CN102894107A - Nutritional walnut oil and production process thereof - Google Patents
Nutritional walnut oil and production process thereof Download PDFInfo
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- CN102894107A CN102894107A CN201110217121.8A CN201110217121A CN102894107A CN 102894107 A CN102894107 A CN 102894107A CN 201110217121 A CN201110217121 A CN 201110217121A CN 102894107 A CN102894107 A CN 102894107A
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Abstract
The invention discloses a nutritional walnut oil and a production process thereof. According to the Chinese dietary reference intakes, Chinese dietary guidelines and living habits and physiological characteristics of specific populations, the invention develops a series of nutrition oil products suitable for specific populations, such as pregnant women, children, students, the middle-aged and the elderly by balancing nutrition demands. The invention has reasonable formula and advanced technology; the raw materials have synergistic effect to achieve functions and effects much better than a single raw material. Compared with other types of vegetable oils, the nutritional walnut oil provided by the invention has the characteristics of high contents of oleic acid, linoleic acid and linolenic acid, and is a natural and high-quality nutritional oil with a reasonable ratio.
Description
Technical field
The present invention relates to a kind of nutrition walnut oil and production technology thereof, belong to grease processing technology field.
Background technology
Edible oil is the daily life necessity.Often fatty acid proportion is unbalanced, nutritional labeling is single for existing single variety edible oil.The nutrition that prior art is produced on the market/ready-mixed oil product mostly is greatly the first generation and second generation product, can not have satisfied people to the demand of health-nutrition ready-mixed oil.Along with improving constantly of people's living standard, revolutionary change has occured in the edible oil consumption idea, and people select the standard of edible oil no longer to rest on the aspect that meets health, safety standard, but more pays attention to health, the nutrition of edible oil.
The present invention according to the nutritive value of walnut oil, is equipped with other multiple natural function greases take walnut oil as base-material, develops serial nutritious walnut oil product for the different consumer groups and all ages and classes section crowd.
Summary of the invention
The object of the invention provides a kind of nutrition walnut oil and production technology thereof.
Technical solution of the present invention is take the aliphatic acid constituent ratio as design object, proposes saturated acid (SFA) in the meals according to " DRIs ": cholesterol acid (MUFA): polyunsaturated acid (PUFA) is 1: 1: 1; Among the PUFA, n-6 and n-3 ratio are (4-6): 1; Suggestion according to Chinese Soclety of Nutrition's " Chinese residents dietary guidelines " and nutritionist, the meals model of suitable for China is for each person every day 300-500g of cereal, the abundant food intake dose of grease is respectively: edible oil 25g, Milk and milk products 100g, beans and bean product 50-100g, animal food fish, fowl, meat, eggs 125-200g; Meet NI's proposed standard with saturated acid (SFA), cholesterol acid (MUFA), polyunsaturated acid (PUFA) three class fatty acid proportions; Satisfy consumer's essential fatty acid needs of every day, the prevention essential fatty acid lacks; Take into account local flavor, the large-scale production of product energy is sold price and is fit to ordinary consumer.
According to above-mentioned designing requirement to the nutritional oil fatty acid proportion, take walnut oil as main basic oil, cooperate camellia seed oil, refining siritch, soybean salad oil, corn oil, peanut oil, sesame oil, Purple Perilla Seed Oil, establish the basic recipe of walnut nutritious oil, on this basis, according to different specific crowds, add targetedly functional component, development pregnant woman type, child's type, students, middle-aged and old type nutrition walnut oil.
Nutrition walnut oil formula of the present invention is walnut oil 30-80 part, camellia seed oil 10-35 part, refining siritch 5-15 part, soybean salad oil 15-35 part, corn oil 5-15 part, peanut oil 5-15 part, sesame oil 5-15 part, Purple Perilla Seed Oil 5-15 part, vitamin E 0.01-0.05 part, ascorbyl palmitate 0.01-0.05 part by weight;
Also contain one or more in DHA (DHA) 0.01-0.1 part, phytosterin ester 0.1-0.5 part, medium-chain fatty glyceride MCT 2-5 part, grape pip procyanidin 0.001-0.05 part.
Every part of the present invention can be per kilogram, per ton or other legal weight measurement unit.
Nutrition walnut oil production method of the present invention is, taking by weighing feedstock oil by prescription adds in the material-compound tank, be incubated 30 ℃-40 ℃, and stirring 40-60min, taking by weighing other raw material by prescription adds in the material-compound tank after a small amount of oil is fully mixed thoroughly in the material-compound tank again, continue to stir 40-60min to even, filtration, can namely get nutrition walnut oil finished product.
Walnut oil of the present invention can for the walnut oil of art methods production, such as commercially available all kinds of walnut oil products, be selected as required.
Walnut oil of the present invention preferably adopts following technique to make: the production technology of the refining walnut oil of a kind of low-temperature cold pressing physics, and production craft step comprises:
1. select; 2. low-temperature cold pressing; 3. walnut crude oil; 4. aquation; 5. dehydration; 6. decolouring; 7. three grades of essence filters;
Describedly be picked as screening and remove the walnut kernel mesometamorphism foreign material such as Renhe irony, stone of damaging by worms;
Described low-temperature cold pressing is that walnut kernel is broken, and preferred particle size after cracking is 2～10mm, sends into the oil press low-temperature cold pressing; The oil expression temperature is preferred≤and 60 ℃; More preferably 25 ℃～50 ℃ of oil expression temperature;
Described low-temperature cold pressing preferably will add walnut shell or walnut grouts in the walnut kernel, addition is preferably 5%～20% of walnut kernel weight; Described walnut shell or the preferred particle size after cracking of walnut grouts are 2～10mm;
Described oil press is 2 screw oil expeller or vertical barrel hydraulic oil press or horizontal hydraulic oil press;
The small-sized one 2 screw oil expeller of described YJY-2: output 10-12kg/h;
Filter to get the walnut crude oil behind the low-temperature cold pressing; Described being filtered into left standstill 12～24h with walnut oil behind the low-temperature cold pressing, gets edible vegetable oil
Filter; Available pot type oil filter;
Described aquation is:
1) takes by weighing citric acid and salt, use the water-soluble solution of 2～5 times of citric acid and salt gross weights, make the citric acid salt solution, be warming up to 40 ℃～80 ℃; Citric Acid Dosage is 0.005%～0.05% of walnut crude oil weight; The salt consumption is 0.5%～2% of walnut crude oil weight;
2) the walnut crude oil is put into hydration tank, oil temperature rises to more than 30 ℃, stirs; Be preferably 30 ℃～60 ℃; The citric acid solution that heats up is slowly added in the walnut crude oil mixing speed 40～50rpm, time 5～10min;
3) when continuing stirring, will remain water and add hydration tank, stir 15～30min, mixing speed 40～50rpm; Total amount of water is walnut crude oil weight 0.5%～1.0% (0.1%～1.5%), comprises above-mentioned dissolving citric acid institute water;
4) insulation is left standstill more than 24 hours more than 30 ℃;
5) after aquation is finished, emit moisture slightly muddy top walnut oil, oil foot is emitted at the bottom of tank;
During the low-fiber oil plant of the 2 screw oil expeller processing high grease of this class of walnut kernel, easily become paste, can be according to an amount of cot or the broken cake of adding of raw material benevolence size, generally 5%～20%.Cot or broken cake that raw material benevolence granularity more broken (such as rice beans size) adds are more; Simultaneously inlet amount also will suitably be controlled, and make squeezing strip ring place oil pump capacity about 50%, and fuel-displaced more clear slag inclusion is few, and prevents from pressing in the thorax grease and expire very much too much, overflow, flow backwards, and causes pressure drop, temperature reduction.Add cot, fuel-displaced lighter color, fuel-displaced dregginess about 10% during 2 screw oil expeller processing walnut oil; Color and luster is dark when adding broken cake, and roasting fragrance is slightly heavy, dregginess 15-20%.
