CN106174545A - A kind of buccal tablet rich in wheat-bran dietary fiber and preparation method thereof - Google Patents
A kind of buccal tablet rich in wheat-bran dietary fiber and preparation method thereof Download PDFInfo
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- CN106174545A CN106174545A CN201610568032.0A CN201610568032A CN106174545A CN 106174545 A CN106174545 A CN 106174545A CN 201610568032 A CN201610568032 A CN 201610568032A CN 106174545 A CN106174545 A CN 106174545A
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- dietary fiber
- dry powder
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- testa tritici
- buccal tablet
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- 235000013325 dietary fiber Nutrition 0.000 title claims abstract description 50
- 229940046011 buccal tablet Drugs 0.000 title claims abstract description 20
- 239000006189 buccal tablet Substances 0.000 title claims abstract description 20
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 235000015099 wheat brans Nutrition 0.000 title claims abstract description 15
- 239000000843 powder Substances 0.000 claims abstract description 61
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 46
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 37
- 230000002779 inactivation Effects 0.000 claims abstract description 22
- HQKMJHAJHXVSDF-UHFFFAOYSA-L magnesium stearate Chemical compound [Mg+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O HQKMJHAJHXVSDF-UHFFFAOYSA-L 0.000 claims abstract description 20
- 235000019202 steviosides Nutrition 0.000 claims abstract description 13
- UEDUENGHJMELGK-HYDKPPNVSA-N Stevioside Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O UEDUENGHJMELGK-HYDKPPNVSA-N 0.000 claims abstract description 12
- 229940013618 stevioside Drugs 0.000 claims abstract description 12
- OHHNJQXIOPOJSC-UHFFFAOYSA-N stevioside Natural products CC1(CCCC2(C)C3(C)CCC4(CC3(CCC12C)CC4=C)OC5OC(CO)C(O)C(O)C5OC6OC(CO)C(O)C(O)C6O)C(=O)OC7OC(CO)C(O)C(O)C7O OHHNJQXIOPOJSC-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 10
- 239000005913 Maltodextrin Substances 0.000 claims abstract description 10
- 235000019359 magnesium stearate Nutrition 0.000 claims abstract description 10
- 229940035034 maltodextrin Drugs 0.000 claims abstract description 10
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 9
- 229920002261 Corn starch Polymers 0.000 claims abstract description 8
- 239000008120 corn starch Substances 0.000 claims abstract description 8
- 239000002244 precipitate Substances 0.000 claims abstract description 8
- 238000002203 pretreatment Methods 0.000 claims abstract description 8
- 238000000034 method Methods 0.000 claims abstract description 7
- 239000000463 material Substances 0.000 claims description 50
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- 241000033870 Citrullus lanatus subsp. vulgaris Species 0.000 claims description 3
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- 102000011759 adducin Human genes 0.000 description 5
- 108010076723 adducin Proteins 0.000 description 5
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- 235000002017 Zea mays subsp mays Nutrition 0.000 description 4
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- 235000012054 meals Nutrition 0.000 description 4
- 244000046052 Phaseolus vulgaris Species 0.000 description 3
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- 230000036541 health Effects 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 229920002488 Hemicellulose Polymers 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- 229930006000 Sucrose Natural products 0.000 description 2
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 2
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- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
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- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
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- 229940032147 starch Drugs 0.000 description 2
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- 235000013618 yogurt Nutrition 0.000 description 2
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
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- 229930091371 Fructose Natural products 0.000 description 1
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 1
- 244000068988 Glycine max Species 0.000 description 1
- 235000010469 Glycine max Nutrition 0.000 description 1
- 208000005016 Intestinal Neoplasms Diseases 0.000 description 1
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- 244000294611 Punica granatum Species 0.000 description 1
- 235000014360 Punica granatum Nutrition 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- 239000004383 Steviol glycoside Substances 0.000 description 1
- 241000396377 Tranes Species 0.000 description 1
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- 150000008131 glucosides Chemical class 0.000 description 1
- 150000004676 glycans Chemical class 0.000 description 1
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- 230000003179 granulation Effects 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 239000000416 hydrocolloid Substances 0.000 description 1
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- 201000002313 intestinal cancer Diseases 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 239000010977 jade Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 235000004213 low-fat Nutrition 0.000 description 1
- 208000030208 low-grade fever Diseases 0.000 description 1
- 239000007937 lozenge Substances 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
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- 229930182488 steviol glycoside Natural products 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of buccal tablet rich in wheat-bran dietary fiber and preparation method thereof, belong to food processing technology field.The method comprises the following steps: pre-treatment;Defat;Enzymolysis;Inactivation;Precipitate with ethanol, be dried;Dispensing;Tabletting.The inventive method prepares dietary fiber dry powder with the side-product Testa Tritici after wheat processing for raw material, it is equipped with the raw material tablettings such as fruit dry powder, corn starch, stevioside, maltodextrin and magnesium stearate again and prepares buccal tablet, substantially increase the utilization rate of Testa Tritici, add a new approach for Testa Tritici recycling simultaneously;The buccal tablet being prepared is easy to carry, rich in there being water soluble dietary fiber, has Constipation, blood sugar lowering, blood fat reducing and the effect such as anticancer;The fruit dry powder adjustable buccal tablet local flavor simultaneously added, good palatability;Whole preparation technology is simple and easy to control, and production efficiency is high, low cost, and suitable large-scale industrial production is applied.
