CN106213114A - Corn dietary fiber effervescent tablet and preparation technology thereof - Google Patents
Corn dietary fiber effervescent tablet and preparation technology thereof Download PDFInfo
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- CN106213114A CN106213114A CN201610567848.1A CN201610567848A CN106213114A CN 106213114 A CN106213114 A CN 106213114A CN 201610567848 A CN201610567848 A CN 201610567848A CN 106213114 A CN106213114 A CN 106213114A
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- Prior art keywords
- dietary fiber
- effervescent tablet
- corn
- acid
- agent
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
- A23L2/395—Dry compositions in a particular shape or form
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/40—Effervescence-generating compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/56—Flavouring or bittering agents
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
- A23L2/60—Sweeteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a kind of corn dietary fiber effervescent tablet and preparation technology thereof, this process prepares dietary fiber dry powder with the side-product skin of Semen Maydis after corn processed for raw material, it is equipped with other adjuvants again and prepares effervescent tablet, substantially increase the utilization rate of skin of Semen Maydis, add a new approach for skin of Semen Maydis recycling simultaneously；The effervescent tablet being prepared is easy for carrying and eating, and expands adaptation population, child, old people and can not swallow the patient of solid preparation and all can use, the correctives that simultaneously adds, sweeting agent adjustable effervescent tablet mouthfeel, good palatability；Effervescent tablet contains abundant water soluble dietary fiber, has Constipation, blood sugar lowering, blood fat reducing and the effect such as anticancer, contains vitamin simultaneously, the aspects such as dyspepsia, the most tired, emotional lability, hypomnesis are had preferable regulation effect.
Description
Technical field
The invention belongs to food processing technology field, be specifically related to a kind of corn dietary fiber effervescent tablet and preparation work thereof
Skill.
Background technology
Along with World Economics and the high speed development of industry, living standards of the people increase substantially, and diet is increasingly fine, because of battalion
The all ciril diseases supporting superfluous and nutritional disorder and produce, as diabetes, cardiovascular and cerebrovascular disease, obesity, intestinal cancer, constipation etc. are tight
Ghost image rings human health.Therefore there is regulation function of human body, prevent disease and sanatory functional food from having enjoyed pass
Note.Dietary fiber has prominent health care as the seventh-largest nutrient, is increasingly becoming the focus that nutritionist is paid close attention to.Meals
Food fiber can be divided into water soluble dietary fiber and the big class of water insoluble dietary fiber two by dissolubility.Dietary fiber by sources divide and
Soybean dietary fiber, corn dietary fiber, wheat-bran dietary fiber etc. can be divided into.The major function of water soluble dietary fiber is to subtract
Cholesterol levels in insufficiency of blood liquid, regulates blood sugar level, thus reduces cardiopathic danger, improve diabetes, and its source is main
Being water fruits and vegetables, Semen sojae atricolor and Herba bromi japonici etc., it includes the hydrocolloid mass such as pectin and part hemicellulose.Water-insoluble meals
Fiber major function is to expand, and can regulate the function of intestinal, prevent constipation, keep big gut health, and it mainly includes cellulose, wood
Quality and part hemicellulose etc..
Western developed country just sets about the research and development to dietary fiber as far back as the seventies, and American and Britain, moral, method are formed
Certain industry size, and occupy a tiny space at food products market.What the Japanese eighties, later-stage utilization water soluble dietary fiber was made
Beverage includes soda pop, lactic acid beverage and fruit juice etc..The external dietary fiber studied mainly has 6 big classes: corn, beans,
Fruit and vegerable, microbial polysaccharide and other natural fibers and synthesis, semisynthetic fibre, count more than 30 kind, is wherein applied to raw
Produce existing more than 10 kinds.At present, dietary fiber application in food is also had and studies widely by China.Especially in beverage and breast system
Application in product, China has produced liquid prandial fibre milk and the patent of relevant liquid form product thereof, and has pointed out dietary fiber
Addition in liquid milk is 7.22-22.4kg/t.Dietary fiber is added in Yoghourt by part researcher, significantly
Change mouthfeel and the rheological behavior of Yoghourt.
Skin of Semen Maydis, Testa oryzae, Testa Tritici and beans skin slag etc. are the side-products of corn processing, and dietary fiber content enriches, has
Increase satiety, Constipation, blood sugar lowering, blood fat reducing and the effect such as anticancer, be important dietary fiber sources.From the openest
Patent and relevant non-document see, the processing dead meal such as application corn, beans, fruit and vegerable makes the document report of diet fiber food
Less.
