CN106172886A - Flos Camelliae Japonicae Semen Juglandis mixed oil and preparation method thereof - Google Patents
Flos Camelliae Japonicae Semen Juglandis mixed oil and preparation method thereof Download PDFInfo
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- CN106172886A CN106172886A CN201610575994.9A CN201610575994A CN106172886A CN 106172886 A CN106172886 A CN 106172886A CN 201610575994 A CN201610575994 A CN 201610575994A CN 106172886 A CN106172886 A CN 106172886A
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- oil
- semen juglandis
- flos camelliae
- camelliae japonicae
- mixed oil
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/06—Preservation of finished products
Abstract
The invention discloses a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil and preparation method thereof, solve the problem that existing edible oil is easily ruined.Technical scheme one Flos Camelliae Japonicae Semen Juglandis mixed oil, described Flos Camelliae Japonicae Semen Juglandis mixed oil in parts by weight, including following components: Camellia oil 45 ~ 58 parts；Walnut oil 18 ~ 26 parts；Oleum Perillae 2 ~ 8 parts；Vitamin E 0.1 ~ 0.2 part；The ratio of the weight portion of wherein said Oleum Perillae and the weight portion of Camellia oil is 1:10, is the mixed oil being processed preparation by Flos Camelliae Japonicae and Semen Juglandis, its rich in vitamin E can slow down the speed that the unsaturated fatty acid in mixed oil is oxidized, there is longer shelf life.
Description
Technical field
The present invention relates to edible oil technical field, particularly to a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil and preparation method thereof.
Background technology
At present, tea oil tree is one of big woody edible oil material seeds in the world four, and Camellia oil is nutritious, cholesterol level
Few, unsaturated fatty acid, oleic acid and linoleic acid content are up to more than 90%, and rich in tea polysaccharide, Saponin, flavone, tea polyphenols, dimension
Multiple nutrients and the functional activity materials such as raw element and plant sterol, have raising immunity, radioprotective, removing free radical, fall three
High, prophylaxis of tumours effect, is the woody health-care edible oil of a kind of high-quality.Walnut oil be use Semen Juglandis be raw material, through overvoltage
Squeeze the vegetable oil that technique is made, fall within edible oil.Walnut oil is equally rich in unsaturated fatty acid, wherein with linolenic acid and Asia
Oleic acid is main, and it is the fatty acid of needed by human body, has reduction blood fat, prevention coronary heart disease and atherosclerotic effect,
Even there is the prevention drug effect such as senile dementia and cancer.But regulation is prepared in the processing of current rare use above two edible oil
The method of oil, great majority are processed only with Camellia or Semen Juglandis and are prepared Camellia oil and walnut oil.
The patent application of Publication No. CN104232292A discloses cold pressing and the method for refining of a kind of Camellia oil, and it is only
Being that processing is prepared Camellia oil and is not directed to walnut oil, technical scheme is: Semen Camelliae carries out camellia seed kernel and Semen Camelliae shell divides
From, roll into material base, then carry out steaming and fry, dry, then material base is fed into cold pressing expeller and squeezes；Carry out again degumming alkali refining, washing,
Decolouring, deodorize, dewaxing, obtain camellia oleosa seed product oil.Although using the quality of the Camellia oil oil of said method processing significantly better than heat
Oil expression, but during Camellia oil refine produces, only focus on product quality indicator, especially organoleptic indicator, do not focus on refining process pair
The impact of Camellia oil Middle nutrition composition, it uses high temperature alkaline solution alkali-refining deacidification and high temperature big adsorbent amount decolouring etc., not only makes
Camellia oil refining yield reduces, and also results in the nutritional labeling plant sterol in Camellia oil and vitamin E loses in a large number, make Camellia oil
Nutritive value be substantially reduced, product quality reduce.
In order to realize the detraction potentiation that Camellia oil produces, it is badly in need of proposing a kind of new Camellia oil production and processing method.
Utility model content
The first object of the present invention is to provide a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil, is the mediation being processed preparation by Flos Camelliae Japonicae and Semen Juglandis
Oil, its rich in vitamin E can slow down the speed that the unsaturated fatty acid in mixed oil is oxidized, there are longer shelf
Phase.
