CN106167951A - A kind of production technology of rabbit floss Rachael blanket - Google Patents
A kind of production technology of rabbit floss Rachael blanket Download PDFInfo
- Publication number
- CN106167951A CN106167951A CN201610693613.7A CN201610693613A CN106167951A CN 106167951 A CN106167951 A CN 106167951A CN 201610693613 A CN201610693613 A CN 201610693613A CN 106167951 A CN106167951 A CN 106167951A
- Authority
- CN
- China
- Prior art keywords
- rachael blanket
- rabbit
- floss
- rabbit floss
- finished product
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
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Classifications
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- D04B—KNITTING
- D04B21/00—Warp knitting processes for the production of fabrics or articles not dependent on the use of particular machines; Fabrics or articles defined by such processes
- D04B21/02—Pile fabrics or articles having similar surface features
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- A—HUMAN NECESSITIES
- A47—FURNITURE; DOMESTIC ARTICLES OR APPLIANCES; COFFEE MILLS; SPICE MILLS; SUCTION CLEANERS IN GENERAL
- A47G—HOUSEHOLD OR TABLE EQUIPMENT
- A47G9/00—Bed-covers; Counterpanes; Travelling rugs; Sleeping rugs; Sleeping bags; Pillows
- A47G9/02—Bed linen; Blankets; Counterpanes
- A47G9/0207—Blankets; Duvets
- A47G9/0223—Blankets
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
- D06B3/10—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C11/00—Teasing, napping or otherwise roughening or raising pile of textile fabrics
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C13/00—Shearing, clipping or cropping surfaces of textile fabrics; Pile cutting; Trimming seamed edges
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06C15/00—Calendering, pressing, ironing, glossing or glazing textile fabrics
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C7/00—Heating or cooling textile fabrics
- D06C7/02—Setting
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
- D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06M11/51—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof
- D06M11/55—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof with sulfur trioxide; with sulfuric acid or thiosulfuric acid or their salts
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
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- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
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Abstract
The present invention relates to woollen blanket preparation field, disclose the production method of a kind of rabbit floss Rachael blanket, including: 1), weaving: to plush yarn and wire gauze successively warping, weave, cut open floss, prepare rabbit floss Rachael blanket semi-finished product；2), prefinishing: by fabric sizing, bristle, hot light, clot；3), dyeing and finishing: by textile dyeing, then to its reduction cleaning, be then passed through acetum and neutralize, wash out cylinder, drying, steaming and color fixing, flexible smooth process, the most again dry；4), Final finishing: fabric drying sizing, front hot light, front bristle, front are scalded cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side scald cut, cutting stitching；5), product inspection, packaging warehouse-in.The rabbit floss Rachael blanket fine hair of the present invention is submissive, stand upright, good springiness, fabric skin-friendly, moisture absorption and desorption property, good permeability, and has the feature of antibiotic health care, environmental protection.
Description
Technical field
The invention belongs to woollen blanket preparation field, particularly relate to that a kind of fine hair color and luster is good, submissive, stand upright, good springiness, fabric parent
Skin, moisture absorption and desorption property, the advantage of good permeability and antibiotic health care, the production work of rabbit floss Rachael blanket of environmental protection
Skill.
Background technology
Along with the raising of people's material and culture level, the requirement of textile is also being improved, is not requiring nothing more than warming, beautiful by people
See, and more focus on comfortableness and functional.Functional textile becomes one of following developing trend of textile industry, will be with
Fine count fiber textile, non-woven fabrics, composite, ep-type material etc. collectively form the big tendency of following textile.Section now
The exploitation developing into functional textile of skill provides guarantee, the most also for textile enterprise's development and product restructuring, rises
To bigger facilitation the added value that improves textile.Study and produce the ecological and healthy function that is beneficial to man
Property textile product, have become as the world today development trend.
In general, the functionalization of textile is mainly realized by two approach: one is the functional treatment by fabric
Realizing, this is also the main path of current functional textile exploitation；Two is the functionalization of textile fabric.Along with science and technology
Development and the gradually enhancing of people's environmental protection consciousness, the limitation of fabric functional Final finishing processing method is increasingly subject to people
Concern, do not only exist the durability of function, the comfortableness of use and safety by the method functional product of obtaining of processing
Defect in terms of property, and inevitable to environment in arranging the course of processing.Merit is processed by functional fiber
Energy property textile then can overcome many drawbacks of fabric functional Final finishing, is the development trend obtaining functional textile.
Hosiery industry, under the leading of new and high technology, is actively adjusted the product mix, and payes attention to new raw material and the exploitation of new product,
Particularly fibre in differentiation and the exploitation of functional fiber kind, greatly promote the development of hosiery industry.At Rachael blanket
Field, along with exploitation and utilization and the progress of technology of novel material, the most constantly widens its product scope.Except conventional
Outside Rachael blanket, develop high in technological content Rachael blanket and become an important developing direction.The each big authority in the world spins
The research of loom structure shows, the development trend in textile product field is to pursue comfortableization and multifunction.
Present consumer does not require nothing more than Rachael blanket and has warmth retention property, has that matte is plentiful, soft comfortable, plain height
Expensive, slim and graceful feel style and fabric good permeability, moisture absorption and desorption property are good, and have antibiotic health care, green ring to woollen blanket
The multifunctionalities such as guarantor have had demand.But on market, Rachael blanket, typically based on acrylon and terylene woollen blanket, also has at home
Least a portion of cotton and Pilus Caprae seu Ovis Rachael blanket, quality scale is relatively low or expensive, it is impossible to meets the market demand, therefore develops
Disclosure satisfy that the Rachael blanket of consumer demand becomes a kind of trend.
Summary of the invention
It is an object of the invention to carry to solve existing Rachael blanket quality scale defect relatively low, expensive
For a kind of fine hair color and luster is good, submissive, stand upright, good springiness, fabric skin-friendly, moisture absorption and desorption property, the advantage of good permeability and anti-
Bacterium keeps healthy, the production technology of the rabbit floss Rachael blanket of environmental protection.