Described dehydration is stirred dehydration for the muddy oil in aquation upper back is put into vacuum hydration plant heating in vacuum, vacuum pressure 0.08～0.2MPa, temperature≤80 ℃; Get sample and put into test tube and do cooling test, when sample in the test tube is cooled to below 30 ℃, still keep clear namely to dewater and finish;
Described decolouring is for adding decolorizer in the walnut oil after will dewatering, and mixing heats, and vacuumizes, and stirs, and filters;
Described decolorizer is active carbon, diatomite, attapulgite; Each composition and walnut oil weight ratio are active carbon 0.1%～0.8%, diatomite 0.5%～1.5%, attapulgite 1%～4.5% in the decolorizer;
Heating-up temperature is 50～80 ℃ during described decolouring;
Evacuated pressure is 0.08～0.2MPa during described decolouring;
Speed of agitator is 20～30rpm during described decolouring;
Described three grades of essence filters for walnut oil after will decolour carry out successively vacuum filtration, diatomite filter filtration ,≤5 μ m membrane filtrations;
Described vacuum filtration vacuum pressure is 0.08～0.2MPa;
Described diatomite filter filter medium is attapulgite and diatomite, and attapulgite and diatomite arbitrary proportion mix, and are preferably attapulgite and diatomite ratio 1～5: 1～50;
Three grades of essence filters namely get the refining walnut oil of low-temperature cold pressing physics of the present invention;
Three grades of rear walnut oils of essence filter preferably add Ascorbyl Palmitate and 0.005%～0.018% vitamin E of walnut oil weight 0.005%～0.02%; The adding method adds mixing in the walnut oil again for Ascorbyl Palmitate and vitamin E being added together in an amount of warm walnut oil after the dissolving;
Through after the assay was approved, can carry out filling and package.
Described physical low-temperature cold pressing production technology of refined walnut oil through the refining table oil that forms of physical refining processes, does not have the bad accessory substance of chemistry refinement, has fully kept the nutritional labeling of walnut.
The refining walnut oil quality index of low-temperature cold pressing physics of the present invention sees Table 1 (implication of % is " w/w ").
Table 1 is made with extra care the walnut oil quality index
Ascorbyl Palmitate is a kind of nontoxic multifunctional and nutritional antioxidant fresh-keeping agent.Have anti-oxidant and nutrition reinforcing function, be used as the antioxygen brightening agent of vitamin E, antioxidant effect is very obvious in grease.And high temperature resistant, be applicable to medicine, health products, cosmetics etc., and be applicable to toast the antioxidant of frying oil.Vitamin E has oxidation resistant effect, also has the acceleration cell division, prevents cell ageing, delaying human body caducity, keep the effect in body youth, vitamin E suppresses in addition lipid peroxide and is deposited in thrombosed effect on the blood vessel, thereby but prevention of arterial is atherosis.The present invention adopts auxotype antioxidant L-ascorbic acid palmitate and vitamin E coupling, and the two Synergistic reaches best antioxidant effect, has avoided the uses such as chemical antioxidants such as TBHQ, has ensured product safety, has effectively prolonged shelf life of products.
Low-temperature cold pressing physics process for refining technology of the present invention, production technology is advanced, reasonable in design, and process is simple to operate, and is safe, failure rate is low, equipment investment is little, and oil yield is high, and energy consumption is low; Do not introduce chemical substance, pollution-free, safe and efficient; Prepared refining walnut oil oil decolorization is effective, long shelf-life, clear; Kept to greatest extent natural nutrient substance and distinctive fragrance in the walnut raw material, free from extraneous odour, the theory of the organic pollution-free food of edible natural of praising highly for present people provides a kind of new selectable consumable products.Product detects through authoritative department, and indices reaches the target level of product quality requirement.
Nutrition walnut oil of the present invention is take walnut oil fat acid proportioning as basic boom, the habits and customs of segmenting rear all kinds of specific crowd (pregnant woman, children, student, the elderly), physilogical characteristics, nutritional need etc. are carried out the refinement adjustment, and the factor of strengthening function targetedly, thereby the balanced nutritious demand that satisfies pregnant woman, children, student, the elderly that comparatively becomes more meticulous.Refining walnut oil product meets the edible oil of Chinese Soclety of Nutrition's recommendation and the reference intake of unrighted acid, is a kind of reasonable mixture ratio, the natural quality grease of high nutrition.This product is rich in the multiple nutritional components such as oleic acid, linoleic acid, leukotrienes and natural VE, meets the consumption concept of modern's nutrition, health, safety.Linoleic acid has the reduction body's cholesterol, and is hypotensive, and softening blood vessel prevents and improves the effects such as atherosclerotic; Human body is grown leukotrienes and immunological regulation has important function; Vitamin E has oxidation resistant effect, also has the acceleration cell division, prevents cell ageing, delaying human body caducity, keep the effect in body youth, vitamin E suppresses in addition lipid peroxide and is deposited in thrombosed effect on the blood vessel, thereby but prevention of arterial is atherosis.The present invention fills a prescription rationally, and technique is advanced, has synergistic function between each raw material, and functional effect is much larger than single raw material.
The serial nutritious walnut oil product of the present invention, pure good, the nutrition complement coordination of raw materials used quality, production technology is easy, and rationally product detects through authoritative department, and indices reaches the target level of product quality requirement.In process of production, guaranteed the pure quality of nutritional oil.The present invention utilizes the local resources advantage, has opened up the new way of a comprehensive deep processing and utilization of agricultural byproducts, has filled up the domestic and international market blank, and product has high nutritive value and wide market prospects.
Grease and carbohydrate, protein are listed as three large basic nutrition compositions of needed by human, have critical role in people's life and economic development.Grease not only have store with release energy, provide essential fatty acid, as the housing construction composition and have peculiar mouthfeel and improve the unique effect of food quality, and can also play the effect of saving and promoting other Nutrients Absorption, the supply of fat-soluble A, vitamin D, vitamin E, vitamin K and absorption need grease as source and medium.From chemical terms, natural oil is comprised of triglyceride saturated and that degree of unsaturation is different more than 95%, and with a small amount of miscellaneous lipid material.
Triglyceride is called for short triglycerides.It is to be formed by three fatty acid molecules and a glycerol molecule condensation.Aliphatic acid accounts for about 95% of whole triglycerides molecular weight, because aliphatic acid proportion in the triglycerides molecule is very large, so they play a leading role on the impact of the physicochemical properties of triglycerides.Say in a sense, the characteristic of grease is determined by the functional fatty acid with specific physiologically active.Will pay close attention to the nutrition of fat and aliphatic acid with the nutrition of paying close attention to edible oil.The kind of aliphatic acid is a lot, and the content of its aliphatic acid of vegetable oil of different cultivars is different, so just determined that also its nutritive value of vegetable oil of different cultivars is different.The physico-chemical property of triglycerides and function depend primarily on kind and the distribution of the fatty acid mixed that forms it, in the natural oil there are more than 800 kinds the aliphatic acid kind.In the plant grease, more with oleic acid and linoleic acid content, be palmitic acid, a-leukotrienes, laurate, stearic acid, myristic acid etc. secondly, kind and the content difference of different types of its aliphatic acid of plant resources are larger.In the terraria take palmitic acid, oleic acid and stearic acid as main; In the marine products fish oil mainly take the polyunsaturated fatty acid of growing carbochain as main.
The functional components that is present in the grease mainly comprises functional unrighted acid, phytosterol, fat-soluble vitamin such as VE, VA etc.Functional fatty acid is to refer in particular to those to derive from the human diet grease, be human nutrition and healthy essential, and some corresponding deficiency diseases of human body and the bright disease of endogenous disease, particularly advanced society such as hypertension, heart disease, cancer, diabetes etc. there is one group of aliphatic acid of positive preventive and therapeutic effect.