The above-mentioned technical purpose of the present invention has the technical scheme that a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil,
Described Flos Camelliae Japonicae Semen Juglandis mixed oil in parts by weight, including following components: Camellia oil 45～58 parts；Walnut oil 18～26 parts；Folium Perillae
Seed oil 2～8 parts；Vitamin E 0.1～0.2 part；The weight portion of wherein said Oleum Perillae and the ratio of the weight portion of Camellia oil
For 1:10.
By technique scheme, Camellia oil has clear, abnormal smells from the patient delicate fragrance, is good edible oil, itself and Fructus Canarii albi
Oil is the most similar, and unsaturated fatty acids pinolenic acid and linoleic acid content are more than 80 percent, compared with other edible oil,
The content of the monounsaturated fatty acid of Camellia oil is the highest in all vegetable oil easily to draw owing to too much taking in satisfied fatty acid
Play hyperlipidemia, cardiovascular disease, and between monounsaturated fatty acid molecule, there is double bond.And the content of vitamin E ratio in Camellia oil
Olive oil exceeds more than one times, and vitamin E has stronger biological activity, it is possible to anti-lipid peroxidation, simultaneously possibly together with Fructus Canarii albi
Unexistent bioactive substance such as camellianin and tea polyphenols in oil, has the reduction several functions such as cholesterol and prophylaxis of tumours.
Unsaturated fatty acid and linoleic acid content in Semen Juglandis are high, and when extracting oils and fats, the quantum of output of oils and fats is big, simultaneously Semen Juglandis in also
Containing essential fatty acids such as linoleic acids, the cholesterol in human serum can be reduced by it, prevent arteriosclerosis and
Thrombosis aspect has positive effect, the most also have aid digestion, fill blood effect；Fructus Perillae oil yield is high, Fructus Perillae
Oil is easily obtained, and in oil, linolenic acid content is up to 85%, mainly possibly together with flavones ingredient, and the aminoacid of needed by human body and big
The vitamin E of amount, and vitamin E is up to 500mg/Kg, therefore adds Oleum Perillae in mixed oil and can be obviously improved tune
With the content of vitamin E in oil, the most also improve the plumpness of other nutrient substance in mixed oil；The vitamin E directly added
The content of mixed oil antioxidant can be significantly improved；But the content being as vitamin E increases, then the non-oxidizability of oils and fats
Gradually strengthening, when vitamin E reaches certain concentration, the non-oxidizability of oils and fats the most easily declines, and the purple in the present invention
The ratio of the weight portion of Fructus Perillae oil and the weight portion of Camellia oil is 1:10, and regulate the weight deal that vitamin E adds be 0.1～
0.2 part so that mixed oil reaches equilibrium state containing vitamin E.Therefore the present invention is by natural containing in Oleum Perillae
Vitamin E and the vitamin E that is added into make mixed oil either in preparation process or within period of guaranteeing the quality, it contains
Unsaturated fatty acid is had all to be difficult to the trans fatty acid being oxidized to have hazardness, so mixed oil has longer shelf life
With the edible phase.
The present invention is further: in parts by weight, described Camellia oil 49～52 parts.
The present invention is further: in parts by weight, described Oleum Perillae 5 parts.
By technique scheme, under above-mentioned allotment ratio, weight portion is the science that Oleum Perillae is the present invention of 5 parts
Allotment ratio so that the content of vitamin E will not be excessive, when the dimension being added into weight portion 0.1～0.2 part again in mixed oil is raw
During element E, the content of vitamin E easily regulates and controls；Mixed oil is still with Camellia oil that weight portion is 49～52 parts and weight portion simultaneously
Be the walnut oil of 18～26 parts be bulk composition, retain Camellia oil and walnut lubricant volatile flavor component, there is strong Jiao
Fragrant.
The present invention is further: also include Oleum Helianthi, in parts by weight, described Oleum Helianthi 4～8 parts.
