CN108300261A - A kind of aqueous low energy cold light source solidification timber coating and preparation method thereof - Google Patents
A kind of aqueous low energy cold light source solidification timber coating and preparation method thereof Download PDFInfo
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- CN108300261A CN108300261A CN201610722957.6A CN201610722957A CN108300261A CN 108300261 A CN108300261 A CN 108300261A CN 201610722957 A CN201610722957 A CN 201610722957A CN 108300261 A CN108300261 A CN 108300261A
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- Prior art keywords
- aqueous
- low energy
- light source
- cold light
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/14—Polyurethanes having carbon-to-carbon unsaturated bonds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Chemical And Physical Treatments For Wood And The Like (AREA)
Abstract
The invention discloses a kind of aqueous low energy cold light sources to cure timber coating and preparation method thereof, is prepared from the following raw materials in parts by weight：Soluble polyurethane acrylate：45%；Water-soluble modified epoxy acrylate：16%；Aqueous dispersion：0.3%；Alcohol 10%；Aqueous Gas aerosils：0.3%；Flatting silica：5%；Waterborne wax emulsion 2%；Water-soluble photoinitiator：4%；Aqueous defoamer：0.3%；Aqueous levelling agent：0.3%；Deionized water：16.7%；Fungicide 0.1%.The present invention is directed to the coating material solidified energy consumption of UV LED low energy is low, and ozone is not generated, do not contain mercury, environmentally safe, to no damage to human body, curing rate is fast, efficient, more environmentally friendly using water as attenuant.
Description
Technical field
The present invention relates to aqueous cold light source coating, and specifically more particularly to aqueous low energy cold light source solidification timber applies
Material.
Background technology
Traditional being consumed energy by UV-cured resin UV coating is high, and UV coating will produce a large amount of during cured
Ozone, environmental pollution is very big, and harm to the human body is big.
Invention content
It is an object of the invention in view of the above shortcomings of the prior art, provide a kind of aqueous low energy cold light source solidification wood
Door coating and preparation method thereof.
The technical proposal of the invention is realized in this way：
A kind of aqueous low energy cold light source solidification timber coating and preparation method thereof, is prepared from the following raw materials in parts by weight：
Soluble polyurethane acrylate：43-47%；
Water-soluble modified epoxy acrylate：14-18%；
Aqueous dispersion：0.1-0.5%；
Alcohol 8-12%；
Aqueous Gas aerosils：0.1-0.5%；
Flatting silica：4-7%；
Waterborne wax emulsion 1-4%；
Water-soluble photoinitiator：2-6%；
Aqueous defoamer：0.1-0.5%；
Aqueous levelling agent：0.1-0.5%；
Deionized water：14-17%；
Fungicide 0.1%；
Above-mentioned a kind of aqueous low energy cold light source solidification timber coating and preparation method thereof, wherein by following parts by weight
Raw material is made：
Soluble polyurethane acrylate：45%；
Water-soluble modified epoxy acrylate：16%；
Aqueous dispersion：0.3%；
Alcohol 10%；
Aqueous Gas aerosils：0.3%；
Flatting silica：5%；
Waterborne wax emulsion 2%；
Water-soluble photoinitiator：4%；
Aqueous defoamer：0.3%；
Aqueous levelling agent：0.3%；
Deionized water：16.7%；
Fungicide 0.1%；
In above-mentioned a kind of aqueous low energy cold light source solidification timber coating and preparation method thereof, flatting silica is silica.
In above-mentioned a kind of aqueous low energy cold light source solidification timber coating and preparation method thereof, the soluble epoxide
Acrylate is formed by epoxy resin and acrylic or methacrylic acid by esterification.
In above-mentioned a kind of aqueous low energy cold light source solidification timber coating and preparation method thereof, described is aqueous light-initiated
Agent is that ketone takes one or more of hydrogen cracking type mixture liquid photoinitiator, phenylglyoxylic acid ester mixture by force.
In above-mentioned a kind of aqueous low energy cold light source solidification timber coating and preparation method thereof, the waterborne wax emulsion
For oxidized polyethylene wax, palm wax.
In above-mentioned a kind of aqueous low energy cold light source solidification timber coating and preparation method thereof, antifoaming agent is poly- silica
Alkane.
In above-mentioned a kind of aqueous low energy cold light source solidification timber coating and preparation method thereof, the aqueous levelling agent
For organic silicon surfactant or polyether-modified dimethyl silicone polymer.