To achieve these goals, the present invention is by the following technical solutions:
The production technology of a kind of rabbit floss Rachael blanket, is plied to yarn using rabbit hair and special fibre former as plush yarn
Material, using polyester drawn yarns as wire gauze raw material, comprises the following steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare rabbit floss Rachael blanket
Semi-finished product；
2), prefinishing: carry out described rabbit floss Rachael blanket semi-finished product shaping, bristle, hot light, clot；
3), dyeing and finishing: the rabbit floss Rachael blanket semi-finished product after prefinishing are positioned in dyeing liquor and dye, then with reduction
Cleanout fluid carries out reduction cleaning to the rabbit floss Rachael blanket semi-finished product after dyeing, after reduction cleaning successively in peracetic acid solution
With, wash out cylinder, drying, steaming and color fixing, after steaming and color fixing use flexible smooth agent rabbit floss Rachael blanket semi-finished product are carried out
Flexible smooth processes, and the most again dries；
4), Final finishing: the rabbit floss Rachael blanket semi-finished product after dyeing and finishing are carried out successively drying and shaping, front hot light, front brush
Hair, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side boiling hot is cut, cutting
Sew up, obtain rabbit floss Rachael blanket finished product；
5), product inspection, packaging warehouse-in；
The preparation method of described plush yarn is as follows: carry out spinning by melt spinning machine after special fibre, rabbit hair being blended,
Prepare plush yarn；Wherein said rabbit hair accounts for the 4-6% of plush yarn gross mass, and special fibre accounts for the 2-of plush yarn gross mass
3%.
In the technical program, the inventive method is according to the feature of rabbit hair, in conjunction with HDR5DPLM30 La Sheer warp knit
The performance of machine, designs the upper machine tissue meeting its characteristic.The plush yarn performance system made according to rabbit hair and special fibre
Determine prefinishing technique；Grey cloth after cuing open floss is first carried out pre-setting and hot light processes, make the carpet surface fine hair crimpness before dyeing
Reducing, pieces dissipates pine and is conducive to dyeing, soft treatment and Final finishing processing.
The present invention selects rabbit hair to pool capital as Rachael blanket plush yarn with special fibre, containing poly-in special fibre
P-phthalic acid propylene diester fiber and nanometer zinc chloride, have antibacterial, the feature of good hygroscopicity, harmless, to skin
Affinity is good.By organizational structure reasonable in design for this raw material, ingenious combination chaining, latitude substrate cloth raw material, by warp knit is weaved,
The research and development of the key technologies such as prefinishing, printing and dyeing and Final finishing production, thus improve quality and the added value of product, make hair
Blanket keep soft, fine and smooth, smooth on the basis of, more have antibiotic health care, the feature such as ventilative nice and cool.Product in use,
Along with the continuous CONTACT WITH FRICTION of human body skin Yu fiber, the effective component in special fibre is constantly discharged from fiber, and quilt
Human body is absorbed, and the successful development of this project meets the needs of Green Textiles, i.e. ensure that the comfortable softness of Rachael blanket
Characteristic, more outstanding natural, green, healthy concept.
As preferably, step 1) described in tricot machine be HDR5DPLM30 type raschel machine, braiding speed is 420r/
Min, L1 and L5 sley bar uses inlaid thread filling inlaid thread, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses through flat
Braiding, form of entrying is for completely to wear；Wherein, the specification of described plush yarn is 150D/72F, and the specification of polyester drawn yarns is 150D/
36F。
As preferably, step 2) sizing time, rabbit floss Rachael blanket semi-finished product are at room temperature immersed in treatment fluid, process
Liquid to 65 DEG C with the ramp of 3 DEG C/min, is then incubated 50min, is drawn by rabbit floss after being cooled to room temperature with the speed of 3 DEG C/min
She Er woollen blanket semi-finished product take out washing, containing following material in treatment fluid: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate
0.22g/L, organic-silicon-modified nano-cerium oxide 3.2g/L, chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20.
As preferably, the preparation method of described organic-silicon-modified nano-cerium oxide is:
A) by ceria nanoparticles, the dimethyl formamide solution of mass concentration 30-50% and acid solution according to 1g:25-
The solid-liquid ratio mixing of 30mL:10-12mL, controls stirring mixing 30-50min at temperature 120-135 DEG C, filters, respectively with water and
Absolute ethanol washing, is vacuum dried 30-60min and obtains primary modified oxidized cerium granule at 130-150 DEG C；
B) primary modified nano cerium oxide granule is mixed according to the solid-liquid ratio of 1g:15-30mL with chemical shearing liquid, be heated to
120-150 DEG C, hydro-thermal reaction 30-45min, cooling, washing, obtain secondary modified nano cerium oxide granule；
C) secondary modified nano cerium oxide granule and 3-(2,3-epoxy the third oxygen) propyl trimethoxy silicane are according to 1g:20-30g's
Quality than mix homogeneously, be heated to 180-220 DEG C keep 3 hours, cooling, filter, washing, after vacuum drying modified Nano without
Machine compound particle.
As preferably, before carrying out dyeing and finishing, the rabbit floss Rachael blanket semi-finished product after prefinishing are carried out pretreatment: by rabbit
Floss Rachael blanket semi-finished product submergence carries out impregnation process, wherein rabbit floss Rachael blanket semi-finished product and the matter of ethanol in ethanol
Amount ratio is 1:5-6, and dip time is 20-40min.
In the technical program, owing to fiber surface has one layer of oil film, therefore when dyeing, due to the obstruct of oil film,
Dyestuff not easily penetrates into into fibrous inside, causes Color poor.And before dyeing, fabric is carried out at dipping in ethanol
Reason, it is possible to dissolve part oil film so that it is lower thickness, it is simple to dyestuff penetration enters fibrous inside, increases color fastness.However it is necessary that
Control dip time and ethanol consumption, it is to avoid oil film excessive dissolution and cause fibre-fibre friction, finally affect the light of fiber surface
Pool degree and smoothness.
As preferably, in step 3) in dyeing time, select high-temperature and high pressure dyeing process dye: prepare at normal temperatures
Dye liquor, the pH of described dye liquor controls at 5.6-6.8；Then being immersed in dye liquor by rabbit floss Rachael blanket semi-finished product, rabbit floss draws
She Er woollen blanket semi-finished product are 1:10 with the mass ratio of dye liquor；Then dye liquor is carried out heat temperature raising: first by dye liquor with 3 DEG C/min
Speed be warming up to 90 DEG C, then dye liquor is warming up to 125-135 DEG C with the speed of 1.5 DEG C/min, last fixation 60min；Its
Middle dye uses during dark product Palanilp nonionic dye；Mibct keton polyester dispersion is used during dye light-coloured prods
Dyestuff.
As preferably, step 3) described in reduction cleaning liquid include the synthesis detergent of 1.5-2.5g/L, 1.0-1.5g/L
Tea saponin, the sodium alginate of 10-15g/L Sargassum powder and 1.0-2.0g/L and water, bath raio 1:25, temperature 50-55 DEG C, during cleaning
Between 25-35min；During the dark product of dye, described reduction cleaning liquid also includes the sodium carbonate of 1-2g/L, the sodium hydrosulfite of 2g/L, 5-
The tea polyphenols of 10g/L and the nano titanium oxide of 0.3-0.5g/L；After reduction cleaning, the concentration of acetum used is
0.5wt%；When flexible smooth processes, carry out arranging the 2-3 second to fabric with flexible smooth agent；Described flexible smooth agent includes ovum
Phospholipid, smooth agent, tween 80 and water, the weight of wherein said lecithin is the 2.5-3% of water weight, and the weight of smooth agent is water
The 1.5-2% of weight, the weight of tween is the 0.5-1% of water weight.
