CN106120319A - A kind of silkete penetrating agent and preparation method thereof - Google Patents
A kind of silkete penetrating agent and preparation method thereof Download PDFInfo
- Publication number
- CN106120319A CN106120319A CN201610507641.5A CN201610507641A CN106120319A CN 106120319 A CN106120319 A CN 106120319A CN 201610507641 A CN201610507641 A CN 201610507641A CN 106120319 A CN106120319 A CN 106120319A
- Authority
- CN
- China
- Prior art keywords
- penetrating agent
- preparation
- silkete penetrating
- parts
- added
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/165—Ethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
- D06M11/70—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with oxides of phosphorus; with hypophosphorous, phosphorous or phosphoric acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
- D06M11/70—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with oxides of phosphorus; with hypophosphorous, phosphorous or phosphoric acids or their salts
- D06M11/71—Salts of phosphoric acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/144—Alcohols; Metal alcoholates
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/282—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
- D06M13/292—Mono-, di- or triesters of phosphoric or phosphorous acids; Salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/03—Polysaccharides or derivatives thereof
- D06M15/13—Alginic acid or derivatives thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Medicinal Preparation (AREA)
- Cosmetics (AREA)
Abstract
The invention provides a kind of silkete penetrating agent and preparation method thereof.Preparation method is as follows: diethylene glycol monobutyl ether is added four mouthfuls of reaction bulbs by (1), and temperature rises to 70 75 DEG C；(2) it is slowly added into phosphorus pentoxide, insulation reaction 12 hours；(3) lauryl alcohol, propylene glycol alginate, erythritol, dalcium biphosphate, lauroylamidopropyl betaine, lauric acid amide of ethanol, sodium citrate, tributyl phosphate, dehydrated alcohol and distilled water are added, stirring reaction 12 hours；(4) it is cooled to room temperature, discharging and get final product.The silkete penetrating agent alkali resistance of the present invention is splendid, and time of penetration is short, and permeability is high, and foaming characteristic is low simultaneously, it is easy to the recovery to sodium hydroxide.
Description
Technical field
The present invention relates to textile material field, be specifically related to a kind of silkete penetrating agent and preparation method thereof.
Background technology
Silkete penetrating agent is mainly used in the mercerized finish of purified cotton yarns or fabric, and mercerization is to make cotton fiber produce
The durability gloss that silk is the same, improves the dimensional stability of finished product, the most also can improve the ability absorbing dyestuff, and imparting is knitted
The feel that thing is soft and plentiful.And should possess following requirements as silkete penetrating agent: (1) can be dissolved in mercerising liquid, and has excellent
Permeability and wettability, be substantially shorter wetting time；(2) resistance to highly basic, maintains a long-term stability in high alkali liquid, and effect changes
Little；(3) do not make the coloring of mercerising liquid and stink occurs；(4) spent lye reclaims when other purposes, does not produce tar and foaming etc.
Disadvantage；(5) make mercerising solution foaming little；(6) usage amount is less than l0-30g/L.But, current most of silkete penetrating agents
All cannot meet above-mentioned requirements, therefore, constantly research and develop the novel silkete penetrating agent meeting above-mentioned performance and there is important value
And meaning.
Summary of the invention
Solve the technical problem that: it is an object of the invention to provide a kind of silkete penetrating agent, alkali resistance is splendid, time of penetration
Short, permeability is high, and foaming characteristic is low simultaneously, it is easy to the recovery to sodium hydroxide.
Technical scheme: a kind of silkete penetrating agent, is prepared from weight portion by following component: diethylene glycol monobutyl ether 50-
70 parts, lauryl alcohol 5-10 part, propylene glycol alginate 1-2 part, phosphorus pentoxide 20-30 part, erythritol 0.5-1 part, phosphoric acid
Calcium dihydrogen 1-2 part, lauroylamidopropyl betaine 0.5-1 part, lauric acid amide of ethanol 1-2 part, sodium citrate 0.1-0.3
Part, tributyl phosphate 0.2-0.5 part, dehydrated alcohol 2-5 part, distilled water 200-300 part.