The composition of oil fatty acid and classification:
Topmost composition is aliphatic acid in the edible oil and fat, difference according to carbon chain lengths can be divided into aliphatic acid short chain, medium chain and LCFA, and be divided into according to the difference of its saturation degree: saturated fatty acid (saturated fatty acid, SFA), monovalence unrighted acid (monounsaturated fatty acid, MUFA), polyvalent unsaturated fatty acid (polyunsaturated fatty acids, PUFA).
Saturated fatty acid (SFA): refer to not contain in the fatty acid molecule unsatisfied chemical bond.
Unrighted acid: contain unsatisfied chemical bond in the fatty acid molecule.
Monounsaturated fatty acids (MUFA): the aliphatic acid (such as oleic acid) that contains two keys in the molecule.
Polyunsaturated fatty acid (PUFA): the aliphatic acid (such as linoleic acid, leukotrienes) that contains two and above pair keys in the molecule.In polyunsaturated fatty acid, what important biomolecule meaning was arranged is n-3 and n-6 series.
Essential fatty acid (essential fatty acid, EFA): human body can not self synthesize, and must be called essential fatty acid by the aliphatic acid of food supply, comprises two kinds of linoleic acid, alpha-linolenic acids.
Functional polyunsaturated fatty acid:
Polyvalent unsaturated fatty acid is again polyenoic acid, refers to contain two or more pairs of keys, carbon chain lengths at 18 or 18 aliphatic acid more than the carbon atom, and they are main body and the core of functional fatty acid research and development.Two keys the more, degree of unsaturation is higher, nutritive value is also higher.Along with the reach of science, some polyunsaturated fatty acid is further appreciated the effect of human body, particularly the linoleic acid in docosahexenoic acid, eicosapentenoic acid and the general vegetable oil (normal coexist with leukotrienes) etc. is the polyunsaturated fatty acid of representative, at present more and more cause people's attention, be called by the nutritionist " functional grease ".
The classification of polyunsaturated fatty acid:
Functional polyunsaturated fatty acid is divided into two large classes according to structure:
N-3 (claiming again ω-3) is polyunsaturated fatty acid:
Refer to count from fatty acid carbon chain methyl end, first pair key appears at the 3rd polyunsaturated fatty acid on the carbon atom, mainly comprises:
Alpha-linolenic acid (α-linolenic acid, α-LNA),
Eicosapentaenoic acid (eicosapentaenoic acid, EPA),
DHA (docosahexaenoic acid, DHA).
N-6 (ω-6) is polyunsaturated fatty acid:
Refer to count from fatty acid carbon chain methyl end, first pair key appears at the 6th polyunsaturated fatty acid on the carbon atom, mainly comprises:
Linoleic acid (finoleic, LA),
Gamma-Linolenic acid (γ-linolenic acid, γ-LNA),
Arachidonic acid (arachidonicacid, AA).
The physiological function of polyunsaturated fatty acid:
In the thirties, if it is found that lack in the food of animal that vegetable oil is will genesis and development bad, skin abnormality, immunity is poor even the low inferior pathology of fecundity, these phenomenons will be alleviated after replenishing vegetable oil in the food, tracing it to its cause, mainly is the effect of the linoleic acid plus linolenic acid in the vegetable oil.Linoleic acid and a-leukotrienes can only can not synthesize in vivo from external world's picked-up, therefore are called as essential fatty acid.Polyunsaturated fatty acid is not only because the linoleic acid of n-6 series and the leukotrienes of n-3 series are the indispensable essential fatty acids of human body, the more important thing is because several polyunsaturated fatty acids of being taken in metabolic conversion or the specific food resource in vivo by them play a part very important in Human Physiology.
Oleic acid:
Monovalence unrighted acid content in vegetable oil take oleic acid as representative is higher.The external up-to-date viewpoint of nutrition circle is thought: oleic acid can reduce T-CHOL and bad cholesterol in the blood.Not being both of it and polyunsaturated fatty acid maximum reducing T-CHOL, bad cholesterol simultaneously, but do not reduced useful cholesterol.Polyunsaturated fatty acid also can reduce useful cholesterol when reducing T-CHOL and bad cholesterol.Nutrition circle calls oleic acid in " safe aliphatic acid ", and the content of oleic acid how much, is the important symbol of evaluation edible oil quality.
Linoleic acid:
Linoleic acid is as the essential fatty acid that is identified the earliest and important polyunsaturated fatty acid, content in our daily edible most greases is all more than 9%, and all higher at the content of main edible vegetable oil and fat and soybean oil, cotton seed oil, walnut oil, rape seed oil, sunflower oil, peanut oil, rice bran oil, sesame wet goods edible oil and fat.Linoleic acid is the aliphatic acid of needed by human, and it is the important component that consists of the human body cell film, and is useful to retina and corticocerebral growth simultaneously.The dyslipidemias increase can cause atherosclerotic in the blood, and linoleic acid can be combined with cholesterol, can reduce the precipitation that cholesterol is combined with saturated fatty acid.So linoleic acid has the reduction body's cholesterol, and is hypotensive, softening blood vessel prevents and improves the effects such as atherosclerotic.Long-term eating can strengthen cardiovascular function, has the prevention skin disease, improves immunity of organisms, promotes the wound healing texts.
Alpha-linolenic acid:
Alpha-linolenic acid has certain content in walnut oil, soybean oil, rape seed oil, sunflower oil.For linoleic acid, the resource of alpha-linolenic acid and daily availability are very different, but have more alpha-linolenic acid resource in some algae and microorganism.Linoleic acid and a-leukotrienes can only can not synthesize in vivo from external world's picked-up, therefore are called the essential fatty acid of human body.(α-LNA) is respectively the precursor of n-6 and n-3 series fatty acid, prolongs through a series of carbochain in vivo and desaturation effect derivation generates other PUFA for linoleic acid (LA) and alpha-linolenic acid.The n-3 polyunsaturated fatty acid also can be called omega-3 polyunsaturated fatty acids (ω-3PUFA).Linolenic physiological function: eliminate new vascular disorder, comprise the reduction cholesterol levels, reduce blood pressure, reduction triglycerides, enhancing blood platelet condense; Prevent diabetic syndrome; Auxiliary for treating cancer; The prevention skin disease; Anti-ageing; The functions such as regulation of physiological functions disorder.Leukotrienes is widely used in the health food as a kind of important function factor.
The nutritive value of walnut oil:
1. the polyunsaturated fatty acid that contains 90%-95% in the walnut oil.Except supplying with a large amount of heat energy of human body, can also adjust the ratio of high and low density lipoprotein cholesterol in the human plasma, can increase the equilibrium concentration of the HDL HDL (good cholesterol) in the human body behind the edible walnut oil, to guarantee that human body is to the requirement of cholesterol.But also can reduce the concentration of low-density lipoprotein LDL (bad cholesterol) in the blood plasma, excessive to prevent cholesterol in human body.
2. the polyunsaturated fatty acid that contains in the walnut oil can be divided into omega-fatty acid (being mainly leukotrienes) and ω-6 aliphatic acid (being mainly linoleic acid).These are the aliphatic acid that human body is necessary and human body can not self synthesize again.So also be called essential fatty acid, according to world medical circle many decades studies have shown that the essential fatty acid of human body: when the ratio of the essential fatty acid content omega-fatty acid of human body and ω-6 aliphatic acid was 1: 4, various diseases was difficult to the invasion human body.And the ratio of contained essential fatty acid just in time is 1: 4 in the olive oil, and is similar with human milk.
3. contain abundant micro-squalene, Flavonoid substances and polyphenolic substance in the walnut oil, can strengthen the immunity of human body, delay senility.
