CN112030316A - Preparation method of novel warm-keeping functional fabric - Google Patents

Preparation method of novel warm-keeping functional fabric Download PDF

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Publication number
CN112030316A
CN112030316A CN202010881371.0A CN202010881371A CN112030316A CN 112030316 A CN112030316 A CN 112030316A CN 202010881371 A CN202010881371 A CN 202010881371A CN 112030316 A CN112030316 A CN 112030316A
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CN
China
Prior art keywords
fabric
aerogel
preparation
dyeing
yarns
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Pending
Application number
CN202010881371.0A
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Chinese (zh)
Inventor
刘沙柯
顾敏芬
孙霞
钟国能
何立锋
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ningbo Daqian Textile Co Ltd
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Ningbo Daqian Textile Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Ningbo Daqian Textile Co Ltd filed Critical Ningbo Daqian Textile Co Ltd
Priority to CN202010881371.0A priority Critical patent/CN112030316A/en
Publication of CN112030316A publication Critical patent/CN112030316A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D03WEAVING
    • D03DWOVEN FABRICS; METHODS OF WEAVING; LOOMS
    • D03D15/00Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F1/00General methods for the manufacture of artificial filaments or the like
    • D01F1/02Addition of substances to the spinning solution or to the melt
    • D01F1/10Other agents for modifying properties
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F6/00Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
    • D01F6/88Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
    • D01F6/92Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M11/00Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
    • D06M11/73Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof
    • D06M11/76Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with carbon or compounds thereof with carbon oxides or carbonates
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/16General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/02Natural fibres, other than mineral fibres
    • D06M2101/04Vegetal fibres
    • D06M2101/06Vegetal fibres cellulosic
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06MTREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2101/00Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
    • D06M2101/16Synthetic fibres, other than mineral fibres
    • D06M2101/30Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M2101/32Polyesters

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Dispersion Chemistry (AREA)
  • Coloring (AREA)

Abstract

According to the novel warm-keeping functional fabric and the preparation method thereof, through research on the traditional aerogel, the aerogel and polyester fibers are blended into filaments to prepare loose and porous aerogel fibers, the aerogel fibers are blended and woven into the middle layer, and then the middle layer is compounded with the cotton-flax surface layer and the cotton-flax inner layer, so that the prepared fabric is skin-friendly, breathable, comfortable and warm-keeping; the aerogel fiber has high porosity, low thermal conductivity and low density, and the honeycomb structure can store 99.8% of air, so that the heat preservation performance and the comfort of the fiber fabric are further improved, and the weight of the fabric is reduced.