In the technical program, when reduction cleaning soft treatment, after cleanout fluid cleans, make rabbit floss Rachael blanket
Have soft smooth, gloss is beautiful, adding Sargassum powder in reduction cleaning liquid is to make it form one layer at carpeted surface
Film protects woollen blanket, has anti-oxidation function；Tea saponin is a kind of nonionic surfactant, therefore, it is possible to as abluent
Using, tea saponin is compared with common abluent simultaneously, has preferable stability, it is possible to fill in the water environment of various hardness
The surface activity of himself is waved in distribution.In addition tea saponin also has certain color fixative blast, increases the effect of color fastness fiber,
When after Woollen blanket printing fixation, it is possible to promote its outward appearance vividness.Na is added when dye is dark3CO3And sodium hydrosulfite, more effectively remove
The loose colour of fiber surface；Add tea polyphenols and nano titanium oxide, be then to improve the anti-oxidation function of woollen blanket and antibiotic property
Energy.
Lecithin is oily matter, has good lubricant effect, it is possible to absorbed by fiber, thus promotes the toughness of fiber
And feel so that the fine hair of woollen blanket has good anti-pressure ability.In addition lecithin is harmless to health, for green material.Tell
Temperature has good emulsification, also is able to increase the dissolubility of lecithin simultaneously.
As preferably, described lecithin is through modification: be 50-60wt% by lecithin, poly-special penta lactone with concentration
The stirring of citric acid solution mix homogeneously post-heating, the mass ratio of wherein said lecithin and citric acid solution is 10:5-7:3-
6, heating-up temperature is 70-80 DEG C, heat time heating time 40-60min；Being gradually added into quality to reactant liquor during heated and stirred is institute
State the hydrogen peroxide solution that concentration is 30wt% of lecithin 20-25%；Hydroxide is dripped to reactant liquor after heated and stirred terminates
Sodium solution, to neutral, finally prepares hydroxylating modified lecithin after vacuum drying.
In the technical program, the mobility of common lecithin is poor, and viscosity is higher, be unfavorable for being absorbed by fiber and
In fiber surface film forming, the mobility of modified lecithin is therefore greatly increased, and is easier to be absorbed and at fiber by fiber
Surface filming.
As preferably, step 4) in Final finishing, drying and shaping uses FIR4 drying and setting machine, inverse hair to enter machine, patent door width
158-162cm, temperature 110-120 DEG C, speed 17-20m/min of shaping；Bristle uses the double roller brushing machine of MB211E type, speed 3-
4m/min, enters machine along hair, and bristle spaces 2.5mm；Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature 120-130
DEG C, speed 7-10m/min；Scalding to cut uses MB322E type high-speed and high-efficiency to scald shearing machine, carries out rabbit floss Rachael blanket front scalding and cuts,
Temperature 120-130 DEG C, speed 8-10m/min；Fluffing uses ME331E raising machine, has carried out rabbit floss Rachael blanket reverse side
Hair, speed 8-10m/min.
As preferably, the preparation method of described special fibre is as follows: takes bamboo powder and adds the concentration to its 8-12 times of quality
For in the sodium hydroxide solution of 8-12wt%, after being uniformly dispersed, heating under reduced pressure is to 110-130 DEG C, and 6-8h is discongested in insulation；After discongesting
It is filtrated to get bamboo powder, then bamboo powder is added to the ethanol solution that concentration is 70-80wt% of its 8-12 times of quality, be heated to
Being incubated 3-5h after 80-90 DEG C, again filter, add water precipitate and pull an oar, making beating to slurry beating degree is 14-16 °
SR, then carries out defibrination, and defibrination is 18-22 ° of SR to slurry beating degree, washes and obtain fiber after distillation of reducing pressure after making beating
Element；Cellulose is added to the ionic liquid of its 18-22 times of quality, obtains cellulose solution；Add in cellulose solution
The PTT Fiber of its quality 0.4-0.6 times and the nanometer zinc chloride of its quality 0.005-0.01 times, stir
Uniformly obtain mixed solution, in mixed solution, then add the calcium chloride solution that isopyknic concentration is 2-4wt%, at 40-
After cross-linking 1-2h at 50 DEG C, transfer liquid nitrogen freezes 1-2 days, then takes out frost thing, thaw with flowing water, prepare special fibre water
Gel, then carry out solvent displacement with dehydrated alcohol, after eventually passing vacuum drying, prepare special fibre.
In the technical program, in the preparation process of the special fibre of the present invention, first prepare cellulose, the inventive method system
Standby cellulolytic activity is high, easily cross-links.Then cellulose is total to PTT Fiber and nano zine oxide
Mixed, add cross-linking agent calcium chloride solution, make partial cross-linked solidification, be then passed through freezing, make cellulose crosslinked sizing, thaw and molten
After agent displacement, preparing special fibre, it is multiple with cellulose that this special fibre is actually PTT Fiber
The aeroge closed, PTT Fiber and the interlaced crosslinking of cellulose, and cellulose and spinning liquid is compatible
Property preferable, the special fibre intensity that spinning obtains is higher, and the load fastness of active substance is high.Additionally, special fibre has higher
Specific surface area so that it is the advantage with moisture absorption and desorption property, good permeability.
Beneficial effects of the present invention, the rabbit floss Rachael blanket of the present invention has that fine hair color and luster is good, submissive, stands upright, elastic
Good, fabric skin-friendly, moisture absorption and desorption property, the advantage of good permeability and antibiotic health care, the feature of environmental protection.
Detailed description of the invention
Technical scheme in the embodiment of the present invention will be carried out clear, complete description below, it is clear that described enforcement
Example is only a part of embodiment of the present invention rather than whole embodiments.Based on the embodiment in the present invention, this area is common
All other embodiments that technical staff is obtained under not making creative work premise, broadly fall into the model of present invention protection
Enclose.
In the present invention, agents useful for same is all commercially available.