4. its every hectogram also contains 0.03 to 0.36 milligram beta carotene, and the vitamin E of 1.2-43 milligram reaches the multiple liposoluble vitamins such as vitamin A, D, F, K, is the necessary nutriment of human organ.Therefore current medical circle is known as walnut oil and benefits one of healthy edible oil most.
Walnut oil and health care:
Long-term edible walnut oil can reach following effect:
1. improve digestive system function: it has the function that reduces hydrochloric acid in gastric juice, stops the diseases such as gastritis and duodenal ulcer occur;
2. protection bone: the natural in the walnut oil and ω-3 can promote bone growth, keeps bone density, reduces the skeleton bulking that causes because of free radical;
3. give protection against cancer: can prevent some canceration (breast cancer, prostate cancer, colon cancer, the cancer of the uterus): omega-fatty acid can also increase the effect of radiotherapy and chemotherapy;
4. radiation proof: often make the computer user more regard it as the good merchantable brand of health-care and skin-care;
5. mother and baby's food: in the nutritional labeling of walnut oil, the leukotrienes that human body can not synthesize, linoleic ratio are similar with breast milk, very easily absorb, and can promote growing of the neural and bone of infant, are pregnant woman's super nutritive product and fetal growth agent;
6. anti-ageing: the antioxidant that contains can be eliminated interior free yl, prevents brain aging, promotes longevity;
7. prevention cardiovascular and cerebrovascular disease: protect from many aspects cardiovascular system.
Vitamin E:
Vitamin E is the summation of tocopherol and tocotrienols.Vitamin E belongs to liposoluble vitamin.Can promote the secretion of corpus luteum hormone in the human body, have the antisterility activity, so claim again C antisterility vitamin.Vitamin E has oxidation resistant effect.Can reduce the harmful peroxide radical level of cell membrane in the human body, prevent from producing senile plaque expelling owing to the free of peroxylradicals makes Skin Cell impaired.Also have the acceleration cell division, prevent cell ageing, delaying human body caducity keeps the effect in body youth.Vitamin E suppresses the effect that lipid peroxide is deposited in shape thrombus on the blood vessel in addition, thereby but prevention of arterial is atherosis.
DHA (DHA) is commonly called as " docosapentaenoic acid ".DHA is important nutritional labeling in infant's nerve cell growth course; With the degree of being quick on the draw in the infant growth process much relations are arranged, so DHA is called as clever aliphatic acid.The fetal birth initial stage, DHA is in large quantities accumulation in human brain tissue until three years old.DHA becomes the abundantest polyunsaturated fatty acid in people's brain cell.It is the main component of brain grey matter and neuroretina, and the content of DHA in optic cell and retinal tissue is up to 40-47%, and the normal function of retinal rod light receptor is played an important role.If lack DHA, can make DHA content decrease in the retinal tissue, thereby cause eyesight and resolving power to descend.Human brain fat accounts for 60%, and wherein DHA accounts for 10% of fat.In optic nerve, retina, account for fat content more than 40%.Enough DHA absorb can cover the required nutrition of brain, increases acuity and the adaptability to changes of brains.Simultaneously, DHA also can assist more healthy nervous system of construction, causes strengthening memory and thinking, improves intelligence.
In the human body of growing up, have from the synthetic ability that is converted into DHA of the leukotrienes of taking in, thus the additional enough a leukotrienes of pregnant woman, just can produce in vivo a large amount of DHA, enter liver and the brain of fetus by placenta.But the efficient of this path for transformation is very low in fetus and infants, and the synthetic quantity of DHA is not enough to satisfy the demand of body development, so must additionally replenish from food.Can say, DHA is the essential fatty acid of children's brain growth.
DHA has obvious facilitation to the brain development of fetus, infant especially.And traditional animal DHA (being deep sea fish oil), because containing the EPA that exceeds standard, EPA suppresses infant's ontogeny, affect bone, neurodevelopment growth, the promotion sex premature, thereby pregnant woman, women breast-feeding their children, children can not eat.World Health Organization (WHO) requires DHA in the polyunsaturated fatty acid of children taking: EPA ratio is greater than 10: 1.DHA in the little algae oil of vegetalitas DHA: EPA ratio is 40: 1, substantially exceeds the requirement of the World Health Organization (WHO).It is the children DHA supplementary source of the unique approval of U.S. food and drug safety Surveillance Authority (FDA).
Phytosterol:
Phytosterol be from corn, soybean grease through physical purification and getting, have the characteristics such as be of high nutritive value, physiologically active is strong.Phytosterol can reduce by reducing cholesterol the risk of cardiovascular disease.It is widely used in the fields such as food, medicine, cosmetics, growth of animal agent and sheet processing, printing, weaving, and is particularly very general as food additives in Europe, is widely used in the food to reduce body's cholesterol.
Phytosterol has stronger antiinflammatory action to human body, has can suppress human body to effects such as the absorption of cholesterol, the katabolism of promotion cholesterol, the biochemistry of inhibition cholesterol synthesize; The heart disease that is used for prophylactic treatment coronary atherosclerosis class has obvious curative effect to treatment ulcer, Skin Squamous Cell Carcinoma, cervical carcinoma etc.; Can promote wound healing, make the muscle hyperplasia, strengthen the capillary circulation; Also can be used as the inhibitor that gall stone forms.Phytosterol has good antioxygen, can make food additives (antioxidant, nourishing additive agent); Also can be used as growth of animal agent raw material, promote growth of animal, promote animal health.
Additional phytosterol can obviously reduce T-CHOL in the blood (TC) and low-density lipoprotein (LDL) content, and do not reduce HDL (HDL) and triglyceride content, LDL/HDL ratio is reduced, and without any obvious side effect, phytosterol has adjuvant treatment effect to hyperlipidemia.Therefore, generally believe that now the phytosterol of absorption or additional capacity helps to reduce the incidence of disease of crowd's coronary heart disease.Studies have shown that, phytosterol has certain inhibitory action to generation and the development of some cancer of body, such as breast cancer, cancer of the stomach, intestinal cancer etc.
Phytosterol is a kind of blending constituent, comprising stigmasterol, sitosterol, campesterol etc.Because phytosterol is nontoxic, it is new resource food for the existing approved of China, can directly join in the food (or beverage), with the nutritive value of improving product.In recent years, more Hesperian food manufacturers have successively developed a series of health foods that contain phytosterol, comprise margarine (margarine), salad dressing, sour milk, chewing gum, biscuit, beverage and other various health foods that contain phytosterol.Behind the launch, quite be subjected to local consumer's welcome.The purposes of phytosterol maximum is the food supplement as norcholesterol, reducing blood lipid.Along with the raising of people's living standard, cardiovascular patient day by day increases, and according to World Health Organization's statistics, angiocardiopathy has become human No.1 killer.Angiocardiopathy results from cholesterol in the deposition of cardiovascular inwall, and for many years, doctors are making great efforts to allow family accept a kind of like this viewpoint always, the intake of cholesterol in the control diet, your health that will more likely often keep healthy.A large amount of scientific facts proved already, and phytosterin ester can stop stomach to the absorption of cholesterol, thereby reduced the concentration of Blood Cholesterol.Phytosterin ester is to be made by esterification by phytosterol and vegetable fatty acids.Wherein phytosterol is the mixture of cupreol, campesterol and stigmasterol, derives from the deodorization distillate of soybean oil, vegetable seed wet goods vegetable oil.This product is a kind of natural multi-functional physiological activator, and is safe, is a kind of functional food ingredient of desirable reduction cholesterol.Phytosterin ester was used as functional food ingredient by FDA (FDA) approval in 2000.FDA thinks, will take in for each person every day the above phytosterin ester of 1.3g and can reach the purpose that reduces cholesterol.
