CN106165907A - A kind of cigarette filter rod containing Thuja extract - Google Patents
A kind of cigarette filter rod containing Thuja extract Download PDFInfo
- Publication number
- CN106165907A CN106165907A CN201610599363.0A CN201610599363A CN106165907A CN 106165907 A CN106165907 A CN 106165907A CN 201610599363 A CN201610599363 A CN 201610599363A CN 106165907 A CN106165907 A CN 106165907A
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- CN
- China
- Prior art keywords
- filter rod
- cigarette
- cigarette filter
- thuja extract
- extract
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/08—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent
- A24D3/10—Use of materials for tobacco smoke filters of organic materials as carrier or major constituent of cellulose or cellulose derivatives
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
Abstract
The present invention provides a kind of cigarette filter rod containing Thuja extract, and it contains Thuja extract.The present invention also provides for Thuja extract for reducing the purposes of phenol content in cigarette mainstream flue gas.The cigarette filter rod containing Thuja extract of the present invention is used for Medicated cigarette, it is possible to effectively reduce the content of phenol in main flume, moreover it is possible to improve the sucking quality of Medicated cigarette, enables in particular to improve the fragrant plumpness of cigarette and reduce miscellaneous QI.
Description
Technical field
The invention belongs to Medicated cigarette field, be specifically related to a kind of cigarette filter rod containing Thuja extract.
Background technology
Phenol is a kind of important harmful substance, and it not only has strong impulse effect to skin and respiratory mucosa, and
Also having carcinogenesis, it is put in the cigarette smoke that Hoffman1990 delivers in the list of 43 kinds of nuisances.
Phenol main source in cigarette mainstream flue gas is glucide thermal decomposition and the Polyphenols such as rutin and chlorogenic acid
Compound cracking produces, and the phenolic compound in cigarette smoke is a kind of protoplasmic toxin, and the mechanism of action is and the egg in cell
White matter generation chemical reaction, makes protein denaturation, further results in cell and loses activity.Additionally, in aldehydes matter in flue gas
Dull sucking quality, abnormal smells from the patient and the medicine burning sensation such as phenolic aldehyde taste, astringent taste and unpleasant, dull suction taste can be produced,
Increase peculiar taste, the complexity tarted up to flue gas, cause astringent taste, pungent, pleasant impression the cleanest, thus the Medicated cigarette system of impact
The mouthfeel of product and suction quality.Therefore, the phenol reducing or removing in cigarette mainstream flue gas, can improve the safety of cigarette products
Property and sucking quality.
After bamboo fiber is the impurity such as the lignin in removal bamboo, pentosan, bamboo powder, pectin, directly carry from bamboo wood
The natural fiber taken.
Cacumen Platycladi (Latin literary fame: Platycladusorientalis (L.) Franco) belongs to aiphyllium.
Summary of the invention
It is an object of the present invention to provide a kind of cigarette filter rod, it is also another object of the present invention to provide one can reduce
The cigarette filter rod of phenol content in main flume, it is also another object of the present invention to provide a kind of smoking property of cigarette quality of improving
Cigarette filter rod.
Inventor is surprisingly it has been found that Thuja extract can effectively reduce the phenol in cigarette mainstream flue gas, simultaneously
Improve the sucking quality of Medicated cigarette.
For realizing said one or multiple purpose, first aspect present invention provides a kind of cigarette filter rod, and it contains Cacumen Platycladi and carries
Take thing.
In one embodiment, the cigarette filter rod of any one of the present invention, it contains single, and described Thuja extract is born
It is loaded on described single.
In one embodiment, the cigarette filter rod of any one of the present invention, it has a following one or more feature:
A) described single is bamboo fiber line；
B) number of described single is 30～50；
C) number of share of stock of described single is 10～30 strands；
D) length of single is identical with cigarette filter rod length；
E) single is parallel with the axis direction of cigarette filter rod；
F) containing 1～5 single in every cigarette filter rod.
