CN103720031A - Preparation method of tobacco extract and application of tobacco extract in cigarettes - Google Patents
Preparation method of tobacco extract and application of tobacco extract in cigarettes Download PDFInfo
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- CN103720031A CN103720031A CN201310703531.2A CN201310703531A CN103720031A CN 103720031 A CN103720031 A CN 103720031A CN 201310703531 A CN201310703531 A CN 201310703531A CN 103720031 A CN103720031 A CN 103720031A
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Abstract
The invention relates to a preparation method of tobacco extract and application of the tobacco extract in cigarettes. The preparation method includes: weighing tobacco material, adding 70-95% ethanol according to the material-liquid mass ratio of 1:5-1:10, adding phosphoric acid or sulfuric acid accounting for 0.5-3% of the tobacco material by weight, performing heat reflux extraction for 1-3 hours at the temperature of 60-90 DEG C, filtering the product, allowing for cooling and clarifying, and subjecting supernate to reduced pressure compression to obtain extract, namely herbal extract; adding the tobacco extract, accounting for 0.05-0.1% of a tobacco leaf set by weight, to the tobacco leaf set. The tobacco extract made by the method is natural and safe, has the significant effect of making tobacco products more fragrant and less irritating, and has high application value. The preparation method is simple and easy, and the technical process is highly repeatable.
Description
Technical field
The present invention relates to preparation and the applied technical field of tobacco extract.
Background technology
In recent years, be accompanied by the propelling of level on cigarette, reduce the coke tar in cigarette amount of releasing and put the jealous deficiency of brought tobacco, it is tobacco business problem demanding prompt solution that satisfaction weakens.
Tobacco extract is a kind of dark-brown thickness lotion, and can be used for increases tobacco nature fragrance in tobacco essence, improves tobacco suction quality.At present, conventional method is tobacco material to be condensed into after polar solvent extracts to cream or water extraction liquid to be got after alcohol precipitation is processed to the concentrated prepared opium paste that obtains of clear liquid, it is general that similar technique is extracted the general quality of prepared opium paste obtaining, exist in prepared opium paste contained aroma component relative amount not high, solvent consumption is large and have the problems such as residual, cannot meet the demand that tobacco industry further develops.Tobacco business urgently wishes that related researcher can provide that more can to improve tobacco jealous for this reason, increases the tobacco extract product of tobacco inherent feature fragrance, promotes the sustainable development of tobacco industry.
In tobacco threshing redrying and production of cigarettes process, a large amount of Discarded Tobacco fragments need to be dropped owing to not meeting production and processing, if the main aroma component in these Discarded Tobacco fragments is carried out to enrichment in suitable mode, in the mode of compensating aroma, again join in cigarette product, to improving product odor characteristic, will play significant effect.Meanwhile, utilize Discarded Tobacco fragment to turn waste into wealth, there is stronger economy and social effect.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of method of utilizing Discarded Tobacco fragment in tobacco production process to prepare tobacco extract is provided, provide a kind of cigarette that improves jealous and reduce the tobacco extract of excitement.The present invention also provides the concrete application of this tobacco extract.
Object of the present invention is achieved through the following technical solutions.
A kind of preparation method of tobacco extract, take tobacco material and pack container into, ratio according to feed liquid mass ratio 1:5～1:10 adds the ethanol of concentration 70～95%, then adds phosphoric acid or the sulfuric acid of tobacco material quality 0.5～3%, and under the condition of 60～90 ℃, hot reflux is extracted 1～3 hour; Products therefrom is cooling supernatant after filtering, gets supernatant reduced pressure concentration, obtains medicinal extract, is tobacco extract.
Tobacco material of the present invention is that tobacco produces discarded tobacco fragment, and broken degree is 40～200 orders.Hot reflux products therefrom is cooled to 10～30 ℃ after filtering, within standing 1～3 hour, makes its natural supernatant.The relative density of gained tobacco extract is controlled at 1.250 ± 0.010, and yield is 40～60%.
