CN106167735A - A kind of former odor type Folium Perillae edible vegetable blend oil and production technology thereof - Google Patents
A kind of former odor type Folium Perillae edible vegetable blend oil and production technology thereof Download PDFInfo
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- CN106167735A CN106167735A CN201610513888.8A CN201610513888A CN106167735A CN 106167735 A CN106167735 A CN 106167735A CN 201610513888 A CN201610513888 A CN 201610513888A CN 106167735 A CN106167735 A CN 106167735A
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- oil
- perillae
- edible vegetable
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/007—Other edible oils or fats, e.g. shortenings, cooking oils characterised by ingredients other than fatty acid triglycerides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23D—EDIBLE OILS OR FATS, e.g. MARGARINES, SHORTENINGS, COOKING OILS
- A23D9/00—Other edible oils or fats, e.g. shortenings, cooking oils
- A23D9/02—Other edible oils or fats, e.g. shortenings, cooking oils characterised by the production or working-up
- A23D9/04—Working-up
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/06—Production of fats or fatty oils from raw materials by pressing
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Microbiology (AREA)
- Edible Oils And Fats (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention provides a kind of former odor type Folium Perillae edible vegetable blend oil and production technology thereof, comprising: the Fructus Perillae being used for preparing former odor type Folium Perillae edible vegetable blend oil is cleared up and bakes seed, obtain the Fructus Perillae processed through roasting seed；Carry out respectively other oil plants clearing up and quenched, obtain conditioned oil plant；Measure Fructus Perillae and the oil content of other oil plants, fatty acid composition and content respectively；Fructus Perillae and other oil plants respective cold pressing oil yield is determined by bench-scale testing, then according to the one-tenth of predetermined Folium Perillae edible vegetable blend oil is grouped into each plant demand calculating Fructus Perillae and other oil plants, by this consumption, Fructus Perillae and other oil plants are mixed again, obtain mixing oil plant；Mixing oil plant is carried out cold pressing, obtains crude oil and grouts；Crude oil is carried out fine straining, obtains cold pressing mixed oil；In cold pressing mixed oil, add natural Vitamin E or tert-butylhydroquinone, then carry out fatty acid composition and content detection, obtain former odor type Folium Perillae edible vegetable blend oil.
Description
Technical field
The present invention relates to a kind of former odor type Folium Perillae edible vegetable blend oil and production technology thereof, belong to Oil processing technology neck
Territory.
Background technology
Shi Kerong, Zhang Zhaowei demonstrate vegetalitas omega-3 fatty acid in " science edible vegetable oil " book and have improvement note
Recall, reduce blood fat, reduce blood glucose, prevent and treat inflammation and cancer physiological function (Shi Kerong, Zhang Zhaowei, 2015, science
Edible vegetable oil, Beijing, Science Press: 25-38)；Meanwhile, it is also analyzed, elaborates the excellent of ten kinds of common edible vegetable oils
Shortcoming (Shi Kerong, Zhang Zhaowei, 2015, science edible vegetable oil, Beijing, Science Press: 84-107), and point out: whether
A lot of people like Oleum Helianthi, the Semen Maydis that Oleum Arachidis hypogaeae semen consumption proportion the most in recent years edible, flavour giving off a strong fragrance constantly rises
All there is the significant deficiency that omega-3 fatty acid is almost nil in oil and thing from abroad olive oil；Although Oleum Perillae, Semen Lini oil contain
Abundant omega-3 fatty acid, but, because its oxidation stability is the poorest, use general processing technique to be difficult to produce safety approval
Product.
Just because of above-mentioned reason, in recent years, occur in that the research report much about Folium Perillae edible vegetable blend oil.Relevant
Typical patent has " a kind of edible health-care oil rich in Oleum Perillae " (Zhou Siming, CN101044875A), " a kind of compound Folium Perillae
Oil formulation and production method thereof " (Zhuan Zongjie, Wei kezhou, Zhuan Huijun, CN1370564A), " Folium Perillae oils and fats and preparation method thereof and
Application " (Li Junlin, CN1271187A), " a kind of Fructus Perillae edible vegetable blend oil rich in essential fatty acid and vitaminF "
(Gao Yinglin, Liu Baolin, CN102113575A).The technical scheme that above-mentioned prior art is announced is essentially all uses it by perilla oil
His vegetable oil is simply in harmonious proportion, dilutes, and in mixed oil, the percentage by weight of Oleum Perillae is general all between 10%-70%, but,
Solve not yet rich in the polyunsaturated fatty acid edible vegetable oil oxidation-stabilized sex chromosome mosaicism in harmonic process.
Patent " a kind of perilla oil and preparation method thereof " (Wang Zhaohai, CN103689125A) discloses a kind of by 70-
78% Oleum Glycines, 0.05-0.12% Folium perillae extract, 0.03-0.1% citric acid monoglyceride, the comprehensive flavouring agent of 2.5-5%, 16-
The technical scheme of the perilla oil of the composition such as 20% Oleum Perillae.Although this technical scheme has the fragrance of perilla oil, but, should
Technology does not accounts for the oxidation-stabilized sex chromosome mosaicism of polyunsaturated fatty acid yet.