In one embodiment, the cigarette filter rod of any one of the present invention, it is by comprising the steps g) and/or step h)
Method prepare:
G) aqueous solution of Thuja extract or Thuja extract is directly applied to cigarette filter rod, is then dried Medicated cigarette filter
Rod；
H) first the aqueous solution of Thuja extract or Thuja extract is put on single, be then dried single, then
Dried single is arranged in cigarette filter rod.
In one embodiment, the cigarette filter rod of any one of the present invention, described cigarette filter rod is the filter of acetate fiber Medicated cigarette
Rod.
Second aspect present invention provides Thuja extract, single containing Thuja extract or the volume of any one of the present invention
Cigarette filter is for reducing the purposes of phenol content in cigarette mainstream flue gas.
Third aspect present invention provides a kind of and reduces the method for phenol content in cigarette mainstream flue gas, comprising: at Medicated cigarette
Filter stick adds Thuja extract, or the single containing Thuja extract is set in cigarette filter rod.
Fourth aspect present invention provides a kind of Medicated cigarette, and it contains the cigarette filter rod of any one of the present invention.
In one embodiment, the cigarette filter rod of any one of the present invention, the purposes of any one of the present invention, the present invention are arbitrary
The method of item or the Medicated cigarette of any one of the present invention, described Thuja extract is Cacumen Platycladi extractum.
In one embodiment, the cigarette filter rod of any one of the present invention, the purposes of any one of the present invention, the present invention are arbitrary
The method of item or the Medicated cigarette of any one of the present invention, described Thuja extract is prepared by the method comprised the steps:
I) Cacumen Platycladi is extracted in a solvent；
J) extracting solution after extracting is filtered, separating filtrate and filter excess；
K) alternatively, filter excess is repeated said extracted and filtration step 1～3 times, and merging filtrate；
L) distillation filtrate, boils off solvent, and gained steams excess and is Thuja extract.
In one embodiment, the cigarette filter rod of any one of the present invention, the purposes of any one of the present invention, or the present invention appoints
The method of one, or the Medicated cigarette of any one of the present invention, it has a following one or more feature:
M), in step i), Cacumen Platycladi is Cacumen Platycladi
N), in step i), Cacumen Platycladi is dry；
O), in step i), Cacumen Platycladi is powder or graininess；
P), in step i), solvent is dehydrated alcohol or ethanol water；
Q), in step i), solvent is ethanol water (the such as ethanol water of concentration 50～70 mass %)；
R), in step i), it is extracted as soak extraction；
S), in step i), the time of extraction is 3～5 hours；
T), in step i), the temperature of extraction is 20～40 DEG C；
U), in step l), the pressure (relative pressure) of distillation is-0.1～-0.05MPa；
V), in step l), the temperature of distillation is 70～80 DEG C；
W), in step l), the yield of Thuja extract is 30～40%.
Beneficial effects of the present invention:
Some embodiments of the present invention have a following one or more beneficial effect:
(1) the preparation method technique of Thuja extract is simple；
(2) the preparation method low cost of Thuja extract；
(3) cigarette filter rod containing Thuja extract is for Medicated cigarette, it is possible to reduce the phenol in cigarette mainstream flue gas；
(4) cigarette filter rod containing Thuja extract is for Medicated cigarette, it is possible to improve the sucking quality of Medicated cigarette；
(5) cigarette filter rod containing Thuja extract is for Medicated cigarette, it is possible to increase the plumpness of the cigarette perfume of Medicated cigarette and reduction
Miscellaneous QI.
Detailed description of the invention
Below by embodiment, technical scheme is described in further detail.
Embodiment 1
1, Thuja extract and the preparation of aqueous solution thereof:
50 mass % ethanol water of 10 times of weight are added by dried side Cacumen Platycladi (Cacumen Biotae) in Cacumen Platycladi dry powder (obtaining after being pulverized)
Solution, at normal temperatures soak extraction 4h, filter extracting solution, separating filtrate and filter excess.Filter excess is repeated above-mentioned immersion and mistake
Filter step 2 time, and merge all of filtrate.Distilling above-mentioned filtrate, boil off solvent, distillation pressure is that-0.07MPa (presses relatively
Power), vapo(u)rizing temperature is 75 DEG C, and gained steams excess and is Thuja extract, and yield is 35%.