Skin of Semen Maydis, is a kind of side-product of corn deep processing enterprise production.Shallow lake will be entered by corn particle after soaking
Powder production process, forms by working procedure processing such as washing, water squeezing, drying.Its main component is fiber, starch, protein etc..
Semen Maydis through soaking, broken after the Semen Maydis epidermis separated, higher containing protein, content of starch, be mainly used in feedstuff industry；
The product that conventional corn fiber is dried after adding Semen Maydis pulp is and adds pulp fibres, and protein content is up to 16%(butt)
Above, mainly for the production of feedstuff.Make dietary fiber by after skin of Semen Maydis enzyme hydrolysis, dietary fiber also known as the 7th nutrient,
There is moisturizing water suction, colloidal sol and gel can be generated in vivo, postpone composition of food diffusion in digestive organs, promote to delay sugar
Point absorption and to inanimate matter and the absorption of organic matter.
Effervescent tablet is a kind of new dosage form, has that drug release rate is fast, dosage is little, takes, the advantage such as easy to carry, and is administered orally
Effervescent tablet is particularly well-suited to again child, old people and can not swallow the patient of solid preparation.At present, there is not yet with processing of farm products
By-product skin of Semen Maydis is waste dietary fiber, and is prepared the document report of oral effervescent tablet.
Summary of the invention
The purpose of the present invention aims to provide a kind of fine with corn processed by-product skin of Semen Maydis for waste aqueous soluble dietary
Dimension, then the process of effervescent tablet is prepared by described water soluble dietary fiber.
Concrete, the preparation technology of corn dietary fiber effervescent tablet of the present invention, comprise the following steps:
(1) preparation of dietary fiber dry powder:
1) pre-treatment: by skin of Semen Maydis remove impurity, pulverizing, crosses 100 mesh sieves, obtains corn fine powder；
2) defat: take corn fine powder, adds the hexanol of corn fine powder volume 3-5 times, soaks under conditions of temperature is 40-60 DEG C
Carry 0.5-1.5h, filter isolated filtrate and filtering residue, by filter residue and drying, obtain defat material；
3) enzymolysis: extracting degreasing material, adds the distilled water of defat volume of material 10-20 times, regulates pH=5.5-6.5, adds defat
The protease of weight of material 2-5%, enzymolysis 30-60min under the Ultrasonic Conditions that temperature is 25-40 DEG C, filters isolated filter
Liquid and filtering residue；Take filtering residue, add the distilled water of filtering residue volume 15-25 times, regulate pH=4.5-5.0, add filtering residue weight 3-8%
Cellulase, enzymolysis 30-60min under the Ultrasonic Conditions that temperature is 25-40 DEG C, filters isolated filtrate and filtering residue；Will
Twice filtrate merges, and obtains enzymolysis solution；
4) inactivation: by enzymolysis solution steam inactivation 8-15min under conditions of temperature is 95-105 DEG C, be cooled to room temperature；
5) dietary fiber extracts: is placed in Rotary Evaporators by the enzymolysis solution after inactivation, is 0.05-0.08Mpa, temperature in pressure
For being concentrated into the 1/3-1/4 of original volume under conditions of 50-60 DEG C；Calculate with enzymolysis solution volume after concentrating, add 3-5 times of volume
95% ethanol, stands 3-8h after mixing, filter isolated filtrate and precipitation material, be placed in dehydrator by precipitation material and dry and wave
Send out ethanol, be subsequently placed in vacuum freeze drier, in temperature for-30～-20 DEG C, vacuum be under conditions of 30～50Pa cold
The dry 5-15h of lyophilizing, obtains dietary fiber dry powder；
(2) preparation of corn dietary fiber effervescent tablet:
1) dispensing: in terms of parts by weight, takes dietary fiber dry powder 40-60 part, acid agent 5-20 part, alkaline agent 5-20 part, diluent
0.5-5 part, sweeting agent 0.5-5 part, adhesive 2-6 part, correctives 1-5 part, lubricant 0.5-2 part, coating agent 0.5-2 part, multiple
Close vitamin 0.05-0.5 part, standby；
2) prepared by acid grain: first diluent and sweeting agent is mixed and makes it fully absorb, and adds dietary fiber dry powder and acid agent, mixed
Even, it is subsequently adding adhesive, pelletizes, 50 DEG C of dry 1-3h, granulate, obtain sour grain；
3) prepared by alkali grain: take alkaline agent and coating agent, mixing, pulverizes, and crosses 100 mesh sieves, obtains alkali grain；
4) prepared by effervescent tablet: acid grain and alkali grain are mixed, and adds correctives, lubricant, compound vitamin, mixing, is finally placed in
Tabletting in tablet machine, obtains described corn dietary fiber effervescent tablet.