By in depth studying discovery, inventor is in patent " a kind of double-deck edible vegetable blend oil with balanced and preparation side thereof
Method " (Shi Kerong, CN 104585355 A) has fully taken into account at polyunsaturated fatty acid (especially alpha-linolenic acid)
In the case of content high (alpha-linolenic acid is not less than 10%), the oxidation-stabilized sex chromosome mosaicism of edible vegetable blend oil, and take phase
The technical measures answered, and, the oxidation stability of final products brings up to be better than the level of part list product oil.But, giving birth to
Produce in practice and find, due to be used for preparing single product oil source of edible vegetable blend oil is different, processing method different and transport,
The impact of storage condition, before preparing mixed oil, there is certain problem in the oxidation stability of himself, no matter causing
In allocation process, how to use strictly protective measure, all can have influence on the qualification rate of final products.This just gives big rule undoubtedly
Mould produces and brings the biggest difficulty, and causes economic loss and the wasting of resources of enterprise.It addition, inventor is in conventional experiment
In research, be all use cold Semen Lini or cold pressed flax seed oil as the main source of omega-3 fatty acid, this is because cold pressing Caulis et Folium Lini
The main volatile ingredient of seed oil is based on alcohols material, and comparatively speaking, in hot moulding Semen Lini oil volatile ingredient, alcohols material is relative
Content declines, and a large amount of maillard reaction product furfural occurs and based on pyrazine, pyrroles, the heteroaromatic compound of pyridine,
Causing aldehydes and heterocyclic material relative amount quickly to raise, it is strong that these feature volatile ingredients give hot moulding Semen Lini oil
Abnormal smells from the patient, but, these heteroaromatic compounds and complex thereof have certain toxic action, therefore shadow to human physiological functions
The loud edible safety to hot moulding Semen Lini oil (Yang Jine, Huang Qingde, Zhou Qi, 2013, cold pressing and hot moulding Semen Lini oil volatility
Comparison of ingredients, China's oil crop journal), but, the palatability of cold pressed flax seed oil does not has hot moulding Caulis et Folium Lini hemp seed oil good exactly.
And cold pressing Oleum Perillae does not contain only the useful Polyphenols volatile substance of up to more than 11 kinds, simultaneously possibly together with rosmarinic acid,
4',5,7-trihydroxyflavone and luteolin etc. (Wu harasses, Ma Fei, Zhang Liangxiao etc., and 2015, high performance liquid chromatography-tandem mass method measures Fructus Perillae
11 kinds of phenolic compounds, analytical chemistry in oil), but, these fragrance matters are after cold pressing, although being all present in perilla oil,
But its fragrance still can not allow people feel out.
Summary of the invention
In order to solve above-mentioned shortcoming and defect, it is an object of the invention to provide a kind of former odor type Folium Perillae food plant and adjust
Production technology with oil.
The present invention also aims to provide the former odor type Folium Perillae food plant prepared by above-mentioned production technology to be in harmonious proportion
Oil.
For reaching above-mentioned purpose, on the one hand, the present invention provides the production work of a kind of former odor type Folium Perillae edible vegetable blend oil
Skill, it comprises the following steps:
(1) Fructus Perillae being used for preparing former odor type Folium Perillae edible vegetable blend oil cleared up successively and baked seed, obtaining
Through the Fructus Perillae that roasting seed processes；
(2) carry out respectively clearing up and quenched to other oil plants being used for preparing former odor type Folium Perillae edible vegetable blend oil,
To through quenched oil plant；
(3) measure described being used for respectively and prepare the Fructus Perillae of former odor type Folium Perillae edible vegetable blend oil and containing of other oil plants
Oil mass, fatty acid composition and content；Determine Fructus Perillae and other oil plants respective cold pressing oil yield by bench-scale testing, then press
It is grouped into according to the one-tenth of predetermined Folium Perillae edible vegetable blend oil to calculate and described is in harmonious proportion for preparing former odor type Folium Perillae food plant
The Fructus Perillae of oil and each plant demand of other oil plants, then by this consumption by the Fructus Perillae processed through roasting seed and through quenched its
He mixes by oil plant, obtains mixing oil plant；
(4) mixing oil plant is carried out cold pressing, obtain crude oil and grouts；
(5) crude oil is carried out fine straining, obtain cold pressing former odor type Folium Perillae edible vegetable blend oil；
(6) in cold pressing former odor type Folium Perillae edible vegetable blend oil, natural Vitamin E or tert-butylhydroquinone are added, so
After carry out fatty acid composition and content detection, obtain described former odor type Folium Perillae edible vegetable blend oil；
Wherein, other oil plants described include the one in Semen Brassicae campestris, sunflower seed, Fructus Maydis and Non-transgenic soybean or several
The combination planted.
According to production technology of the present invention, it is preferable that other oil plants described include Semen Brassicae campestris, sunflower seed and corn germ
Bud.
According to production technology of the present invention, it is preferable that in step (1), (2), described cleaning is in such a way
Carry out:
The size of the seed according to Fructus Perillae and other oil plants for preparing former odor type Folium Perillae edible vegetable blend oil, will
Fructus Perillae and other oil plants are delivered to selecting crude drugs with winnower respectively, screen out in combination unit, to remove dust, light materials, to screen out broken seed
Grain, immature seed, screen out bigger material；
Wherein Fructus Perillae and other oil plants time of staying in combination unit are the 10-60 second, and thickness is 5-20 millimeter.
Fructus Perillae and other oil plants are first carried out fatty acid composition in oil content and oils and fats after cleaning more respectively to it
Mensuration with content, it is possible to ensure the accuracy of follow-up mixing match.
According to production technology of the present invention, light materials involved in step (1), (2) scale removal process refers to oil plant
Plant broken blade, and bigger material refers to oilseed plant stem and leaf.
According to production technology of the present invention, it is preferable that in step (1),
The roasting seed temperature of described Fructus Perillae is 120-170 DEG C, and the roasting seed time is 10-45 minute；It is highly preferred that roasting seed temperature
For 130-160 DEG C, the roasting seed time is 15-30 minute；It is further preferred that roasting seed temperature is 140-150 DEG C, the roasting seed time is
20-25 minute.Described roasting seed operation is implemented in Oil processing common apparatus.