Thuja extract is mixed with water 10:90 in mass ratio, is configured to the Cacumen Platycladi extract aqueous solution of 10 mass %.
2, the preparation of the bamboo fiber line containing Thuja extract:
Bamboo fiber is prepared as, by spinning process, the bamboo fiber line that specification is 40s/20 (40,20 strands).Should
Blank bamboo fiber is immersed in the Cacumen Platycladi extract solution of above-mentioned 10% concentration, takes out after 2h, and is dried at 60 DEG C,
Obtain the bamboo fiber line containing Thuja extract.
3, the preparation of the cigarette filter rod containing Thuja extract
Bamboo fiber line containing Thuja extract is caused on cigarette filter stick forming machine by traction positioner, passes through
Filter stick formation equipment adds filter tip center to, and single is parallel to the axis direction of filter stick, adds in every cigarette filter rod
A piece bamboo fiber line containing Thuja extract, obtains the cigarette filter rod containing Thuja extract after filter stick formation.
Embodiment 2
1, Thuja extract and the preparation of aqueous solution thereof:
In Cacumen Platycladi dry powder, add 50 mass % ethanol waters of 10 times of volumes, soak 4h at normal temperatures, filter
Extracting solution, separating filtrate and filter excess.Filter excess is repeated above-mentioned immersion and filtration step 2 times, and merges all of filtrate.Steam
Evaporating above-mentioned filtrate, boil off solvent, distillation pressure is-0.07MPa (relative pressure), and vapo(u)rizing temperature is 75 DEG C, and gained steams excess i.e.
For Thuja extract, yield is 35%.
Thuja extract is mixed with water 15:85 in mass ratio, is configured to the Cacumen Platycladi extract aqueous solution of 15 mass %.
2, the preparation of the bamboo fiber line containing Thuja extract:
Bamboo fiber is prepared as, by spinning process, the bamboo fiber line that specification is 45s/20 (45,20 strands).Should
Blank bamboo fiber is immersed in the Cacumen Platycladi extract solution of above-mentioned 15% concentration, takes out after 2h, and is dried at 60 DEG C,
Obtain the bamboo fiber line containing Thuja extract.
3, the preparation of the cigarette filter rod containing Thuja extract
Bamboo fiber line containing Thuja extract is caused on cigarette filter stick forming machine by traction positioner, passes through
Filter tip former adds filter tip center to, and single is parallel to the axis direction of filter stick, adds in every cigarette filter rod
A piece bamboo fiber line containing Thuja extract, obtains the cigarette filter rod containing Thuja extract after filter stick formation.
Embodiment 3
1, Thuja extract and the preparation of aqueous solution thereof:
In Cacumen Platycladi dry powder, add 50 mass % ethanol waters of 10 times of volumes, soak 4h at normal temperatures, filter
Extracting solution, separating filtrate and filter excess.Filter excess is repeated above-mentioned immersion and filtration step 2 times, and merges all of filtrate.Steam
Evaporating above-mentioned filtrate, boil off solvent, distillation pressure is-0.07MPa (relative pressure), and vapo(u)rizing temperature is 75 DEG C, and gained steams excess i.e.
For Thuja extract, yield is 35%.
Thuja extract is mixed with water 20:80 in mass ratio, is configured to the Cacumen Platycladi extract aqueous solution of 20 mass %.
2, the preparation of the bamboo fiber line containing Thuja extract:
Bamboo fiber is prepared as, by spinning process, the bamboo fiber line that specification is 39s/20 (39,20 strands).Should
Blank bamboo fiber is immersed in the Cacumen Platycladi extract solution of above-mentioned 20% concentration, takes out after 2h, and is dried at 60 DEG C,
Obtain the bamboo fiber line containing Thuja extract.