It is further preferred that described a kind of silkete penetrating agent, following component it is prepared from weight portion: diethylene glycol
Monobutyl ether 55-65 part, lauryl alcohol 6-9 part, propylene glycol alginate 1.1-1.6 part, phosphorus pentoxide 22-28 part, erythritol
0.6-0.9 part, dalcium biphosphate 1.2-1.7 part, lauroylamidopropyl betaine 0.6-0.9 part, lauric acid amide of ethanol
1.3-1.7 part, sodium citrate 0.15-0.25 part, tributyl phosphate 0.3-0.4 part, dehydrated alcohol 3-4 part, distilled water 220-280
Part.
The preparation method of above-mentioned silkete penetrating agent comprises the following steps:
(1) diethylene glycol monobutyl ether is added four mouthfuls of reaction bulbs, temperature is risen to 70-75 DEG C；
(2) it is slowly added into phosphorus pentoxide, insulation reaction 1-2 hour；
(3) lauryl alcohol, propylene glycol alginate, erythritol, dalcium biphosphate, lauroylamidopropyl betaine, cocos nucifera oil are added
Acid diglycollic amide, sodium citrate, tributyl phosphate, dehydrated alcohol and distilled water, stirring reaction 1-2 hour；
(4) it is cooled to room temperature, discharging and get final product.
Further, the preparation method of described a kind of silkete penetrating agent, described step (1) is warming up to 71-74 DEG C.
Further, the preparation method of described a kind of silkete penetrating agent, in described step (2), the insulation reaction time is
Hour 1..5.
Further, the preparation method of described a kind of silkete penetrating agent, in described step (3), the stirring response time is
1.5 hour.
Beneficial effect: the alkali resistance of the silkete penetrating agent of the present invention is splendid, resistance to sodium hydroxide solution mass concentration reaches
291g/L, time of penetration is short, the most only needs 97s, and permeability is high, and meanwhile, foaming characteristic is low, it is easy to the recovery to sodium hydroxide.
Detailed description of the invention
Embodiment 1
A kind of silkete penetrating agent, is prepared from weight portion by following component: diethylene glycol monobutyl ether 50 parts, lauryl alcohol 5 parts, sea
Propylene glycol alginate 1 part, phosphorus pentoxide 20 parts, erythritol 0.5 part, dalcium biphosphate 1 part, lauroylamidopropyl betaine
0.5 part, lauric acid amide of ethanol 1 part, sodium citrate 0.1-0.3 part, tributyl phosphate 0.2 part, dehydrated alcohol 2 parts, distillation
200 parts of water.
The preparation method of above-mentioned silkete penetrating agent is: diethylene glycol monobutyl ether is added four mouthfuls of reaction bulbs by (1), by temperature liter
To 70 DEG C；(2) it is slowly added into phosphorus pentoxide, insulation reaction 1 hour；(3) lauryl alcohol, propylene glycol alginate, red moss are added
Sugar alcohol, dalcium biphosphate, lauroylamidopropyl betaine, lauric acid amide of ethanol, sodium citrate, tributyl phosphate, anhydrous
Ethanol and distilled water, stirring reaction 1 hour；(4) it is cooled to room temperature, discharging and get final product.
Embodiment 2
A kind of silkete penetrating agent, is prepared from weight portion by following component: diethylene glycol monobutyl ether 55 parts, lauryl alcohol 6 parts, sea
Propylene glycol alginate 1.1 parts, phosphorus pentoxide 22 parts, erythritol 0.6 part, dalcium biphosphate 1.2 parts, dodecanamide propyl are sweet
0.6 part of dish alkali, lauric acid amide of ethanol 1.3 parts, sodium citrate 0.15 part, tributyl phosphate 0.3 part, dehydrated alcohol 3 parts, steaming
Distilled water 220 parts.