Description

Preparation method of novel warm-keeping functional fabric
Technical Field
The invention relates to the field of novel fabrics, in particular to a preparation method of a novel warm-keeping functional fabric.
Background
Along with the progress and development of society, the material and cultural living standard of people is improved year by year, and the consumption level of clothes is also changed fundamentally. The traditional single clothes can not meet the requirements of people on the variety diversification of clothes any more, but pay more attention to the organic combination of applicability, comfort, health care and safety. At present, the clothing industry has entered an era that is won by new materials, new technologies, new processes and new products, and the fashion change of the clothing will be developed and changed by the innovation of the fabric. In a form of complying with the requirement of the diversified development trend of new textile materials, the research on the manufacturing method of the novel fabric is of great significance.
The aerogel is a porous material with an internal network structure filled with gas and a solid-like appearance with extremely low density, has the characteristics of high porosity, low thermal conductivity, low density and the like, and is very suitable for serving as a thermal insulation material. The honeycomb structure in the aerogel can store 99.8% of air, and can achieve good heat storage and preservation effects; meanwhile, heat conduction and heat convection can be blocked, and a heat insulation effect is achieved; the air permeability of the fabric is higher than that of common velvet materials due to the porosity of the aerogel, and the fabric is comfortable to wear. The existing warm-keeping fabric in the market is thick and heavy, is heavy to wear, has certain oppressive property on the body, and is poor in experience feeling; meanwhile, the thermal clothes have poor air permeability and poor wearing comfort. The combination of aerogel made fibers with traditional fabric fiber layers is a new research direction for solving the above problems.
At present, a novel light breathable, heat-insulating and warm-keeping fabric is urgently needed in the market.
Disclosure of Invention
The invention aims to overcome the defects in the prior art and provides a preparation method of a novel warm-keeping functional fabric.
The invention adopts the following technical scheme for solving the technical problems:
a novel thermal functional fabric is produced by three-thread sweater machine with cotton and linen yarn as face yarn, blended yarn of aerogel fiber and cotton and linen fiber as intermediate yarn, and 10s all cotton yarn as terry yarn.
Further, the specific method for preparing the aerogel fiber is as follows: after the polyester spinning solution is melted, adding the aerogel powder into the spinning solution on line before spinning, and achieving a uniform state; then the aerogel fiber is obtained by spraying out through a spinneret orifice, and then carrying out fiber forming, primary fiber drafting orientation, fiber heat setting and winding.
Furthermore, the fineness of the aerogel fibers is 50D-100D.
Further, the semi-finished fabric has the following specifications: the gram weight is 150-.
Further, the coil length of the semi-finished fabric is 11-12 mm.
The preparation method of the novel warm-keeping functional fabric further comprises the steps of dyeing and finishing, brushing, shearing and operating the semi-finished fabric to obtain the novel warm-keeping functional fabric.
Further, the dyeing and finishing method comprises the following steps:
s1: soaking the woven fabric in a pretreatment liquid containing sodium carbonate and a refined emulsifier, and treating at the temperature of 80-98 ℃ for 15-40 min;
s2: performing acid neutralization on the fabric pretreated in the step S1 at the temperature of 20-40 ℃ for 5-20 min;
s3: dyeing the fabric neutralized by the acid in the step S2;
s4: and (3) carrying out reduction cleaning on the fabric dyed in the step S3 at 80-90 ℃ for 20-30 min, then carrying out acid neutralization at 55-65 ℃ for 10-30 min, finally treating the fabric with crude oil at 20-30 ℃ for 15-20 min, and drying.
Further, the dyeing in the step S3 requires adding a dye-philic leveling agent for treatment for 10-15 min, then adding a dispersant and a disperse dye, adjusting the pH to 4-4.5 with glacial acetic acid, and finally dyeing at 120-140 ℃ for 30-60 min.
Furthermore, the gram weight of the novel thermal functional fabric is less than or equal to 280g/m2
Furthermore, the thickness of the novel warm-keeping functional fabric is 3-5 mm.
Compared with the prior art, the invention has the following advantages:
according to the preparation method of the novel warm-keeping functional fabric, provided by the invention, through the research on the traditional aerogel, the aerogel and polyester fibers are blended into filaments to prepare loose and porous aerogel fibers, the aerogel fibers are blended and woven into the middle layer, and then the middle layer is compounded with the cotton-flax surface layer and the cotton-flax inner layer, so that the prepared fabric is skin-friendly, breathable, comfortable and warm-keeping; the aerogel fiber has high porosity, low thermal conductivity and low density, and the honeycomb structure can store 99.8% of air, so that the heat preservation performance and the comfort of the fiber fabric are further improved, and the weight of the fabric is reduced.
Detailed Description
The present invention is further illustrated by the following examples, which are not to be construed as limiting the invention.
It should be noted that the embodiments and features of the embodiments may be combined with each other without conflict.
