CN106113186A - A kind of method of Wooden modifying - Google Patents

A kind of method of Wooden modifying Download PDF

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Publication number
CN106113186A
CN106113186A CN201610631191.0A CN201610631191A CN106113186A CN 106113186 A CN106113186 A CN 106113186A CN 201610631191 A CN201610631191 A CN 201610631191A CN 106113186 A CN106113186 A CN 106113186A
Authority
CN
China
Prior art keywords
dried
timber
immersion
moisture content
content less
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610631191.0A
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Chinese (zh)
Inventor
唐荣燕
王博
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nanjing Bojun New Material Co Ltd
Original Assignee
Nanjing Bojun New Material Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nanjing Bojun New Material Co Ltd filed Critical Nanjing Bojun New Material Co Ltd
Priority to CN201610631191.0A priority Critical patent/CN106113186A/en
Publication of CN106113186A publication Critical patent/CN106113186A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/02Processes; Apparatus
    • B27K3/0207Pretreatment of wood before impregnation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K3/00Impregnating wood, e.g. impregnation pretreatment, for example puncturing; Wood impregnation aids not directly involved in the impregnation process
    • B27K3/02Processes; Apparatus
    • B27K3/08Impregnating by pressure, e.g. vacuum impregnation
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/001Heating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27KPROCESSES, APPARATUS OR SELECTION OF SUBSTANCES FOR IMPREGNATING, STAINING, DYEING, BLEACHING OF WOOD OR SIMILAR MATERIALS, OR TREATING OF WOOD OR SIMILAR MATERIALS WITH PERMEANT LIQUIDS, NOT OTHERWISE PROVIDED FOR; CHEMICAL OR PHYSICAL TREATMENT OF CORK, CANE, REED, STRAW OR SIMILAR MATERIALS
    • B27K5/00Treating of wood not provided for in groups B27K1/00, B27K3/00
    • B27K5/007Treating of wood not provided for in groups B27K1/00, B27K3/00 using pressure

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Wood Science & Technology (AREA)
  • Forests & Forestry (AREA)
  • Chemical And Physical Treatments For Wood And The Like (AREA)

Abstract

A kind of method that the invention discloses Wooden modifying, comprises the steps: 1) timber to be modified is positioned in immersion can, carry out suction process when heating, air in this immersion can completely or almost completely is excluded;2) maintaining the vacuum state of step 1), immersion can is cooled to less than 25 DEG C, is incorporated in immersion can by the Wood modifier of 05 DEG C, until being totally submerged by timber, then pressurizes;3) after being emptied by impregnation liquid, lumber kiln dried stage by stage delivered to by evacuation heating precuring timber, 55 DEG C are dried to moisture content less than 30%, 65 DEG C are dried to moisture content less than 20%, and 80 DEG C are dried to moisture content less than 15%, and 120 DEG C are dried to moisture content less than 8%;5) dried timber carries out thermosetting compression process, the method using this Wooden modifying on hot press, and the volume rate of body weight gain of timber is greatly enhanced.