The preparation method of above-mentioned silkete penetrating agent is: diethylene glycol monobutyl ether is added four mouthfuls of reaction bulbs by (1), by temperature liter
To 71 DEG C；(2) it is slowly added into phosphorus pentoxide, insulation reaction 1.5 hours；(3) lauryl alcohol, propylene glycol alginate, red is added
Moss sugar alcohol, dalcium biphosphate, lauroylamidopropyl betaine, lauric acid amide of ethanol, sodium citrate, tributyl phosphate, nothing
Water-ethanol and distilled water, stirring reaction 1.5 hours；(4) it is cooled to room temperature, discharging and get final product.
Embodiment 3
A kind of silkete penetrating agent, is prepared from weight portion by following component: diethylene glycol monobutyl ether 60 parts, lauryl alcohol 7.5 parts,
Propylene glycol alginate 1.5 parts, phosphorus pentoxide 25 parts, erythritol 0.75 part, dalcium biphosphate 1.5 parts, lauramide third
Base glycine betaine 0.75 part, lauric acid amide of ethanol 1.5 parts, sodium citrate 0.2 part, tributyl phosphate 0.35 part, dehydrated alcohol
3.5 parts, distilled water 250 parts.
The preparation method of above-mentioned silkete penetrating agent is: diethylene glycol monobutyl ether is added four mouthfuls of reaction bulbs by (1), by temperature liter
To 72 DEG C；(2) it is slowly added into phosphorus pentoxide, insulation reaction 1.5 hours；(3) lauryl alcohol, propylene glycol alginate, red is added
Moss sugar alcohol, dalcium biphosphate, lauroylamidopropyl betaine, lauric acid amide of ethanol, sodium citrate, tributyl phosphate, nothing
Water-ethanol and distilled water, stirring reaction 1.5 hours；(4) it is cooled to room temperature, discharging and get final product.
Embodiment 4
A kind of silkete penetrating agent, is prepared from weight portion by following component: diethylene glycol monobutyl ether 65 parts, lauryl alcohol 9 parts, sea
Propylene glycol alginate 1.6 parts, phosphorus pentoxide 28 parts, erythritol 0.9 part, dalcium biphosphate 1.7 parts, dodecanamide propyl are sweet
0.9 part of dish alkali, lauric acid amide of ethanol 1.7 parts, sodium citrate 0.25 part, tributyl phosphate 0.4 part, dehydrated alcohol 4 parts, steaming
Distilled water 280 parts.
The preparation method of above-mentioned silkete penetrating agent is: diethylene glycol monobutyl ether is added four mouthfuls of reaction bulbs by (1), by temperature liter
To 74 DEG C；(2) it is slowly added into phosphorus pentoxide, insulation reaction 1.5 hours；(3) lauryl alcohol, propylene glycol alginate, red is added
Moss sugar alcohol, dalcium biphosphate, lauroylamidopropyl betaine, lauric acid amide of ethanol, sodium citrate, tributyl phosphate, nothing
Water-ethanol and distilled water, stirring reaction 1.5 hours；(4) it is cooled to room temperature, discharging and get final product.
Embodiment 5
A kind of silkete penetrating agent, is prepared from weight portion by following component: diethylene glycol monobutyl ether 70 parts, lauryl alcohol 10 parts,
Propylene glycol alginate 2 parts, phosphorus pentoxide 30 parts, erythritol 1 part, dalcium biphosphate 2 parts, lauroylamidopropyl betaine
1 part, lauric acid amide of ethanol 2 parts, sodium citrate 0.3 part, tributyl phosphate 0.5 part, dehydrated alcohol 5 parts, distilled water 300
Part.
The preparation method of above-mentioned silkete penetrating agent is: diethylene glycol monobutyl ether is added four mouthfuls of reaction bulbs by (1), by temperature liter
To 75 DEG C；(2) it is slowly added into phosphorus pentoxide, insulation reaction 2 hours；(3) lauryl alcohol, propylene glycol alginate, red moss are added
Sugar alcohol, dalcium biphosphate, lauroylamidopropyl betaine, lauric acid amide of ethanol, sodium citrate, tributyl phosphate, anhydrous
Ethanol and distilled water, stirring reaction 2 hours；(4) it is cooled to room temperature, discharging and get final product.