Embodiment 1
The production technology of a kind of rabbit floss Rachael blanket, is plied to yarn using rabbit hair and special fibre former as plush yarn
Material, using polyester drawn yarns as wire gauze raw material, comprises the following steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare rabbit floss Rachael blanket
Semi-finished product；Tricot machine is HDR5DPLM30 type raschel machine, and braiding speed is that 420r/min, L1 and L5 sley bar uses inlaid thread
Filling inlaid thread, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses and knits through flat sennit, and form of entrying is for completely to wear；Its
In, the specification of described plush yarn is 150D/72F, and the specification of polyester drawn yarns is 150D/36F；
2), prefinishing: carry out described rabbit floss Rachael blanket semi-finished product shaping, bristle, hot light, clot；During sizing, by rabbit floss
Rachael blanket semi-finished product at room temperature immerse in treatment fluid, and treatment fluid, is then incubated to 65 DEG C with the ramp of 3 DEG C/min
Rabbit floss Rachael blanket semi-finished product are taken out washing after being cooled to room temperature with the speed of 3 DEG C/min, contain in treatment fluid by 50min
Following material: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate 0.22g/L, organic-silicon-modified nano-cerium oxide 3.2g/L,
Chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20；The preparation method of described organic-silicon-modified nano-cerium oxide is:
A) by ceria nanoparticles, the dimethyl formamide solution of mass concentration 30% and acid solution according to 1g:25mL:10mL
Solid-liquid ratio mixing, control stirring mixing 30min at temperature 120 DEG C, filter, respectively with water and absolute ethanol washing, at 130 DEG C
Vacuum drying 30min obtains primary modified oxidized cerium granule；
B) primary modified nano cerium oxide granule is mixed according to the solid-liquid ratio of 1g:15mL with chemical shearing liquid, be heated to 120
DEG C, hydro-thermal reaction 30min, cooling, washing, obtain secondary modified nano cerium oxide granule；
C) secondary modified nano cerium oxide granule and 3-(2,3-epoxy the third oxygen) propyl trimethoxy silicane are according to the matter of 1g:20g
Measure ratio mix homogeneously, be heated to 180 DEG C and keep 3 hours, cooling, filter, washing, after vacuum drying, obtain modified Nano inorganic chemical
Composition granule；
Before carrying out dyeing and finishing, the rabbit floss Rachael blanket semi-finished product after prefinishing are carried out pretreatment: by rabbit floss Rachael blanket
Semi-finished product submergence carries out impregnation process in ethanol, and wherein rabbit floss Rachael blanket semi-finished product are 1:5 with the mass ratio of ethanol, leaching
The stain time is 20min；
3), dyeing and finishing: the rabbit floss Rachael blanket semi-finished product after prefinishing are positioned in dyeing liquor and dye, then with reduction
Cleanout fluid carries out reduction cleaning to the rabbit floss Rachael blanket semi-finished product after dyeing, after reduction cleaning successively in peracetic acid solution
With, wash out cylinder, drying, steaming and color fixing, after steaming and color fixing use flexible smooth agent rabbit floss Rachael blanket semi-finished product are carried out
Flexible smooth processes, and the most again dries；During dyeing, high-temperature and high pressure dyeing process is selected to dye: to prepare dying easily at normal temperatures
Liquid, the pH of described dye liquor controls at 5.6-6.8；Then being immersed in dye liquor by rabbit floss Rachael blanket semi-finished product, rabbit floss draws house
That woollen blanket semi-finished product are 1:10 with the mass ratio of dye liquor；Then dye liquor is carried out heat temperature raising: first by dye liquor with 3 DEG C/min's
Speed is warming up to 90 DEG C, then with the speed of 1.5 DEG C/min, dye liquor is warming up to 125-135 DEG C, last fixation 60min；Wherein
Dye uses during dark product Palanilp nonionic dye；Mibct keton polyester dispersion dye is used during dye light-coloured prods
Material；
Reduction cleaning liquid includes synthesis detergent, the tea saponin of 1.0g/L, 10g/L Sargassum powder and the Sargassum of 1.0g/L of 1.5g/L
Acid sodium and water, bath raio 1:25, temperature 50 C, scavenging period 25min；During the dark product of dye, described reduction cleaning liquid also includes 1g/
The sodium carbonate of L, the sodium hydrosulfite of 2g/L, the tea polyphenols of 5g/L and the nano titanium oxide of 0.3g/L；Acetic acid used after reduction cleaning
The concentration of solution is 0.5wt%；When flexible smooth processes, carry out arranging the 2-3 second to fabric with flexible smooth agent；Described softness
Smooth agent includes that lecithin, smooth agent, tween 80 and water, the weight of wherein said lecithin are the 2.5% of water weight, smooth agent
Weight is water weight 1.5%, the weight of tween is the 0.5% of water weight；
Lecithin is through modification: lecithin, poly-special penta lactone are mixed homogeneously with the citric acid solution that concentration is 50wt%
Post-heating stirs, and wherein said lecithin is 10:5:3 with the mass ratio of citric acid solution, and heating-up temperature is 70 DEG C, heat time heating time
40min；Being gradually added into, to reactant liquor, the concentration that quality is described lecithin 20% during heated and stirred is the double of 30wt%
Oxygen aqueous solution；To reactant liquor dropping sodium hydroxide solution to neutral after heated and stirred terminates, finally after vacuum drying, prepare hydroxyl
Base modified lecithin；
4), Final finishing: the rabbit floss Rachael blanket semi-finished product after dyeing and finishing are carried out successively drying and shaping, front hot light, front brush
Hair, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side boiling hot is cut, cutting
Sew up, obtain rabbit floss Rachael blanket finished product；In Final finishing, drying and shaping uses FIR4 drying and setting machine, inverse hair to enter machine, sizing
Door width 158cm, temperature 110 DEG C, speed 17m/min of shaping；The double roller brushing machine of bristle employing MB211E type, speed 3m/min, suitable
Mao Jinji, bristle spaces 2.5mm；Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature 120 DEG C, speed 7m/
min；Scalding to cut uses MB322E type high-speed and high-efficiency to scald shearing machine, carries out rabbit floss Rachael blanket front scalding and cuts, temperature 120 DEG C, speed
Degree 8m/min；Fluffing uses ME331E raising machine, fluffs rabbit floss Rachael blanket reverse side, speed 8m/min；
5), product inspection, packaging warehouse-in；
The preparation method of described plush yarn is as follows: carry out spinning by melt spinning machine after special fibre, rabbit hair being blended,
Prepare plush yarn；Wherein said rabbit hair accounts for the 4% of plush yarn gross mass, and special fibre accounts for the 2% of plush yarn gross mass；
The preparation method of special fibre is as follows: takes bamboo powder and adds the sodium hydroxide solution that concentration is 8wt% to its 8 times of quality
In, after being uniformly dispersed, heating under reduced pressure to 110 DEG C, 6h is discongested in insulation；Be filtrated to get bamboo powder after discongesting, then bamboo powder is added to its 8
In the ethanol solution that concentration is 70wt% of times quality, it is incubated 3h after being heated to 80 DEG C, again filters, precipitate is added water
Pulling an oar, making beating is 14 ° of SR to slurry beating degree, then carries out defibrination, and defibrination to slurry beating degree is 18 ° of SR, after making beating
Wash and obtain cellulose after distillation of reducing pressure；Cellulose is added to the ionic liquid of its 18 times of quality, obtains fiber
Cellulose solution；PTT Fiber and its quality 0.005 times of its quality 0.4 times is added in cellulose solution
Nanometer zinc chloride, is uniformly mixing to obtain mixed solution, then adds the chlorination that isopyknic concentration is 2wt% in mixed solution
Calcium solution, after cross-linking 1h, freezes 1 day in transfer liquid nitrogen, then takes out frost thing, thaw with flowing water, prepare special type at 40 DEG C
Fiber water gel, then carry out solvent displacement with dehydrated alcohol, after eventually passing vacuum drying, prepare special fibre.