In above-mentioned a kind of aqueous low energy cold light source solidification timber coating and preparation method thereof, the deionized water is gone
Anion in water removal and cation constituent
Above-mentioned a kind of aqueous low energy cold light source solidification timber coating and preparation method thereof, the preparation method is：
By soluble polyurethane acrylate, soluble epoxide acrylate, aqueous dispersion is put into container, is existed with dispersion machine
Disperse 3-7min under conditions of rotating speed 600-800rpm/min, until being uniformly mixed；Put into again alcohol, aqueous Gas aerosils,
Flatting silica, waterborne wax emulsion, water-soluble photoinitiator, aqueous defoamer, aqueous levelling agent, deionized water and fungicide, with point
It dissipates machine and disperses 10-20min, inspection by sampling under conditions of rotating speed 1200-1500 rpm/min；When fineness reaches≤20 microns,
Coating painting is scraped on a glass without shrinkage cavity phenomenon, and auxiliary agent is put into, and is disperseed 3-7min with rotating speed 600-800rpm/min, is uniformly mixed
Afterwards, aqueous low energy cold light source solidification timber coating is obtained.
The beneficial effects of the present invention are：In UV LED（Light emitting diode）The coating material solidified energy consumption of low energy is low, and not
Ozone is generated, does not contain mercury, environmentally safe, to no damage to human body, curing rate is fast, efficient, is released using water as alkene
Agent is more environmentally friendly.
Specific implementation mode
Described a kind of aqueous low energy cold light source solidification timber coating and preparation method thereof, by the original of following parts by weight
Material is made：
Soluble polyurethane acrylate：45%；
Water-soluble modified epoxy acrylate：16%；
Aqueous dispersion：0.3%；
Alcohol 10%；
Aqueous Gas aerosils：0.3%；
Flatting silica：5%；
Waterborne wax emulsion 2%；
Water-soluble photoinitiator：4%；
Aqueous defoamer：0.3%；
Aqueous levelling agent：0.3%；
Deionized water：16.7%；
Fungicide 0.1%；
The flatting silica is silica.
The soluble epoxide acrylate is by epoxy resin and acrylic or methacrylic acid by esterification
At.
The water-soluble photoinitiator is that ketone takes hydrogen cracking type mixture liquid photoinitiator, the mixing of phenylglyoxylic acid esters by force
One or more of object.
The waterborne wax emulsion is oxidized polyethylene wax, palm wax.
Antifoaming agent is polysiloxanes.
The aqueous levelling agent is organic silicon surfactant or polyether-modified dimethyl silicone polymer.
The deionized water removes the anion and cation constituent in water removal
Above-mentioned a kind of aqueous low energy cold light source solidification timber coating and preparation method thereof, the preparation method is：
By soluble polyurethane acrylate, soluble epoxide acrylate, aqueous dispersion is put into container, is existed with dispersion machine
Disperse 3-7min under conditions of rotating speed 600-800rpm/min, until being uniformly mixed；Put into again alcohol, aqueous Gas aerosils,
Flatting silica, waterborne wax emulsion, water-soluble photoinitiator, aqueous defoamer, aqueous levelling agent, deionized water and fungicide, with point
It dissipates machine and disperses 10-20min, inspection by sampling under conditions of rotating speed 1200-1500 rpm/min；When fineness reaches≤20 microns,
Coating painting is scraped on a glass without shrinkage cavity phenomenon, and auxiliary agent is put into, and is disperseed 3-7min with rotating speed 600-800rpm/min, is uniformly mixed
Afterwards, a kind of aqueous low energy cold light source solidification timber coating and preparation method thereof is obtained.