According to production technology of the present invention, it is preferable that in step (2),
The refining temperature of described Semen Brassicae campestris, sunflower seed and Fructus Maydis is 25-85 DEG C, and moisture is 6wt%-
10wt%, it is highly preferred that refining temperature is 55-80 DEG C, moisture is 6wt%-9wt%；It is further preferred that refining temperature
For 65-80 DEG C, moisture is 7wt%-8wt%；
The refining temperature of described Non-transgenic soybean is 35-55 DEG C, and moisture is 6wt%-10wt%；It is highly preferred that
Refining temperature is 35-50 DEG C, and moisture is 6wt%-9wt%；It is further preferred that refining temperature be 45-50 DEG C, moisture contains
Amount is 7wt%-8wt%.
According to production technology of the present invention, in step (2), every kind of oil plant (Semen Allii Tuberosi, sunflower seed, Fructus Maydis or
Non-transgenic soybean) conditioning period be 20-35 minute.Described quenched realization in modifying device.This modifying device
The conventional equipment used for this area.
According to production technology of the present invention, it is preferable that the mixing described in step (3) also includes pre-compounding process, and this is pre-
Sneak out journey to carry out according to step in detail below:
The consumption oil plant less than 33wt% is first mixed, obtains premix material；Then, then by consumption higher than 33wt%'s
Oil plant mixes with described premix material, obtains described mixing oil plant.
According to production technology of the present invention, " consumption oil plant less than 33wt% " in pre-compounding process includes Fructus Perillae
And/or other oil plants, " consumption oil plant higher than 33wt% " also includes Fructus Perillae and/or other oil plants.
According to production technology of the present invention, the present invention is higher than the oil plant of 33wt% with premix material therebetween to consumption
Consumption proportion do not make specific requirement, those skilled in the art can need to select suitable consumption proportion according to field operation.
According to production technology of the present invention, because determining the most respectively in step (3) for preparing described former perfume (or spice)
The Fructus Perillae of type Folium Perillae edible vegetable blend oil and the oil content of other oil plants, fatty acid composition and content, and with trying on a small scale
Test and determine Fructus Perillae and other oil plants respective cold pressing oil yield, then adjust according still further to predetermined former odor type Folium Perillae food plant
With the becoming to be grouped into and calculate the described Fructus Perillae for producing former odor type Folium Perillae edible vegetable blend oil and other oil plants of oil
Each plant demand, and carry out oil plant mixing according to this consumption, thus ensure that the cold pressing former odor type Folium Perillae food that this production technology obtains
Qualification rate with plant blend oil product 100%.
According to production technology of the present invention, in step (3): be used for producing described former odor type described in measuring respectively purple
The Fructus Perillae of Soviet Union's edible vegetable blend oil and the oil content of other oil plants, fatty acid composition and content, test with small-scale cold pressing
Determine Fructus Perillae and other oil plants respective cold pressing oil yield, then according to predetermined former odor type Folium Perillae edible vegetable blend oil
Become to be grouped into calculate described for producing Fructus Perillae and the consumption of other oil plants of former odor type Folium Perillae edible vegetable blend oil, so
After mix.
Wherein, described oil content is measured according to the requirement of GB/T14488.1, described fatty acid composition and content according to
The requirement of GB/T 17376 and GB/T 17377 is measured.Oil plant (Fructus Perillae and other oil plants) proportioning of the present invention is based on
The measurement result of various oil plant oil content, cold pressing oil yield and fatty acid composition and content carries out calculated, this calculating
As a result, it is in the case of cold pressing process parameter constant, after carrying out the single factor experiment of different ratio, obtains optimum proportioning.
According to production technology of the present invention, in step (3), carry out premixed operation before mixing and oil plant can be made to mix
Close more abundant；Described premixed operation and married operation are all at oil plant insulation conveying and mixing arrangement (Authorization Notice No. CN
Realize in 205055869U).The premixed operation of the present invention and married operation all enter in mixing arrangement in oil plant insulation conveying
OK, can fundamentally solve the problem of oxidation of former odor type Folium Perillae edible vegetable blend oil, increase the stability of product.
According to production technology of the present invention, the insulation conveying of described oil plant and mixing arrangement include the oil plant storage that can be incubated
Tank, the outlet of described oil storage tank is connected to the entrance of an oil plant conveying auger that can be incubated, going out of described oil plant conveying auger
Mouth connects a stirring storage tank that can be incubated, and described stirring tank inside is provided with agitating device.
The insulation conveying of described oil plant includes substrate oil storage tank and regulation oil storage tank, institute with the oil storage tank of mixing arrangement
State and on the outer wall of substrate oil storage tank, be provided with the first vacuum interlayer that can be incubated, the outer wall of described regulation oil storage tank is arranged
Having the second vacuum interlayer that can be incubated, the outlet of described substrate oil storage tank and described regulation oil storage tank is all defeated with described oil plant
The entrance sending auger connects.
The insulation of described oil plant carries the outlet of substrate oil storage tank with mixing arrangement and entering of described oil plant conveying auger
The first oil plant flow-control lock it is provided with, the outlet of described regulation oil storage tank and the entrance of described oil plant conveying auger between Kou
Between be provided with the second oil plant flow-control lock.
The substrate oil storage tank of the insulation conveying of described oil plant and mixing arrangement and the volume size of described regulation oil storage tank
Ratio is 2.5～3.5:1, and the thickness range of described first vacuum interlayer and described second vacuum interlayer is 20～60 millimeters.
The insulation of described oil plant carries the first oil plant flow-control lock with mixing arrangement and described second oil plant flow-control
All mark is divided with 0～6 etc. on lock.
The insulation conveying of described oil plant and the agitating device of mixing arrangement include that can rotate with the central shaft being vertically arranged, straight
The most tapered umbrella watt slot type structure, the upper surface of described umbrella watt slot type structure include multiple along bus arrange watt
Groove, multiple described watt grooves are uniformly distributed along the circumference of described umbrella watt slot type structure, and described stirring storage tank top is provided with auger
Connector, the lower edge of described auger connector is positioned at the surface of described watt groove outer；The central shaft of described oil plant conveying auger
Angle between the central axis of line and described umbrella watt slot type structure is 30～60 °.