Embodiment 2
The production technology of a kind of rabbit floss Rachael blanket, is plied to yarn using rabbit hair and special fibre former as plush yarn
Material, using polyester drawn yarns as wire gauze raw material, comprises the following steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare rabbit floss Rachael blanket
Semi-finished product；Tricot machine is HDR5DPLM30 type raschel machine, and braiding speed is that 420r/min, L1 and L5 sley bar uses inlaid thread
Filling inlaid thread, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses and knits through flat sennit, and form of entrying is for completely to wear；Its
In, the specification of described plush yarn is 150D/72F, and the specification of polyester drawn yarns is 150D/36F；
2), prefinishing: carry out described rabbit floss Rachael blanket semi-finished product shaping, bristle, hot light, clot；During sizing, by rabbit floss
Rachael blanket semi-finished product at room temperature immerse in treatment fluid, and treatment fluid, is then incubated to 65 DEG C with the ramp of 3 DEG C/min
Rabbit floss Rachael blanket semi-finished product are taken out washing after being cooled to room temperature with the speed of 3 DEG C/min, contain in treatment fluid by 50min
Following material: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate 0.22g/L, organic-silicon-modified nano-cerium oxide 3.2g/L,
Chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20；
The preparation method of described organic-silicon-modified nano-cerium oxide is:
A) by ceria nanoparticles, the dimethyl formamide solution of mass concentration 40% and acid solution according to 1g:28mL:11mL
Solid-liquid ratio mixing, control stirring mixing 40min at temperature 125 DEG C, filter, respectively with water and absolute ethanol washing, at 150 DEG C
Vacuum drying 50min obtains primary modified oxidized cerium granule；
B) primary modified nano cerium oxide granule is mixed according to the solid-liquid ratio of 1g:20mL with chemical shearing liquid, be heated to 130
DEG C, hydro-thermal reaction 35min, cooling, washing, obtain secondary modified nano cerium oxide granule；
C) secondary modified nano cerium oxide granule and 3-(2,3-epoxy the third oxygen) propyl trimethoxy silicane are according to the matter of 1g:25g
Measure ratio mix homogeneously, be heated to 190 DEG C and keep 3 hours, cooling, filter, washing, after vacuum drying, obtain modified Nano inorganic chemical
Composition granule；
Before carrying out dyeing and finishing, the rabbit floss Rachael blanket semi-finished product after prefinishing are carried out pretreatment: by rabbit floss Rachael blanket
Semi-finished product submergence carries out impregnation process in ethanol, and wherein rabbit floss Rachael blanket semi-finished product are 1:5.5 with the mass ratio of ethanol,
Dip time is 30min；
3), dyeing and finishing: the rabbit floss Rachael blanket semi-finished product after prefinishing are positioned in dyeing liquor and dye, then with reduction
Cleanout fluid carries out reduction cleaning to the rabbit floss Rachael blanket semi-finished product after dyeing, after reduction cleaning successively in peracetic acid solution
With, wash out cylinder, drying, steaming and color fixing, after steaming and color fixing use flexible smooth agent rabbit floss Rachael blanket semi-finished product are carried out
Flexible smooth processes, and the most again dries；During dyeing, high-temperature and high pressure dyeing process is selected to dye: to prepare dying easily at normal temperatures
Liquid, the pH of described dye liquor controls 5.9；Then rabbit floss Rachael blanket semi-finished product are immersed in dye liquor, rabbit floss La Sheermao
Blanket semi-finished product are 1:10 with the mass ratio of dye liquor；Then dye liquor is carried out heat temperature raising: first by dye liquor with the speed of 3 DEG C/min
It is warming up to 90 DEG C, then dye liquor is warming up to 125-135 DEG C with the speed of 1.5 DEG C/min, last fixation 60min；Wherein in dye
Palanilp nonionic dye is used during dark product；Mibct keton polyester dispersion dyestuff is used during dye light-coloured prods；
Reduction cleaning liquid includes synthesis detergent, the tea saponin of 1.3g/L, 13g/L Sargassum powder and the Sargassum of 1.7g/L of 1.8g/L
Acid sodium and water, bath raio 1:25, temperature 53 DEG C, scavenging period 30min；During the dark product of dye, described reduction cleaning liquid also includes
The sodium carbonate of 1.2g/L, the sodium hydrosulfite of 2g/L, the tea polyphenols of 7.2g/L and the nano titanium oxide of 0.4g/L；Institute after reduction cleaning
It is 0.5wt% by the concentration of acetum；When flexible smooth processes, carry out arranging the 2-3 second to fabric with flexible smooth agent；Institute
State flexible smooth agent and include that lecithin, smooth agent, tween 80 and water, the weight of wherein said lecithin are the 2.8% of water weight,
The weight of smooth agent is the 1.7% of water weight, and the weight of tween is the 0.6% of water weight；Lecithin is through modification: by ovum phosphorus
Fat, poly-special penta lactone are mixed homogeneously post-heating and are stirred with the citric acid solution that concentration is 55wt%, wherein said lecithin and lemon
The mass ratio of lemon acid solution is 10:6:5, and heating-up temperature is 77 DEG C, heat time heating time 46min；To reaction during heated and stirred
Liquid is gradually added into the hydrogen peroxide solution that concentration is 30wt% that quality is described lecithin 23%；To instead after heated and stirred terminates
Answer drop hydro-oxidation sodium solution to neutral, finally after vacuum drying, prepare hydroxylating modified lecithin；
4), Final finishing: the rabbit floss Rachael blanket semi-finished product after dyeing and finishing are carried out successively drying and shaping, front hot light, front brush
Hair, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side boiling hot is cut, cutting
Sew up, obtain rabbit floss Rachael blanket finished product；In Final finishing, drying and shaping uses FIR4 drying and setting machine, inverse hair to enter machine, sizing
Door width 159cm, temperature 117 DEG C, speed 18m/min of shaping；The double roller brushing machine of bristle employing MB211E type, speed 3.5m/min,
Entering machine along hair, bristle spaces 2.5mm；Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature 127 DEG C, speed 8m/
min；Scalding to cut uses MB322E type high-speed and high-efficiency to scald shearing machine, carries out rabbit floss Rachael blanket front scalding and cuts, temperature 125 DEG C, speed
Degree 9m/min；Fluffing uses ME331E raising machine, fluffs rabbit floss Rachael blanket reverse side, speed 9m/min；
5), product inspection, packaging warehouse-in；
The preparation method of described plush yarn is as follows: carry out spinning by melt spinning machine after special fibre, rabbit hair being blended,
Prepare plush yarn；Wherein said rabbit hair accounts for the 5% of plush yarn gross mass, and special fibre accounts for the 2.5% of plush yarn gross mass；
The preparation method of special fibre is as follows: takes bamboo powder and adds to the sodium hydroxide that concentration is 10wt% of its 9 times of quality molten
In liquid, after being uniformly dispersed, heating under reduced pressure to 120 DEG C, 7h is discongested in insulation；It is filtrated to get bamboo powder after discongesting, then bamboo powder is added extremely
The concentration of its 10 times of quality is in the ethanol solution of 75wt%, is incubated 4h, again filters, to precipitate after being heated to 85 DEG C
Adding water and pull an oar, making beating is 15 ° of SR to slurry beating degree, then carries out defibrination, and defibrination to slurry beating degree is 19 ° of SR, beats
Wash after slurry and obtain cellulose after distillation of reducing pressure；Cellulose is added to the ionic liquid of its 20 times of quality, obtains
Cellulose solution；PTT Fiber and its quality 0.007 of its quality 0.5 times is added in cellulose solution
Nanometer zinc chloride again, is uniformly mixing to obtain mixed solution, and then adding isopyknic concentration in mixed solution is 3wt%'s
Calcium chloride solution, after cross-linking 1.5h, freezes 1 day in transfer liquid nitrogen, then takes out frost thing, thaw with flowing water at 45 DEG C, system
Obtain special fibre hydrogel, then carry out solvent displacement with dehydrated alcohol, after eventually passing vacuum drying, prepare special fibre.