By technique scheme, the human consumption of Oleum Helianthi leads up to more than 96%, although (be in harmonious proportion without linolenic acid
Linolenic acid in oil can come from Camellia oil and walnut oil), but it contains abundant linoleic acid, significantly reduces cholesterol, anti-
Hemostatic tube hardening and the effect of prevention coronary heart disease.It addition, the content of a tocopherol that physiologically active is the strongest is than general in Oleum Helianthi
Plant innage.By being added into Oleum Helianthi, regulate mixed oil Linoleic acid content contain with vitamin E not introducing linolenic acid
The balanced proportion of amount, thus reach to be easy to the purpose that absorption of human body utilizes.
The present invention is further: also including synergist, in parts by weight, described synergist is citric acid 0.05～0.35
Part and ascorbic acid 0.04～0.08 part.
By technique scheme, it is added into a certain amount of citric acid and ascorbic acid can cross the antioxygen extending vitamin E
Change effect so that vitamin E has the effect preventing unsaturated fatty acid oxidized for a long time, and citric acid and ascorbic acid are to people
Body non-hazardous, on the contrary after human body takes in mixed oil with ascorbic acid, improve effective to mixed oil Middle nutrition material of the intestines and stomach
Absorb and quickly absorb, improve the absorbance of mixed oil Middle nutrition material, taste after life-time service mixed oil, can be improved, strengthen
Body constitution, especially has obvious curative effects to obesity.
The second object of the present invention is to provide the preparation method of a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil, it is possible to prepare above-mentioned richness
Mixed oil containing vitamin E, mixed oil has longer shelf life.
The above-mentioned technical purpose of the present invention has the technical scheme that one prepares above-mentioned Flos Camelliae Japonicae Semen Juglandis
The method of mixed oil, comprises the steps: step 1, selection: use disintegrating machine respectively to Flos Camelliae Japonicae and walnut shell-breaking, removes rotten
Camellia and Semen Juglandis, selection high-quality Camellia and Semen Juglandis；Step 2, decortication: use the deionized water containing diluted alkaline 2% to step
Semen Juglandis in rapid 1 soaks, decortication processes 30～60min；Step 3, dries: use dehydrator to enter the Semen Juglandis in step 2
Row dried so that it is water content 3%～5%；Step 4, squeezing: the Semen Juglandis that Camellia step 2 obtained and step 3 obtain
Core is respectively placed in two squeezers squeezing and obtains Flos Camelliae Japonicae crude oil and oil residue mixing compound and Semen Juglandis crude oil and the mixing of the dregs of fat
Thing；Add precipitant to be centrifuged two kinds of crude oils and the dregs of fat processing, remove the dregs of fat and obtain Flos Camelliae Japonicae pure wool oil and Semen Juglandis pure wool oil；
Step 5, purifies: add deionized water in the Flos Camelliae Japonicae pure wool oil in step 4 and Semen Juglandis pure wool oil, quiet after stirring 30～60min
Put, be layered and remove layer of diw, extract upper strata fluid and respectively obtain Camellia oil and walnut oil；Step 6, allotment: by formula
Camellia oil, walnut oil, Oleum Perillae and the vitamin E of amount carry out being mixed to get mixed oil.
By technique scheme, reduce Camellia and vitamin E or other battalion during mixed oil prepared by Semen Juglandis
The number of dropouts formed point, obtain mixed oil still rich in vitamin E, the unsaturated fatty acid in mixed oil can be slowed down oxidized
Speed, the advantage with shelf life length；The output capacity of mixed oil can be improved simultaneously.
The present invention is further: in described step 4, uses Burdick lamp that Flos Camelliae Japonicae pure wool oil and Semen Juglandis pure wool oil are irradiated 60
～80min.
By technique scheme, can produce a small amount of aflatoxin B 1 in expressing process, aflatoxin B 1 is
A kind of noxious substance, is ingested and can be detrimental to health into the human body, and uses Burdick lamp to irradiate pure wool oil, and ultraviolet can
Aflatoxin B 1 in pure wool oil is degraded；Ultraviolet can kill the antibacterial produced in expressing process simultaneously, therefore
Cleanliness factor and the edible safety of mixed oil can be improved by the irradiation of ultraviolet etc..