Description
Technical field
The invention belongs to food processing technology field, be specifically related to a kind of buccal tablet rich in wheat-bran dietary fiber and preparation thereof
Method.
Background technology
Along with World Economics and the high speed development of industry, living standards of the people increase substantially, and diet is increasingly fine, because of battalion
The all ciril diseases supporting superfluous and nutritional disorder and produce, as diabetes, cardiovascular and cerebrovascular disease, obesity, intestinal cancer, constipation etc. are tight
Ghost image rings human health.Therefore there is regulation function of human body, prevent disease and sanatory functional food from having enjoyed pass
Note.Dietary fiber has prominent health care as the seventh-largest nutrient, is increasingly becoming the focus that nutritionist is paid close attention to.Meals
Food fiber can be divided into water soluble dietary fiber and the big class of water insoluble dietary fiber two by dissolubility.Dietary fiber by sources divide and
Soybean dietary fiber, corn dietary fiber, wheat-bran dietary fiber etc. can be divided into.The major function of water soluble dietary fiber is to subtract
Cholesterol levels in insufficiency of blood liquid, regulates blood sugar level, thus reduces cardiopathic danger, improve diabetes, and its source is main
Being water fruits and vegetables, Semen sojae atricolor and Herba bromi japonici etc., it includes the hydrocolloid mass such as pectin and part hemicellulose.Water-insoluble meals
Fiber major function is to expand, and can regulate the function of intestinal, prevent constipation, keep big gut health, and it mainly includes cellulose, wood
Quality and part hemicellulose etc..
Western developed country just sets about the research and development to dietary fiber as far back as the seventies, and American and Britain, moral, method are formed
Certain industry size, and occupy a tiny space at food products market.What the Japanese eighties, later-stage utilization water soluble dietary fiber was made
Beverage includes soda pop, lactic acid beverage and fruit juice etc..The external dietary fiber studied mainly has 6 big classes: corn, beans,
Fruit and vegerable, microbial polysaccharide and other natural fibers and synthesis, semisynthetic fibre, count more than 30 kind, is wherein applied to raw
Produce existing more than 10 kinds.At present, dietary fiber application in food is also had and studies widely by China.Especially in beverage and breast system
Application in product, China has produced liquid prandial fibre milk and the patent of relevant liquid form product thereof, and has pointed out dietary fiber
Addition in liquid milk is 7.22-22.4kg/t.Dietary fiber is added in Yoghourt by part researcher, significantly
Change mouthfeel and the rheological behavior of Yoghourt.
Testa Tritici, Testa oryzae, skin of Semen Maydis and beans skin slag etc. are the side-products of corn processing, and dietary fiber content enriches, has
Increase satiety, Constipation, blood sugar lowering, blood fat reducing and the effect such as anticancer, be important dietary fiber sources.From the openest
Patent and relevant non-document see, the processing dead meal such as application corn, beans, fruit and vegerable makes the document report of diet fiber food
Less.
Summary of the invention
The purpose of the present invention has aimed to provide one and has extracted water soluble dietary fiber with Testa Tritici for raw material, and utilizes its meals
The process of food lozenge prepared by fiber.