Further illustrating as the present invention, described acid agent selected from citric acid, tartaric acid, fumaric acid, malic acid, oneself two
Acid.
Further illustrating as the present invention, described alkaline agent is selected from sodium carbonate, sodium bicarbonate.
Further illustrating as the present invention, described diluent is selected from mannitol.
Further illustrating as the present invention, described sweeting agent is selected from steviosin, acesulfame potassium, Bath Ba Tian, sucrose, sweetness
Element.
Further illustrating as the present invention, described adhesive is selected from polyvinylpyrrolidone (PVP-K30) ethanol solution,
Concentration is 2-5%.
Further illustrating as the present invention, described correctives is selected from orange flavor, Fructus Citri Limoniae essence, flavoring banana essence, Herba Menthae
Essence, flavoring orange essence.
Further illustrating as the present invention, described lubricant is magnesium stearate, and described coating agent is Polyethylene Glycol (PEG)
6000。
Further illustrating as the present invention, described compound vitamin include vitamin B1, vitamin B2, vitamin B6,
Vitamin B12, vitamin C.
Another object of the present invention is to provide a kind of corn dietary fiber using said method to be prepared to steep
Rise sheet.
Compared with prior art, the present invention reaches to provide the benefit that:
1) present invention prepares dietary fiber dry powder with the side-product skin of Semen Maydis after corn processed for raw material, then is equipped with other adjuvant systems
Standby effervescent tablet, substantially increases the utilization rate of skin of Semen Maydis, adds a new approach for skin of Semen Maydis recycling simultaneously；
2) effervescent tablet being prepared is easy for carrying and eating, and expands adaptation population, child, old people and can not swallow solid
The patient of body preparation all can use, the correctives that simultaneously adds, sweeting agent adjustable effervescent tablet mouthfeel, good palatability；
3) effervescent tablet contains abundant water soluble dietary fiber, has Constipation, blood sugar lowering, blood fat reducing and the effect such as anticancer,
Contain vitamin simultaneously, the aspects such as dyspepsia, the most tired, emotional lability, hypomnesis are had preferable regulation effect.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail, the present embodiment be only the present invention is made clearer
Illustrate rather than limitation of the present invention.
Embodiment 1
The preparation technology of a kind of corn dietary fiber effervescent tablet, comprises the following steps:
(1) preparation of dietary fiber dry powder:
1) pre-treatment: by skin of Semen Maydis remove impurity, pulverizing, crosses 100 mesh sieves, obtains corn fine powder；
2) defat: take corn fine powder, adds the hexanol of corn fine powder volume 3 times, extracts under conditions of temperature is 60 DEG C
1.5h, filters isolated filtrate and filtering residue, by filter residue and drying, obtains defat material；
3) enzymolysis: extracting degreasing material, adds the distilled water of defat volume of material 20 times, regulates pH=6.5, adds defat material weight
The protease of amount 3%, enzymolysis 60min under the Ultrasonic Conditions that temperature is 40 DEG C, filters isolated filtrate and filtering residue；Take filter
Slag, adds the distilled water of filtering residue volume 15 times, regulates pH=5.0, adds the cellulase of filtering residue weight 8%, is 30 DEG C in temperature
Ultrasonic Conditions under enzymolysis 30min, filter isolated filtrate and filtering residue；Twice filtrate is merged, obtains enzymolysis solution；
4) inactivation: by enzymolysis solution steam inactivation 12min under conditions of temperature is 100 DEG C, be cooled to room temperature；
5) dietary fiber extract: will inactivation after enzymolysis solution be placed in Rotary Evaporators, in pressure be 0.06Mpa, temperature be 50
The 1/4 of original volume it is concentrated under conditions of DEG C；Calculate with enzymolysis solution volume after concentrating, add 95% ethanol of 5 times of volumes, mixing
Rear standing 8h, filters isolated filtrate and precipitation material, precipitation material is placed in dehydrator ethanol of drying and volatilize, is subsequently placed in
