CN106118385A - A kind of UV LED low-yield solidification mahogany furniture coating and preparation method thereof - Google Patents
A kind of UV LED low-yield solidification mahogany furniture coating and preparation method thereof Download PDFInfo
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- CN106118385A CN106118385A CN201610707084.1A CN201610707084A CN106118385A CN 106118385 A CN106118385 A CN 106118385A CN 201610707084 A CN201610707084 A CN 201610707084A CN 106118385 A CN106118385 A CN 106118385A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
- C09D163/10—Epoxy resins modified by unsaturated compounds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/14—Polyurethanes having carbon-to-carbon unsaturated bonds
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The present invention provides a kind of UV LED low-yield solidification mahogany furniture coating and preparation method thereof, and described UV LED low-yield solidification mahogany furniture coating is made up of according to the component of mass fraction following: urethane acrylate oligomer 23 27 parts；Epoxy acrylate oligomer 24 28 parts；Trimethylolpropane trimethacrylate 15 19 parts；Aerosil 0.1 0.5 parts；Light trigger 24 parts；Active ammonia coinitiator: 37 parts；Filling powder: 20 25 parts；Auxiliary agent: 0.4 0.6 parts.Described mahogany furniture coating effectively utilizes UV LED to carry out fast setting as ultraviolet source, there is energy efficient, reduce use cost, the feature of environmental protection, and the curing rate of described coating is fast, and the film performance of formation is good, and the adhesive force on mahogany furniture is strong.
Description
Technical field
The present invention relates to paint field, particularly relate to a kind of UV LED low-yield solidification mahogany furniture coating and preparation side thereof
Method.
Background technology
Traditional UV coating refers to UV-cured resin UV coating, i.e. utilize ultraviolet as solidification the energy, at room temperature
The resin UV coating of lower Quick cross-linking film forming.But traditional UV light source is mainly high voltage mercury lamp, metal halid lamp, and it has electricity
Power consume big, caloric value big, electric energy to the low shortcoming of the conversion ratio of ultraviolet, owing to caloric value is big, easily cause the deformation of base material
Or damage, additionally, high voltage mercury lamp contains noxious substance hydrargyrum, and produce ozone, pollute environment, endanger healthy.
Therefore, prior art needs to improve further.
Summary of the invention
In view of the deficiencies in the prior art, the invention reside in a kind of UV LED low-yield solidification mahogany furniture coating of offer and
Preparation method, can utilize UV-LED lamp to carry out the fast setting of mahogany furniture coating as light source, it is intended to solve to use tradition UV
High energy consumption that light source curing UV photocureable coating brings, high cost, the problem of environmental pollution.
Technical scheme is as follows:
A kind of UV LED low-yield solidification mahogany furniture coating, wherein, described UV LED low-yield solidification mahogany furniture coating by
Form according to the component of mass fraction below:
Urethane acrylate oligomer 23-27 part；
Epoxy acrylate oligomer 24-28 part；
Trimethylolpropane trimethacrylate: 15-19 part；
Aerosil: 0.1-0.5 part；
Light trigger: 2-4 part；
Active ammonia coinitiator: 3-7 part；
Filling powder: 20-25 part；
Auxiliary agent: 0.4-0.6 part.
Described UV LED low-yield solidification mahogany furniture coating, wherein, described UV LED low-yield solidification mahogany furniture
Coating is made up of according to the component of mass fraction following:
Urethane acrylate oligomer 25 parts；
Epoxy acrylate oligomer 26 parts；
Trimethylolpropane trimethacrylate: 17.2 parts；
Aerosil: 0.3 part；
Light trigger: 3 parts；
Active ammonia coinitiator: 5 parts；
Filling powder: 23 parts；
Auxiliary agent: 0.5 part.
Described UV LED low-yield solidification mahogany furniture coating, wherein, described light trigger is the liquid of ketone hydrogen-abstraction
One or more in light trigger, trimethylbenzene acyl group diphenyl phosphine oxide and 2-isopropyl thioxanthone isomer mixture.
Described UV LED low-yield solidification mahogany furniture coating, wherein, described active ammonia coinitiator be active ammonia or
DMAA.
Described UV LED low-yield solidification mahogany furniture coating, wherein, described filling powder is by superfine talcum powder, titanium dioxide
Silicon flatting silica and politef wax composition.
Preferably, described filling powder is by the politef wax that mass ratio is 3:5:15, silicon dioxide flatting silica and to surpass
Fine and smooth stone powder forms.