The application of tobacco extract of the present invention in cigarette, makes an addition to described tobacco extract in cigarette leaf group, and addition is 0.05～0.1% of leaf group weight.
The present invention is using the Discarded Tobacco fragment of tobacco industry as raw material, can realize resource makes full use of, and improve the mode of only utilizing single solvent to extract in traditional tobacco extract production process, by adding appropriate acid flux material to make the aroma component in tobacco obtain effective stripping, obtain and there is the tobacco extract that suction quality is obviously better than common tobacco extract.The present invention's application ethanol-phosphoric acid or ethanol-sulfuric acid, as solvent, increase the aroma component in gained tobacco extract, and the effect of thorn falls in generation flavouring.The natural safety of prepared tobacco extract, thorn is fallen in tobacco product flavouring positive effect, has higher using value.The inventive method is simple, and technical process repeatability is high.
The specific embodiment
Below in conjunction with example, further describe the present invention.
Embodiment 1
Take red large tobacco leaf (C2F) fragment 200g and pack container into, add 2000g70% ethanol, then add 1g phosphoric acid, with electric jacket, heat and at 90 ℃, extract 2 hours.Products therefrom is cooled to 20 ℃ after filtering, and standing 1h gets supernatant and is evaporated to paste, and lotion relative density is 1.258, obtains tobacco extract 110g.
By tobacco extract in mass ratio 0.1% ratio add red large tobacco leaf (X3F), its Analyses Methods for Sensory Evaluation Results is in Table 1.
Embodiment 2
Take red large tobacco leaf (C2F) fragment 1000g and pack round-bottomed flask into, add 7000g90% ethanol, then add 15g sulfuric acid, with electric jacket, heat and at 80 ℃, extract 1 hour.Products therefrom is cooled to 25 ℃ after filtering, and standing 1.5h gets supernatant and is evaporated to paste, and lotion relative density is 1.245, obtains tobacco extract 548g.
By tobacco extract in mass ratio 0.07% ratio add red large tobacco leaf (X3F), its Analyses Methods for Sensory Evaluation Results is in Table 1.
Embodiment 3
Take red large tobacco leaf (C2F) fragment 2000g and pack container into, add 10000g95% ethanol, then add 60g phosphoric acid, with electric jacket, heat and at 60 ℃, extract 3 hours.Products therefrom is cooled to 28 ℃ after filtering, and standing 2h gets supernatant and is evaporated to paste, and lotion relative density is 1.255, obtains tobacco extract 1162g.
By tobacco extract in mass ratio 0.05% ratio add red large tobacco leaf (X3F), its Analyses Methods for Sensory Evaluation Results is in Table 1.
The sensory evaluating smoking result of the tobacco extract of table 1 Different treatments and addition on red large tobacco leaf (X3F)
Claims (5)
1. the preparation method of a tobacco extract, it is characterized in that, take tobacco material and pack container into, according to the ratio of feed liquid mass ratio 1:5～1:10, add the ethanol of concentration 70～95%, add phosphoric acid or the sulfuric acid of tobacco material quality 0.5～3%, under the condition of 60～90 ℃, hot reflux is extracted 1～3 hour again; Products therefrom is cooling supernatant after filtering, gets supernatant reduced pressure concentration, obtains medicinal extract, is tobacco extract.
2. the preparation method of a kind of tobacco extract according to claim 1, is characterized in that, described tobacco material is that tobacco produces discarded tobacco fragment, and broken degree is 40～200 orders.
3. the preparation method of a kind of tobacco extract according to claim 1, is characterized in that, hot reflux products therefrom is cooled to 10～30 ℃ after filtering, within standing 1～3 hour, makes its natural supernatant.
4. the preparation method of a kind of tobacco extract according to claim 1, is characterized in that, the relative density of gained tobacco extract is controlled at 1.250 ± 0.010, and yield is 40～60%.