Medium-chain fatty glyceride (hot certain herbaceous plants with big flowers acid glyceride):
Medium-chain fatty glyceride is called for short MCT, is widely used in numerous food preparation and processing, is a kind of aliphatic acid that contains the sad and C10:0 certain herbaceous plants with big flowers acid of C8:0, is referred to as medium-chain fatty glyceride.
Medium-chain fatty glyceride extracts from coconut oil or in the palm-kernel oil.They are mixtures of saturated triglycerides, and main is sad (C8H16O2) and certain herbaceous plants with big flowers acid (C10H20O2), and their content is not less than 95%, be a kind of be water white transparency, free-pouring liquid.The difference of median chain triglyceride oil and long chain triglycerides maximum is its unique metabolic pathway: triglyceride is resolved into glycerine and aliphatic acid by bile and pancreatic secretion in duodenum, LCFA enter intestinal mucosa through behind the resterification with the Protein formation chylomicron, enter blood circulation by Lymphatic Circulation, excess intake can be stored in the adipose tissue; Medium chain fatty acid then directly enters liver by portal vein, and the oxidation energy supply is not stored in the adipose tissue in liver.When gall-bladder or pancreas normally when secretion of bile and pancreatic secretion, long chain triglycerides just can't absorb in metabolism, even and median chain triglyceride oil does not decompose, also can pass through intestinal mucosa access door vein, participate in normal metabolism, improve the absorption of other nutriment, such as mineral matter, essential fatty acid etc.
Medium-chain fatty glyceride can be applied in:
Baby milk powder can promote growing of infant, especially to early stage baby or underfed child.Such as the PediaSure of Abbott Laboratories, just added MCT.
Beverage and health products can satisfy the sportsman, the special population of the large or fat-reducing of physical training person's homenergic consumption.
The picked-up of medium-chain fatty glyceride (MCT) has the effect that the black alcohol of serum courage, the black alcohol of liver and gall are reduced, and because of edible higher fatty acid, that high cholesterol food causes artery sclerosis, DVT patient and obese patient, MCT can play special effect.Median chain triglyceride oil also has some superior physicochemical properties: oxidation stability, low viscosity etc.Usually utilize its stronger oxidation stability and low viscosity, diffusivity to replace beeswax and mineral oil to be used for raisins, the candy of transparent wrapper as antitack agent.The functional characteristic of medium-chain fatty glyceride has caused some experts and scholars' concern, and some research reports have been arranged, believe along with continuous popularization, therefore median chain triglyceride oil is bound to become another focus in the functional food additives, and the health-product market of China also can be and more flourishing.
Compared with common vegetable oil, the molecular weight of MCT is lower, and smoke point about about 160 degrees centigrade, therefore may be used for baking or frying greatly hardly.In the active batching of the pH value food larger than low moisture or lipase, all oils all is hydrolyzed into free fatty and glycerine.The aliphatic acid of long-chain does not exert an influence to food without any taste.
Grape pip procyanidin:
Grape pip procyanidin is the new and effective natural material that can not synthesize in a kind of human body that extracts from grape pip.It is anti-oxidant, the strongest material of removing free radical ability that present occurring in nature is found, its antioxidation activity is 50 times, ascorbic 20 times of the plain E of dimension, it can effectively remove unnecessary free radical in the human body, has the superpower effect that delays senility and strengthen immunity.Anti-oxidant, antiallergy, antifatigue are built up health, are improved sub-health state and delay senility, improve the symptoms such as irritated irritability, dizzy weak, failure of memory.
1. OPC is a kind of new and effective antioxidant, is that the most potent free radical scavenger of finding is so far given one's regards, and has very strong activity in vivo, and absorbs rapidly fully.The dazzled ability of Green Tea Extract that experiment showed, OPC is 50 times of vitamin E, ascorbic 20 times.And absorb rapidly fully, can reach the highest haemoconcentration in oral 20 minutes, metabolic half life is for 7 hours.2. can reduce the initiation potential of the illnesss such as heart disease, cancer, early ageing, arthritis.3. strengthen the vascular wall resistance.4. reduce the initiation potential of diabetes.5. strengthen skin elasticity and soft and smooth property, the prevention sunray is to the effects such as radiation injury of skin.
In sum, auxotype walnut oil of the present invention and other various plants oil phase ratios have the characteristics of high oleic acid, high linoleic acid, high linolenic content, are a kind of reasonable mixture ratio, the natural high-quality grease of high nutrition.
The specific embodiment
The following examples help the present invention of those skilled in the art's comprehend, but do not limit the present invention in any way.
Embodiment 1
Take by weighing respectively in walnut oil 30kg, camellia seed oil 10kg, refining siritch 5kg, soybean salad oil 35kg, corn oil 5kg, peanut oil 15kg, sesame oil 5kg, the Purple Perilla Seed Oil 5kg adding material-compound tank, be incubated 30 ℃-35 ℃, and stirring 40-60min, take by weighing respectively vitamin E 0.01kg, ascorbyl palmitate 0.02kg, after a small amount of oil is fully mixed thoroughly in the material-compound tank, add again in the material-compound tank, continue to stir 40-60min to even, filtration, can namely get the nutrition walnut oil.
Preferably, above-mentioned nutrition walnut oil also contains DHA 0.01kg, phytosterin ester 0.1kg, medium-chain fatty glyceride MCT2kg, grape pip procyanidin 0.001kg; Namely taking by weighing feedstock oil by above-mentioned prescription adds in the material-compound tank, be incubated 30 ℃-35 ℃, and stirring 40-60min, take by weighing respectively vitamin E, ascorbyl palmitate, DHA, phytosterin ester, medium-chain fatty glyceride MCT, grape pip procyanidin by above-mentioned prescription, after a small amount of oil is fully mixed thoroughly in the material-compound tank, add again in the material-compound tank, continue to stir 40-60min to even, filtration, can namely get preferred nutrition walnut oil.
Embodiment 2
Take by weighing respectively in walnut oil 80kg, camellia seed oil 30kg, refining siritch 15kg, soybean salad oil 15kg, corn oil 15kg, peanut oil 5kg, sesame oil 10kg, the Purple Perilla Seed Oil 15kg adding material-compound tank, be incubated 30 ℃-35 ℃, and stirring 40-60min, take by weighing respectively vitamin E 0.05kg, ascorbyl palmitate 0.05kg, after a small amount of oil is fully mixed thoroughly in the material-compound tank, add again in the material-compound tank, continue to stir 40-60min to even, filtration, can namely get the nutrition walnut oil.
Preferably, above-mentioned nutrition walnut oil also contains DHA 0.1kg, phytosterin ester 0.5kg, medium-chain fatty glyceride MCT5kg, grape pip procyanidin 0.05kg; Namely taking by weighing feedstock oil by above-mentioned prescription adds in the material-compound tank, be incubated 30 ℃-35 ℃, and stirring 40-60min, take by weighing respectively vitamin E, ascorbyl palmitate, DHA, phytosterin ester, medium-chain fatty glyceride MCT, grape pip procyanidin by above-mentioned prescription, after a small amount of oil is fully mixed thoroughly in the material-compound tank, add again in the material-compound tank, continue to stir 40-60min to even, filtration, can namely get preferred nutrition walnut oil.
Embodiment 3
Take by weighing respectively in walnut oil 60kg, camellia seed oil 35kg, refining siritch 10kg, soybean salad oil 20kg, corn oil 10kg, peanut oil 10kg, sesame oil 10kg, the Purple Perilla Seed Oil 10kg adding material-compound tank, be incubated 30 ℃-35 ℃, and stirring 40-60min, take by weighing respectively vitamin E 0.03kg, ascorbyl palmitate 0.02kg, after a small amount of oil is fully mixed thoroughly in the material-compound tank, add again in the material-compound tank, continue to stir 40-60min to even, filtration, can namely get the nutrition walnut oil.