Described UV LED low-yield solidification mahogany furniture coating, wherein, described auxiliary agent is the dispersant of 3:2 by mass ratio
Form with defoamer.
Described UV LED low-yield solidification mahogany furniture coating, wherein, described defoamer is BYK141, described dispersant
For the block copolymer containing pigment affinity groups or structuring acrylic copolymer.
A kind of preparation method of UV LED as above low-yield solidification mahogany furniture coating, wherein, described preparation side
Method is:
By urethane acrylate oligomer, epoxy acrylate oligomer, trimethylolpropane trimethacrylate puts into container
In, under conditions of rotating speed 600-800rpm/min, disperse 3-7min with dispersion machine, to mix homogeneously；
Put into aerosil, light trigger, active ammonia coinitiator again, fill powder, with dispersion machine at rotating speed 1200-1500
10-20min, pick test is disperseed under conditions of rpm/min；
When fineness reach≤20 microns time, put into auxiliary agent, with rotating speed 600-800rpm/min disperse 3-7min, after mix homogeneously,
To UV LED low-yield solidification mahogany furniture coating.
Beneficial effect: the present invention provides a kind of UV LED low-yield solidification mahogany furniture coating and preparation method thereof, and this is red
Wooden furniture coating effectively utilizes UV LED to carry out fast setting as ultraviolet source, has the effect that 1, energy efficient: with
Traditional high voltage mercury lamp is compared, UV-LED(UV LED) electrical-optical conversion efficiency high, can save 50%-75%'s
Electric power；2, use cost is reduced: UV LED is a cold light source, due to not output in infrared range of spectrum, therefore to painting
Material carries out in solidification process, need not re-use the cooling device of complexity, such as chill roll and gobo, therefore can be used for thermo-responsive
Base material；3, environmental protection: owing to using UV-LED not produce ozone, environmentally safe during carrying out paint solidification；4, solidification
Speed is fast, and the film performance of formation is good, and hardness is strong, and the adhesive force on mahogany furniture is strong.
Detailed description of the invention
For making the purpose of the present invention, technical scheme and effect clearer, clear and definite, below to the present invention the most specifically
Bright.Should be appreciated that specific embodiment described herein, only in order to explain the present invention, is not intended to limit the present invention.
The present invention provides a kind of UV LED low-yield solidification mahogany furniture coating, wherein, the described low-yield solidification of UV LED
Mahogany furniture coating is made up of according to the component of mass fraction following:
Urethane acrylate oligomer 23-27 part；
Epoxy acrylate oligomer 24-28 part；
Trimethylolpropane trimethacrylate: 15-19 part；
Aerosil: 0.1-0.5 part；
Light trigger: 2-4 part；
Active ammonia coinitiator: 3-7 part；
Filling powder: 20-25 part；
Auxiliary agent: 0.4-0.6 part.
Wherein, described light trigger is the liquid light trigger of ketone hydrogen-abstraction, trimethylbenzene acyl group diphenyl phosphine oxide
With one or more in 2-isopropyl thioxanthone isomer mixture.
Wherein, in described formula, mass fraction is that the aerosil of 0.1-0.5 part coordinates other components to coating
Fill powder and there is good anti-settling effect, it is possible to improve the stability of the gloss of film that coating is formed.
Wherein, described active ammonia coinitiator is active ammonia or DMAA.
Wherein, described filling powder is made up of superfine talcum powder, silicon dioxide flatting silica and politef wax.Preferably,
Described filling powder is made up of politef wax, silicon dioxide flatting silica and the superfine talcum powder that mass ratio is 3:5:15.On
State filling powder other compositions of arranging in pairs or groups and improving extinction and the fillibility of coating of proportioning, strengthen the paint film that described coating formed
Feel.
In the formula of described coating, described auxiliary agent is made up of the dispersant that mass ratio is 3:2 and defoamer.Preferably, institute
Stating defoamer is BYK141, and described dispersant is the block copolymer containing pigment affinity groups or structuring acrylic copolymer.
The UV LED low-yield solidification mahogany furniture coating being made up of each component of above-mentioned mass fraction is for redwood man
The application of tool is designed, and not only has the UV LED utilizing energy transformation ratio high and carries out fast setting, and at mahogany furniture
The adhesive force that surface forms coating is good, and hardness is strong, and the feel of coating and glossiness are good.