3, the preparation of the cigarette filter rod containing Thuja extract
Bamboo fiber line containing Thuja extract is caused on cigarette filter stick forming machine by traction positioner, passes through
Filter tip former adds filter tip center to, and single is parallel to the axis direction of filter stick, adds in every cigarette filter rod
A piece bamboo fiber line containing Thuja extract, obtains the cigarette filter rod containing Thuja extract after filter stick formation.
Embodiment 4
1, Thuja extract and the preparation of aqueous solution thereof:
In Cacumen Platycladi dry powder, add 50 mass % ethanol waters of 10 times of volumes, soak 4h at normal temperatures, filter.
Repeat above-mentioned immersion and filtration step 2 times under the same conditions, and merge all of filtrate.Distill above-mentioned filtrate, boil off solvent,
Distillation pressure is-0.07MPa (relative pressure), and vapo(u)rizing temperature is 75 DEG C, and gained steams excess and is Thuja extract, and yield is
35%.
Thuja extract is mixed with water 15:85 in mass ratio, is configured to the Cacumen Platycladi extract aqueous solution of 15 mass %.
2, the preparation of the cigarette filter rod containing Thuja extract:
The Cacumen Platycladi extract solution 50mg of above-mentioned 15% concentration is dripped on the cigarette filter rod of a Medicated cigarette, treats that it is certainly
The most dried, put back to Cigarette.
Analyze and detect the detection of phenol content in 1-main flume:
Prepare the cigarette sample of embodiment 1～4 and blank cigarette sample, according to YC/T 255-2008 cigarette mainstream flue gas
Mensuration-the high performance liquid chromatography of middle major phenolic compound detects, the content of phenol, reduction rate in detection main flume
For embodiment relative to the reduction rate of blank cigarette sample, testing result is as shown in table 1 below:
Table 1
| Phenol content (μ g/ props up) | Reduction rate | |
| Embodiment 1 | 11.48 | 10.3% |
| Embodiment 2 | 11.26 | 12.0% |
| Embodiment 3 | 10.16 | 20.6% |
| Embodiment 4 | 11.43 | 10.7% |
| Blank | 12.80 |
Analyze detection 2-Sensory Quality of Cigarette to evaluate
According to the cigarette sample to embodiment 1～4 of the Sensory Quality of Cigarette evaluation criterion in GB GB 5606.4-2005
Smokeing panel test with blank cigarette sample, result is as shown in table 2 and table 3.
Table 2
Table 3
| Sample ID | Analyses Methods for Sensory Evaluation Results |
| Embodiment 1 | Cigarette perfume (or spice) is full, thoroughly sends out, still harmony, slightly miscellaneous QI, and pleasant impression is clean |
| Embodiment 2 | Cigarette perfume (or spice) is full, clearly, still harmony, slightly stimulate, pleasant impression is clean |
| Embodiment 3 | Cigarette perfume (or spice) is the fullest, clearly, still harmony, seemingly there is miscellaneous QI, pleasant impression is clean |
| Embodiment 4 | Cigarette perfume (or spice) is full, still harmony, seemingly has miscellaneous QI, and pleasant impression is clean |
| Blank sample | Flue gas is the most muddy, throat's microstimulation, relatively miscellaneous QI, owes harmony, and pleasant impression is clean |
1 and 2 is detected, relative to blank sample, in the main flume of the Medicated cigarette of embodiment 1～4, benzene from above-mentioned analysis
Phenol content is lower；And, the Medicated cigarette sensory evaluation score of embodiment 1～4 is higher.Therefore, Thuja extract or carry containing Cacumen Platycladi
The bamboo fiber taking thing adds in cigarette filter rod, it is possible to effectively reduces the content of phenol in main flume, can also improve simultaneously
The sucking quality of Medicated cigarette, enables in particular to improve the fragrant plumpness of cigarette and reduce miscellaneous QI.
Finally should be noted that: above example is only in order to illustrate that technical scheme is not intended to limit；To the greatest extent
The present invention has been described in detail by pipe with reference to preferred embodiment, and those of ordinary skill in the field are it is understood that still
The detailed description of the invention of the present invention can be modified or portion of techniques feature is carried out equivalent；Without deviating from this
The spirit of bright technical scheme, it all should be contained in the middle of the technical scheme scope that the present invention is claimed.