Preferably, above-mentioned scheme, described a kind of aqueous low energy cold light source solidification timber coating and preparation method thereof,
It is prepared from the following raw materials in parts by weight；
Described a kind of aqueous low energy cold light source solidification timber coating and preparation method thereof, by the raw material system of following parts by weight
At：
Soluble polyurethane acrylate：45%；
Water-soluble modified epoxy acrylate：16%；
Aqueous dispersion：0.3%；
Alcohol 10%；
Aqueous Gas aerosils：0.3%；
Flatting silica：5%；
Waterborne wax emulsion 2%；
Water-soluble photoinitiator：4%；
Aqueous defoamer：0.3%；
Aqueous levelling agent：0.3%；
Deionized water：16.7%；
Fungicide 0.1%；
By soluble polyurethane acrylate, soluble epoxide acrylate, aqueous dispersion is put into container, is existed with dispersion machine
Disperse 3-7min under conditions of rotating speed 600-800rpm/min, until being uniformly mixed；Put into again alcohol, aqueous Gas aerosils,
Flatting silica, waterborne wax emulsion, water-soluble photoinitiator, aqueous defoamer, aqueous levelling agent, deionized water and fungicide, with point
It dissipates machine and disperses 10-20min, inspection by sampling under conditions of rotating speed 1200-1500 rpm/min；When fineness reaches≤20 microns,
Coating painting is scraped on a glass without shrinkage cavity phenomenon, auxiliary agent is put into, 3-7min is disperseed with rotating speed 600-800rpm/min, mixing is equal
After even, aqueous low energy cold light source solidification timber coating is obtained.
The curing for the aqueous low energy cold light source solidification timber coating being prepared into is as follows：
Aqueous low energy cold light source solidification timber coating is applied on test plate (panel), by 65 DEG C of infrared temperature, 5 minutes, coating
After the moisture evaporation of test plate (panel), start LED curing apparatus, the light-emitting area used adjusts line speed for 620mmx50mm
（25m/min）, coating is formed on test plate (panel).
To keep technical scheme of the present invention clearer, clear, it is exemplified below embodiment to the present invention further specifically
It is bright.
Embodiment 1
A kind of aqueous low energy cold light source solidification timber coating of present invention offer and preparation method thereof, wherein described one kind is aqueous
Low energy cold light source solidification timber coating and preparation method thereof is grouped as by following group in percentage by weight：
Soluble polyurethane acrylate：45%；
Water-soluble modified epoxy acrylate：16%；
Aqueous dispersion：0.3%；
Alcohol 10%；
Aqueous Gas aerosils：0.3%；
Flatting silica：5%；
Waterborne wax emulsion 2%；
Water-soluble photoinitiator：4%；
Aqueous defoamer：0.3%；
Aqueous levelling agent：0.3%；
Deionized water：16.7%；
Fungicide 0.1%；
The present invention also provides the preparation methods that a kind of aqueous low energy cold light source cures timber coating and preparation method thereof, wherein
The preparation method is that：
By soluble polyurethane acrylate, soluble epoxide acrylate, aqueous dispersion is put into container, is existed with dispersion machine
Disperse 5min under conditions of rotating speed 700rpm/min, until being uniformly mixed；Put into again alcohol, aqueous Gas aerosils, flatting silica,
Waterborne wax emulsion, water-soluble photoinitiator, aqueous defoamer, aqueous levelling agent, deionized water and fungicide are being turned with dispersion machine
Disperse 15min, inspection by sampling under conditions of 1350 rpm/min of speed；When fineness reaches≤20 microns, coating painting is scraped in glass
Without shrinkage cavity phenomenon on plate, auxiliary agent is put into, a kind of aqueous low energy is obtained with rotating speed 700rpm/min dispersions 5min after mixing
Measure cold light source solidification timber coating and preparation method thereof.
A kind of viscosity of aqueous low energy cold light source solidification timber coating made from the present embodiment is 1500mPa.S（25℃
）, fineness≤20 micron, curing rate 25m/min, curing light source 395nm.After tested, the painting formed on mahogany furniture
The hardness of layer is Chinese pencil 1H, is detected by GB9286-88S standards, and the adhesive force of coating is up to 0 grade, waterproof anti-scratch performance
Good, the feel and aesthetics of the coating are best.
Embodiment 2
A kind of aqueous low energy cold light source solidification timber coating of present invention offer and preparation method thereof, wherein described one kind is aqueous
Low energy cold light source solidification timber coating and preparation method thereof is grouped as by following group in percentage by weight：
Soluble polyurethane acrylate：45%；
Water-soluble modified epoxy acrylate：16%；
Aqueous dispersion：0.3%；
Alcohol 10%；
Aqueous Gas aerosils：0.3%；
Flatting silica：5%；
Waterborne wax emulsion 2%；
Water-soluble photoinitiator：4%；
Aqueous defoamer：0.3%；
Aqueous levelling agent：0.3%；
Deionized water：16.7%；
Fungicide 0.1%；
Wherein, water-soluble photoinitiator is phenylglyoxylic acid ester mixture, and flatting silica is silica flatting silica, model
TS100, antifoaming agent BYK-093, dispersant are the block copolymer or acrylic copolymer ammonium salt of the affinity groups containing pigment.