Description

A kind of method of Wooden modifying
Technical field
A kind of method that present invention relates particularly to Wooden modifying.
Background technology
Timber is widely used in as a kind of renewable environmental friendliness shaped material and lives closely bound up place with people, as Building, furniture etc., it is easily processed, and carrying capacity of environment is little, be steel, cement incomparable, but, timber as one organic Natural macromolecular material, exists inflammable, perishable, easily damage by worms, size is unstable, physical and mechanical property energy consumption is low problem, this A little problems make the application of timber be very limited, in order to overcome the disadvantages mentioned above of timber, people think timber impregnates change its Functional improvement reagent of character, such as, fire retardant, preservative, antifungus agent and the resin etc. of its mechanical property of change.
In Wooden modifying of the prior art, using vacuum impregnation to process, the purpose of do so, is in order to as far as possible The air being present in timber capillary tube is extracted out and goes, then, be injected in timber impregnating liquid under stress, due to when wood In material, air cannot drain, and the internal pressure of wood cell wall and external pressure pressure reduction to a great extent is the least, thus timber The ability of absorption impregnating fluid.
Summary of the invention
A kind of method that Wooden modifying is provided of the present invention.
In order to solve the problems referred to above, the technical solution adopted in the present invention is such, a kind of method of Wooden modifying, bag Include following steps:
1) timber to be modified is positioned in immersion can, carries out suction process, by this immersion can hollow when heating Gas completely or almost completely excludes, and suction time is 2-4 hour, and vacuum is 2400-2600Pa, and temperature is 100- 120℃;
2) maintain the vacuum state of step 1), after immersion can is cooled to room temperature, the Wood modifier of 0-5 DEG C is incorporated into and impregnates In tank, until being totally submerged by timber, then pressurizeing, the process time is 6-8 hour, pressure >=1.0MPa;
3) evacuation heating precuring 0.5-1 hour after being emptied by impregnation liquid, vacuum is 2400-2600Pa, and temperature is 45- 50℃;
4) lumber kiln dried stage by stage delivered to by the timber after precuring, and 55 DEG C are dried to moisture content less than 30%, 65 DEG C Being dried to moisture content less than 20%, 80 DEG C are dried to moisture content less than 15%, and 120 DEG C are dried to moisture content less than 8%;
5) dried timber carries out thermosetting compression process on hot press, and pressure is 9-11MPa, and temperature is 185-200 DEG C.
Preferably, step 2) in pressure be 1.0-1.5MPa, step 2) in immersion can be cooled to 0-5 DEG C.
Preferably, after the air that Wood modifier is contained in getting rid of it under vacuum, it is re-introduced in immersion can.
The Wood modifier that Wood modifier of the present invention is known in the art.
Beneficial effect: 1, the present invention is in a heated state, timber can expand, now evacuation under state, air in timber Discharging all or almost all, after cooling, then with after cold modifying agent immersion, in timber, remaining air compresses and causes true Dummy status, so borrows external air pressure fall Wood modification agent to be pressed onto in timber, improves and impregnate effect, the volume weightening finish of timber Rate is greatly enhanced.
2, the pre-heat cure of the present invention decreases timber and moves to the outflow of Wood modifier during dry kiln.
3, precuring of the present invention uses and is dried stage by stage, saves while energy, Wood modifier coagulation result good and Uniformly.
Detailed description of the invention
Embodiment 1
A kind of method of Wooden modifying, comprises the steps:
1) timber to be modified is positioned in immersion can, carries out suction process, by this immersion can hollow when heating Gas completely or almost completely excludes, and suction time is 2-4 hour, and vacuum is 2400-2600Pa, and temperature is 100- 120℃;
2) maintain the vacuum state of step 1), after immersion can is cooled to room temperature, the Wood modifier of 0-5 DEG C (is made in vacuum After the air contained in it of lower eliminating) it is incorporated in immersion can, until timber is totally submerged, then pressurize, process the time For 6-8 hour, pressure was 1.0-1.5MPa;
3) evacuation heating precuring 0.5-1 hour after being emptied by impregnation liquid, vacuum is 2400-2600Pa, and temperature is 45- 50℃;
4) lumber kiln dried stage by stage delivered to by the timber after precuring, and 55 DEG C are dried to moisture content less than 30%, 65 DEG C Being dried to moisture content less than 20%, 80 DEG C are dried to moisture content less than 15%, and 120 DEG C are dried to moisture content less than 8%;
5) dried timber carries out thermosetting compression process on hot press, and pressure is 9-11MPa, and temperature is 185-200 DEG C.
Embodiment 2
A kind of method of Wooden modifying, comprises the steps:
1) timber to be modified is positioned in immersion can, carries out suction process, by this immersion can hollow when heating Gas completely or almost completely excludes, and suction time is 2-4 hour, and vacuum is 2400-2600Pa, and temperature is 100- 120℃;
2) maintain the vacuum state of step 1), after immersion can is cooled to 0-5 DEG C, the Wood modifier of 0-5 DEG C (is made in vacuum After the air contained in it of lower eliminating) it is incorporated in immersion can, until timber is totally submerged, then pressurize, process the time For 6-8 hour, pressure was 1.0-1.5MPa;
3) evacuation heating precuring 0.5-1 hour after being emptied by impregnation liquid, vacuum is 2400-2600Pa, and temperature is 45- 50℃;
4) lumber kiln dried stage by stage delivered to by the timber after precuring, and 55 DEG C are dried to moisture content less than 30%, 65 DEG C Being dried to moisture content less than 20%, 80 DEG C are dried to moisture content less than 15%, and 120 DEG C are dried to moisture content less than 8%;
5) dried timber carries out thermosetting compression process on hot press, and pressure is 9-11MPa, and temperature is 185-200 DEG C.
After above-mentioned method of modifying, the volume rate of body weight gain of timber respectively reaches 42%, and 45%.
Embodiment described above is only to be described the preferred embodiment of the present invention, the not model to the present invention Enclose and be defined, on the premise of designing spirit without departing from the present invention, the those of ordinary skill in the art technical side to the present invention Various deformation that case is made and improvement, all should fall in the protection domain that claims of the present invention determines.