In vacuum freeze drier, in temperature for-26 DEG C, vacuum be 40Pa under conditions of lyophilization 10h, obtain dietary fiber do
Powder；
(2) preparation of corn dietary fiber effervescent tablet:
1) dispensing: in terms of parts by weight, takes 60 parts of dietary fiber dry powder, acid agent fumaric acid 20 parts, alkaline agent sodium carbonate 20 parts, dilution
(polyvinylpyrrolidone (PVP-K30) ethanol solution, concentration is for 3 parts of agent mannitol, sweeting agent Bath Ba Tian 3 parts, adhesive
5%) 2 parts, correctives flavoring banana essence 3 parts, magnesium stearate lubricant 0.5 part, coating agent (Polyethylene Glycol (PEG) 6000) 0.5 part,
Compound vitamin 0.5 part, standby；
2) prepared by acid grain: first diluent and sweeting agent is mixed and makes it fully absorb, and adds dietary fiber dry powder and acid agent, mixed
Even, it is subsequently adding adhesive, pelletizes, 50 DEG C of dry 3h, granulate, obtain sour grain；
3) prepared by alkali grain: take alkaline agent and coating agent, mixing, pulverizes, and crosses 100 mesh sieves, obtains alkali grain；
4) prepared by effervescent tablet: acid grain and alkali grain are mixed, and adds correctives, lubricant, compound vitamin, mixing, is finally placed in
Tabletting in tablet machine, obtains described corn dietary fiber effervescent tablet.
Embodiment 2
The preparation technology of a kind of corn dietary fiber effervescent tablet, comprises the following steps:
(1) preparation of dietary fiber dry powder:
1) pre-treatment: by skin of Semen Maydis remove impurity, pulverizing, crosses 100 mesh sieves, obtains corn fine powder；
2) defat: take corn fine powder, adds the hexanol of corn fine powder volume 3-5 times, extracts under conditions of temperature is 60 DEG C
0.5h, filters isolated filtrate and filtering residue, by filter residue and drying, obtains defat material；
3) enzymolysis: extracting degreasing material, adds the distilled water of defat volume of material 20 times, regulates pH=5.5, adds defat material weight
The protease of amount 2%, enzymolysis 60min under the Ultrasonic Conditions that temperature is 40 DEG C, filters isolated filtrate and filtering residue；Take filter
Slag, adds the distilled water of filtering residue volume 25 times, regulates pH=4.5, adds the cellulase of filtering residue weight 3%, is 25 DEG C in temperature
Ultrasonic Conditions under enzymolysis 45min, filter isolated filtrate and filtering residue；Twice filtrate is merged, obtains enzymolysis solution；
4) inactivation: by enzymolysis solution steam inactivation 15min under conditions of temperature is 95 DEG C, be cooled to room temperature；
5) dietary fiber extract: will inactivation after enzymolysis solution be placed in Rotary Evaporators, in pressure be 0.05Mpa, temperature be 60
The 1/3 of original volume it is concentrated under conditions of DEG C；Calculate with enzymolysis solution volume after concentrating, add 95% ethanol of 3 times of volumes, mixing
Rear standing 8h, filters isolated filtrate and precipitation material, precipitation material is placed in dehydrator ethanol of drying and volatilize, is subsequently placed in
In vacuum freeze drier, in temperature for-24 DEG C, vacuum be 50Pa under conditions of lyophilization 5h, obtain dietary fiber do
Powder；
(2) preparation of corn dietary fiber effervescent tablet:
1) dispensing: in terms of parts by weight, takes 40 parts of dietary fiber dry powder, acid agent citric acid 10 parts, alkaline agent sodium carbonate 15 parts, dilution
2 parts of agent mannitol, sweeting agent steviosin 2 parts, adhesive (polyvinylpyrrolidone (PVP-K30) ethanol solution, concentration is 3%) 3
Part, correctives orange flavor 3 parts, magnesium stearate lubricant 1 part, coating agent (Polyethylene Glycol (PEG) 6000) 0.5 part, compound dimension
Raw element 0.1 part, standby；
2) prepared by acid grain: first diluent and sweeting agent is mixed and makes it fully absorb, and adds dietary fiber dry powder and acid agent, mixed
Even, it is subsequently adding adhesive, pelletizes, 50 DEG C of dry 1h, granulate, obtain sour grain；
3) prepared by alkali grain: take alkaline agent and coating agent, mixing, pulverizes, and crosses 100 mesh sieves, obtains alkali grain；
4) prepared by effervescent tablet: acid grain and alkali grain are mixed, and adds correctives, lubricant, compound vitamin, mixing, is finally placed in
Tabletting in tablet machine, obtains described corn dietary fiber effervescent tablet.