Concrete, the preparation method of the buccal tablet rich in wheat-bran dietary fiber of the present invention, comprise the following steps:
1) pre-treatment: by Testa Tritici remove impurity, pulverizing, crosses 100 mesh sieves, obtains Testa Tritici fine powder;
2) defat: take Testa Tritici fine powder, adds the hexanol of Testa Tritici fine powder volume 3-5 times, soaks under conditions of temperature is 40-60 DEG C
Carry 1-2h, filter isolated filtrate and filtering residue, by filter residue and drying, obtain defat material;
3) enzymolysis: extracting degreasing material, adds the distilled water of defat volume of material 15-25 times, regulates pH=5.5-6.5, adds defat
The protease of weight of material 1-3%, enzymolysis 30-60min under the Ultrasonic Conditions that temperature is 25-40 DEG C, filters isolated filter
Liquid and filtering residue;Take filtering residue, add the distilled water of filtering residue volume 15-25 times, regulate pH=4.5-5.0, add filtering residue weight 3-8%
Cellulase, enzymolysis 30-60min under the Ultrasonic Conditions that temperature is 25-40 DEG C, filters isolated filtrate and filtering residue;Will
Twice filtrate merges, and obtains enzymolysis solution;
4) inactivation: by enzymolysis solution steam inactivation 8-15min under conditions of temperature is 95-105 DEG C, be cooled to room temperature;
5) precipitate with ethanol, be dried: will inactivation after enzymolysis solution be placed in Rotary Evaporators, in pressure be 0.05-0.08Mpa, temperature be
The 1/3-1/4 of original volume it is concentrated under conditions of 50-60 DEG C;Calculate with enzymolysis solution volume after concentrating, add 3-5 times of volume
95% ethanol, stands 3-8h after mixing, filter isolated filtrate and precipitation material, be placed in dehydrator by precipitation material and dry and wave
Send out ethanol, be subsequently placed in vacuum freeze drier, in temperature for-30~-20 DEG C, vacuum be under conditions of 30~50Pa cold
The dry 5-15h of lyophilizing, obtains dietary fiber dry powder;
6) dispensing: in terms of parts by weight, take dietary fiber dry powder 20-40 part, fruit dry powder 20-40 part, corn starch 3-8 part,
Stevioside 0.3-1 part, maltodextrin 0.5-3 part, magnesium stearate 0.1-1 part, drinkable water 15-25 part, mixing, material must be mixed;
7) tabletting: mixing is expected pelletize, then dries the dry granule preparing water content less than 1%, be finally placed in tablet machine pressure
Sheet, to obtain final product.
Testa Tritici, i.e. Testa Tritici, wheat processing milling by products, wheat yellow, lamellar or powdery.Rich cellulose and vitamin,
Main uses have edible, be used as medicine, feedstuff, wine brewing etc..Testa Tritici contains abundant dietary fiber, is the nutrition of needed by human
Element, can improve the fibre composition in food, can improve constipation situation, can promote the excretion of fat and nitrogen, to facing simultaneously
The preventive and therapeutic effect of bed common fiber shortage property disease is significant.
Stevioside is a kind of new type natural sweeting agent that essence carries from catananche's Folium Stevlae Rebaudianae (or claiming Folium Chrysanthemi), and
South America use Folium Stevlae Rebaudianae has had centuries history as medicinal herbs with for sugar.The data of international sweeting agent industry shows, Flos Chrysanthemi
Glucoside has been widely used in Asia, North America, South America and EU countries in the production of food, beverage, flavouring agent.China is complete
Ball main steviol glycosides manufacturing country.The calorific value of stevioside is only the 1/300 of sucrose, is not absorbed, do not produce after taking in human body
Heat, is diabetes and sweeting agent that bariatric patients is suitable for.When stevioside is mixed with sucrose fructose or isomerized sugar, can improve
Its sugariness, improves taste.Can be used for confection, cake, beverage, solid beverage, fried snack food, flavouring agent, preserve.
Maltodextrin (also referred to as wheat Trane) is hydrolyzed through minuent by starch, purifies, is spray-dried and makes, without free
The starch derivatives of starch.English abbreviation be MD. have that viscosity is big, thickening property is strong, dissolubility is good, instant capacity is good, carrier-mediated
Good, ferment little, moisture absorption is low, free from extraneous odour, sugariness are low, the feature such as human body is prone to digest and assimilate, low grade fever, low fat, is food work
One of optimal basic material in industry, and obtain increasingly in paper industry, daily-use chemical industry, fine chemistry industry, medical industry
It is widely applied.