The present invention is further: in described step 5, is extracted the Flos Camelliae Japonicae accounting for total upper strata fluid 85%～90% by tipping
Pure wool oil, pours into residue pure wool oil and removes ionized water equipped with filtering in the filter of micropore filtering film.
By technique scheme, although it is simple to operate to extract upper strata fluid by the way of toppling over, it can be difficult to accurately
Controlling the assurance amount of toppling over, when the deionized water of lower floor is dumped in catcher along with fluid, the mixed oil obtained contains
Ionized water causes purity low, and therefore the present invention uses and topples over the fluid accounting for total upper strata fluid 85%～90%, remaining pure wool oil
Using micropore filtering film that deionized water and pure wool oil are carried out separation to regather, the micropore filtering film containing certain pore size is to pure wool
When oil and deionized water separate, the deionized water molecule that molecular particle size is little can pass through micropore filtering film thus be removed,
The oil molecule that molecular particle size is big then can not pass through micropore filtering film, stay in separation process the upside of micropore filtering film from
And collect purpose after reaching to separate.Therefore this programme can improve the purity of mixed oil, then improves the quality of mixed oil,
In the output capacity of processing mixed oil, promote a ladder simultaneously.
The present invention is further: in described step 5, and residue Flos Camelliae Japonicae pure wool oil is joined filter and at sucking filtration bar by amount
Sucking filtration process is carried out under part.
By technique scheme, use micropore filtering film is when separating deionized water and pure wool oil, due to oil
The mobility of molecule is less than normal, and therefore the rate of filtration is slow, and the deionized water being blended in fluid is difficult to through micropore filtering film quilt
Separate and remove, and when using suction filter pump that the mixture of deionized water and fluid is carried out sucking filtration, it is possible to form a negative pressure state
Sucking filtration chamber so that deionized water from the side of micropore filtering film quickly by the opposite side of sucking filtration to micropore filtering film, thus
Realize accelerating deionized water and the separation of fluid, reduce and separate the use time.
The present invention is further: described step 4 and described step 5 are carried out the most under nitrogen protection.
By technique scheme, the squeezing of Semen Juglandis and purification process are carried out the most under nitrogen protection, and nitrogen is to squeezing
The pure wool oil and the extraction upper strata fluid that go out have protective effect, and oxygen is discharged when being passed through preparation container processes by nitrogen, in isolation
The unsaturated fatty acid being prevented from pure wool oil or upper strata fluid under air condition is oxidized, is passed through nitrogen simultaneously and removes oxygen
Gas is easier compared to the operation that vacuum removes oxygen, to container also without particular/special requirement, implements operability bigger.
In sum: one, the Flos Camelliae Japonicae Semen Juglandis mixed oil using the preparation method of the present invention and raw material components to obtain belongs to
The mixed oil of spleen benefiting and stimulating the appetite, does not contain only the nutritional labeling of crab oil, but also containing the nutritional labeling in walnut oil, adds simultaneously
The Oleum Perillae entered and Oleum Helianthi enable to the ratio of the linoleic acid in mixed oil and vitamin E and reach balance, thus reach
Taking in, to human body, the purpose that mixed oil is easy to absorb, it is of value to the physical and mental health of human body, spleen-and-stomach-invigorating；Its two, in mixed oil
The antioxidant such as rich in vitamin E, in addition with citric acid and the potentiation of ascorbic acid so that mixed oil has considerably long
Shelf life, be also less likely to occur to ruin in the simultaneously edible period after uncapping, this is mainly vitamin E and is prevented from being in harmonious proportion
Unsaturated fatty acid in oil is difficult to oxidized；Its three, by use physical squeezing method, do not introduce the alkali liquor etc. that concentration is high
Prepared by chemical agent, thus the nutrient substance in mixed oil will not run off, and not only the quality of mixed oil is protected, and seeks in mixed oil
Form point the fullest, long-time edible after improve in body balanced in nutrition；Simultaneously when pure wool oil is purified
Use micropore filtering film to separate pure wool oil and deionized water with the mode of sucking filtration, on the one hand make the purity in mixed oil more
On the other hand height, in the case of moisture is low, mixed oil is not easy to ruin, and can carry out pure wool oil point after going up largely
From purification, improve the output capacity of oil expression.