Embodiment 3
The preparation technology of a kind of corn dietary fiber effervescent tablet, comprises the following steps:
(1) preparation of dietary fiber dry powder:
1) pre-treatment: by skin of Semen Maydis remove impurity, pulverizing, crosses 100 mesh sieves, obtains corn fine powder；
2) defat: take corn fine powder, adds the hexanol of corn fine powder volume 4 times, extracts 1h under conditions of temperature is 50 DEG C,
Filter isolated filtrate and filtering residue, by filter residue and drying, obtain defat material；
3) enzymolysis: extracting degreasing material, adds the distilled water of defat volume of material 15 times, regulates pH=6.0, adds defat material weight
The protease of amount 3%, enzymolysis 45min under the Ultrasonic Conditions that temperature is 35 DEG C, filters isolated filtrate and filtering residue；Take filter
Slag, adds the distilled water of filtering residue volume 20 times, regulates pH=4.8, adds the cellulase of filtering residue weight 5%, is 30 DEG C in temperature
Ultrasonic Conditions under enzymolysis 30min, filter isolated filtrate and filtering residue；Twice filtrate is merged, obtains enzymolysis solution；
4) inactivation: by enzymolysis solution steam inactivation 8min under conditions of temperature is 105 DEG C, be cooled to room temperature；
5) dietary fiber extract: will inactivation after enzymolysis solution be placed in Rotary Evaporators, in pressure be 0.08Mpa, temperature be 50
The 1/4 of original volume it is concentrated under conditions of DEG C；Calculate with enzymolysis solution volume after concentrating, add 95% ethanol of 4 times of volumes, mixing
Rear standing 4h, filters isolated filtrate and precipitation material, precipitation material is placed in dehydrator ethanol of drying and volatilize, is subsequently placed in
In vacuum freeze drier, in temperature for-25 DEG C, vacuum be 40Pa under conditions of lyophilization 15h, obtain dietary fiber do
Powder；
(2) preparation of corn dietary fiber effervescent tablet:
1) dispensing: in terms of parts by weight, takes 50 parts of dietary fiber dry powder, acid agent adipic acid 15 parts, alkaline agent sodium carbonate 15 parts, dilution
3 parts of agent mannitol, sweeting agent cyclamate 3 parts, adhesive (polyvinylpyrrolidone (PVP-K30) ethanol solution, concentration is 3%) 5
Part, correctives flavoring orange essence 1.5 parts, magnesium stearate lubricant 1.5 parts, coating agent (Polyethylene Glycol (PEG) 6000) 1 part, compound
Vitamin 0.3 part, standby；
2) prepared by acid grain: first diluent and sweeting agent is mixed and makes it fully absorb, and adds dietary fiber dry powder and acid agent, mixed
Even, it is subsequently adding adhesive, pelletizes, 50 DEG C of dry 2h, granulate, obtain sour grain；
3) prepared by alkali grain: take alkaline agent and coating agent, mixing, pulverizes, and crosses 100 mesh sieves, obtains alkali grain；
4) prepared by effervescent tablet: acid grain and alkali grain are mixed, and adds correctives, lubricant, compound vitamin, mixing, is finally placed in
Tabletting in tablet machine, obtains described corn dietary fiber effervescent tablet.