Claims (4)

1. the method for a Wooden modifying, it is characterised in that comprise the steps:
1) timber to be modified is positioned in immersion can, carries out suction process, by this immersion can hollow when heating Gas completely or almost completely excludes, and suction time is 2-4 hour, and vacuum is 2400-2600Pa, and temperature is 100- 120℃;
2) maintaining the vacuum state of step 1), immersion can is cooled to less than 25 DEG C, is incorporated into by the Wood modifier of 0-5 DEG C and impregnates In tank, until being totally submerged by timber, then pressurizeing, the process time is 6-8 hour, pressure >=1.0MPa;
3) evacuation heating precuring 0.5-1 hour after being emptied by impregnation liquid, vacuum is 2400-2600Pa, and temperature is 45- 50℃;
4) lumber kiln dried stage by stage delivered to by the timber after precuring, and 55 DEG C are dried to moisture content less than 30%, 65 DEG C Being dried to moisture content less than 20%, 80 DEG C are dried to moisture content less than 15%, and 120 DEG C are dried to moisture content less than 8%;
5) dried timber carries out thermosetting compression process on hot press, and pressure is 9-11MPa, and temperature is 185-200 DEG C.
The method of a kind of Wooden modifying the most according to claim 1, it is characterised in that step 2) in immersion can be cooled to 0- 5℃。
The method of a kind of Wooden modifying the most according to claim 1, it is characterised in that step 2) in pressure be 1.0- 1.5MPa。
The method of a kind of Wooden modifying the most according to claim 1, it is characterised in that Wood modifier is under vacuum After air contained in getting rid of it, it is re-introduced in immersion can.
CN201610631191.0A 2016-08-04 2016-08-04 A kind of method of Wooden modifying Pending CN106113186A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610631191.0A CN106113186A (en) 2016-08-04 2016-08-04 A kind of method of Wooden modifying

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610631191.0A CN106113186A (en) 2016-08-04 2016-08-04 A kind of method of Wooden modifying

Publications (1)

Publication Number Publication Date
CN106113186A true CN106113186A (en) 2016-11-16

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107718204A (en) * 2017-09-12 2018-02-23 海宁恒森家具有限公司 A kind of preparation method of flame-proof antibiotic timber
CN110815462A (en) * 2019-11-18 2020-02-21 中国林业科学研究院木材工业研究所 Treatment method of impregnated rubber wood
US11498240B2 (en) 2017-12-29 2022-11-15 Ahf, Llc Densified wood including process for preparation

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102398289A (en) * 2011-10-28 2012-04-04 夏国华 Wood modifying method
CN102433983A (en) * 2011-08-25 2012-05-02 上海黎众木业有限公司 Full-poplar multilayer engineered solid wood flooring and production method thereof
CN102941605A (en) * 2012-10-24 2013-02-27 永港伟方(北京)科技股份有限公司 Special wood modifier and preparation method thereof
CN105751335A (en) * 2016-03-10 2016-07-13 内蒙古农业大学 Novel modified wood and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102433983A (en) * 2011-08-25 2012-05-02 上海黎众木业有限公司 Full-poplar multilayer engineered solid wood flooring and production method thereof
CN102398289A (en) * 2011-10-28 2012-04-04 夏国华 Wood modifying method
CN102941605A (en) * 2012-10-24 2013-02-27 永港伟方(北京)科技股份有限公司 Special wood modifier and preparation method thereof
CN105751335A (en) * 2016-03-10 2016-07-13 内蒙古农业大学 Novel modified wood and preparation method thereof

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
达道安 主编: "《真空设计手册》", 31 July 2004, 国防工业出版社 *

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107718204A (en) * 2017-09-12 2018-02-23 海宁恒森家具有限公司 A kind of preparation method of flame-proof antibiotic timber
CN108748499A (en) * 2017-09-12 2018-11-06 海宁恒森家具有限公司 The preparation method of modified flame-proof antibiotic timber
CN107718204B (en) * 2017-09-12 2019-02-22 海宁恒森家具有限公司 A kind of preparation method of flame-proof antibiotic timber
US11498240B2 (en) 2017-12-29 2022-11-15 Ahf, Llc Densified wood including process for preparation
US11931917B2 (en) 2017-12-29 2024-03-19 Ahf, Llc Densified wood including process for preparation
CN110815462A (en) * 2019-11-18 2020-02-21 中国林业科学研究院木材工业研究所 Treatment method of impregnated rubber wood

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Application publication date: 20161116