The present invention also provides a kind of aqueous low energy cold light sources a kind of as described above to cure timber coating and preparation method thereof, institute
Stating preparation method is：
By soluble polyurethane acrylate, soluble epoxide acrylate, aqueous dispersion is put into container, is existed with dispersion machine
Disperse 7min under conditions of rotating speed 600rpm/min, until being uniformly mixed；Put into again alcohol, aqueous Gas aerosils, flatting silica,
Waterborne wax emulsion, water-soluble photoinitiator, aqueous defoamer, aqueous levelling agent, deionized water and fungicide are being turned with dispersion machine
Disperse 20min, inspection by sampling under conditions of 1200 rpm/min of speed；When fineness reaches≤20 microns, coating painting is scraped in glass
Without shrinkage cavity phenomenon on plate, auxiliary agent is put into, a kind of aqueous low energy is obtained with rotating speed 600rpm/min dispersions 7min after mixing
Measure cold light source solidification timber coating and preparation method thereof.
A kind of viscosity of aqueous low energy cold light source solidification timber coating made from the present embodiment is 1500mPa.S（25℃
）, curing rate 25m/min, curing light source 395nm.The hardness of the coating formed on timber furniture is Chinese pencil 1H,
For the adhesive force of coating up to 0 grade, waterproof anti-scratch performance is good.
Embodiment 3
A kind of aqueous low energy cold light source solidification timber coating of present invention offer and preparation method thereof, wherein described for a kind of water
Property low energy cold light source solidification timber coating and preparation method thereof be grouped as by following group in percentage by weight：
Soluble polyurethane acrylate：45%；
Water-soluble modified epoxy acrylate：16%；
Aqueous dispersion：0.3%；
Alcohol 10%；
Aqueous Gas aerosils：0.3%；
Flatting silica：5%；
Waterborne wax emulsion 2%；
Water-soluble photoinitiator：4%；
Aqueous defoamer：0.3%；
Aqueous levelling agent：0.3%；
Deionized water：16.7%；
Fungicide 0.1%；
Wherein, photoinitiator is phenylglyoxylic acid ester mixture, and flatting silica is silica flatting silica, and model TS100 disappears
Infusion is BYK-093, and dispersant is the block copolymer of the affinity groups containing pigment.
The present invention also provides a kind of as described above for a kind of aqueous low energy cold light source solidification timber coating and its preparation
Method, the preparation method is that：
By soluble polyurethane acrylate, soluble epoxide acrylate, aqueous dispersion is put into container, is existed with dispersion machine
Disperse 3min under conditions of rotating speed 800rpm/min, until being uniformly mixed；Put into again alcohol, aqueous Gas aerosils, flatting silica,
Waterborne wax emulsion, water-soluble photoinitiator, aqueous defoamer, aqueous levelling agent, deionized water and fungicide are being turned with dispersion machine
Disperse 10min, inspection by sampling under conditions of 1500 rpm/min of speed；When fineness reaches≤20 microns, coating painting is scraped in glass
Without shrinkage cavity phenomenon on plate, auxiliary agent is put into, 3min is disperseed with rotating speed 800rpm/min, after mixing, is obtained for a kind of aqueous low
Energy cold light source cures timber coating and preparation method thereof.
A kind of the present embodiment viscosity obtained for curing timber coating for aqueous low energy cold light source is 1500mPa.S（25
℃ ）, curing rate 25m/min, curing light source 395nm.The hardness of the coating formed on timber is Chinese pencil 1H, is applied
For the adhesive force of layer up to 0 grade, waterproof anti-scratch performance is good.
The aqueous low energy cold light source of the present invention cures timber paint in UV LED（Light emitting diode）Low energy is coating material solidified
It consumes energy low, and does not generate ozone, do not contain mercury, environmentally safe, to no damage to human body, curing rate is fast, efficient,
It is more environmentally friendly using water as attenuant.