Magnesium stearate is that white is easily without the fine powder of grittiness;Micro-have special smell;Soapy feeling is had with contact skin.At water, ethanol
Or insoluble in ether, it is mainly used as lubricant, antiplastering aid, fluidizer.Particularly suitable oils, the granulation of extract medicament, make
Granule there is good mobility and compressibility.Fluidizer it is used as in direct compression.Be alternatively arranged as filter aid, clarifier and
Drip infusion, and the suspending agent of liquid preparation, thickening agent.
Further illustrating as the present invention, described fruit dry powder include Fructus Mali pumilae dry powder, Fructus Vitis viniferae dry powder, Fructus Musae dry powder, kind
Punica granatum L. dry powder, Citrullus vulgaris dry powder.
Invention also provides the buccal tablet rich in wheat-bran dietary fiber being prepared by said method.
Compared with prior art, the present invention reaches to provide the benefit that:
1) present invention prepares dietary fiber dry powder with the side-product Testa Tritici after wheat processing for raw material, then is equipped with fruit dry powder, jade
Buccal tablet prepared by the raw material tablettings such as rice starch, stevioside, maltodextrin and magnesium stearate, substantially increases the utilization rate of Testa Tritici, with
Time be that Testa Tritici recycling adds a new approach;
2) buccal tablet being prepared is easy to carry, rich in there being water soluble dietary fiber, has Constipation, blood sugar lowering, blood fat reducing
With the effect such as anticancer;The fruit dry powder adjustable buccal tablet local flavor simultaneously added, good palatability;
3) whole preparation technology is simple and easy to control, and production efficiency is high, low cost, and suitable large-scale industrial production is applied.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, the present embodiment be only the present invention is made clearer
Illustrate rather than limitation of the present invention.
Embodiment 1
Rich in the preparation method of the buccal tablet of wheat-bran dietary fiber, comprise the following steps:
1) pre-treatment: by Testa Tritici remove impurity, pulverizing, crosses 100 mesh sieves, obtains Testa Tritici fine powder;
2) defat: take Testa Tritici fine powder, adds the hexanol of Testa Tritici fine powder volume 4 times, extracts 2h under conditions of temperature is 50 DEG C,
Filter isolated filtrate and filtering residue, by filter residue and drying, obtain defat material;
3) enzymolysis: extracting degreasing material, adds the distilled water of defat volume of material 20 times, regulates pH=6.0, adds defat material weight
The protease of amount 1%, enzymolysis 40min under the Ultrasonic Conditions that temperature is 35 DEG C, filters isolated filtrate and filtering residue;Take filter
Slag, adds the distilled water of filtering residue volume 20 times, regulates pH=4.8, adds the cellulase of filtering residue weight 5%, is 35 DEG C in temperature
Ultrasonic Conditions under enzymolysis 40min, filter isolated filtrate and filtering residue;Twice filtrate is merged, obtains enzymolysis solution;
4) inactivation: by enzymolysis solution steam inactivation 12min under conditions of temperature is 100 DEG C, be cooled to room temperature;
5) precipitate with ethanol, be dried: will inactivation after enzymolysis solution be placed in Rotary Evaporators, in pressure be 0.06Mpa, temperature be 55 DEG C
Under the conditions of be concentrated into the 1/3 of original volume;Calculate with enzymolysis solution volume after concentrating, add 95% ethanol of 3 times of volumes, quiet after mixing
Put 5h, filter isolated filtrate and precipitation material, precipitation material is placed in dehydrator ethanol of drying and volatilize, is subsequently placed in vacuum
In freezer dryer, in temperature for-24 DEG C, vacuum be 35Pa under conditions of lyophilization 10h, obtain dietary fiber dry powder;
6) dispensing: in terms of parts by weight, takes 30 parts of dietary fiber dry powder, 30 parts of Fructus Mali pumilae dry powder, corn starch 5 parts, stevioside 0.5
Part, maltodextrin 0.5 part, magnesium stearate 0.5 part, drinkable water 15 parts, mixing, material must be mixed;
7) tabletting: mixing is expected pelletize, then dries the dry granule preparing water content less than 1%, be finally placed in tablet machine pressure
Sheet, to obtain final product.