Preferably, above-mentioned nutrition walnut oil also contains medium-chain fatty glyceride MCT 5kg, grape pip procyanidin 0.05kg; Namely taking by weighing feedstock oil by above-mentioned prescription adds in the material-compound tank, be incubated 30 ℃-35 ℃, and stirring 40-60min, take by weighing respectively vitamin E, ascorbyl palmitate, medium-chain fatty glyceride MCT, grape pip procyanidin by above-mentioned prescription, after a small amount of oil is fully mixed thoroughly in the material-compound tank, add again in the material-compound tank, continue to stir 40-60min to even, filtration, can namely get preferred nutrition walnut oil.
Embodiment 4
Take by weighing respectively in walnut oil 50kg, camellia seed oil 10kg, refining siritch 5kg, soybean salad oil 18kg, corn oil 8kg, peanut oil 7kg, sesame oil 6kg, the Purple Perilla Seed Oil 11kg adding material-compound tank, be incubated 30 ℃-35 ℃, and stirring 40-60min, take by weighing respectively vitamin E 0.04kg, ascorbyl palmitate 0.01kg, after a small amount of oil is fully mixed thoroughly in the material-compound tank, add again in the material-compound tank, continue to stir 40-60min to even, filtration, can namely get the nutrition walnut oil.
Preferably, above-mentioned nutrition walnut oil also contain DHA 0.02kg, phytosterin ester 0.3kg; Namely taking by weighing feedstock oil by above-mentioned prescription adds in the material-compound tank, be incubated 30 ℃-35 ℃, and stirring 40-60min, take by weighing respectively vitamin E, ascorbyl palmitate, DHA, phytosterin ester by above-mentioned prescription, after a small amount of oil is fully mixed thoroughly in the material-compound tank, add again in the material-compound tank, continue to stir 40-60min to even, filtration, can namely get preferred nutrition walnut oil.
Embodiment 5
Take by weighing respectively in walnut oil 75kg, camellia seed oil 17kg, refining siritch 7kg, soybean salad oil 21kg, corn oil 5.5kg, peanut oil 7kg, sesame oil 8kg, the Purple Perilla Seed Oil 13kg adding material-compound tank, be incubated 30 ℃-35 ℃, and stirring 40-60min, take by weighing respectively vitamin E 0.04kg, ascorbyl palmitate 0.01kg, after a small amount of oil is fully mixed thoroughly in the material-compound tank, add again in the material-compound tank, continue to stir 40-60min to even, filtration, can namely get the nutrition walnut oil.
Preferably, above-mentioned nutrition walnut oil also contains DHA 0.03kg, grape pip procyanidin 0.001kg; Namely taking by weighing feedstock oil by above-mentioned prescription adds in the material-compound tank, be incubated 30 ℃-35 ℃, and stirring 40-60min, take by weighing respectively vitamin E, ascorbyl palmitate, DHA, grape pip procyanidin by above-mentioned prescription, after a small amount of oil is fully mixed thoroughly in the material-compound tank, add again in the material-compound tank, continue to stir 40-60min to even, filtration, can namely get preferred nutrition walnut oil.
Embodiment 6
Nutrition walnut oil formula and production technology are with embodiment 1.
Described raw material walnut oil is the refining walnut oil of low-temperature cold pressing physics, and its production technology technique is as follows:
1. select; The walnut kernel mesometamorphism foreign material such as Renhe irony, stone of damaging by worms are removed in screening;
2. low-temperature cold pressing; Walnut kernel is broken, and particle size after cracking is 3～8mm, sends into the oil press low-temperature cold pressing; More preferably 45 ℃～50 ℃ of oil expression temperature; Low-temperature cold pressing will add walnut shell or walnut grouts in the walnut kernel, addition is 5% of walnut kernel weight; Described walnut shell or the preferred particle size after cracking of walnut grouts are 3～8mm; Described oil press is the small-sized one 2 screw oil expeller of YJY-2, output 10-12kg/h;
3. walnut crude oil; Filter to get the walnut crude oil behind the low-temperature cold pressing; Described being filtered into left standstill 12h with walnut oil behind the low-temperature cold pressing, gets edible vegetable oil and filters; Use the pot type oil filter;
4. aquation;
1) takes by weighing citric acid and salt, use the water-soluble solution of 2 times of citric acid and salt gross weights, make the citric acid salt solution, be warming up to 40 ℃; Citric Acid Dosage is 0.02% of walnut crude oil weight; The salt consumption is 0.5% of walnut crude oil weight;
2) the walnut crude oil is put into hydration tank, oil temperature rises to more than 30 ℃, stirs; The citric acid solution that heats up is slowly added in the walnut crude oil mixing speed 40rpm, time 10min;
3) when continuing stirring, will remain water and add hydration tank, stir 25～30min, mixing speed 40～45rpm; Total amount of water is walnut crude oil weight 1.0%, comprises above-mentioned dissolving citric acid institute water;
4) insulation is left standstill more than 24 hours more than 30 ℃;
5) after aquation is finished, emit moisture slightly muddy top walnut oil, oil foot is emitted at the bottom of tank;
5. dehydration; The muddy oil in aquation upper back is put into vacuum hydration plant heating in vacuum stir dehydration, vacuum pressure 0.1MPa, temperature≤60 ℃; Get sample and put into test tube and do cooling test, when sample in the test tube is cooled to below 30 ℃, still keep clear namely to dewater and finish;
6. decolouring; Add decolorizer in the walnut oil after will dewatering, mixing, heating vacuumizes, and stirs, and filters;
Described decolorizer is active carbon, diatomite, attapulgite; Each composition and walnut oil weight ratio are active carbon 0.1%, diatomite 1.5%, attapulgite 1%% in the decolorizer; Heating-up temperature is 50 ℃ during described decolouring;
Evacuated pressure is 0.1MPa during described decolouring; Speed of agitator is 20rpm during described decolouring;
7. three grades of essence filters;
Described three grades of essence filters for walnut oil after will decolour carry out successively vacuum filtration, diatomite filter filtration ,≤5 μ m membrane filtrations;
Described vacuum filtration vacuum pressure is 0.08MPa; Described diatomite filter filter medium is attapulgite and diatomite, and attapulgite and diatomite arbitrary proportion mix,
Three grades of essence filters namely get the refining walnut oil of low-temperature cold pressing physics of the present invention;
Three grades of rear walnut oils of essence filter add Ascorbyl Palmitate and 0.010% vitamin E of walnut oil weight 0.01%; The adding method adds mixing in the walnut oil again for walnut oil weight Ascorbyl Palmitate and vitamin E being added together in an amount of warm 30 ℃ of walnut oils after the dissolving;
Through after the assay was approved, can carry out filling and package.
Embodiment 7
Nutrition walnut oil formula and production technology are with embodiment 2.
Described raw material walnut oil is the refining walnut oil of low-temperature cold pressing physics, and its production technology technique is as follows:
1. select; The walnut kernel mesometamorphism foreign material such as Renhe irony, stone of damaging by worms are removed in screening;
2. low-temperature cold pressing; Walnut kernel is broken, and particle size after cracking is 3～8mm, sends into the oil press low-temperature cold pressing; More preferably 45 ℃～50 ℃ of oil expression temperature; Low-temperature cold pressing will add walnut shell or walnut grouts in the walnut kernel, addition is 5% of walnut kernel weight; Described walnut shell or the preferred particle size after cracking of walnut grouts are 3～8mm;
Described oil press is the vertical barrel hydraulic oil press;
3. walnut crude oil; Filter to get the walnut crude oil behind the low-temperature cold pressing; Described being filtered into left standstill 18h with walnut oil behind the low-temperature cold pressing,
Getting edible vegetable oil filters; Use the pot type oil filter;
4. aquation;
1) takes by weighing citric acid and salt, use the water-soluble solution of 5 times of citric acid and salt gross weights, make the citric acid salt solution, be warming up to 80 ℃; Citric Acid Dosage is 0.05% of walnut crude oil weight; The salt consumption is 2% of walnut crude oil weight;
2) the walnut crude oil is put into hydration tank, oil temperature rises to 60 ℃; The citric acid solution that heats up is slowly added in the walnut crude oil mixing speed 50rpm, time 5min;
3) when continuing stirring, will remain water and add hydration tank, stir 20～25min, mixing speed 45～50rpm; Total amount of water is walnut crude oil weight 1.5%, comprises above-mentioned dissolving citric acid institute water;
4) insulation is left standstill more than 60 hours more than 60 ℃;
5) after aquation is finished, emit moisture slightly muddy top walnut oil, oil foot is emitted at the bottom of tank;
Take by weighing citric acid by walnut filtered crude oil total amount.Salt?