The bus of the umbrella watt slot type structure of the insulation conveying of described oil plant and mixing arrangement and described umbrella watt slot type structure
Central axis between angle be 50～70 °.
The insulation conveying of described oil plant is provided with, on the outer wall of the stirring storage tank of mixing arrangement, the 3rd vacuum clip that can be incubated
Layer, described stirring storage tank includes the end socket being arranged at top and the cone the most tapered with the diameter that described end socket is connected, described
Being provided with described auger connector on end socket, the outlet at bottom of described cone is provided with the 3rd oil plant flow-control lock.
The bottom of the umbrella watt slot type structure of the insulation conveying of described oil plant and mixing arrangement is positioned at the top of described cone, institute
State umbrella watt slot type structure the base diameter that base diameter is described end socket 70～90%.
The insulation conveying of described oil plant is 20～60 millimeters with the thickness range of the 3rd vacuum interlayer of mixing arrangement, described cone
The drift angle scope of body is 50～80 °.
According to production technology of the present invention, it is preferable that in step (4), described cold pressing is carried out in such a way:
Mixing oil plant is delivered to cold pressing device 20-35 DEG C, carry out cold pressing processing under the conditions of 25-35MPa, until should
Criticize mixing oil plant all to process, then complete cold pressing processing.
According to production technology of the present invention, it is preferable that in step (5), described fine straining is carried out in such a way:
Crude oil cold pressing obtained is delivered in microporous filter carry out fine straining, the wherein pore of polyamide microporous membrane
Footpath is 10-25 micron；Fine straining Oil-temperature control is at 50-80 DEG C, and operation pressure is 0.1-0.6MPa.Fine straining of the present invention is processed
Persistently to carry out, till this batch whole fine straining of cold pressing crude oil completes.
According to production technology of the present invention, it is preferable that in step (5), in described fine straining step, it is passed through nitrogen
Carry out oxygen barrier protection；
It is highly preferred that the consumption of described nitrogen controls as 1-10L/min.
According to production technology of the present invention, the certified products obtained by step (6), again through fill, i.e. can be become
Product.
According to production technology of the present invention, it is preferable that in step (6), eat with described cold pressing former odor type Folium Perillae
The quality meter of plant blend oil, the addition of described natural Vitamin E is 1g/Kg, the addition of described tert-butylhydroquinone
For 0.1g/Kg.
According to production technology of the present invention, the present invention is in the following process obtaining crude oil, and omnidistance employing pours nitrogen
The mode of gas carries out oxygen barrier protection to high unsaturated fatty acid therein.
According to production technology of the present invention, wherein, described selecting crude drugs with winnower, screen out combination unit, modifying device, roasting seed dress
Put, cold pressing device, microporous filter are the conventional equipment of this area, and those skilled in the art can be according to field operation need
Said apparatus is rationally selected, as long as being capable of goal of the invention.
According to production technology of the present invention, the one-tenth of described former odor type Folium Perillae edible vegetable blend oil be grouped into meet with
Lower condition: be in terms of 100% by the gross weight of described former odor type Folium Perillae edible vegetable blend oil, omega-3 fatty acid content and remaining fat
Fat acid content all meets food safety company standard " the former fragrant edible blend oil of Folium Perillae " Q/SHHF 0007S-2014 individual features and refers to
Target requirement.
On the other hand, present invention also offers a kind of production technology by above-mentioned former odor type Folium Perillae edible vegetable blend oil raw
Produce the former odor type Folium Perillae edible vegetable blend oil obtained, wherein, with the gross weight of this former odor type Folium Perillae edible vegetable blend oil be
100% meter, omega-3 fatty acid and remaining content of fatty acid all meet the requirement of Q/SHHF 0007S-2014 individual features index.Its
In, described " remaining fatty acid " includes linoleic acid, oleic acid, stearic acid, Palmic acid.
At present, prior art not yet breaks through the oxidation-stabilized sex chromosome mosaicism of polyunsaturated fatty acid, especially omega-3 fatty acid,
This be also prior art product in one of the highest reason of omega-3 fatty acid content.First, what the present invention used is not the most anti-
Exposing aerial finished product edible vegetable oil again is raw material, but uses under shell and protein molecule are tightly protected
Fresh plant oil seed is that former odor type Folium Perillae edible vegetable blend oil directly prepared by raw material.On the one hand this avoid mediation substrate
Finished product vegetable oil and regulation vegetable oil oxidative rancidity problem in storage, transport, harmonic process, on the other hand, the present invention is raw
The Natural antioxidant in the former odor type Folium Perillae edible vegetable blend oil of output can increase considerably the oxidation stability of product.
Secondly, former odor type Folium Perillae edible vegetable blend oil production technology provided by the present invention is directly to use mixing oil plant
Carry out the processing of edible vegetable blend oil, so, make the two kinds high unsaturated essential fatty acid (ω 6 being present in oilseed
With ω 3), owing to it has a protection of oil plant cell, thus avoid be prepared as edible vegetable oil respectively after storing, transporting, adjusting
Oxidative rancidity problem during joining.
Additionally, the present invention uses after first individually Fructus Perillae being baked seed, then carry out the processing technique of mixing squeezing, technology controlling and process
Upper guarantee Fructus Perillae does not bursts during roasting seed, thus ensure that omega-3 fatty acid is not oxidized, meanwhile, in follow-up mixing
Expressing process makes the fragrance matter in Fructus Perillae enter in oil, make the Folium Perillae edible vegetable blend oil prepared have perfume (or spice)
Taste.