Comparative example 1
The present embodiment is not contain lauroylamidopropyl betaine and lauric acid amide of ethanol with the difference of embodiment 5.Tool
Say body and be:
A kind of silkete penetrating agent, is prepared from weight portion by following component: diethylene glycol monobutyl ether 70 parts, lauryl alcohol 10 parts,
Propylene glycol alginate 2 parts, phosphorus pentoxide 30 parts, erythritol 1 part, dalcium biphosphate 2 parts, sodium citrate 0.3 part, phosphoric acid
Tributyl 0.5 part, dehydrated alcohol 5 parts, distilled water 300 parts.
The preparation method of above-mentioned silkete penetrating agent is: diethylene glycol monobutyl ether is added four mouthfuls of reaction bulbs by (1), by temperature liter
To 75 DEG C；(2) it is slowly added into phosphorus pentoxide, insulation reaction 2 hours；(3) lauryl alcohol, propylene glycol alginate, red moss are added
Sugar alcohol, dalcium biphosphate, sodium citrate, tributyl phosphate, dehydrated alcohol and distilled water, stirring reaction 2 hours；(4) it is cooled to
Room temperature, discharging and get final product.
Comparative example 2
The present embodiment is not contain dalcium biphosphate and tributyl phosphate with the difference of embodiment 5.Specifically:
A kind of silkete penetrating agent, is prepared from weight portion by following component: diethylene glycol monobutyl ether 70 parts, lauryl alcohol 10 parts,
Propylene glycol alginate 2 parts, phosphorus pentoxide 30 parts, erythritol 1 part, lauroylamidopropyl betaine 1 part, coconut oil diethyl
Alkylolamides 2 parts, sodium citrate 0.3 part, dehydrated alcohol 5 parts, distilled water 300 parts.
The preparation method of above-mentioned silkete penetrating agent is: diethylene glycol monobutyl ether is added four mouthfuls of reaction bulbs by (1), by temperature liter
To 75 DEG C；(2) it is slowly added into phosphorus pentoxide, insulation reaction 2 hours；(3) lauryl alcohol, propylene glycol alginate, red moss are added
Sugar alcohol, lauroylamidopropyl betaine, lauric acid amide of ethanol, sodium citrate, dehydrated alcohol and distilled water, stir reaction 2
Hour；(4) it is cooled to room temperature, discharging and get final product.
The partial properties index of material of the present invention see table, it may be seen that the alkali resistance of this material is splendid, and resistance to hydrogen-oxygen
Changing sodium solution mass concentration and reach 291g/L, time of penetration is short, the most only needs 97s, and permeability is high, and meanwhile, foaming characteristic is low, it is easy to
Recovery to sodium hydroxide.
The partial properties index of table 1 silkete penetrating agent
| Name of product | Alkali resistance NaOH(g/L) | Time of penetration (/s) | Bubble ratio |
| Embodiment 1 | 284 | 103 | 0 |
| Embodiment 2 | 287 | 101 | 0 |
| Embodiment 3 | 289 | 100 | 0 |
| Embodiment 4 | 291 | 97 | 0 |
| Embodiment 5 | 288 | 98 | 0 |
| Comparative example 1 | 271 | 105 | 0 |
| Comparative example 2 | 274 | 114 | 1 |
Claims (6)
1. a silkete penetrating agent, it is characterised in that: it is prepared from weight portion by following component: diethylene glycol monobutyl ether 50-
70 parts, lauryl alcohol 5-10 part, propylene glycol alginate 1-2 part, phosphorus pentoxide 20-30 part, erythritol 0.5-1 part, phosphoric acid
Calcium dihydrogen 1-2 part, lauroylamidopropyl betaine 0.5-1 part, lauric acid amide of ethanol 1-2 part, sodium citrate 0.1-0.3
Part, tributyl phosphate 0.2-0.5 part, dehydrated alcohol 2-5 part, distilled water 200-300 part.