Embodiment 4
The preparation technology of a kind of corn dietary fiber effervescent tablet, comprises the following steps:
(1) preparation of dietary fiber dry powder:
1) pre-treatment: by skin of Semen Maydis remove impurity, pulverizing, crosses 100 mesh sieves, obtains corn fine powder；
2) defat: take corn fine powder, adds the hexanol of corn fine powder volume 4 times, extracts 1h under conditions of temperature is 50 DEG C,
Filter isolated filtrate and filtering residue, by filter residue and drying, obtain defat material；
3) enzymolysis: extracting degreasing material, adds the distilled water of defat volume of material 15 times, regulates pH=6.0, adds defat material weight
The protease of amount 4%, enzymolysis 35min under the Ultrasonic Conditions that temperature is 35 DEG C, filters isolated filtrate and filtering residue；Take filter
Slag, adds the distilled water of filtering residue volume 25 times, regulates pH=4.7, adds the cellulase of filtering residue weight 4%, is 35 DEG C in temperature
Ultrasonic Conditions under enzymolysis 40min, filter isolated filtrate and filtering residue；Twice filtrate is merged, obtains enzymolysis solution；
4) inactivation: by enzymolysis solution steam inactivation 10min under conditions of temperature is 100 DEG C, be cooled to room temperature；
5) dietary fiber extract: will inactivation after enzymolysis solution be placed in Rotary Evaporators, in pressure be 0.07Mpa, temperature be 55
The 1/4 of original volume it is concentrated under conditions of DEG C；Calculate with enzymolysis solution volume after concentrating, add 95% ethanol of 5 times of volumes, mixing
Rear standing 3h, filters isolated filtrate and precipitation material, precipitation material is placed in dehydrator ethanol of drying and volatilize, is subsequently placed in
In vacuum freeze drier, in temperature for-30 DEG C, vacuum be 30Pa under conditions of lyophilization 12h, obtain dietary fiber do
Powder；
(2) preparation of corn dietary fiber effervescent tablet:
1) dispensing: in terms of parts by weight, takes 50 parts of dietary fiber dry powder, 20 parts of agent tartaric acid of acid, alkaline agent sodium bicarbonate 5 parts, dilute
Release 5 parts of agent mannitol, sweeting agent acesulfame potassium 0.5 part, (polyvinylpyrrolidone (PVP-K30) ethanol solution, concentration is adhesive
2%) 6 parts, correctives Fructus Citri Limoniae essence 5 parts, magnesium stearate lubricant 0.5 part, coating agent (Polyethylene Glycol (PEG) 6000) 2 parts, multiple
Close vitamin 0.2 part, standby；
2) prepared by acid grain: first diluent and sweeting agent is mixed and makes it fully absorb, and adds dietary fiber dry powder and acid agent, mixed
Even, it is subsequently adding adhesive, pelletizes, 50 DEG C of dry 2h, granulate, obtain sour grain；
3) prepared by alkali grain: take alkaline agent and coating agent, mixing, pulverizes, and crosses 100 mesh sieves, obtains alkali grain；
4) prepared by effervescent tablet: acid grain and alkali grain are mixed, and adds correctives, lubricant, compound vitamin, mixing, is finally placed in
Tabletting in tablet machine, obtains described corn dietary fiber effervescent tablet.
Embodiment 5
The preparation technology of a kind of corn dietary fiber effervescent tablet, comprises the following steps:
(1) preparation of dietary fiber dry powder:
1) pre-treatment: by skin of Semen Maydis remove impurity, pulverizing, crosses 100 mesh sieves, obtains corn fine powder；
2) defat: take corn fine powder, adds the hexanol of corn fine powder volume 3 times, extracts 1h under conditions of temperature is 45 DEG C,
Filter isolated filtrate and filtering residue, by filter residue and drying, obtain defat material；
3) enzymolysis: extracting degreasing material, adds the distilled water of defat volume of material 15 times, regulates pH=6.0, adds defat material weight
The protease of amount 3%, enzymolysis 40min under the Ultrasonic Conditions that temperature is 35 DEG C, filters isolated filtrate and filtering residue；Take filter
Slag, adds the distilled water of filtering residue volume 20 times, regulates pH=4.8, adds the cellulase of filtering residue weight 7%, is 35 DEG C in temperature
Ultrasonic Conditions under enzymolysis 35min, filter isolated filtrate and filtering residue；Twice filtrate is merged, obtains enzymolysis solution；
4) inactivation: by enzymolysis solution steam inactivation 8-15min under conditions of temperature is 95-105 DEG C, be cooled to room temperature；
5) dietary fiber extract: will inactivation after enzymolysis solution be placed in Rotary Evaporators, in pressure be 0.06Mpa, temperature be 55
The 1/3 of original volume it is concentrated under conditions of DEG C；Calculate with enzymolysis solution volume after concentrating, add 95% ethanol of 4 times of volumes, mixing
Rear standing 5h, filters isolated filtrate and precipitation material, precipitation material is placed in dehydrator ethanol of drying and volatilize, is subsequently placed in
In vacuum freeze drier, in temperature for-20 DEG C, vacuum be 35Pa under conditions of lyophilization 8h, obtain dietary fiber do
Powder；
(2) preparation of corn dietary fiber effervescent tablet:
1) dispensing: in terms of parts by weight, takes 40 parts of dietary fiber dry powder, acid agent malic acid 5 parts, alkaline agent sodium bicarbonate 15 parts, dilute
Release 1 part of agent mannitol, sweeting agent sucrose 4 parts, adhesive (polyvinylpyrrolidone (PVP-K30) ethanol solution, concentration is 4%) 4
Part, correctives Mint Essence 4 parts, magnesium stearate lubricant 2 parts, coating agent (Polyethylene Glycol (PEG) 6000) 1.5 parts, compound dimension
Raw element 0.4 part, standby；
2) prepared by acid grain: first diluent and sweeting agent is mixed and makes it fully absorb, and adds dietary fiber dry powder and acid agent, mixed
Even, it is subsequently adding adhesive, pelletizes, 50 DEG C of dry 1h, granulate, obtain sour grain；
3) prepared by alkali grain: take alkaline agent and coating agent, mixing, pulverizes, and crosses 100 mesh sieves, obtains alkali grain；
4) prepared by effervescent tablet: acid grain and alkali grain are mixed, and adds correctives, lubricant, compound vitamin, mixing, is finally placed in
Tabletting in tablet machine, obtains described corn dietary fiber effervescent tablet.