Detailed description of the invention
Hereinafter the present invention is described in further detail.
Embodiment 1 to embodiment 5 prepares mixed oil, step 1, selection: use disintegrating machine respectively by following method
To Flos Camelliae Japonicae and walnut shell-breaking, remove rotten Camellia and Semen Juglandis, selection high-quality Camellia and Semen Juglandis；Step 2, decortication: adopt
With the deionized water containing diluted alkaline 2%, the Semen Juglandis immersion in step 1, decortication are processed 45min；Step 3, dries: uses and dries
Machine is dried process to the Semen Juglandis in step 2 so that it is water content 3%～5%；Step 4, squeezing: the mountain that step 2 is obtained
The Semen Juglandis that camellia oleosa seed and step 3 obtain be respectively placed in two squeezers squeezing obtain Flos Camelliae Japonicae crude oil and oil residue mixing compound and
Semen Juglandis crude oil and the mixture of the dregs of fat；Add precipitant to be centrifuged two kinds of crude oils and the dregs of fat processing, remove the dregs of fat and obtain mountain
Tea pure wool oil and Semen Juglandis pure wool oil；Step 5, purifies: the Flos Camelliae Japonicae pure wool oil in step 4 adds deionization in Semen Juglandis pure wool oil
Water, stands, is layered and removes layer of diw after stirring 45min, extracts upper strata fluid and respectively obtains Camellia oil and walnut oil；Step
Rapid 6, allotment: carry out being mixed to get mixed oil by the Camellia oil of formula ratio, walnut oil, Oleum Perillae and vitamin E；Step 7, presses
The Oleum Helianthi of formula ratio, citric acid, ascorbic acid are added in above-mentioned mixed oil.
The wherein component of the Flos Camelliae Japonicae Semen Juglandis mixed oil of embodiment 1 to embodiment 5 and parts by weight such as form 1 to form 5 thereof
Shown in.
Embodiment 1: a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil
The form 1 Flos Camelliae Japonicae each component of Semen Juglandis mixed oil and parts by weight thereof
| Component | Number (part) | Component | Number (part) |
| Camellia oil | 45 | Oleum Perillae | 8.0 |
| Walnut oil | 26 | Vitamin E | 0.15 |
Embodiment 2: a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil
The form 2 Flos Camelliae Japonicae each component of Semen Juglandis mixed oil and parts by weight thereof
Embodiment 3: a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil
The form 3 Flos Camelliae Japonicae each component of Semen Juglandis mixed oil and parts by weight thereof
| Component | Number (part) | Component | Number (part) |
| Camellia oil | 52 | Oleum Perillae | 5.2 |
| Walnut oil | 18 | Vitamin E | 0.20 |
| Oleum Helianthi | 8.0 | / | / |
Embodiment 4: a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil
The form 4 Flos Camelliae Japonicae each component of Semen Juglandis mixed oil and parts by weight thereof
| Component | Number (part) | Component | Number (part) |
| Camellia oil | 50 | Oleum Perillae | 2.0 |
| Walnut oil | 22 | Vitamin E | 0.20 |
| Oleum Helianthi | 6.0 | Citric acid | 0.050 |
| Ascorbic acid | 0.080 | / | / |
Embodiment 5: a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil
The form 5 Flos Camelliae Japonicae each component of Semen Juglandis mixed oil and parts by weight thereof
| Component | Number (part) | Component | Number (part) |
| Camellia oil | 50 | Oleum Perillae | 5.0 |
| Walnut oil | 22 | Vitamin E | 0.20 |
| Oleum Helianthi | 6.0 | Citric acid | 0.35 |
| Ascorbic acid | 0.040 | / | / |
Comparative example 1: a kind of edible oil and preparation method thereof: the cold pressing in documents and essence in preparation method employing background technology
Smelting method, edible oil is the Camellia oil using the method to prepare.