Preferably, described UV LED low-yield solidification mahogany furniture coating is made up of according to the component of mass fraction following:
Urethane acrylate oligomer 25 parts；
Epoxy acrylate oligomer 26 parts；
Trimethylolpropane trimethacrylate: 17.2 parts；
Aerosil: 0.3 part；
Light trigger: 3 parts；
Active ammonia coinitiator: 5 parts；
Filling powder: 23 parts；
Auxiliary agent: 0.5 part.
The present invention also provides for the preparation method of a kind of UV LED as above low-yield solidification mahogany furniture coating, its
In, described preparation method is:
By urethane acrylate oligomer, epoxy acrylate oligomer, trimethylolpropane trimethacrylate puts into container
In, under conditions of rotating speed 600-800rpm/min, disperse 3-7min with dispersion machine, to mix homogeneously；
Put into aerosil, light trigger, active ammonia coinitiator again, fill powder, with dispersion machine at rotating speed 1200-1500
10-20min, pick test is disperseed under conditions of rpm/min；
When fineness reach≤20 microns time, put into auxiliary agent, with rotating speed 600-800rpm/min disperse 3-7min, after mix homogeneously,
To UV LED low-yield solidification mahogany furniture coating.
The curing of the UV LED low-yield solidification mahogany furniture coating being prepared as is as follows:
Starting LED curing apparatus, the light-emitting area of employing is 620mmx50mm, is placed on conveyer belt by test plate (panel), adjusts conveyer belt
Speed (25m/min), is applied to low-yield for UV LED solidification mahogany furniture coating on test plate (panel), forms coating on test plate (panel).
For making technical scheme clearer, clear and definite, it is exemplified below embodiment to the present invention the most specifically
Bright.
Embodiment 1
The present invention provides a kind of UV LED low-yield solidification mahogany furniture coating, wherein, described UV LED low-yield solidification redwood
Coatings for furniture is made up of the component of following mass fraction:
Urethane acrylate oligomer 25 parts；
Epoxy acrylate oligomer 26 parts；
Trimethylolpropane trimethacrylate 17.2 parts；
Aerosil 0.3 part；
Light trigger: 3%；
Active ammonia coinitiator: 5%；
Filling powder: 23%；
Auxiliary agent: 0.5%.
Described auxiliary agent is made up of the dispersant that mass ratio is 3:2 and defoamer.
Wherein, light trigger is the liquid light trigger of ketone hydrogen-abstraction, and active ammonia coinitiator is active ammonia, fills powder
Being made up of politef wax, silicon dioxide flatting silica and the superfine talcum powder that mass ratio is 3:5:15, defoamer is BYK141,
Dispersant is the block copolymer containing pigment affinity groups.
The present invention also provides for the preparation method of a kind of above-mentioned UV LED low-yield solidification mahogany furniture coating, wherein, described
Preparation method is: by urethane acrylate oligomer, epoxy acrylate oligomer, trimethylolpropane trimethacrylate is thrown
Enter in container, under conditions of rotating speed 700rpm/min, disperse 5min with dispersion machine, to mix homogeneously；Put into gas phase titanium dioxide again
Silicon, light trigger, active ammonia coinitiator, filling powder, disperse 15min with dispersion machine under conditions of rotating speed 1300rpm/min,
Pick test；
When fineness reach≤20 microns time, put into auxiliary agent, with rotating speed 700rpm/min disperse 5min, after mix homogeneously, obtain UV
LED low-yield solidification mahogany furniture coating.
Testing result: the viscosity of the coating of preparation is 2000mPa.S(25 DEG C), fineness≤20 micron, curing rate is
25m/min, curing light source is 395nm.After tested, the hardness of the coating formed on mahogany furniture is China pencil hardness 1H,
Detecting by GB9286-88S standard, the adhesive force of coating reaches 0 grade, and feel and the aesthetics of described coating are optimal.
Embodiment 2
The present invention provides a kind of UV LED low-yield solidification mahogany furniture coating, wherein, described UV LED low-yield solidification redwood
Coatings for furniture is made up of following component in percentage by weight:
Urethane acrylate oligomer 23 parts；
Epoxy acrylate oligomer 28 parts；
Trimethylolpropane trimethacrylate: 15 parts；
Aerosil: 0.5 part；
Light trigger: 4 parts；
Active ammonia coinitiator: 7 parts；
Filling powder: 20 parts；
Auxiliary agent: 0.4 part.
Described auxiliary agent is made up of the dispersant that mass ratio is 3:2 and defoamer.