A kind of silkete penetrating agent the most according to claim 1, it is characterised in that: by following component with weight portion preparation
Become: diethylene glycol monobutyl ether 55-65 part, lauryl alcohol 6-9 part, propylene glycol alginate 1.1-1.6 part, phosphorus pentoxide 22-28
Part, erythritol 0.6-0.9 part, dalcium biphosphate 1.2-1.7 part, lauroylamidopropyl betaine 0.6-0.9 part, coconut oil two
Glycollic amide 1.3-1.7 part, sodium citrate 0.15-0.25 part, tributyl phosphate 0.3-0.4 part, dehydrated alcohol 3-4 part, distillation
Water 220-280 part.
3. the preparation method of a kind of silkete penetrating agent described in any one of claim 1 to 2, it is characterised in that: include following step
Rapid:
(1) diethylene glycol monobutyl ether is added four mouthfuls of reaction bulbs, temperature is risen to 70-75 DEG C；
(2) it is slowly added into phosphorus pentoxide, insulation reaction 1-2 hour；
(3) lauryl alcohol, propylene glycol alginate, erythritol, dalcium biphosphate, lauroylamidopropyl betaine, cocos nucifera oil are added
Acid diglycollic amide, sodium citrate, tributyl phosphate, dehydrated alcohol and distilled water, stirring reaction 1-2 hour；
(4) it is cooled to room temperature, discharging and get final product.
The preparation method of a kind of silkete penetrating agent the most according to claim 3, it is characterised in that: described step (1) rises
Temperature is to 71-74 DEG C.
The preparation method of a kind of silkete penetrating agent the most according to claim 3, it is characterised in that: described step (2) is protected
The temperature response time is 1..5 hour.
The preparation method of a kind of silkete penetrating agent the most according to claim 3, it is characterised in that: described step is stirred in (3)
Mixing the response time is 1.5 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610507641.5A CN106120319A (en) | 2016-07-01 | 2016-07-01 | A kind of silkete penetrating agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610507641.5A CN106120319A (en) | 2016-07-01 | 2016-07-01 | A kind of silkete penetrating agent and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106120319A true CN106120319A (en) | 2016-11-16 |
Family
ID=57468660
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610507641.5A Withdrawn CN106120319A (en) | 2016-07-01 | 2016-07-01 | A kind of silkete penetrating agent and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106120319A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107780211A (en) * | 2017-10-20 | 2018-03-09 | 江苏新瑞贝科技股份有限公司 | A kind of bleeding agent and preparation method thereof |
| CN107794753A (en) * | 2017-10-20 | 2018-03-13 | 江苏新瑞贝科技股份有限公司 | A kind of high temperature resistant bleeding agent and preparation method thereof |
| CN107805941A (en) * | 2017-10-20 | 2018-03-16 | 江苏新瑞贝科技股份有限公司 | A kind of low-foaming penetrating agent and preparation method thereof |
| CN115182165A (en) * | 2022-08-25 | 2022-10-14 | 苏州联胜化学有限公司 | Preparation method of denim sizing penetrating agent |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101434890A (en) * | 2007-11-16 | 2009-05-20 | 比亚迪股份有限公司 | Water-soluble washing agent composition |
| CN101575804A (en) * | 2009-04-25 | 2009-11-11 | 中山市巴斯基化工有限公司 | Alkali-resistant penetrant for short-process pretreatment of pure-cotton woven fabric |
| CN105002755A (en) * | 2015-07-01 | 2015-10-28 | 广东灵捷制造化工有限公司 | Rapid alkali-resistant penetrating agent, and preparation method thereof |
| CN105214348A (en) * | 2015-09-28 | 2016-01-06 | 潘红 | A kind of defoamer |
-
2016
- 2016-07-01 CN CN201610507641.5A patent/CN106120319A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101434890A (en) * | 2007-11-16 | 2009-05-20 | 比亚迪股份有限公司 | Water-soluble washing agent composition |