Embodiment 3
The production technology of a kind of rabbit floss Rachael blanket, is plied to yarn using rabbit hair and special fibre former as plush yarn
Material, using polyester drawn yarns as wire gauze raw material, comprises the following steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare rabbit floss Rachael blanket
Semi-finished product；Tricot machine is HDR5DPLM30 type raschel machine, and braiding speed is that 420r/min, L1 and L5 sley bar uses inlaid thread
Filling inlaid thread, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses and knits through flat sennit, and form of entrying is for completely to wear；Its
In, the specification of described plush yarn is 150D/72F, and the specification of polyester drawn yarns is 150D/36F；
2), prefinishing: carry out described rabbit floss Rachael blanket semi-finished product shaping, bristle, hot light, clot；During sizing, by rabbit floss
Rachael blanket semi-finished product at room temperature immerse in treatment fluid, and treatment fluid, is then incubated to 65 DEG C with the ramp of 3 DEG C/min
Rabbit floss Rachael blanket semi-finished product are taken out washing after being cooled to room temperature with the speed of 3 DEG C/min, contain in treatment fluid by 50min
Following material: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate 0.22g/L, organic-silicon-modified nano-cerium oxide 3.2g/L,
Chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20；
The preparation method of described organic-silicon-modified nano-cerium oxide is:
A) by ceria nanoparticles, the dimethyl formamide solution of mass concentration 50% and acid solution according to 1g:30mL:12mL
Solid-liquid ratio mixing, control stirring mixing 50min at temperature 135 DEG C, filter, respectively with water and absolute ethanol washing, at 150 DEG C
Vacuum drying 60min obtains primary modified oxidized cerium granule；
B) primary modified nano cerium oxide granule is mixed according to the solid-liquid ratio of 1g:30mL with chemical shearing liquid, be heated to 150
DEG C, hydro-thermal reaction 45min, cooling, washing, obtain secondary modified nano cerium oxide granule；
C) secondary modified nano cerium oxide granule and 3-(2,3-epoxy the third oxygen) propyl trimethoxy silicane are according to the matter of 1g:30g
Measure ratio mix homogeneously, be heated to 220 DEG C and keep 3 hours, cooling, filter, washing, after vacuum drying, obtain modified Nano inorganic chemical
Composition granule；
Before carrying out dyeing and finishing, the rabbit floss Rachael blanket semi-finished product after prefinishing are carried out pretreatment: by rabbit floss Rachael blanket
Semi-finished product submergence carries out impregnation process in ethanol, and wherein rabbit floss Rachael blanket semi-finished product are 1:6 with the mass ratio of ethanol, leaching
The stain time is 40min；
3), dyeing and finishing: the rabbit floss Rachael blanket semi-finished product after prefinishing are positioned in dyeing liquor and dye, then with reduction
Cleanout fluid carries out reduction cleaning to the rabbit floss Rachael blanket semi-finished product after dyeing, after reduction cleaning successively in peracetic acid solution
With, wash out cylinder, drying, steaming and color fixing, after steaming and color fixing use flexible smooth agent rabbit floss Rachael blanket semi-finished product are carried out
Flexible smooth processes, and the most again dries；During dyeing, high-temperature and high pressure dyeing process is selected to dye: to prepare dying easily at normal temperatures
Liquid, the pH of described dye liquor controls 6.8；Then rabbit floss Rachael blanket semi-finished product are immersed in dye liquor, rabbit floss La Sheermao
Blanket semi-finished product are 1:10 with the mass ratio of dye liquor；Then dye liquor is carried out heat temperature raising: first by dye liquor with the speed of 3 DEG C/min
It is warming up to 90 DEG C, then dye liquor is warming up to 135 DEG C with the speed of 1.5 DEG C/min, last fixation 60min；Wherein dark in dye
Palanilp nonionic dye is used during product；Mibct keton polyester dispersion dyestuff is used during dye light-coloured prods；
Reduction cleaning liquid includes synthesis detergent, the tea saponin of 1.5g/L, 15g/L Sargassum powder and the Sargassum of 2.0g/L of 2.5g/L
Acid sodium and water, bath raio 1:25, temperature 55 DEG C, scavenging period 35min；During the dark product of dye, described reduction cleaning liquid also includes 2g/
The sodium carbonate of L, the sodium hydrosulfite of 2g/L, the tea polyphenols of 10g/L and the nano titanium oxide of 0.5g/L；Acetic acid used after reduction cleaning
The concentration of solution is 0.5wt%；When flexible smooth processes, carry out arranging the 2-3 second to fabric with flexible smooth agent；Described softness
Smooth agent includes that lecithin, smooth agent, tween 80 and water, the weight of wherein said lecithin are the 3% of water weight, smooth agent
Weight is the 2% of water weight, and the weight of tween is the 1% of water weight；Lecithin is through modification: by lecithin, poly-special penta lactone
Post-heating of mixing homogeneously with the citric acid solution that concentration is 50-60wt% stirs, wherein said lecithin and citric acid solution
Mass ratio is 10:7:6, and heating-up temperature is 80 DEG C, heat time heating time 60min；It is gradually added into reactant liquor during heated and stirred
Quality is the hydrogen peroxide solution that concentration is 30wt% of described lecithin 25%；Hydrogen is dripped to reactant liquor after heated and stirred terminates
Sodium hydroxide solution, to neutral, finally prepares hydroxylating modified lecithin after vacuum drying；
4), Final finishing: the rabbit floss Rachael blanket semi-finished product after dyeing and finishing are carried out successively drying and shaping, front hot light, front brush
Hair, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side boiling hot is cut, cutting
Sew up, obtain rabbit floss Rachael blanket finished product；In Final finishing, drying and shaping uses FIR4 drying and setting machine, inverse hair to enter machine, sizing