In the former odor type Folium Perillae edible vegetable blend oil that the present invention prepares, not only fatty acid composition meets food safety
Company standard " the former fragrant edible blend oil of Folium Perillae " Q/SHHF 0007S-2014 requirement, and it has the distinctive fragrance of perilla oil
And oxidation stability is preferable, it is a kind of can to equalize the delicious food of supplementary omega-3 fatty acid, healthy oil product.
Accompanying drawing explanation
Fig. 1 is the technological process of production schematic diagram of the former odor type Folium Perillae edible vegetable blend oil of the embodiment of the present invention 1；
Fig. 2 is the technological process of production schematic diagram of the former odor type Folium Perillae edible vegetable blend oil of the embodiment of the present invention 2；
Fig. 3 is the technological process of production schematic diagram of the former odor type Folium Perillae edible vegetable blend oil of the embodiment of the present invention 3；
Fig. 4 is the electrical conductivity relation with the time of the former odor type Folium Perillae edible vegetable blend oil that the embodiment of the present invention 1 obtains
Curve chart；
Fig. 5 is the electrical conductivity relation with the time of the former odor type Folium Perillae edible vegetable blend oil that the embodiment of the present invention 2 obtains
Curve chart；
Fig. 6 is the electrical conductivity relation with the time of the former odor type Folium Perillae edible vegetable blend oil that the embodiment of the present invention 3 obtains
Curve chart.
Detailed description of the invention
In order to the technical characteristic of the present invention, purpose and beneficial effect are more clearly understood from, in conjunction with in detail below
Technical scheme is carried out described further below by embodiment and Figure of description, but it is not intended that to the present invention can
The restriction of practical range.
Test case 1
This test case carries out roasting seed process, to determine to the Fructus Perillae being used for preparing former odor type Folium Perillae edible vegetable blend oil
The technological parameter of roasting seed, such as: roasting seed temperature, roasting seed time；Wherein, described roasting seed operation is real in Oil processing common apparatus
Executing, the concrete operations of roasting seed are also the conventional means of this area, are not repeated herein.
Through orthogonal test, determine that the optimal roasting seed time is 20-25 minute, under conditions of the roasting seed time is 25 minutes, really
Surely baking seed temperature, it is as shown in table 1 that Fructus Perillae bakes seed experimental result；
Table 1 Fructus Perillae bakes seed experimental result
During from table 1 it follows that roasting seed temperature is 120-170 DEG C, after roasting seed, Fructus Perillae seed is complete；But temperature is relatively
Time low, after roasting seed, fragrance is thin, and when temperature is higher, can produce burnt odor taste after roasting seed.It can also be seen that work as from table 1
When temperature is higher than 170 DEG C, after roasting seed, Fructus Perillae can burst；Therefore, to sum up experimental result, the Fructus Perillae of the application bakes seed
Optimum temperature is 140-150 DEG C, and the roasting seed time is 20-25 minute.
Embodiment 1
Present embodiments provide a kind of former with fresh Fructus Perillae, Semen Brassicae campestris, sunflower seed and Fructus Maydis for raw material production
The method of odor type Folium Perillae edible vegetable blend oil, its technological process is as it is shown in figure 1, specifically include following steps:
Fructus Perillae, Semen Brassicae campestris, sunflower seed and Fructus Maydis are delivered to respective cleaning plant (selecting crude drugs with winnower, screen out combination dress
Put) in carry out dedusting, remove impurity cleaning, the oil plant time of staying in a device is 10 seconds, and thickness is 5 millimeters；
Then, in addition to Fructus Perillae, then it is delivered to respective modifying device is carried out quenched respectively, the refining temperature of Semen Brassicae campestris
Be 65 DEG C, adjust to moisture be 7%；The refining temperature of sunflower seed and Fructus Maydis is 65 DEG C, adjusts to moisture and is
7%；
Fructus Perillae after cleaning is transported in roasting seed device carry out roasting seed, and the roasting seed temperature of Fructus Perillae is 120 DEG C, the time
It it is 45 minutes；
Separately sampled, measure fatty acid composition and content by the requirement of GB/T 17376 and GB/T 17377, by GB/
The requirement of T14488.1 measures oil content and carries out cold pressing test on a small scale and determine that respective cold pressing oil yield (obtains weight of oil ÷
Oil plant weight × 100%), the mixing match of various oil plant is then calculated by the requirement of table 2, result is as shown in table 3.As not having
Specified otherwise, content of the present invention is " weight percentage ".
Table 2 company standard " the former fragrant edible vegetable blend oil of Folium Perillae " fatty acid composition characteristic index
Table 3 detects and result of calculation
By the result of calculation in table 3, weigh 500 kg of oil Semen Allii Tuberosi, 180 kilograms of Fructus Perillae, 180 kilograms of sunflower seeds, 140,000
Gram Fructus Maydis；First use oil plant insulation conveying with mixing arrangement (Authorization Notice No. CN 205055869U) by Fructus Perillae, sunflower
Seed, Fructus Maydis premix, and press the velocity ratio (volume ratio) of 1:1 (premix material: Semen Brassicae campestris) the most again by premix material and Brassica campestris L
Seed mixes with mixing arrangement in oil plant insulation conveying, it is ensured that various oil plant mix homogeneously, obtains mixing oil plant；
Mixing oil plant after mix homogeneously is delivered to cold pressing expeller, 20 DEG C, carry out cold pressing processing under the conditions of 25MPa.Will
The crude oil obtained is delivered in microporous filter, carries out fine straining, and polyamide microporous membrane (PA) capillary aperture is 25 microns, fine straining
Oil-temperature control is at 50 DEG C, and operation pressure is 0.1MPa, meanwhile, pours nitrogen with the speed of 1 liter/min；Obtain cold through fine straining
Squeeze former odor type Folium Perillae edible vegetable blend oil；
Fatty acid composition and content, result such as table 4 institute of product is measured by the requirement of GB/T 17376 and GB/T 17377
Show.