Embodiment 2
Rich in the preparation method of the buccal tablet of wheat-bran dietary fiber, comprise the following steps:
1) pre-treatment: by Testa Tritici remove impurity, pulverizing, crosses 100 mesh sieves, obtains Testa Tritici fine powder;
2) defat: take Testa Tritici fine powder, adds the hexanol of Testa Tritici fine powder volume 3 times, extracts 2h under conditions of temperature is 60 DEG C,
Filter isolated filtrate and filtering residue, by filter residue and drying, obtain defat material;
3) enzymolysis: extracting degreasing material, adds the distilled water of defat volume of material 25 times, regulates pH=5.5, adds defat material weight
The protease of amount 3%, enzymolysis 35min under the Ultrasonic Conditions that temperature is 40 DEG C, filters isolated filtrate and filtering residue;Take filter
Slag, adds the distilled water of filtering residue volume 25 times, regulates pH=5.0, adds the cellulase of filtering residue weight 8%, is 40 DEG C in temperature
Ultrasonic Conditions under enzymolysis 50min, filter isolated filtrate and filtering residue;Twice filtrate is merged, obtains enzymolysis solution;
4) inactivation: by enzymolysis solution steam inactivation 8min under conditions of temperature is 95 DEG C, be cooled to room temperature;
5) precipitate with ethanol, be dried: will inactivation after enzymolysis solution be placed in Rotary Evaporators, in pressure be 0.08Mpa, temperature be 50 DEG C
Under the conditions of be concentrated into the 1/4 of original volume;Calculate with enzymolysis solution volume after concentrating, add 95% ethanol of 5 times of volumes, quiet after mixing
Put 3h, filter isolated filtrate and precipitation material, precipitation material is placed in dehydrator ethanol of drying and volatilize, is subsequently placed in vacuum
In freezer dryer, in temperature for-20 DEG C, vacuum be 50Pa under conditions of lyophilization 8h, obtain dietary fiber dry powder;
6) dispensing: in terms of parts by weight, takes 20 parts of dietary fiber dry powder, 40 parts of Fructus Vitis viniferae dry powder, corn starch 8 parts, stevioside 0.3
Part, maltodextrin 1 part, magnesium stearate 1 part, drinkable water 25 parts, mixing, material must be mixed;
7) tabletting: mixing is expected pelletize, then dries the dry granule preparing water content less than 1%, be finally placed in tablet machine pressure
Sheet, to obtain final product.
Embodiment 3
Rich in the preparation method of the buccal tablet of wheat-bran dietary fiber, comprise the following steps:
1) pre-treatment: by Testa Tritici remove impurity, pulverizing, crosses 100 mesh sieves, obtains Testa Tritici fine powder;
2) defat: take Testa Tritici fine powder, adds the hexanol of Testa Tritici fine powder volume 3 times, extracts under conditions of temperature is 45 DEG C
1.5h, filters isolated filtrate and filtering residue, by filter residue and drying, obtains defat material;
3) enzymolysis: extracting degreasing material, adds the distilled water of defat volume of material 15 times, regulates pH=6.5, adds defat material weight
The protease of amount 1%, enzymolysis 45min under the Ultrasonic Conditions that temperature is 35 DEG C, filters isolated filtrate and filtering residue;Take filter
Slag, adds the distilled water of filtering residue volume 25 times, regulates pH=4.5, adds the cellulase of filtering residue weight 3%, is 25 DEG C in temperature
Ultrasonic Conditions under enzymolysis 60min, filter isolated filtrate and filtering residue;Twice filtrate is merged, obtains enzymolysis solution;
4) inactivation: by enzymolysis solution steam inactivation 10min under conditions of temperature is 105 DEG C, be cooled to room temperature;
5) precipitate with ethanol, be dried: will inactivation after enzymolysis solution be placed in Rotary Evaporators, in pressure be 0.08Mpa, temperature be 50 DEG C
Under the conditions of be concentrated into the 1/3 of original volume;Calculate with enzymolysis solution volume after concentrating, add 95% ethanol of 4 times of volumes, quiet after mixing
Put 4h, filter isolated filtrate and precipitation material, precipitation material is placed in dehydrator ethanol of drying and volatilize, is subsequently placed in vacuum
In freezer dryer, in temperature for-30 DEG C, vacuum be 30Pa under conditions of lyophilization 5h, obtain dietary fiber dry powder;
6) dispensing: in terms of parts by weight, takes 40 parts of dietary fiber dry powder, 20 parts of Fructus Musae dry powder, corn starch 8 parts, stevioside 1
Part, maltodextrin 2 parts, magnesium stearate 0.1 part, drinkable water 20 parts, mixing, material must be mixed;
7) tabletting: mixing is expected pelletize, then dries the dry granule preparing water content less than 1%, be finally placed in tablet machine pressure
Sheet, to obtain final product.