Wherein, light trigger is trimethylbenzene acyl group diphenyl phosphine oxide, and active ammonia coinitiator is dimethyl allene acyl
Amine, filling powder is the politef wax of 3:6:11, silicon dioxide flatting silica and superfine talcum powder composition, and defoamer is
BYK141, dispersant is structuring acrylic copolymer.
The present invention also provides for the preparation method of a kind of UV LED as above low-yield solidification mahogany furniture coating, described
Preparation method is:
By urethane acrylate oligomer, epoxy acrylate oligomer, trimethylolpropane trimethacrylate puts into container
In, under conditions of rotating speed 600rpm/min, disperse 7min with dispersion machine, to mix homogeneously；
Put into aerosil, light trigger, active ammonia coinitiator again, fill powder, with dispersion machine at rotating speed 1200rpm/
20min, pick test is disperseed under conditions of min；
When fineness reach≤20 microns time, put into auxiliary agent, with rotating speed 600rpm/min disperse 7min, after mix homogeneously, obtain UV
LED low-yield solidification mahogany furniture coating.
Testing result: the viscosity of the coating of preparation is 2000mPa.S(25 DEG C), fineness≤20 micron, curing rate is
25m/min, curing light source is 395nm.After tested, the hardness of the coating formed on mahogany furniture is China pencil hardness 1H,
Detecting by GB9286-88S standard, the adhesive force of coating reaches 0 grade, and feel and the aesthetics of described coating are good.
Embodiment 3
The present invention provides a kind of UV LED low-yield solidification mahogany furniture coating, wherein, described UV LED low-yield solidification redwood
Coatings for furniture is made up of following component in percentage by weight:
Urethane acrylate oligomer 27 parts；
Epoxy acrylate oligomer 24 parts；
Trimethylolpropane trimethacrylate: 19 parts；
Aerosil: 0.1 part；
Light trigger: 2 parts；
Active ammonia coinitiator: 3 parts；
Filling powder: 25 parts；
Auxiliary agent: 0.6 part.
Described auxiliary agent is made up of the dispersant that mass ratio is 3:2 and defoamer.
Wherein, light trigger is 2-isopropyl thioxanthone isomer mixture, and active ammonia coinitiator is active ammonia, fills out
Filling politef wax, silicon dioxide flatting silica and superfine talcum powder composition that powder is 6:6:13, defoamer is BYK141, dispersion
Agent is the block copolymer containing pigment affinity groups.
The present invention also provides for the preparation method of a kind of UV LED as above low-yield solidification mahogany furniture coating, institute
Stating preparation method is:
By urethane acrylate oligomer, epoxy acrylate oligomer, trimethylolpropane trimethacrylate puts into container
In, under conditions of rotating speed 800rpm/min, disperse 3min with dispersion machine, to mix homogeneously；
Put into aerosil, light trigger, active ammonia coinitiator again, fill powder, with dispersion machine at rotating speed 1500rpm/
10min, pick test is disperseed under conditions of min；
When fineness reach≤20 microns time, put into auxiliary agent, with rotating speed 800rpm/min disperse 3min, after mix homogeneously, obtain UV
LED low-yield solidification mahogany furniture coating.
Testing result: the viscosity of the coating of preparation is 2000mPa.S(25 DEG C), fineness≤20 micron, curing rate is
25m/min, curing light source is 395nm.After tested, the hardness of the coating formed on mahogany furniture is China pencil hardness 1H,
Detecting by GB9286-88S standard, the adhesive force of coating reaches 0 grade, and feel and the aesthetics of described coating are good.
It should be appreciated that the application of the present invention is not limited to above-mentioned citing, for those of ordinary skills, can
To be improved according to the above description or to convert, all these modifications and variations all should belong to the guarantor of claims of the present invention
Protect scope.
Claims (9)
1. a UV LED low-yield solidification mahogany furniture coating, it is characterised in that described UV LED low-yield solidification redwood man
Tool coating is made up of according to the component of mass fraction following:
Urethane acrylate oligomer 23-27 part；
Epoxy acrylate oligomer 24-28 part；
Trimethylolpropane trimethacrylate 15-19 part；
Aerosil 0.1-0.5 part；
Light trigger 2-4 part；
Active ammonia coinitiator 3-7 part；
Fill powder 20-25 part；
Auxiliary agent 0.4-0.6 part.