Door width 162cm, temperature 120 DEG C, speed 20m/min of shaping；The double roller brushing machine of bristle employing MB211E type, speed 4m/min, suitable
Mao Jinji, bristle spaces 2.5mm；Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature 130 DEG C, speed 10m/
min；Scalding to cut uses MB322E type high-speed and high-efficiency to scald shearing machine, carries out rabbit floss Rachael blanket front scalding and cuts, temperature 130 DEG C, speed
Degree 10m/min；Fluffing uses ME331E raising machine, fluffs rabbit floss Rachael blanket reverse side, speed 10m/min；
5), product inspection, packaging warehouse-in；
The preparation method of described plush yarn is as follows: carry out spinning by melt spinning machine after special fibre, rabbit hair being blended,
Prepare plush yarn；Wherein said rabbit hair accounts for the 6% of plush yarn gross mass, and special fibre accounts for the 3% of plush yarn gross mass；
The preparation method of special fibre is as follows: takes bamboo powder and adds to the sodium hydroxide that concentration is 12wt% of its 12 times of quality molten
In liquid, after being uniformly dispersed, heating under reduced pressure to 130 DEG C, 8h is discongested in insulation；It is filtrated to get bamboo powder after discongesting, then bamboo powder is added extremely
The concentration of its 12 times of quality is in the ethanol solution of 80wt%, is incubated 5h, again filters, to precipitate after being heated to 90 DEG C
Adding water and pull an oar, making beating is 16 ° of SR to slurry beating degree, then carries out defibrination, and defibrination to slurry beating degree is 22 ° of SR, beats
Wash after slurry and obtain cellulose after distillation of reducing pressure；Cellulose is added to the ionic liquid of its 22 times of quality, obtains
Cellulose solution；PTT Fiber and its quality 0.01 of its quality 0.6 times is added in cellulose solution
Nanometer zinc chloride again, is uniformly mixing to obtain mixed solution, and then adding isopyknic concentration in mixed solution is 4wt%'s
Calcium chloride solution, after cross-linking 1-2h, freezes 2 days in transfer liquid nitrogen, then takes out frost thing, thaw with flowing water at 50 DEG C, system
Obtain special fibre hydrogel, then carry out solvent displacement with dehydrated alcohol, after eventually passing vacuum drying, prepare special fibre.
Raw materials used, equipment in the present invention, unless otherwise noted, is the conventional raw material of this area, equipment；In the present invention
Method therefor, unless otherwise noted, is the conventional method of this area.
The above, be only presently preferred embodiments of the present invention, not impose any restrictions the present invention, every according to the present invention
Any simple modification, change and the equivalent transformation that above example is made by technical spirit, all still falls within the technology of the present invention side
The protection domain of case.
Claims (10)
1. the production technology of a rabbit floss Rachael blanket, it is characterised in that be plied to yarn with rabbit hair and special fibre
As plush yarn raw material, using polyester drawn yarns as wire gauze raw material, comprise the following steps:
1), weaving: on tricot machine, plush yarn and wire gauze are successively carried out warping, weaves, cut open floss, prepare rabbit floss Rachael blanket
Semi-finished product；
2), prefinishing: carry out described rabbit floss Rachael blanket semi-finished product shaping, bristle, hot light, clot；
3), dyeing and finishing: the rabbit floss Rachael blanket semi-finished product after prefinishing are positioned in dyeing liquor and dye, then with reduction
Cleanout fluid carries out reduction cleaning to the rabbit floss Rachael blanket semi-finished product after dyeing, after reduction cleaning successively in peracetic acid solution
With, wash out cylinder, drying, steaming and color fixing, after steaming and color fixing use flexible smooth agent rabbit floss Rachael blanket semi-finished product are carried out
Flexible smooth processes, and the most again dries；
4), Final finishing: the rabbit floss Rachael blanket semi-finished product after dyeing and finishing are carried out successively drying and shaping, front hot light, front brush
Hair, front scald cut, back side fluffing, back side bristle, back side hot light, the back side grab cut, multiple sizing, front scald cut, the back side boiling hot is cut, cutting
Sew up, obtain rabbit floss Rachael blanket finished product；
5), product inspection, packaging warehouse-in；
The preparation method of described plush yarn is as follows: carry out spinning by melt spinning machine after special fibre, rabbit hair being blended,
Prepare plush yarn；Wherein said rabbit hair accounts for the 4-6% of plush yarn gross mass, and special fibre accounts for the 2-of plush yarn gross mass
3%.
The production technology of a kind of rabbit floss Rachael blanket the most according to claim 1, it is characterised in that step 1) described in
Tricot machine is HDR5DPLM30 type raschel machine, and braiding speed is that 420r/min, L1 and L5 sley bar uses inlaid thread filling lining
Latitude, L2 Yu L4 sley bar uses inlaid thread filling chaining, and L3 wool yarn sley bar uses and knits through flat sennit, and form of entrying is for completely to wear；Wherein, described
The specification of plush yarn is 150D/72F, and the specification of polyester drawn yarns is 150D/36F.
The production technology of a kind of rabbit floss Rachael blanket the most according to claim 1, it is characterised in that step 2) sizing
Time, rabbit floss Rachael blanket semi-finished product are at room temperature immersed in treatment fluid, treatment fluid with the ramp of 3 DEG C/min to 65
DEG C, then it is incubated 50min, after being cooled to room temperature with the speed of 3 DEG C/min, rabbit floss Rachael blanket semi-finished product are taken out washing, place
Containing following material in reason liquid: sodium silicate 0.2g/L, Matrii Sulfas Exsiccatus 2g/L, aluminium silicate 0.22g/L, organic-silicon-modified nano oxidized
Cerium 3.2g/L, chitin 1.5g/L and penetrating agent 0.5g/L, bath raio 1:20.