5. dehydration; The muddy oil in aquation upper back is put into vacuum hydration plant heating in vacuum stir dehydration, vacuum pressure 0.08MPa, 80 ℃ of temperature; Get sample and put into test tube and do cooling test, when sample in the test tube is cooled to below 30 ℃, still keep clear namely to dewater and finish;
6. decolouring; Add decolorizer in the walnut oil after will dewatering, mixing, heating vacuumizes, and stirs, and filters;
Described decolorizer is active carbon, diatomite, attapulgite; Each composition and walnut oil weight ratio are active carbon 0.8%, diatomite 0.5%, attapulgite 3.5% in the decolorizer; Heating-up temperature is 80 ℃ during described decolouring;
Evacuated pressure is 0.08MPa during described decolouring; Speed of agitator is 30rpm during described decolouring;
7. three grades of essence filters;
Described three grades of essence filters for walnut oil after will decolour carry out successively vacuum filtration, diatomite filter filtration ,≤5 μ m membrane filtrations;
Described vacuum filtration vacuum pressure is 0.2MPa; Described diatomite filter filter medium is attapulgite and diatomite, attapulgite and diatomite mixed proportion 1: 1;
Three grades of essence filters namely get the refining walnut oil of low-temperature cold pressing physics of the present invention;
Three grades of rear walnut oils of essence filter add Ascorbyl Palmitate and 0.018% vitamin E of walnut oil weight 0.005%; The adding method adds mixing in the walnut oil again for Ascorbyl Palmitate and vitamin E being added together in an amount of warm 35 ℃ of walnut oils after the dissolving;
Through after the assay was approved, can carry out filling and package.
Embodiment 8
Nutrition walnut oil formula and production technology are with embodiment 3.
Described raw material walnut oil is the refining walnut oil of low-temperature cold pressing physics, and its production technology technique is as follows:
1. select; The walnut kernel mesometamorphism foreign material such as Renhe irony, stone of damaging by worms are removed in screening;
2. low-temperature cold pressing; Walnut kernel is broken, and particle size after cracking is 5～10mm, sends into the oil press low-temperature cold pressing; The oil expression temperature is preferred≤and 60 ℃; More preferably 35 ℃～45 ℃ of oil expression temperature; Described oil press is the horizontal hydraulic oil press;
3. walnut crude oil; Filter to get the walnut crude oil behind the low-temperature cold pressing; Described being filtered into left standstill 24h with walnut oil behind the low-temperature cold pressing, gets edible vegetable oil and filters; Use the pot type oil filter;
4. aquation;
1) takes by weighing citric acid and salt, use the water-soluble solution of 3 times of citric acid and salt gross weights, make the citric acid salt solution, be warming up to 60 ℃; Citric Acid Dosage is 0.005% of walnut crude oil weight; The salt consumption is 1% of walnut crude oil weight;
2) the walnut crude oil is put into hydration tank, oil temperature rises to 30 ℃; The citric acid solution that heats up is slowly added in the walnut crude oil mixing speed 45rpm, time 8min;
3) when continuing stirring, will remain water and add hydration tank, stir 15～20min, mixing speed 40～45rpm; Total amount of water is walnut crude oil weight 0.1%, comprises above-mentioned dissolving citric acid institute water;
4) insulation is about 30 ℃, leaves standstill more than 48 hours;
5) after aquation is finished, emit moisture slightly muddy top walnut oil, oil foot is emitted at the bottom of tank;
5. dehydration; The muddy oil in aquation upper back is put into vacuum hydration plant heating in vacuum stir dehydration, vacuum pressure 0.2MPa, 40 ℃ of temperature; Get sample and put into test tube and do cooling test, when sample in the test tube is cooled to below 30 ℃, still keep clear namely to dewater and finish;
6. decolouring; Add decolorizer in the walnut oil after will dewatering, mixing, heating vacuumizes, and stirs, and filters;
Described decolorizer is active carbon, diatomite, attapulgite; Each composition and walnut oil weight ratio are active carbon 0.4%, diatomite 1.0%, attapulgite 4.0% in the decolorizer; Heating-up temperature is 60 ℃ during described decolouring;
Evacuated pressure is 0.2MPa during described decolouring; Speed of agitator is 25～30rpm during described decolouring;
7. three grades of essence filters;
Described three grades of essence filters for walnut oil after will decolour carry out successively vacuum filtration, diatomite filter filtration ,≤5 μ m membrane filtrations;
Described vacuum filtration vacuum pressure is 0.1MPa; Described diatomite filter filter medium is attapulgite and diatomite, attapulgite and diatomite mixed proportion 1: 50;
Three grades of essence filters namely get the refining walnut oil of low-temperature cold pressing physics of the present invention;
Three grades of rear walnut oils of essence filter add Ascorbyl Palmitate and 0.005% vitamin E of walnut oil weight 0.02%; The adding method adds mixing in the walnut oil again for Ascorbyl Palmitate and vitamin E being added together in an amount of warm 40 ℃ of walnut oils after the dissolving;
Through after the assay was approved, can carry out filling and package.
Embodiment 9
Nutrition walnut oil formula and production technology are with embodiment 4.
Described raw material walnut oil is the refining walnut oil of low-temperature cold pressing physics, and its production technology technique is as follows:
1. select; The walnut kernel mesometamorphism foreign material such as Renhe irony, stone of damaging by worms are removed in screening;
2. low-temperature cold pressing; Walnut kernel is broken, and particle size after cracking is 2～8mm, sends into the oil press low-temperature cold pressing; More preferably 25 ℃～30 ℃ of oil expression temperature; Described oil press is the small-sized one 2 screw oil expeller of YJY-2, output 10-12kg/h;
3. walnut crude oil; Filter to get the walnut crude oil behind the low-temperature cold pressing; Described being filtered into left standstill 12h with walnut oil behind the low-temperature cold pressing, gets edible vegetable oil and filters; Use the pot type oil filter;
4. aquation;
1) takes by weighing citric acid and salt, use the water-soluble solution of 2 times of citric acid and salt gross weights, make the citric acid salt solution, be warming up to 40 ℃; Citric Acid Dosage is 0.02% of walnut crude oil weight; The salt consumption is 0.5% of walnut crude oil weight;
2) the walnut crude oil is put into hydration tank, oil temperature rises to more than 30 ℃, stirs; The citric acid solution that heats up is slowly added in the walnut crude oil mixing speed 40rpm, time 10min;
3) when continuing stirring, will remain water and add hydration tank, stir 25～30min, mixing speed 40～45rpm; Total amount of water is walnut crude oil weight 1.0%, comprises above-mentioned dissolving citric acid institute water;
4) insulation is left standstill more than 24 hours more than 30 ℃;
5) after aquation is finished, emit moisture slightly muddy top walnut oil, oil foot is emitted at the bottom of tank;
5. dehydration; The muddy oil in aquation upper back is put into vacuum hydration plant heating in vacuum stir dehydration, vacuum pressure 0.2MPa, 40 ℃ of temperature; Get sample and put into test tube and do cooling test, when sample in the test tube is cooled to below 30 ℃, still keep clear namely to dewater and finish;
6. decolouring; Add decolorizer in the walnut oil after will dewatering, mixing, heating vacuumizes, and stirs, and filters;
Described decolorizer is active carbon, diatomite, attapulgite; Each composition and walnut oil weight ratio are active carbon 0.6%, diatomite 0.8%, attapulgite 4.5% in the decolorizer; Heating-up temperature is 50～80 ℃ during described decolouring;
Evacuated pressure is 0.15MPa during described decolouring; Speed of agitator is 25rpm during described decolouring;
7. three grades of essence filters;
Described three grades of essence filters for walnut oil after will decolour carry out successively vacuum filtration, diatomite filter filtration ,≤5 μ m membrane filtrations;
Described vacuum filtration vacuum pressure is 0.2MPa; Described diatomite filter filter medium is attapulgite and diatomite, attapulgite and diatomite mixed proportion 1: 1;
Three grades of essence filters namely get the refining walnut oil of low-temperature cold pressing physics of the present invention;
Three grades of rear walnut oils of essence filter add Ascorbyl Palmitate and 0.018% vitamin E of walnut oil weight 0.005%; The adding method adds mixing in the walnut oil again for Ascorbyl Palmitate and vitamin E being added together in an amount of warm 35 ℃ of walnut oils after the dissolving;
Through after the assay was approved, can carry out filling and package.