Embodiment 4
Rich in the preparation method of the buccal tablet of wheat-bran dietary fiber, comprise the following steps:
1) pre-treatment: by Testa Tritici remove impurity, pulverizing, crosses 100 mesh sieves, obtains Testa Tritici fine powder;
2) defat: take Testa Tritici fine powder, adds the hexanol of Testa Tritici fine powder volume 5 times, extracts 1h under conditions of temperature is 45 DEG C,
Filter isolated filtrate and filtering residue, by filter residue and drying, obtain defat material;
3) enzymolysis: extracting degreasing material, adds the distilled water of defat volume of material 25 times, regulates pH=5.5, adds defat material weight
The protease of amount 2%, enzymolysis 30min under the Ultrasonic Conditions that temperature is 30 DEG C, filters isolated filtrate and filtering residue;Take filter
Slag, adds the distilled water of filtering residue volume 15 times, regulates pH=4.8, adds the cellulase of filtering residue weight 6%, is 30 DEG C in temperature
Ultrasonic Conditions under enzymolysis 40min, filter isolated filtrate and filtering residue;Twice filtrate is merged, obtains enzymolysis solution;
4) inactivation: by enzymolysis solution steam inactivation 15min under conditions of temperature is 100 DEG C, be cooled to room temperature;
5) precipitate with ethanol, be dried: will inactivation after enzymolysis solution be placed in Rotary Evaporators, in pressure be 0.05Mpa, temperature be 50 DEG C
Under the conditions of be concentrated into the 1/4 of original volume;Calculate with enzymolysis solution volume after concentrating, add 95% ethanol of 4 times of volumes, quiet after mixing
Put 4h, filter isolated filtrate and precipitation material, precipitation material is placed in dehydrator ethanol of drying and volatilize, is subsequently placed in vacuum
In freezer dryer, in temperature for-26 DEG C, vacuum be 45Pa under conditions of lyophilization 15h, obtain dietary fiber dry powder;
6) dispensing: in terms of parts by weight, takes 25 parts of dietary fiber dry powder, 25 parts of Fructus psidii guajavae immaturus dry powder, corn starch 6 parts, stevioside
0.3 part, maltodextrin 3 parts, magnesium stearate 0.5 part, drinkable water 15 parts, mixing, material must be mixed;
7) tabletting: mixing is expected pelletize, then dries the dry granule preparing water content less than 1%, be finally placed in tablet machine pressure
Sheet, to obtain final product.
Embodiment 5
Rich in the preparation method of the buccal tablet of wheat-bran dietary fiber, comprise the following steps:
1) pre-treatment: by Testa Tritici remove impurity, pulverizing, crosses 100 mesh sieves, obtains Testa Tritici fine powder;
2) defat: take Testa Tritici fine powder, adds the hexanol of Testa Tritici fine powder volume 3 times, extracts under conditions of temperature is 50 DEG C
1.5h, filters isolated filtrate and filtering residue, by filter residue and drying, obtains defat material;
3) enzymolysis: extracting degreasing material, adds the distilled water of defat volume of material 20 times, regulates pH=6.0, adds defat material weight
The protease of amount 2%, enzymolysis 45min under the Ultrasonic Conditions that temperature is 33 DEG C, filters isolated filtrate and filtering residue;Take filter
Slag, adds the distilled water of filtering residue volume 20 times, regulates pH=4.7, adds the cellulase of filtering residue weight 6%, is 35 DEG C in temperature
Ultrasonic Conditions under enzymolysis 45min, filter isolated filtrate and filtering residue;Twice filtrate is merged, obtains enzymolysis solution;
4) inactivation: by enzymolysis solution steam inactivation 10min under conditions of temperature is 105 DEG C, be cooled to room temperature;
5) precipitate with ethanol, be dried: will inactivation after enzymolysis solution be placed in Rotary Evaporators, in pressure be 0.06Mpa, temperature be 55 DEG C
Under the conditions of be concentrated into the 1/3 of original volume;Calculate with enzymolysis solution volume after concentrating, add 95% ethanol of 4 times of volumes, quiet after mixing
Put 6h, filter isolated filtrate and precipitation material, precipitation material is placed in dehydrator ethanol of drying and volatilize, is subsequently placed in vacuum
In freezer dryer, in temperature for-25 DEG C, vacuum be 40Pa under conditions of lyophilization 10h, obtain dietary fiber dry powder;
6) dispensing: in terms of parts by weight, takes 30 parts of dietary fiber dry powder, 30 parts of Citrullus vulgaris dry powder, corn starch 5 parts, stevioside 0.5
Part, maltodextrin 1.5 parts, magnesium stearate 0.5 part, drinkable water 20 parts, mixing, material must be mixed;
7) tabletting: mixing is expected pelletize, then dries the dry granule preparing water content less than 1%, be finally placed in tablet machine pressure
Sheet, to obtain final product.