The ultimate principle of the present invention, principal character and advantage have more than been shown and described.Those skilled in the art should
Understanding, the present invention is not restricted to the described embodiments, and the simply explanation present invention's described in above-described embodiment and description is former
Reason, without departing from the spirit and scope of the present invention, the present invention also has various changes and modifications, these changes and improvements
Both fall within scope of the claimed invention.Claimed scope is by appending claims and equivalent circle thereof
Fixed.
Claims (10)
1. the preparation technology of a corn dietary fiber effervescent tablet, it is characterised in that comprise the following steps:
(1) preparation of dietary fiber dry powder:
1) pre-treatment: by skin of Semen Maydis remove impurity, pulverizing, crosses 100 mesh sieves, obtains corn fine powder；
2) defat: take corn fine powder, adds the hexanol of corn fine powder volume 3-5 times, soaks under conditions of temperature is 40-60 DEG C
Carry 0.5-1.5h, filter isolated filtrate and filtering residue, by filter residue and drying, obtain defat material；
3) enzymolysis: extracting degreasing material, adds the distilled water of defat volume of material 10-20 times, regulates pH=5.5-6.5, adds defat
The protease of weight of material 2-5%, enzymolysis 30-60min under the Ultrasonic Conditions that temperature is 25-40 DEG C, filters isolated filter
Liquid and filtering residue；Take filtering residue, add the distilled water of filtering residue volume 15-25 times, regulate pH=4.5-5.0, add filtering residue weight 3-8%
Cellulase, enzymolysis 30-60min under the Ultrasonic Conditions that temperature is 25-40 DEG C, filters isolated filtrate and filtering residue；Will
Twice filtrate merges, and obtains enzymolysis solution；
4) inactivation: by enzymolysis solution steam inactivation 8-15min under conditions of temperature is 95-105 DEG C, be cooled to room temperature；
5) dietary fiber extracts: is placed in Rotary Evaporators by the enzymolysis solution after inactivation, is 0.05-0.08Mpa, temperature in pressure
For being concentrated into the 1/3-1/4 of original volume under conditions of 50-60 DEG C；Calculate with enzymolysis solution volume after concentrating, add 3-5 times of volume
95% ethanol, stands 3-8h after mixing, filter isolated filtrate and precipitation material, be placed in dehydrator by precipitation material and dry and wave
Send out ethanol, be subsequently placed in vacuum freeze drier, in temperature for-30～-20 DEG C, vacuum be under conditions of 30～50Pa cold
The dry 5-15h of lyophilizing, obtains dietary fiber dry powder；
(2) preparation of corn dietary fiber effervescent tablet:
1) dispensing: in terms of parts by weight, takes dietary fiber dry powder 40-60 part, acid agent 5-20 part, alkaline agent 5-20 part, diluent
0.5-5 part, sweeting agent 0.5-5 part, adhesive 2-6 part, correctives 1-5 part, lubricant 0.5-2 part, coating agent 0.5-2 part, multiple
Close vitamin 0.05-0.5 part, standby；
2) prepared by acid grain: first diluent and sweeting agent is mixed and makes it fully absorb, and adds dietary fiber dry powder and acid agent, mixed
Even, it is subsequently adding adhesive, pelletizes, 50 DEG C of dry 1-3h, granulate, obtain sour grain；
3) prepared by alkali grain: take alkaline agent and coating agent, mixing, pulverizes, and crosses 100 mesh sieves, obtains alkali grain；
4) prepared by effervescent tablet: acid grain and alkali grain are mixed, and adds correctives, lubricant, compound vitamin, mixing, is finally placed in
Tabletting in tablet machine, obtains described corn dietary fiber effervescent tablet.