The production technology of a kind of rabbit floss Rachael blanket the most according to claim 3, it is characterised in that described organosilicon
The preparation method of modified nano-cerium oxide is:
A) by ceria nanoparticles, the dimethyl formamide solution of mass concentration 30-50% and acid solution according to 1g:25-
The solid-liquid ratio mixing of 30mL:10-12mL, controls stirring mixing 30-50min at temperature 120-135 DEG C, filters, respectively with water and
Absolute ethanol washing, is vacuum dried 30-60min and obtains primary modified oxidized cerium granule at 130-150 DEG C；
B) primary modified nano cerium oxide granule is mixed according to the solid-liquid ratio of 1g:15-30mL with chemical shearing liquid, be heated to
120-150 DEG C, hydro-thermal reaction 30-45min, cooling, washing, obtain secondary modified nano cerium oxide granule；
C) secondary modified nano cerium oxide granule and 3-(2,3-epoxy the third oxygen) propyl trimethoxy silicane are according to 1g:20-30g's
Quality than mix homogeneously, be heated to 180-220 DEG C keep 3 hours, cooling, filter, washing, after vacuum drying modified Nano without
Machine compound particle.
The production technology of a kind of rabbit floss Rachael blanket the most according to claim 1, it is characterised in that carrying out dyeing and finishing
Before, the rabbit floss Rachael blanket semi-finished product after prefinishing are carried out pretreatment: rabbit floss Rachael blanket semi-finished product are immersed in second
Carrying out impregnation process in alcohol, wherein rabbit floss Rachael blanket semi-finished product are 1:5-6 with the mass ratio of ethanol, and dip time is 20-
40min。
The production technology of a kind of rabbit floss Rachael blanket the most according to claim 1, it is characterised in that in step 3) in
During dyeing, high-temperature and high pressure dyeing process is selected to dye: preparing dye liquor at normal temperatures, the pH of described dye liquor controls at 5.6-
6.8；Then rabbit floss Rachael blanket semi-finished product are immersed in dye liquor, rabbit floss Rachael blanket semi-finished product and the mass ratio of dye liquor
For 1:10；Then dye liquor is carried out heat temperature raising: first dye liquor is warming up to 90 DEG C with the speed of 3 DEG C/min, then by dye liquor
It is warming up to 125-135 DEG C, last fixation 60min with the speed of 1.5 DEG C/min；Dye wherein uses during dark product Palanilp
Nonionic dye；Mibct keton polyester dispersion dyestuff is used during dye light-coloured prods.
The production technology of a kind of rabbit floss Rachael blanket the most according to claim 1, it is characterised in that step 3) described in
Reduction cleaning liquid includes synthesis detergent, the tea saponin of 1.0-1.5g/L, 10-15g/L Sargassum powder and the 1.0-of 1.5-2.5g/L
The sodium alginate of 2.0g/L and water, bath raio 1:25, temperature 50-55 DEG C, scavenging period 25-35min；During the dark product of dye, described
Reduction cleaning liquid also includes the sodium carbonate of 1-2g/L, the sodium hydrosulfite of 2g/L, the tea polyphenols of 5-10g/L and the nanometer of 0.3-0.5g/L
Titanium dioxide；After reduction cleaning, the concentration of acetum used is 0.5wt%；When flexible smooth processes, use flexible smooth agent
Carry out fabric arranging the 2-3 second；Described flexible smooth agent includes lecithin, smooth agent, tween 80 and water, wherein said ovum phosphorus
The weight of fat is the 2.5-3% of water weight, and the weight of smooth agent is the 1.5-2% of water weight, and the weight of tween is the 0.5-of water weight
1%.
The production technology of a kind of rabbit floss Rachael blanket the most according to claim 7, it is characterised in that described lecithin warp
Cross modification: post-heating of lecithin, poly-special penta lactone being mixed homogeneously with the citric acid solution that concentration is 50-60wt% stirs
Mixing, wherein said lecithin is 10:5-7:3-6 with the mass ratio of citric acid solution, and heating-up temperature is 70-80 DEG C, heat time heating time
40-60min；Being gradually added into, to reactant liquor, the concentration that quality is described lecithin 20-25% during heated and stirred is
The hydrogen peroxide solution of 30wt%；To reactant liquor dropping sodium hydroxide solution to neutral after heated and stirred terminates, last vacuum is done
Hydroxylating modified lecithin is prepared after dry.
The production technology of a kind of rabbit floss Rachael blanket the most according to claim 1, it is characterised in that step 4) Final finishing
In, drying and shaping uses FIR4 drying and setting machine, inverse hair to enter machine, patent door width 158-162cm, temperature 110-120 DEG C, sizing speed
Degree 17-20m/min；Bristle uses the double roller brushing machine of MB211E type, speed 3-4m/min, enters machine along hair, and bristle spaces 2.5mm；
Hot light uses SME473H type list roller secondary to scald shearing machine, hot light temperature 120-130 DEG C, speed 7-10m/min；Scald and cut employing
MB322E type high-speed and high-efficiency scalds shearing machine, carries out rabbit floss Rachael blanket front scalding and cuts, temperature 120-130 DEG C, speed 8-10m/
min；Fluffing uses ME331E raising machine, fluffs rabbit floss Rachael blanket reverse side, speed 8-10m/min.
10., according to the production technology of a kind of rabbit floss Rachael blanket described in claim 1 or 2 or 3 or 5 or 9, its feature exists
In, the preparation method of special fibre is as follows: takes bamboo powder and adds the hydroxide that concentration is 8-12wt% to its 8-12 times of quality
In sodium solution, after being uniformly dispersed, heating under reduced pressure is to 110-130 DEG C, and 6-8h is discongested in insulation；Bamboo powder it is filtrated to get after discongesting, then will
Bamboo powder adds to the ethanol solution that concentration is 70-80wt% of its 8-12 times of quality, is incubated 3-5h after being heated to 80-90 DEG C,
Again filtering, add water precipitate and pull an oar, making beating is 14-16 ° of SR to slurry beating degree, then carries out defibrination, mill
Slurry is 18-22 ° of SR to slurry beating degree, washes and obtain cellulose after distillation of reducing pressure after making beating；Cellulose is added extremely
In the ionic liquid of its 18-22 times of quality, obtain cellulose solution；Its quality 0.4-0.6 times is added in cellulose solution
PTT Fiber and the nanometer zinc chloride of its quality 0.005-0.01 times, be uniformly mixing to obtain mixed solution,
Then in mixed solution, add the calcium chloride solution that isopyknic concentration is 2-4wt%, after cross-linking 1-2h at 40-50 DEG C,
Transfer liquid nitrogen freezes 1-2 days, then takes out frost thing, thaw with flowing water, prepare special fibre hydrogel, then use dehydrated alcohol
Carry out solvent displacement, after eventually passing vacuum drying, prepare special fibre.
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| CN106167951B (en) | 2019-02-15 |
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