mixture stirring after mix homogeneously in step (3) is cooled to 35-40 DEG C, crosses and filter to remove impurity,
To antirust oil.
Embodiment 2:
A kind of thermostable rustproof oil for processing stamping parts, is grouped into by the one-tenth of following weight portion: 70 parts of machinery oil, resistance to
High temperature film former 20 parts, silane coupler 15 parts, benzotriazole 6 parts, lanoline 10 parts, imidazoline two thiourea 3 parts, dehydration mountain
Pears alcohol monoleate 10 parts, barium mahogany sulfonate 10 parts, triethanolamine 12 parts, dimethicone 5 parts, sulfonated castor oil 13 parts.
For processing the preparation method of the thermostable rustproof oil of stamping parts, comprise the following steps:
(1) machinery oil is joined in container, thermal dehydration；
(2) machinery oil after dehydration adds high temperature resistant film former, is warming up to 110-130 DEG C when stirring,
Add silane coupler, react 1-2h；
(3) compounding substances that step (2) obtains is cooled to 70-80 DEG C, adds lanoline, imidazoline two thiourea, benzene a pair of horses going side by side
Triazole, barium mahogany sulfonate, stir, to be dissolved after continue to be cooled to 55-65 DEG C, add sorbitan monooleate,
Triethanolamine, dimethicone, sulfonated castor oil, continue to be uniformly mixed；
(4) the mixture stirring after mix homogeneously in step (3) is cooled to 35-40 DEG C, crosses and filter to remove impurity,
To antirust oil.
Embodiment 3:
A kind of thermostable rustproof oil for processing stamping parts, is grouped into by the one-tenth of following weight portion: 63 parts of machinery oil, resistance to
High temperature film former 13 parts, silane coupler 8 parts, benzotriazole 4 parts, lanoline 3 parts, imidazoline two thiourea 2 parts, Sorbitan
Alcohol monoleate 5 parts, barium mahogany sulfonate 7 parts, triethanolamine 8 parts, dimethicone 7 parts, sulfonated castor oil 7 parts.
For processing the preparation method of the thermostable rustproof oil of stamping parts, comprise the following steps:
(1) machinery oil is joined in container, thermal dehydration；
(2) machinery oil after dehydration adds high temperature resistant film former, is warming up to 110-130 DEG C when stirring,
Add silane coupler, react 1-2h；
(3) compounding substances that step (2) obtains is cooled to 70-80 DEG C, adds lanoline, imidazoline two thiourea, benzene a pair of horses going side by side
Triazole, barium mahogany sulfonate, stir, to be dissolved after continue to be cooled to 55-65 DEG C, add sorbitan monooleate,
Triethanolamine, dimethicone, sulfonated castor oil, continue to be uniformly mixed；
(4) the mixture stirring after mix homogeneously in step (3) is cooled to 35-40 DEG C, crosses and filter to remove impurity,
To antirust oil.
Embodiment 4:
A kind of thermostable rustproof oil for processing stamping parts, is grouped into by the one-tenth of following weight portion: 67 parts of machinery oil, resistance to
High temperature film former 16 parts, silane coupler 13 parts, benzotriazole 5 parts, lanoline 6 parts, imidazoline two thiourea 3 parts, dehydration mountain
Pears alcohol monoleate 7 parts, barium mahogany sulfonate 9 parts, triethanolamine 10 parts, dimethicone 10 parts, sulfonated castor oil 6 parts.
For processing the preparation method of the thermostable rustproof oil of stamping parts, comprise the following steps:
(1) machinery oil is joined in container, thermal dehydration；
(2) machinery oil after dehydration adds high temperature resistant film former, is warming up to 110-130 DEG C when stirring,
Add silane coupler, react 1-2h；
(3) compounding substances that step (2) obtains is cooled to 70-80 DEG C, adds lanoline, imidazoline two thiourea, benzene a pair of horses going side by side
Triazole, barium mahogany sulfonate, stir, to be dissolved after continue to be cooled to 55-65 DEG C, add sorbitan monooleate,
Triethanolamine, dimethicone, sulfonated castor oil, continue to be uniformly mixed；
(4) the mixture stirring after mix homogeneously in step (3) is cooled to 35-40 DEG C, crosses and filter to remove impurity,
To antirust oil.
Embodiment 5:
A kind of thermostable rustproof oil for processing stamping parts, is grouped into by the one-tenth of following weight portion: 64 parts of machinery oil, resistance to
High temperature film former 15 parts, silane coupler 10 parts, benzotriazole 5 parts, lanoline 4 parts, imidazoline two thiourea 2 parts, dehydration mountain
Pears alcohol monoleate 6 parts, barium mahogany sulfonate 8 parts, triethanolamine 9 parts, dimethicone 4 parts, sulfonated castor oil 11 parts.