The ultimate principle of the present invention, principal character and advantage have more than been shown and described.Those skilled in the art should
Understanding, the present invention is not restricted to the described embodiments, and the simply explanation present invention's described in above-described embodiment and description is former
Reason, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, these changes and improvements
Both fall within scope of the claimed invention.Claimed scope is by appending claims and equivalent circle thereof
Fixed.
Claims (3)
1. the preparation method rich in the buccal tablet of wheat-bran dietary fiber, it is characterised in that comprise the following steps:
1) pre-treatment: by Testa Tritici remove impurity, pulverizing, crosses 100 mesh sieves, obtains Testa Tritici fine powder;
2) defat: take Testa Tritici fine powder, adds the hexanol of Testa Tritici fine powder volume 3-5 times, soaks under conditions of temperature is 40-60 DEG C
Carry 1-2h, filter isolated filtrate and filtering residue, by filter residue and drying, obtain defat material;
3) enzymolysis: extracting degreasing material, adds the distilled water of defat volume of material 15-25 times, regulates pH=5.5-6.5, adds defat
The protease of weight of material 1-3%, enzymolysis 30-60min under the Ultrasonic Conditions that temperature is 25-40 DEG C, filters isolated filter
Liquid and filtering residue;Take filtering residue, add the distilled water of filtering residue volume 15-25 times, regulate pH=4.5-5.0, add filtering residue weight 3-8%
Cellulase, enzymolysis 30-60min under the Ultrasonic Conditions that temperature is 25-40 DEG C, filters isolated filtrate and filtering residue;Will
Twice filtrate merges, and obtains enzymolysis solution;
4) inactivation: by enzymolysis solution steam inactivation 8-15min under conditions of temperature is 95-105 DEG C, be cooled to room temperature;
5) precipitate with ethanol, be dried: will inactivation after enzymolysis solution be placed in Rotary Evaporators, in pressure be 0.05-0.08Mpa, temperature be
The 1/3-1/4 of original volume it is concentrated under conditions of 50-60 DEG C;Calculate with enzymolysis solution volume after concentrating, add 3-5 times of volume
95% ethanol, stands 3-8h after mixing, filter isolated filtrate and precipitation material, be placed in dehydrator by precipitation material and dry and wave
Send out ethanol, be subsequently placed in vacuum freeze drier, in temperature for-30~-20 DEG C, vacuum be under conditions of 30~50Pa cold
The dry 5-15h of lyophilizing, obtains dietary fiber dry powder;
6) dispensing: in terms of parts by weight, take dietary fiber dry powder 20-40 part, fruit dry powder 20-40 part, corn starch 3-8 part,
Stevioside 0.3-1 part, maltodextrin 0.5-3 part, magnesium stearate 0.1-1 part, drinkable water 15-25 part, mixing, material must be mixed;
7) tabletting: mixing is expected pelletize, then dries the dry granule preparing water content less than 1%, be finally placed in tablet machine pressure
Sheet, to obtain final product.
The most according to claim 1 rich in the preparation method of buccal tablet of wheat-bran dietary fiber, it is characterised in that described dried fruit
Powder includes Fructus Mali pumilae dry powder, Fructus Vitis viniferae dry powder, Fructus Musae dry powder, Fructus psidii guajavae immaturus dry powder, Citrullus vulgaris dry powder.
3. the buccal tablet rich in wheat-bran dietary fiber, it is characterised in that by the preparation of claim 1 or 2 arbitrary described method
?.
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CN110623194A (en) * | 2018-06-23 | 2019-12-31 | 泗水永昶食品有限公司 | Food rich in wheat bran dietary fiber and preparation method thereof |
CN111513257A (en) * | 2020-04-28 | 2020-08-11 | 南京素汇保健食品有限公司 | Preparation method of low-temperature coupling cooked oatmeal |
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Application publication date: 20161207 |