Claims (11)
1. a cigarette filter rod, it contains Thuja extract.
2. the cigarette filter rod of claim 1, it contains single, and described Thuja extract is carried on described single.
3. the cigarette filter rod of claim 2, it has a following one or more feature:
A) described single is bamboo fiber line；
B) number of described single is 30～50；
C) number of share of stock of described single is 10～30 strands；
D) length of single is identical with cigarette filter rod length；
E) single is parallel with the axis direction of cigarette filter rod；
F) containing 1～5 single in every cigarette filter rod.
4. the cigarette filter rod of any one of claims 1 to 3, its by comprise the steps g) and/or step h) method prepare:
G) aqueous solution of Thuja extract or Thuja extract is directly applied to cigarette filter rod, is then dried cigarette filter rod；
H) first the aqueous solution of Thuja extract or Thuja extract is put on single, be then dried single, then will be dry
Single after dry is arranged in cigarette filter rod.
5. the cigarette filter rod of claim 1, described cigarette filter rod is acetate fiber cigarette filter rod.
6. the cigarette filter rod of Thuja extract, single containing Thuja extract or claim 1 is used for reducing Medicated cigarette main flow
The purposes of phenol content in flue gas.
7. reduce a method for phenol content in cigarette mainstream flue gas, comprising: add Thuja extract in cigarette filter rod,
Or the single containing Thuja extract is set in cigarette filter rod.
8. a Medicated cigarette, it contains the cigarette filter rod of any one of Claims 1 to 5.
9. the cigarette filter rod of any one of Claims 1 to 5, the purposes of claim 6, the method for claim 7 or claim 8
Medicated cigarette, described Thuja extract is Cacumen Platycladi extractum.
10. the cigarette filter rod of any one of Claims 1 to 5, the purposes of claim 6, the method for claim 7 or claim
The Medicated cigarette of 8, described Thuja extract is prepared by the method comprised the steps:
I) Cacumen Platycladi is extracted in a solvent；
J) extracting solution after extracting is filtered, separating filtrate and filter excess；
K) alternatively, filter excess is repeated said extracted and filtration step 1～3 times, and merging filtrate；
L) distillation filtrate, boils off solvent, and gained steams excess and is Thuja extract.
The cigarette filter rod of 11. claim 10, the purposes of claim 10, the method for claim 10 or the volume of claim 10
Cigarette, it has a following one or more feature:
M), in step i), Cacumen Platycladi is Cacumen Platycladi
N), in step i), Cacumen Platycladi is dry；
O), in step i), Cacumen Platycladi is powder or graininess；
P), in step i), solvent is dehydrated alcohol；
Q), in step i), solvent is ethanol water (the such as ethanol water of concentration 50～70 mass %)；
R), in step i), it is extracted as soak extraction；
S), in step i), the time of extraction is 3～5 hours；
T), in step i), the temperature of extraction is 20～40 DEG C；
U), in step l), the pressure of distillation is-0.1～-0.05MPa；
V), in step l), the temperature of distillation is 70～80 DEG C；
W), in step l), the yield of Thuja extract is 30～40%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610599363.0A CN106165907A (en) | 2016-07-28 | 2016-07-28 | A kind of cigarette filter rod containing Thuja extract |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610599363.0A CN106165907A (en) | 2016-07-28 | 2016-07-28 | A kind of cigarette filter rod containing Thuja extract |
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| CN106165907A true CN106165907A (en) | 2016-11-30 |
Family
ID=58065585
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| CN201610599363.0A Pending CN106165907A (en) | 2016-07-28 | 2016-07-28 | A kind of cigarette filter rod containing Thuja extract |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110419776A (en) * | 2019-08-11 | 2019-11-08 | 云南农业大学 | A kind of pure natural cigarette smoke adsorbent and its preparation, application method |
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