Claims (9)
1. nutrition walnut oil, it is characterized in that, prescription is walnut oil 30-80 part, camellia seed oil 10-35 part, refining siritch 5-15 part, soybean salad oil 15-35 part, corn oil 5-15 part, peanut oil 5-15 part, sesame oil 5-15 part, Purple Perilla Seed Oil 5-15 part, vitamin E 0.01-0.05 part, ascorbyl palmitate 0.01-0.05 part by weight.
2. a kind of nutrition walnut oil according to claim 1, it is characterized in that, also contain one or more in DHA (DHA) 0.01-0.1 part, phytosterin ester 0.1-0.5 part, medium-chain fatty glyceride MCT 2-5 part, grape pip procyanidin 0.001-0.05 part.
3. nutrition walnut oil according to claim 1 and 2, it is characterized in that, production method is, taking by weighing feedstock oil by prescription adds in the material-compound tank, be incubated 30 ℃-40 ℃, and stir 40-60min, take by weighing other raw material by prescription and after a small amount of oil is fully mixed thoroughly in the material-compound tank, add again in the material-compound tank, continue to stir 40-60min to even, filtration, can get product.
4. nutrition walnut oil according to claim 1 and 2 is characterized in that, described walnut oil adopts following technique to make:
1. select; 2. low-temperature cold pressing; 3. walnut crude oil; 4. aquation; 5. dehydration; 6. decolouring; 7. three grades of essence filters;
Described low-temperature cold pressing is that walnut kernel is broken, sends into the oil press low-temperature cold pressing; The oil expression temperature is preferred≤and 60 ℃;
Described aquation is:
1) takes by weighing citric acid and salt, use the water-soluble solution of 2～5 times of citric acid and salt gross weights, make the citric acid salt solution, be warming up to 40 ℃～80 ℃; Citric Acid Dosage is 0.02% (0.005%～0.05%) of walnut crude oil weight; The salt consumption is 0.5%～2% of walnut crude oil weight;
2) the walnut crude oil is put into hydration tank, oil temperature rises to more than 30 ℃, stirs; Be preferably 30 ℃～60 ℃; The citric acid solution that heats up is slowly added in the walnut crude oil mixing speed 40～50rpm, time 5～10min;
3) when continuing stirring, will remain water and add hydration tank, stir 15～30min, mixing speed 40～50rpm; Total amount of water is walnut crude oil weight 0.5%～1.0% (0.1%～1.5%), comprises above-mentioned dissolving citric acid institute water;
4) insulation is left standstill more than 24 hours more than 30 ℃;
5) after aquation is finished, emit moisture slightly muddy top walnut oil, oil foot is emitted at the bottom of tank;
Described dehydration is stirred dehydration for the muddy oil in aquation upper back is put into vacuum hydration plant heating in vacuum, vacuum pressure 0.08～0.2MPa, temperature≤80 ℃; Get sample and put into test tube and do cooling test, when sample in the test tube is cooled to below 30 ℃, still keep clear namely to dewater and finish.
5. described nutrition walnut oil according to claim 4 is characterized in that, described walnut kernel particle size after cracking is 2～10mm, 25 ℃～50 ℃ of oil expression temperature.
6. described nutrition walnut oil according to claim 4 is characterized in that, described low-temperature cold pressing preferably will add walnut shell or walnut grouts in the walnut kernel, and addition is 5%～20% of walnut kernel weight; Described walnut shell or walnut grouts particle size after cracking are 2～10mm.
7. described nutrition walnut oil according to claim 4 is characterized in that, described decolouring is for adding decolorizer in the walnut oil after will dewater, mixing, and heating vacuumizes, and stirs filtration;
Described decolorizer is active carbon, diatomite, attapulgite; Each composition and walnut oil weight ratio are active carbon 0.1%～0.8%, diatomite 0.5%～1.5%, attapulgite 1%～4.5% in the decolorizer;
Heating-up temperature is 50～80 ℃ during described decolouring; Evacuated pressure is 0.08～0.2MPa during described decolouring; Speed of agitator is 20～30rpm during described decolouring.
8. described nutrition walnut oil according to claim 4 is characterized in that, described three grades of essence filters for walnut oil after will decolour carry out successively vacuum filtration, diatomite filter filtration ,≤5 μ m membrane filtrations;
Described vacuum filtration vacuum pressure is 0.08～0.2MPa;
Described diatomite filter filter medium is attapulgite and diatomite, and attapulgite and diatomite arbitrary proportion mix, and are preferably attapulgite and diatomite ratio 1～5: 1～50; Three grades of essence filters namely get the refining walnut oil of low-temperature cold pressing physics of the present invention.
9. described nutrition walnut oil according to claim 4 is characterized in that, walnut oils add Ascorbyl Palmitate and 0.005%～0.018% vitamin Es of walnut oil weight 0.005%～0.02% after three grades of essence filters; The adding method adds mixing in the walnut oil again for after will adding together in the walnut oil dissolving with vitamin E; Through after the assay was approved, can carry out filling and package.
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| CN104543047A (en) * | 2015-02-09 | 2015-04-29 | 陕西大统投资股份有限公司 | Preservation method of cold-squeezed walnut oil |
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| CN105901169A (en) * | 2016-04-15 | 2016-08-31 | 安徽华安食品有限公司 | Soybean oil nourishing and invigorating the brain and a preparing method thereof |
| CN106172886A (en) * | 2016-07-19 | 2016-12-07 | 杭州雪梨花食品有限公司 | Flos Camelliae Japonicae Semen Juglandis mixed oil and preparation method thereof |
| CN107198248A (en) * | 2017-06-06 | 2017-09-26 | 四川阿尔康生物工程有限责任公司 | A kind of plant oil composition of antiatherosclerosis |
| CN107535619A (en) * | 2017-08-27 | 2018-01-05 | 湖北古月香粮油科技有限公司 | Stone mill walnut formula oil |
| CN112674178A (en) * | 2020-12-01 | 2021-04-20 | 武汉轻工大学 | Preparation method of walnut direct drinking oil |
| CN112715685A (en) * | 2020-12-30 | 2021-04-30 | 广州市国味油脂食品有限公司 | Vegetable blend oil suitable for pregnant women and lying-in women |
| CN112715684A (en) * | 2020-12-30 | 2021-04-30 | 广州市国味油脂食品有限公司 | Special blend oil for students |
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