UV LED the most according to claim 1 low-yield solidification mahogany furniture coating, it is characterised in that described UV LED is low
Energy-curable mahogany furniture coating is made up of according to the component of mass fraction following:
Urethane acrylate oligomer 25 parts；
Epoxy acrylate oligomer 26 parts；
Trimethylolpropane trimethacrylate 17.2 parts；
Aerosil 0.3 part；
Light trigger 3 parts；
Active ammonia coinitiator 5 parts；
Fill 23 parts of powder；
Auxiliary agent 0.5 part.
UV LED the most according to claim 1 low-yield solidification mahogany furniture coating, it is characterised in that described light trigger
Liquid light trigger, trimethylbenzene acyl group diphenyl phosphine oxide and 2-isopropyl thioxanthone isomer for ketone hydrogen-abstraction are mixed
One or more in compound.
UV LED the most according to claim 1 low-yield solidification mahogany furniture coating, it is characterised in that described active ammonia is altogether
Initiator is active ammonia or DMAA.
UV LED the most according to claim 1 low-yield solidification mahogany furniture coating, it is characterised in that described filling powder by
Superfine talcum powder, silicon dioxide flatting silica and politef wax composition.
UV LED the most according to claim 5 low-yield solidification mahogany furniture coating, it is characterised in that described filling powder is
It is made up of politef wax, silicon dioxide flatting silica and the superfine talcum powder that mass ratio is 3:5:15.
7. according to the UV LED low-yield solidification mahogany furniture coating according to any one of claim 1 or 2, it is characterised in that
Described auxiliary agent is made up of the dispersant that mass ratio is 3:2 and defoamer.
UV LED the most according to claim 7 low-yield solidification mahogany furniture coating, it is characterised in that described defoamer is
BYK141, described dispersant is the block copolymer containing pigment affinity groups or structuring acrylic copolymer.
9. a preparation method for the UV LED low-yield solidification mahogany furniture coating as according to any one of claim 1-8,
It is characterized in that, described preparation method is:
By urethane acrylate oligomer, epoxy acrylate oligomer, trimethylolpropane trimethacrylate puts into container
In, under conditions of rotating speed 600-800rpm/min, disperse 3-7min with dispersion machine, to mix homogeneously；
Put into aerosil, light trigger, active ammonia coinitiator again, fill powder, with dispersion machine at rotating speed 1200-1500
10-20min, pick test is disperseed under conditions of rpm/min；
When fineness reach≤20 microns time, put into auxiliary agent, with rotating speed 600-800rpm/min disperse 3-7min, after mix homogeneously,
To UV LED low-yield solidification mahogany furniture coating.
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| CN201610707084.1A CN106118385B (en) | 2016-08-23 | 2016-08-23 | A kind of UV LED low energy solidification mahogany furniture coating and preparation method thereof |
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| CN201610707084.1A CN106118385B (en) | 2016-08-23 | 2016-08-23 | A kind of UV LED low energy solidification mahogany furniture coating and preparation method thereof |
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| CN106118385B CN106118385B (en) | 2018-03-27 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107722714A (en) * | 2017-12-05 | 2018-02-23 | 佛山君帝环保科技有限公司 | A kind of UV curable water-bornes environment-friendly ink |
| CN108485480A (en) * | 2016-12-13 | 2018-09-04 | 君子兰化工（上海）有限公司 | Improved UVLED photocureable coating |
| CN108659680A (en) * | 2018-05-23 | 2018-10-16 | 广东顺德三阳化学有限公司 | LED light cures mending paste, preparation method and restorative procedure |
| CN110437731A (en) * | 2019-08-27 | 2019-11-12 | 浙江佑泰新材料科技有限公司 | A kind of UV-LED photocuring vacuum coating bottom coating and preparation method thereof |
| CN110922864A (en) * | 2019-11-21 | 2020-03-27 | 上海巴德士化工新材料有限公司 | UV (ultraviolet) spraying high-transmittance matte clear finish paint and preparation method thereof |
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| CN110922864A (en) * | 2019-11-21 | 2020-03-27 | 上海巴德士化工新材料有限公司 | UV (ultraviolet) spraying high-transmittance matte clear finish paint and preparation method thereof |
| CN110922864B (en) * | 2019-11-21 | 2021-08-17 | 上海巴德士化工新材料有限公司 | UV (ultraviolet) spraying high-transmittance matte clear finish paint and preparation method thereof |
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| Publication number | Publication date |
|---|---|
| CN106118385B (en) | 2018-03-27 |
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