Embodiment 6: the preparation method of a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil, is with the difference of embodiment 5, in step 4,
Use Burdick lamp that Flos Camelliae Japonicae pure wool oil and Semen Juglandis pure wool oil are irradiated 70min.
Embodiment 7: the preparation method of a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil, is with the difference of embodiment 6, in step 5,
Extracted the Flos Camelliae Japonicae pure wool oil accounting for total upper strata fluid 90% by tipping, residue Flos Camelliae Japonicae pure wool oil is poured into equipped with 0.1 nanometer
Micropore filtering film filter in filter remove ionized water.
Comparative example 2: the preparation method of a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil, is with the difference of embodiment 6, in step 5,
Extracted the Flos Camelliae Japonicae pure wool oil accounting for total upper strata fluid 90% by tipping, residue Flos Camelliae Japonicae pure wool oil is poured into equipped with 100 nanometers
Micropore filtering film filter in filter remove ionized water.
Embodiment 8: the preparation method of a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil, is with the difference of embodiment 7, in step 5,
Extracted the Flos Camelliae Japonicae pure wool oil accounting for total upper strata fluid 90% by tipping, residue Flos Camelliae Japonicae pure wool oil is toppled over 50ml/min flow
Enter in the filter of the micropore filtering film equipped with 0.1 nanometer, use vacuum filtration pumping to filter filtration in 1 hour and remove ionized water,
Collect upper strata fluid and be recovered in mixed oil.
Comparative example 3: the preparation method of a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil, is with the difference of embodiment 7, in step 5,
Extracted the Flos Camelliae Japonicae pure wool oil accounting for total upper strata fluid 90% by tipping, residue Flos Camelliae Japonicae pure wool oil pure wool oil is flowed with 50ml/min
Amount pours in the filter of the micropore filtering film equipped with 0.1 nanometer, and natural filtration is filtered and removed ionized water for 1 hour, collects
Upper strata fluid is also recovered in mixed oil.
Comparative example 4: the preparation method of a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil, is with the difference of embodiment 7, in step 5,
Extracted the Flos Camelliae Japonicae pure wool oil accounting for total upper strata fluid 90% by tipping, residue Flos Camelliae Japonicae pure wool oil is disposably all poured into dress
Have in the filter of micropore filtering film of 0.1 nanometer, use vacuum filtration pumping to filter filtration in 1 hour and remove ionized water, collect
Upper strata fluid is also recovered in mixed oil.
Embodiment 9: the preparation method of a kind of Flos Camelliae Japonicae Semen Juglandis mixed oil, is with the difference of embodiment 8, step 4 and
Described step 5 is carried out the most under nitrogen protection, and wherein step 4 is for closing squeezing, with 50ml3/ min nitrogen intake discharges sky
Gas, and step 5 uses and closes sucking filtration, with 50ml3/ min nitrogen intake air-out, prevents dioxygen oxidation insatiable hunger in air
And oils and fats.
Mixed oil performance characterization one, the content of vitamin E detection in regulation oil: use NY/T 1598-2008 " to eat and plant
Vitamin e ingredient and the mensuration of content in thing oil " to the mediation in embodiment 1 to embodiment 9 and comparative example 1 to comparative example 4
Oil or each pre-treatment of Camellia oil 5 groups detect the content (mg/g) of its vitamin E, and record result is as shown in table 6.
Product property characterizes two, by GB 2716 to in embodiment 1 to embodiment 9 and comparative example 1 to comparative example 4
Mixed oil or each 5 groups of Camellia oil be tracked monitoring, record its rotten time, i.e. shelf life (my god), record result is such as
Shown in form 6.
Form 6: the content of the vitamin E of mixed oil or Camellia oil and shelf life performance parameter
This specific embodiment is only explanation of the invention, and it is not limitation of the present invention, and those skilled in the art exist
As required the present embodiment can be made after reading this specification and there is no the amendment of creative contribution, but as long as in the present invention
Right in all protected by Patent Law.