5. the application of the tobacco extract preparing as any one of claim 1～5 in cigarette, is characterized in that, described tobacco extract is made an addition in cigarette leaf group, and addition is 0.05～0.1% of leaf group weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310703531.2A CN103720031A (en) | 2013-12-19 | 2013-12-19 | Preparation method of tobacco extract and application of tobacco extract in cigarettes |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310703531.2A CN103720031A (en) | 2013-12-19 | 2013-12-19 | Preparation method of tobacco extract and application of tobacco extract in cigarettes |
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| CN103720031A true CN103720031A (en) | 2014-04-16 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201310703531.2A Pending CN103720031A (en) | 2013-12-19 | 2013-12-19 | Preparation method of tobacco extract and application of tobacco extract in cigarettes |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104783324A (en) * | 2015-03-17 | 2015-07-22 | 湖北中烟工业有限责任公司 | Method for preparing tobacco cell extract |
| CN104905399A (en) * | 2015-06-02 | 2015-09-16 | 湖北中烟工业有限责任公司 | Preparation method of 50% aromatic tobacco extract |
| CN109211720A (en) * | 2018-11-17 | 2019-01-15 | 中国烟草总公司郑州烟草研究院 | A method of preparing the one-stop measurement tobacco dichloromethane extract content of metering |
| CN109439435A (en) * | 2018-12-14 | 2019-03-08 | 湖北中烟工业有限责任公司 | The preparation method and application of the flavouring essence for tobacco of fumigation extract and the extract containing fumigation |
| CN111349323A (en) * | 2020-04-30 | 2020-06-30 | 贵州省烟草公司遵义市公司 | Mixed resin based on tobacco extract additive and prepared biodegradable film |
| CN113133540A (en) * | 2021-05-19 | 2021-07-20 | 四川中烟工业有限责任公司 | Method for preparing cigar flavor from cigar wastes, flavor and application |
-
2013
- 2013-12-19 CN CN201310703531.2A patent/CN103720031A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104783324A (en) * | 2015-03-17 | 2015-07-22 | 湖北中烟工业有限责任公司 | Method for preparing tobacco cell extract |
| CN104905399A (en) * | 2015-06-02 | 2015-09-16 | 湖北中烟工业有限责任公司 | Preparation method of 50% aromatic tobacco extract |
| CN109211720A (en) * | 2018-11-17 | 2019-01-15 | 中国烟草总公司郑州烟草研究院 | A method of preparing the one-stop measurement tobacco dichloromethane extract content of metering |
| CN109439435A (en) * | 2018-12-14 | 2019-03-08 | 湖北中烟工业有限责任公司 | The preparation method and application of the flavouring essence for tobacco of fumigation extract and the extract containing fumigation |
| CN111349323A (en) * | 2020-04-30 | 2020-06-30 | 贵州省烟草公司遵义市公司 | Mixed resin based on tobacco extract additive and prepared biodegradable film |
| CN113133540A (en) * | 2021-05-19 | 2021-07-20 | 四川中烟工业有限责任公司 | Method for preparing cigar flavor from cigar wastes, flavor and application |
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Address after: 650106 No. 41, medical Road, hi tech Zone, Yunnan, Kunming Applicant after: Yunnan Zhongyan Reconstituted Tobacco Co., Ltd. Address before: 650106 No. 41, medical Road, hi tech Zone, Yunnan, Kunming Applicant before: Yunnan Zhongyan Kunchuan Ruisheng Technology Co., Ltd. |
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| COR | Change of bibliographic data |
Free format text: CORRECT: APPLICANT; FROM: YUNNAN ZHONGYAN KUNCHUAN RUISHENG TECHNOLOGY CO., LTD. TO: YUNNAN ZHONGYAN RECONSTITUTED TOBACCO CO., LTD. |
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Application publication date: 20140416 |