Table 4 former odor type Folium Perillae edible vegetable blend oil fatty acid compositional analysis result
| Cold pressing former odor type Folium Perillae edible vegetable blend oil | |
| Linoleic acid content (%) | 37.00 |
| Alpha-linolenic acid content (%) | 15.09 |
| Oleic acid content (%) | 38.82 |
| Stearate acid content (%) | 4.23 |
| Palmitic acid content (%) | 4.76 |
| AOM value (hour) | 15.79 |
As can be seen from Table 4, the present embodiment produces the former odor type Folium Perillae edible vegetable blend oil obtained is qualified products.Adopt
The oxidation stability of the former odor type Folium Perillae edible vegetable blend oil that the present embodiment prepares is measured by method well known in the art
(AOM value), the electrical conductivity of the former odor type Folium Perillae edible vegetable blend oil that the present embodiment obtains and graph of relation such as Fig. 4 of time
Shown in, figure 4, it is seen that its oxidation stability (AOM value) can reach 15.79 hours.
In Fig. 4 to Fig. 6, the change of the passage oils and fats electrical conductivity of the time that is as that conductivity variations line represents, vertically
Straight line be the marking line of peak, Trendline is that instrument automatically generates.
Embodiment 2
Present embodiments provide a kind of with fresh Semen Brassicae campestris, Fructus Perillae, sunflower seed for raw material prepare former odor type Folium Perillae food
By the method for plant blend oil, its technological process is as in figure 2 it is shown, specifically include following steps:
Semen Brassicae campestris, Fructus Perillae and sunflower seed are delivered to respectively in respective cleaning plant (selecting crude drugs with winnower, screen out combination unit)
Carrying out dedusting, remove impurity cleaning, the oil plant time of staying in a device is 10 seconds, and thickness is 5 millimeters；
Then, in addition to Fructus Perillae, then it is delivered to respective modifying device is carried out quenched respectively, the refining temperature of Semen Brassicae campestris
Be 65 DEG C, adjust to moisture be 7%；The refining temperature of sunflower seed is 65 DEG C, adjust to moisture be 7%；Will cleaning
After Fructus Perillae be transported in roasting seed device carry out roasting seed, the roasting seed temperature of Fructus Perillae is 140 DEG C, and the time is 25 minutes.
Separately sampled, measure fatty acid composition and content by the requirement of GB/T 17376 and GB/T 17377, by GB/
The requirement of T14488.1 measures oil content and carries out cold pressing test on a small scale and determine that respective cold pressing oil yield (obtains weight of oil ÷
Oil plant weight × 100%), the mixing match of various oil plant is then calculated by the requirement of table 2, result is as shown in table 5.
Table 5 detects and result of calculation
| Semen Brassicae campestris | Fructus Perillae | Sunflower seed | |
| Oil content (% wet basis) | 50.1 | 51.6 | 39.6 |
| Cold pressing oil yield (% wet basis) | 30.0 | 40.0 | 45.0 |
| Content of fatty acid in oils and fats | |||
| Linoleic acid content (%) | 28.03 | 10.2 | 62.01 |
| Alpha-linolenic acid content (%) | 8.1 | 58.5 | 0.01 |
| Oleic acid content (%) | 57.47 | 21.0 | 22.05 |
| Stearate acid content (%) | 2.4 | 1.9 | 7,85 |
| Palmitic acid content (%) | 4.0 | 6.4 | 8.08 |
| Oil plant mixing match (Wt%) | 50 | 19.0 | 31.0 |
By the result of calculation in table 5, weigh 500 kilograms of Semen Allii Tuberosi, 190 kilograms of Fructus Perillae, 310 kilograms of sunflower seeds；First use
Fructus Perillae, sunflower seed are premixed by oil plant insulation conveying with mixing arrangement (Authorization Notice No. CN 205055869U), then press
Premix material and Semen Brassicae campestris are carried and mixing arrangement by the velocity ratio (volume ratio) of 1:1 (premix material: Semen Brassicae campestris) again with oil plant insulation
Mix, it is ensured that various oil plant mix homogeneously, obtain mixing oil plant；
Mixing oil plant after mix homogeneously is delivered to cold pressing expeller, 20 DEG C, carry out cold pressing processing under the conditions of 25MPa.Will
The crude oil obtained is delivered in microporous filter carry out fine straining, and polyamide microporous membrane (PA) capillary aperture is 25 microns, fine straining
Oil-temperature control is at 50 DEG C, and operation pressure is 0.1MPa, meanwhile, pours nitrogen with the speed of 1 liter/min；Obtain cold through fine straining
Squeeze former odor type Folium Perillae edible vegetable blend oil；
Fatty acid composition and content, result such as table 6 institute of product is measured by the requirement of GB/T 17376 and GB/T 17377
Show.
Table 6 former odor type Folium Perillae edible vegetable blend oil fatty acid compositional analysis result
| Cold pressing former odor type Folium Perillae edible vegetable blend oil | |
| Linoleic acid content (%) | 37.28 |
| Alpha-linolenic acid content (%) | 15.51 |
| Oleic acid content (%) | 36.39 |
| Stearate acid content (%) | 4.75 |
| Palmitic acid content (%) | 4.75 |
| AOM value (hour) | 15.50 |
As can be seen from Table 6, the former odor type Folium Perillae edible vegetable blend oil that the present embodiment prepares is qualified products.Adopt
The oxidation stability of the former odor type Folium Perillae edible vegetable blend oil that the present embodiment prepares is measured by method well known in the art
(AOM value), the electrical conductivity of the former odor type Folium Perillae edible vegetable blend oil that the present embodiment obtains and graph of relation such as Fig. 5 of time
Shown in, from figure 5 it can be seen that its oxidation stability (AOM value) can reach 15.50 hours.