Example 1
A method for preparing novel warm-keeping functional fabric adopts a three-line sweater machine to take cotton and linen yarns as face yarns, take blended yarns of aerogel fibers and cotton and linen fibers as intermediate yarns, take 10s all cotton yarns as terry yarns to carry out three-dimensional weaving, weave a fiber aerogel layer by the aerogel fibers with the fineness of 50DD, compound a surface layer and an inner layer through glue on two sides of the intermediate layer, and prepare the fabric with the gram weight of 180g/m2The width of the fabric is 150CM, and the length of the coil is 11 mm.
The preparation method of the novel warm-keeping functional fabric further comprises the steps of dyeing and finishing, brushing, shearing and operating the semi-finished fabric to obtain the fabric with the gram weight of 250g/m2(ii) a The thickness of the novel warm-keeping functional fabric is 3 mm.
As a preferred embodiment, the dyeing and finishing method is as follows:
s1: soaking the woven fabric in a pretreatment liquid containing sodium carbonate and a refined emulsifier, and treating at 80 ℃ for 15 min;
s2: performing acid neutralization on the fabric pretreated in the step S1 at the temperature of 20 ℃ for 5 min;
s3: dyeing the fabric neutralized by the acid in the step S2;
s4: and (4) carrying out reduction cleaning on the fabric dyed in the step S3 at 80 ℃ for 20min, then carrying out acid neutralization at 55 ℃ for 10min, finally treating the fabric at 20 ℃ for 15min by using wool oil, and drying.
As a preferred example, the dyeing in step S3 requires adding a dye-philic leveling agent for 10min, then adding a dispersant and a disperse dye, adjusting pH to 4 with glacial acetic acid, and dyeing at 120 deg.C for 30 min.
Example 2
A method for preparing novel warm-keeping functional fabric adopts a three-line sweater machine to take cotton and linen yarns as face yarns, take blended yarns of aerogel fibers and cotton and linen fibers as intermediate yarns, take 10s all cotton yarns as terry yarns to carry out three-dimensional weaving, weave a fiber aerogel layer by the aerogel fibers with the fineness of 50DD, compound a surface layer and an inner layer through glue on two sides of the intermediate layer, and prepare 160/M gram weight2And the width 152CM and the length of the coil are 11 mm.
The preparation method of the novel warm-keeping functional fabric further comprises the steps of dyeing and finishing, brushing, shearing and operating the semi-finished fabric to obtain the fabric with the gram weight of 260g/m2(ii) a The thickness of the novel warm-keeping functional fabric is 5 mm.
As a preferred embodiment, the dyeing and finishing method is as follows:
s1: soaking the woven fabric in a pretreatment liquid containing sodium carbonate and a refined emulsifier, and treating at 80 ℃ for 15 min;
s2: performing acid neutralization on the fabric pretreated in the step S1 at the temperature of 20 ℃ for 5 min;
s3: dyeing the fabric neutralized by the acid in the step S2;
s4: and (4) carrying out reduction cleaning on the fabric dyed in the step S3 at 80 ℃ for 20min, then carrying out acid neutralization at 55 ℃ for 10min, finally treating the fabric at 20 ℃ for 15min by using wool oil, and drying.
As a preferred example, the dyeing in step S3 requires adding a dye-philic leveling agent for 10min, then adding a dispersant and a disperse dye, adjusting pH to 4 with glacial acetic acid, and dyeing at 120 deg.C for 30 min.
Example 3
A method for preparing novel warm-keeping functional fabric adopts a three-thread sweater machine to take cotton and linen yarns as face yarns, take blended yarns of aerogel fibers and cotton and linen fibers as intermediate yarns, take 10s all cotton yarns as terry yarns to carry out three-dimensional weaving, weave a fiber aerogel layer by the aerogel fibers with the fineness of 50DD, compound a surface layer and an inner layer through glue on two sides of the intermediate layer, and prepare the fabric with the gram weight of 170/M2The width of the fabric is 150CM, and the length of the coil is 12 mm.
The preparation method of the novel warm-keeping functional fabric further comprises the steps of dyeing and finishing, brushing, shearing and operating the semi-finished fabric to obtain the fabric with the gram weight of 270g/m2(ii) a The thickness of the novel warm-keeping functional fabric is 3 mm.
As a preferred embodiment, the dyeing and finishing method is as follows:
s1: soaking the woven fabric in a pretreatment liquid containing sodium carbonate and a refined emulsifier, and treating at 80 ℃ for 15 min;
s2: performing acid neutralization on the fabric pretreated in the step S1 at the temperature of 20 ℃ for 5 min;
s3: dyeing the fabric neutralized by the acid in the step S2;
s4: and (4) carrying out reduction cleaning on the fabric dyed in the step S3 at 80 ℃ for 20min, then carrying out acid neutralization at 55 ℃ for 10min, finally treating the fabric at 20 ℃ for 15min by using wool oil, and drying.
As a preferred example, the dyeing in step S3 requires adding a dye-philic leveling agent for 10min, then adding a dispersant and a disperse dye, adjusting pH to 4 with glacial acetic acid, and dyeing at 120 deg.C for 30 min.
The foregoing detailed description of the preferred embodiments of the invention has been presented. It should be understood that numerous modifications and variations could be devised by those skilled in the art in light of the present teachings without departing from the inventive concepts. Therefore, the technical solutions that can be obtained by a person skilled in the art through logic analysis, reasoning or limited experiments based on the prior art according to the concept of the present invention should be within the scope of the claims of the present invention.