| CN101575804A (en) * | 2009-04-25 | 2009-11-11 | 中山市巴斯基化工有限公司 | Alkali-resistant penetrant for short-process pretreatment of pure-cotton woven fabric |
| CN105002755A (en) * | 2015-07-01 | 2015-10-28 | 广东灵捷制造化工有限公司 | Rapid alkali-resistant penetrating agent, and preparation method thereof |
| CN105214348A (en) * | 2015-09-28 | 2016-01-06 | 潘红 | A kind of defoamer |
Non-Patent Citations (3)
| Title |
|---|
| 刘建平: "丝光渗透剂的制备与应用", 《印染》 * |
| 孙宝国: "《食品添加剂》", 30 September 2008 * |
| 李东光: "《实用美发用品配方手册》", 31 January 2010 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107780211A (en) * | 2017-10-20 | 2018-03-09 | 江苏新瑞贝科技股份有限公司 | A kind of bleeding agent and preparation method thereof |
| CN107794753A (en) * | 2017-10-20 | 2018-03-13 | 江苏新瑞贝科技股份有限公司 | A kind of high temperature resistant bleeding agent and preparation method thereof |
| CN107805941A (en) * | 2017-10-20 | 2018-03-16 | 江苏新瑞贝科技股份有限公司 | A kind of low-foaming penetrating agent and preparation method thereof |
| CN115182165A (en) * | 2022-08-25 | 2022-10-14 | 苏州联胜化学有限公司 | Preparation method of denim sizing penetrating agent |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106120319A (en) | A kind of silkete penetrating agent and preparation method thereof | |
| CN103194893B (en) | Softener and preparation method thereof | |
| CN103321065A (en) | High-temperature leveling agent, and preparation method and application thereof | |
| CN108976386A (en) | One kind containing natural plants antibacterial and mouldproof compound polyurethane material and preparation method thereof | |
| CN103524201A (en) | Composite material for vegetation restoration and preparation method thereof | |
| CN108018715A (en) | A kind of preparation method of antiflaming finishing agent and fire-retardant regenerated cellulose fiber | |
| CN106592225A (en) | Aromatherapy skin-protection type non-ironing finishing liquid for shirts and finishing method thereof | |
| CN109322164A (en) | One kind is based on hyperbranched poly ester derivant multifunction finishing agent and its preparation and application | |
| CN106592224A (en) | Wear-resisting ironing-free finishing liquid of shirt and finishing method of wear-resisting ironing-free finishing liquid | |
| CN106397776A (en) | Double amino type block polyether amino silicone oil and preparation method thereof | |
| CN105755834A (en) | Novel washable flame-retardant coating and preparation method thereof | |
| CN106283643A (en) | A kind of bafta non-ironing and antibacteria agent and preparation method thereof | |
| CN104074049A (en) | Anti-bacterial clothing softening agent | |
| CN106758200A (en) | The uvioresistant protection type noniron finish liquid and its method for sorting of a kind of shirt | |
| CN103103756A (en) | Linen-imitation finishing agent and preparation method thereof | |
| CN104313877A (en) | Coupling agent modifying method for bamboo fibers | |
| CN105088757A (en) | Preparation method of printing and dyeing finishing agent used for fabric | |
| CN107780211A (en) | A kind of bleeding agent and preparation method thereof | |
| CN107805941A (en) | A kind of low-foaming penetrating agent and preparation method thereof | |
| CN108951126A (en) | A kind of preparation method of nano-negative ion lace fabric | |
| CN107740270A (en) | A kind of environment-friendly antibacterial softener and preparation method thereof | |
| CN110731557B (en) | Constant-temperature blood circulation-promoting radiation-proof silver fiber bra, mold cup and preparation process thereof | |
| CN104233798A (en) | Refreshing and ventilating towel softener | |
| CN109837759B (en) | Antibacterial flame-retardant finishing agent for denim fabric and preparation method thereof | |
| CN107904951A (en) | A kind of preparation method of fluffy looped fabric |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20161116 |
|
| WW01 | Invention patent application withdrawn after publication |