Embodiment 3
Present embodiments provide and a kind of prepare former odor type Folium Perillae with fresh Semen Brassicae campestris, Fructus Perillae, Fructus Maydis for raw material
The method of edible vegetable blend oil, its technological process is as it is shown on figure 3, specifically include following steps:
Semen Brassicae campestris, Fructus Perillae, Fructus Maydis are delivered to respectively in respective cleaning plant (selecting crude drugs with winnower, screen out combination unit)
Carrying out dedusting, remove impurity cleaning, the oil plant time of staying in a device is 10 seconds, and thickness is 5 millimeters；
Then, in addition to Fructus Perillae, then it is delivered to respective modifying device is carried out quenched respectively, Semen Brassicae campestris, Fructus Maydis
Refining temperature be 65 DEG C, adjust to moisture be 7%；It is transported to the Fructus Perillae after cleaning in roasting seed device bake
Seed, the roasting seed temperature of Fructus Perillae is 160 DEG C, and the time is 10 minutes；
Separately sampled, measure fatty acid composition and content by GB/T 17376 and GB/T 17377 requirement, by GB/
T14488.1 requires to measure oil content and carry out cold pressing test on a small scale to determine that respective cold pressing oil yield (obtains weight of oil ÷ oil
Material weight × 100%), the mixing match of oil plant is calculated the most again by the requirement of table 2, result is as shown in table 7.
Table 7 detects and result of calculation
| Semen Brassicae campestris | Fructus Perillae | Fructus Maydis | |
| Oil content (% wet basis) | 50.1 | 51.6 | 40.0 |
| Cold pressing oil yield (% wet basis) | 30.0 | 40.0 | 40.00 |
| Content of fatty acid in oils and fats | |||
| Linoleic acid content (%) | 28.03 | 10.2 | 60.01 |
| Alpha-linolenic acid content (%) | 8.1 | 58.5 | 0.45 |
| Oleic acid content (%) | 57.47 | 21.0 | 21.05 |
| Stearate acid content (%) | 2.4 | 1.9 | 6,85 |
| Palmitic acid content (%) | 4.0 | 6.4 | 11.64 |
| Oil plant mixing match (Wt%) | 50 | 18.0 | 32.0 |
By the result of calculation in table 7, weigh 500 kg of oil Semen Allii Tuberosi, 180 kilograms of Fructus Perillae, 320 kg corn plumules, will
Fructus Perillae, Fructus Maydis first premix, so with mixing arrangement (Authorization Notice No. CN 205055869U) with oil plant insulation conveying
Premix material and Semen Brassicae campestris are carried with oil plant insulation and mix by velocity ratio (volume ratio) again that press 1:1 (premix material: Semen Brassicae campestris) afterwards
Device carries out mix homogeneously, obtains mixing oil plant；
Mixing oil plant after mix homogeneously is delivered to cold pressing expeller, 20 DEG C, carry out cold pressing processing under the conditions of 25MPa.Will
The crude oil obtained is delivered in microporous filter carry out fine straining, and polyamide microporous membrane (PA) capillary aperture is 25 microns, fine straining
Oil-temperature control is at 50 DEG C, and operation pressure is 0.1MPa, meanwhile, pours nitrogen with the speed of 1 liter/min；Obtain cold through fine straining
Squeeze former odor type Folium Perillae edible vegetable blend oil；
Fatty acid composition and content, result such as table 8 institute of product is measured by the requirement of GB/T 17376 and GB/T 17377
Show.
Table 8 former odor type Folium Perillae edible vegetable blend oil fatty acid compositional analysis result
As can be seen from Table 8, the former odor type Folium Perillae edible vegetable blend oil that the present embodiment prepares is qualified products.Adopt
The oxidation stability of the former odor type Folium Perillae edible vegetable blend oil that the present embodiment prepares is measured by method well known in the art
(AOM value), graph of relation such as Fig. 6 institute of the electrical conductivity of the former fragrant edible vegetable blend oil of Folium Perillae that the present embodiment obtains and time
Show, from fig. 6 it can be seen that its oxidation stability (AOM value) can reach 16.10 hours.
Claims (10)
1. a production technology for former odor type Folium Perillae edible vegetable blend oil, it comprises the following steps:
(1) Fructus Perillae for preparing former odor type Folium Perillae edible vegetable blend oil is cleared up successively and is baked seed, obtain through
The Fructus Perillae that roasting seed processes；
(2) to carrying out cleaning and quenched respectively for preparing other oil plants of former odor type Folium Perillae edible vegetable blend oil, obtain through
Cross quenched oil plant；
(3) described Fructus Perillae and the oil-containing of other oil plants for preparing former odor type Folium Perillae edible vegetable blend oil is measured respectively
Amount, fatty acid composition and content；Fructus Perillae and other oil plants respective cold pressing oil yield is determined by bench-scale testing, then according to
The one-tenth of predetermined Folium Perillae edible vegetable blend oil be grouped into calculate described for preparing former odor type Folium Perillae edible vegetable blend oil
Fructus Perillae and each plant demand of other oil plants, then by this consumption by the Fructus Perillae processed through roasting seed and through quenched other
Oil plant mixes, and obtains mixing oil plant；
(4) mixing oil plant is carried out cold pressing, obtain crude oil and grouts；
(5) crude oil is carried out fine straining, obtain cold pressing former odor type Folium Perillae edible vegetable blend oil；
(6) in cold pressing former odor type Folium Perillae edible vegetable blend oil, add natural Vitamin E or tert-butylhydroquinone, then enter
Row fatty acid composition and content detection, obtain described former odor type Folium Perillae edible vegetable blend oil；
Wherein, other oil plants described include one or more in Semen Brassicae campestris, sunflower seed, Fructus Maydis and Non-transgenic soybean
Combination；
Preferably, other oil plants described include Semen Brassicae campestris, sunflower seed and Fructus Maydis.