The preparation technology of corn dietary fiber effervescent tablet the most according to claim 1, it is characterised in that described acid agent is selected from lemon
Lemon acid, tartaric acid, fumaric acid, malic acid, adipic acid.
The preparation technology of corn dietary fiber effervescent tablet the most according to claim 1, it is characterised in that described alkaline agent is selected from carbon
Acid sodium, sodium bicarbonate.
The preparation technology of corn dietary fiber effervescent tablet the most according to claim 1, it is characterised in that described diluent is selected from
Mannitol.
The preparation technology of corn dietary fiber effervescent tablet the most according to claim 1, it is characterised in that described sweeting agent is selected from
Steviosin, acesulfame potassium, Bath Ba Tian, sucrose, cyclamate.
The preparation technology of corn dietary fiber effervescent tablet the most according to claim 1, it is characterised in that described adhesive is selected from
Polyvinylpyrrolidone (PVP-K30) ethanol solution, concentration is 2-5%.
The preparation technology of corn dietary fiber effervescent tablet the most according to claim 1, it is characterised in that described correctives is selected from
Orange flavor, Fructus Citri Limoniae essence, flavoring banana essence, Mint Essence, flavoring orange essence.
The preparation technology of corn dietary fiber effervescent tablet the most according to claim 1, it is characterised in that described lubricant is hard
Fatty acid magnesium, described coating agent is Polyethylene Glycol (PEG) 6000.
The preparation technology of corn dietary fiber effervescent tablet the most according to claim 1, it is characterised in that described compound vitamin
Including vitamin B1, vitamin B2, vitamin B6, vitamin B12, vitamin C.
10. a corn dietary fiber effervescent tablet, it is characterised in that be prepared by the arbitrary described method of claim 1-9.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610567848.1A CN106213114A (en) | 2016-07-19 | 2016-07-19 | Corn dietary fiber effervescent tablet and preparation technology thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610567848.1A CN106213114A (en) | 2016-07-19 | 2016-07-19 | Corn dietary fiber effervescent tablet and preparation technology thereof |
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Cited By (7)
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| CN109258866A (en) * | 2018-09-04 | 2019-01-25 | 四川理工学院 | A kind of green tea soluble dietary fiber effervescent tablet and its preparation process |
| CN112335803A (en) * | 2019-08-06 | 2021-02-09 | 吉林省绿色食品工程研究院 | Process for preparing black corn carbonated beverage and product thereof |
| CN114304465A (en) * | 2022-01-27 | 2022-04-12 | 陇南市祥宇油橄榄开发有限责任公司 | Olive leaf extract effervescent tablet and preparation method thereof |
| US11718594B2 (en) | 2016-09-21 | 2023-08-08 | Celanese International Corporation | Acesulfame potassium compositions and processes for producing same |
| US11724994B2 (en) | 2016-09-21 | 2023-08-15 | Celanese International Corporation | Acesulfame potassium compositions and processes for producing same |
| US11724993B2 (en) | 2016-09-21 | 2023-08-15 | Celanese International Corporation | Acesulfame potassium compositions and processes for producing same |
| US11731948B2 (en) | 2016-09-21 | 2023-08-22 | Celanese International Corporation | Acesulfame potassium compositions and processes for producing same |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| US11718594B2 (en) | 2016-09-21 | 2023-08-08 | Celanese International Corporation | Acesulfame potassium compositions and processes for producing same |
| US11724994B2 (en) | 2016-09-21 | 2023-08-15 | Celanese International Corporation | Acesulfame potassium compositions and processes for producing same |
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| CN112335803A (en) * | 2019-08-06 | 2021-02-09 | 吉林省绿色食品工程研究院 | Process for preparing black corn carbonated beverage and product thereof |
| CN114304465A (en) * | 2022-01-27 | 2022-04-12 | 陇南市祥宇油橄榄开发有限责任公司 | Olive leaf extract effervescent tablet and preparation method thereof |
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Application publication date: 20161214 |