Claims (10)
1. a kind of aqueous low energy cold light source solidification timber coating and preparation method thereof, it is characterised in that：By following parts by weight
Raw material be made：
Soluble polyurethane acrylate：43-47%；
Water-soluble modified epoxy acrylate：14-18%；
Aqueous dispersion：0.1-0.5%；
Alcohol 8-12%；
Aqueous Gas aerosils：0.1-0.5%；
Flatting silica：4-7%；
Waterborne wax emulsion 1-4%；
Water-soluble photoinitiator：2-6%；
Aqueous defoamer：0.1-0.5%；
Aqueous levelling agent：0.1-0.5%；
Deionized water：14-17%；
Fungicide 0.1%；.
2. a kind of aqueous low energy cold light source solidification timber coating according to claim 1 and preparation method thereof, feature
It is, the aqueous low energy cold light source cures timber coating, is prepared from the following raw materials in parts by weight：
Soluble polyurethane acrylate：45%；
Water-soluble modified epoxy acrylate：16%；
Aqueous dispersion：0.3%；
Alcohol 10%；
Aqueous Gas aerosils：0.3%；
Flatting silica：5%；
Waterborne wax emulsion 2%；
Water-soluble photoinitiator：4%；
Aqueous defoamer：0.3%；
Aqueous levelling agent：0.3%；
Deionized water：16.7%；
Fungicide 0.1%；.
3. a kind of aqueous low energy cold light source solidification timber coating according to claim 1 and preparation method thereof, feature
It is, the flatting silica is silica.
4. aqueous low energy cold light source according to claim 1 cures timber coating, which is characterized in that the water solubility
Epoxy acrylate is formed by epoxy resin and acrylic or methacrylic acid by esterification.
5. a kind of aqueous low energy cold light source solidification timber coating according to claim 1 and preparation method thereof, feature
It is, the water-soluble photoinitiator is that ketone takes hydrogen cracking type mixture liquid photoinitiator, phenylglyoxylic acid ester mixture by force
One or more of.
6. a kind of aqueous low energy cold light source solidification timber coating according to claim 1 and preparation method thereof, feature
It is, the waterborne wax emulsion is oxidized polyethylene wax or palm wax.
7. a kind of aqueous low energy cold light source solidification timber coating according to claim 1 and preparation method thereof, feature
It is, the antifoaming agent is polysiloxanes.
8. a kind of aqueous low energy cold light source solidification timber coating according to claim 1 and preparation method thereof, feature
It is, the aqueous levelling agent is organic silicon surfactant or polyether-modified dimethyl silicone polymer.
9. a kind of aqueous low energy cold light source solidification timber coating according to claim 1 and preparation method thereof, feature
It is, the deionized water removes the anion and cation constituent in water removal.
10. a kind of aqueous low energy cold light source solidification timber coating according to any one of claim 1-10 and its system
Preparation Method, which is characterized in that the preparation method is：
By soluble polyurethane acrylate, soluble epoxide acrylate, aqueous dispersion is put into container, is existed with dispersion machine
Disperse 3-7min under conditions of rotating speed 600-800rpm/min, until being uniformly mixed；Put into again alcohol, aqueous Gas aerosils,
Flatting silica, waterborne wax emulsion, water-soluble photoinitiator, aqueous defoamer, aqueous levelling agent, deionized water and fungicide, with point
It dissipates machine and disperses 10-20min, inspection by sampling under conditions of rotating speed 1200-1500 rpm/min；When fineness reaches≤20 microns,
Coating painting is scraped on a glass without shrinkage cavity phenomenon, and auxiliary agent is put into, and is disperseed 3-7min with rotating speed 600-800rpm/min, is uniformly mixed
Afterwards, aqueous low energy cold light source solidification timber coating is obtained.
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| CN201610722957.6A CN108300261A (en) | 2016-08-25 | 2016-08-25 | A kind of aqueous low energy cold light source solidification timber coating and preparation method thereof |
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|---|---|---|---|
| CN201610722957.6A CN108300261A (en) | 2016-08-25 | 2016-08-25 | A kind of aqueous low energy cold light source solidification timber coating and preparation method thereof |
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| CN115651509A (en) * | 2022-10-20 | 2023-01-31 | 湖州市南浔区绿色家居产业研究院 | Photocuring floor coating and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN110066578A (en) * | 2019-05-21 | 2019-07-30 | 临沂优彩新能源环保科技有限公司 | A kind of aqueous UV surface treating agent of woodenware |
| CN115651509A (en) * | 2022-10-20 | 2023-01-31 | 湖州市南浔区绿色家居产业研究院 | Photocuring floor coating and preparation method thereof |
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Application publication date: 20180720 |