Production technology the most according to claim 1, it is characterised in that in step (1), (2), described cleaning is according to following
Mode is carried out:
The size of the seed according to Fructus Perillae and other oil plants for preparing former odor type Folium Perillae edible vegetable blend oil, by Folium Perillae
Seed and other oil plants are delivered to selecting crude drugs with winnower respectively, screen out in combination unit, to remove dust, light materials, to screen out broken seed, not
Ripe seed, screens out bigger material；
Wherein Fructus Perillae and other oil plants time of staying in combination unit are the 10-60 second, and thickness is 5-20 millimeter.
Production technology the most according to claim 1, it is characterised in that in step (1),
The roasting seed temperature of described Fructus Perillae is 120-170 DEG C, and the roasting seed time is 10-45 minute；Preferably, roasting seed temperature is 130-
160 DEG C, the roasting seed time is 15-30 minute；It is highly preferred that roasting seed temperature is 140-150 DEG C, the roasting seed time is 20-25 minute.
Production technology the most according to claim 1, it is characterised in that in step (2),
The refining temperature of described Semen Brassicae campestris, sunflower seed and Fructus Maydis is 25-85 DEG C, and moisture is 6wt%-10wt%, excellent
Selection of land, refining temperature is 55-80 DEG C, and moisture is 6wt%-9wt%；It is highly preferred that refining temperature is 65-80 DEG C, moisture
Content is 7wt%-8wt%；
The refining temperature of described Non-transgenic soybean is 35-55 DEG C, and moisture is 6wt%-10wt%；Preferably, quenched temperature
Degree is for 35-50 DEG C, and moisture is 6wt%-9wt%；It is highly preferred that refining temperature be 45-50 DEG C, moisture be 7wt%-
8wt%.
Production technology the most according to claim 1, it is characterised in that the mixing described in step (3) also includes pre-compounding process,
This pre-compounding process is carried out according to step in detail below:
The consumption oil plant less than 33wt% is first mixed, obtains premix material；Then, then consumption is higher than the oil plant of 33wt%
Mix with described premix material, obtain described mixing oil plant.
Production technology the most according to claim 1, it is characterised in that in step (4), described cold pressing is in such a way
Carry out:
Mixing oil plant is delivered to cold pressing device 20-35 DEG C, carry out cold pressing processing under the conditions of 25-35MPa.
Production technology the most according to claim 1, it is characterised in that in step (5), described fine straining is in such a way
Carry out:
Crude oil cold pressing obtained is delivered in microporous filter carry out fine straining, and wherein the capillary aperture of polyamide microporous membrane is
10-25 micron；Fine straining Oil-temperature control is at 50-80 DEG C, and operation pressure is 0.1-0.6MPa.
8. according to the production technology described in claim 1 or 7, it is characterised in that in step (5), in described fine straining step
It is passed through nitrogen and carries out oxygen barrier protection；
Preferably, the consumption of described nitrogen controls as 1-10L/min.
Production technology the most according to claim 1, it is characterised in that in step (6), with described cold pressing former odor type Folium Perillae
The quality meter of edible vegetable blend oil, the addition of described natural Vitamin E is 1g/Kg, adding of described tert-butylhydroquinone
Dosage is 0.1g/Kg.
10. one kind is produced by the production technology of the former odor type Folium Perillae edible vegetable blend oil described in any one of claim 1-9
The former odor type Folium Perillae edible vegetable blend oil arrived, wherein, with the gross weight of this former odor type Folium Perillae edible vegetable blend oil for 100%
Meter, omega-3 fatty acid and remaining content of fatty acid all meet the requirement of Q/SHHF 0007S-2014 individual features index.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106962507A (en) * | 2017-05-02 | 2017-07-21 | 桦南仙紫食品科技有限公司 | Soybean purple perilla ready-mixed oil and processing method |
| CN107815347A (en) * | 2016-01-06 | 2018-03-20 | 卜敏 | A kind of white rapeseed oil of rapeseed |
| CN108378140A (en) * | 2018-03-08 | 2018-08-10 | 丽江先锋食品开发有限公司 | A kind of purple perilla seed ready-mixed oil of high unsaturated fatty acid content |
| CN111876236A (en) * | 2020-08-15 | 2020-11-03 | 金健植物油有限公司 | Flavor pressed vegetable oil and preparation method thereof |
| CN112352842A (en) * | 2020-11-08 | 2021-02-12 | 王瑞雪 | Preparation method of edible oil |
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| CN104585355A (en) * | 2015-01-13 | 2015-05-06 | 三河汇福生物科技有限公司 | Double-layer equilibrium edible vegetable blend oil and preparation method thereof |
| CN104642566A (en) * | 2014-06-18 | 2015-05-27 | 刘新 | Edible blending oil |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN104642566A (en) * | 2014-06-18 | 2015-05-27 | 刘新 | Edible blending oil |
| CN104585355A (en) * | 2015-01-13 | 2015-05-06 | 三河汇福生物科技有限公司 | Double-layer equilibrium edible vegetable blend oil and preparation method thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107815347A (en) * | 2016-01-06 | 2018-03-20 | 卜敏 | A kind of white rapeseed oil of rapeseed |
| CN106962507A (en) * | 2017-05-02 | 2017-07-21 | 桦南仙紫食品科技有限公司 | Soybean purple perilla ready-mixed oil and processing method |
| CN108378140A (en) * | 2018-03-08 | 2018-08-10 | 丽江先锋食品开发有限公司 | A kind of purple perilla seed ready-mixed oil of high unsaturated fatty acid content |
| CN111876236A (en) * | 2020-08-15 | 2020-11-03 | 金健植物油有限公司 | Flavor pressed vegetable oil and preparation method thereof |
| CN112352842A (en) * | 2020-11-08 | 2021-02-12 | 王瑞雪 | Preparation method of edible oil |
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