For processing the preparation method of the thermostable rustproof oil of stamping parts, comprise the following steps:
(1) machinery oil is joined in container, thermal dehydration；
(2) machinery oil after dehydration adds high temperature resistant film former, is warming up to 110-130 DEG C when stirring,
Add silane coupler, react 1-2h；
(3) compounding substances that step (2) obtains is cooled to 70-80 DEG C, adds lanoline, imidazoline two thiourea, benzene a pair of horses going side by side
Triazole, barium mahogany sulfonate, stir, to be dissolved after continue to be cooled to 55-65 DEG C, add sorbitan monooleate,
Triethanolamine, dimethicone, sulfonated castor oil, continue to be uniformly mixed；
(4) the mixture stirring after mix homogeneously in step (3) is cooled to 35-40 DEG C, crosses and filter to remove impurity,
To antirust oil.
It should be noted that in this article, the relational terms of such as first and second or the like is used merely to a reality
Body or operation separate with another entity or operating space, and deposit between not necessarily requiring or imply these entities or operating
Relation or order in any this reality.And, term " includes ", " comprising " or its any other variant are intended to
Comprising of nonexcludability, so that include that the process of a series of key element, method, article or equipment not only include that those are wanted
Element, but also include other key elements being not expressly set out, or also include for this process, method, article or equipment
Intrinsic key element.In the case of there is no more restriction, statement " including ... " key element limited, it is not excluded that
Including process, method, article or the equipment of described key element there is also other identical element.
Above example only in order to technical scheme to be described, is not intended to limit；Although with reference to previous embodiment
The present invention is described in detail, it will be understood by those within the art that: it still can be to aforementioned each enforcement
Technical scheme described in example is modified, or wherein portion of techniques feature is carried out equivalent；And these amendment or
Replace, do not make the essence of appropriate technical solution depart from the spirit and scope of various embodiments of the present invention technical scheme.
Claims (6)
1. the thermostable rustproof oil being used for processing stamping parts, it is characterised in that be grouped into by the one-tenth of following weight portion: machinery
Oil 60-70 part, high temperature resistant film former 10-20 part, silane coupler 5-15 part, benzotriazole 4-6 part, lanoline 3-10 part,
Imidazoline two thiourea 2-3 part, sorbitan monooleate 4-10 part, barium mahogany sulfonate 6-10 part, triethanolamine 7-12 part is auxiliary
Help additive 10-18 part.
2. the thermostable rustproof oil for processing stamping parts as claimed in claim 1, it is characterised in that by following weight portion
One-tenth is grouped into: machinery oil 63-67 part, high temperature resistant film former 13-16 part, silane coupler 8-13 part, benzotriazole 4-5 part,
Lanoline 3-6 part, imidazoline two thiourea 2-3 part, sorbitan monooleate 5-7 part, barium mahogany sulfonate 7-9 part, three ethanol
Amine 8-10 part, auxiliary additive 14-16.
3. the thermostable rustproof oil for processing stamping parts as claimed in claim 2, it is characterised in that by following weight portion
One-tenth is grouped into: 64 parts of machinery oil, high temperature resistant film former 15 parts, silane coupler 10 parts, benzotriazole 5 parts, lanoline 4 parts,
Imidazoline two thiourea 2 parts, sorbitan monooleate 6 parts, barium mahogany sulfonate 8 parts, triethanolamine 9 parts, auxiliary additive 15
Part.
4. the thermostable rustproof oil for processing stamping parts as claimed in claim 3, it is characterised in that described high temperature resistant film forming
Agent is fluorinated polyimide resin.
5. the thermostable rustproof oil for processing stamping parts as claimed in claim 3, it is characterised in that described auxiliary additive
For dimethicone and the mixture of sulfonated castor oil.
6. a preparation method for the thermostable rustproof oil for processing stamping parts as described in claim 1-5 is arbitrary, including
Following steps:
(1) machinery oil is joined in container, thermal dehydration；
(2) machinery oil after dehydration adds high temperature resistant film former, be warming up to 110-130 DEG C when stirring, add
Silane coupler, reacts 1-2h；
(3) compounding substances that step (2) obtains is cooled to 70-80 DEG C, adds lanoline, imidazoline two thiourea, benzene a pair of horses going side by side three nitrogen
Azoles, barium mahogany sulfonate, stir, to be dissolved after continue to be cooled to 55-65 DEG C, add sorbitan monooleate, three second
Hydramine, dimethicone, sulfonated castor oil, continue to be uniformly mixed；
(4) the mixture stirring after mix homogeneously in step (3) is cooled to 35-40 DEG C, crosses and filter to remove impurity, i.e. can be prevented
Rust oil.
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