Claims (10)

1. A preparation method of a novel warm-keeping functional fabric is characterized in that a three-thread sweater machine is adopted, cotton and linen yarns are used as face yarns, blended yarns of aerogel fibers and cotton and linen fibers are used as intermediate yarns, and 10s all cotton yarns are used as loop yarns to be subjected to three-dimensional weaving to obtain a semi-finished fabric.
2. The method according to claim 1, wherein the aerogel fibers are prepared by the following specific method: after the polyester spinning solution is melted, adding the aerogel powder into the spinning solution on line before spinning, and achieving a uniform state; then the aerogel fiber is obtained by spraying out through a spinneret orifice, and then carrying out fiber forming, primary fiber drafting orientation, fiber heat setting and winding.
3. The preparation method according to claim 1, wherein the fineness of the aerogel fibers is 50D to 100D.
4. The method of manufacturing of claim 1, wherein the semi-finished shell fabric specifications are: grammes weight of 150-200G/M2Breadth 150-.
5. The manufacturing method according to claim 1, wherein the coil length of the semi-finished fabric is 11-12 mm.
6. The preparation method of the novel thermal functional fabric according to claims 1 to 5, further comprising the steps of dyeing and finishing the semi-finished fabric, brushing and shearing to obtain the novel thermal functional fabric.
7. The preparation method of claim 6, wherein the dyeing and finishing method comprises the following steps:
s1: soaking the woven fabric in a pretreatment liquid containing sodium carbonate and a refined emulsifier, and treating at the temperature of 80-98 ℃ for 15-40 min;
s2: performing acid neutralization on the fabric pretreated in the step S1 at the temperature of 20-40 ℃ for 5-20 min;
s3: dyeing the fabric neutralized by the acid in the step S2;
s4: and (3) carrying out reduction cleaning on the fabric dyed in the step S3 at 80-90 ℃ for 20-30 min, then carrying out acid neutralization at 55-65 ℃ for 10-30 min, finally treating the fabric with crude oil at 20-30 ℃ for 15-20 min, and drying.
8. The preparation method according to claim 6, wherein the dyeing in step S3 requires adding a dye-philic leveling agent for 10-15 min, then adding a dispersant and a disperse dye, adjusting pH to 4-4.5 with glacial acetic acid, and finally dyeing at 120-140 ℃ for 30-60 min.
9. The preparation method of claim 6, wherein the grammage of the novel thermal functional fabric is less than or equal to 280g/m2
10. The preparation method of claim 6, wherein the thickness of the novel thermal functional fabric is 3mm to 5 mm.
CN202010881371.0A 2020-08-27 2020-08-27 Preparation method of novel warm-keeping functional fabric Pending CN112030316A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114214775A (en) * 2021-12-27 2022-03-22 山东兰雁纺织服装有限公司 Multifunctional jean fabric and preparation method thereof
WO2023280087A1 (en) * 2021-07-09 2023-01-12 武汉格物感知信息科技有限公司 Thermal management fabric, preparation method therefor, and application thereof

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JP6641061B1 (en) * 2019-11-14 2020-02-05 株式会社コゼットクリエーション Airgel-containing laminated sheet and method for producing aerogel-containing laminated sheet
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2023280087A1 (en) * 2021-07-09 2023-01-12 武汉格物感知信息科技有限公司 Thermal management fabric, preparation method therefor, and application thereof
CN114214775A (en) * 2021-12-27 2022-03-22 山东兰雁纺织服装有限公司 Multifunctional jean fabric and preparation method thereof

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Application publication date: 20201204