Claims (10)
1. a Flos Camelliae Japonicae Semen Juglandis mixed oil, it is characterised in that described Flos Camelliae Japonicae Semen Juglandis mixed oil in parts by weight, including following group
Point: Camellia oil 45 ~ 58 parts；Walnut oil 18 ~ 26 parts；Oleum Perillae 2 ~ 8 parts；Vitamin E 0.1 ~ 0.2 part；Wherein said Fructus Perillae
The weight portion of oil is 1:10 with the ratio of the weight portion of Camellia oil.
Flos Camelliae Japonicae Semen Juglandis mixed oil the most according to claim 1, it is characterised in that in parts by weight, described Camellia oil 49 ~ 52
Part.
Flos Camelliae Japonicae Semen Juglandis mixed oil the most according to claim 1, it is characterised in that in parts by weight, described Oleum Perillae 5
Part.
Flos Camelliae Japonicae Semen Juglandis mixed oil the most according to claim 1, it is characterised in that also include Oleum Helianthi, with weight portion
Meter, described Oleum Helianthi 4 ~ 8 parts.
Flos Camelliae Japonicae Semen Juglandis mixed oil the most according to claim 4, it is characterised in that also include synergist, in parts by weight,
Described synergist is citric acid 0.05 ~ 0.35 part and 0.04 ~ 0.08 part of ascorbic acid.
6. the method preparing Flos Camelliae Japonicae Semen Juglandis mixed oil as claimed in claim 5, it is characterised in that comprise the steps:
Step 1, selection: use disintegrating machine respectively to Flos Camelliae Japonicae and walnut shell-breaking, remove rotten Camellia and Semen Juglandis, choose high-quality Flos Camelliae Japonicae
Seed and Semen Juglandis；Step 2, decortication: use containing diluted alkaline 2% deionized water in step 1 Semen Juglandis soak, decortication process 30 ~
60 min；Step 3, dries: use dehydrator that the Semen Juglandis in step 2 is dried process so that it is water content 3% ~ 5%；Step
Rapid 4, squeezing: the Semen Juglandis that Camellia step 2 obtained and step 3 obtain is respectively placed in two squeezers to squeeze and obtains
Flos Camelliae Japonicae crude oil and oil residue mixing compound and Semen Juglandis crude oil and the mixture of the dregs of fat；Add precipitant two kinds of crude oils and the dregs of fat are carried out
Centrifugal treating, removes the dregs of fat and obtains Flos Camelliae Japonicae pure wool oil and Semen Juglandis pure wool oil；Step 5, purifies: the Flos Camelliae Japonicae pure wool oil in step 4
With addition deionized water in Semen Juglandis pure wool oil, stand, be layered and remove layer of diw after stirring 30 ~ 60 min, extract upper strata
Fluid respectively obtains Camellia oil and walnut oil；Step 6, allotment: by the Camellia oil of formula ratio, walnut oil, Oleum Perillae and Wei Sheng
Element E carries out being mixed to get mixed oil.
Preparation method the most according to claim 6, it is characterised in that in described step 4, uses Burdick lamp pure to Flos Camelliae Japonicae
Crude oil and Semen Juglandis pure wool oil irradiate 60 ~ 80 min.
Preparation method the most according to claim 7, it is characterised in that in described step 5, is extracted by tipping and accounts on total
The Flos Camelliae Japonicae pure wool oil of layer fluid 85% ~ 90%, pours into residue Flos Camelliae Japonicae pure wool oil and filters equipped with in the filter of micropore filtering film
Remove ionized water.
Preparation method the most according to claim 8, it is characterised in that in described step 5, by oily for residue Flos Camelliae Japonicae pure wool by amount
Join filter and under the conditions of sucking filtration, carry out sucking filtration process.
Preparation method the most according to claim 9, it is characterised in that described step 4 and described step 5 are all protected at nitrogen
Protect down carry out.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108913339A (en) * | 2018-07-24 | 2018-11-30 | 正安县铜兴粮油有限责任公司 | A kind of beans mixing grain and oil and preparation method thereof |
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