CN106109531A - A kind of production method of Flos Lonicerae breaking cellular wall decoction pieces - Google Patents
A kind of production method of Flos Lonicerae breaking cellular wall decoction pieces Download PDFInfo
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- CN106109531A CN106109531A CN201610554166.7A CN201610554166A CN106109531A CN 106109531 A CN106109531 A CN 106109531A CN 201610554166 A CN201610554166 A CN 201610554166A CN 106109531 A CN106109531 A CN 106109531A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/35—Caprifoliaceae (Honeysuckle family)
- A61K36/355—Lonicera (honeysuckle)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/0087—Galenical forms not covered by A61K9/02 - A61K9/7023
- A61K9/0095—Drinks; Beverages; Syrups; Compositions for reconstitution thereof, e.g. powders or tablets to be dispersed in a glass of water; Veterinary drenches
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
- A61K9/16—Agglomerates; Granulates; Microbeadlets ; Microspheres; Pellets; Solid products obtained by spray drying, spray freeze drying, spray congealing,(multiple) emulsion solvent evaporation or extraction
- A61K9/1605—Excipients; Inactive ingredients
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/15—Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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Abstract
The invention discloses the production method of a kind of Flos Lonicerae breaking cellular wall decoction pieces, belong to Chinese medicine production technical field.It comprises the steps: (1) raw material selection;(2) it is dried;(3) pulverize, sieve;(4) wall breaking pulverization;(5) pelletize;(6) packaging;(7) storage.The Flos Lonicerae breaking cellular wall decoction pieces of the present invention, uses the form of teabag, i.e. steeps and i.e. drink, easy to use;Product uses vibrating dryer to dry, and drying materials is uniform, and drying time is short;Material is after wall breaking pulverization, and plant cell wall framework is destroyed, so that product obtains the rapid dissolution of composition when brewing, and dissolved element content is gone out high than general wild honeysuckle flower tea bubble.
Description
Technical field
The present invention relates to the production method of a kind of Flos Lonicerae breaking cellular wall decoction pieces, belong to Chinese medicine production technical field.
Background technology
Flos Lonicerae is the general name that ash chain hairy honeysuckle, Flos Lonicerae, Lonicera confusa, Huang take off the flower of hairy honeysuckle.General early summer flower
Gather before opening, be dried.
" Flos Lonicerae is separated by Chinese Pharmacopoeia 2005 version from Flos Lonicerae, and define Flos Lonicerae be caprifoliaceae plant ash
Chain hairy honeysuckle Lonicera macranthoides Hand.-Mazz., Flos Lonicerae Lonicera hypoglauca Miq,
Lonicera confusa Lonicera confusa D C. or Huang take off hairy honeysuckle Lonicera fulvotomentosa Hsu et
The flower that the dry flower of S.C.Cheng or band are just opened.Flos Lonicerae is then caprifoliaceae plant Radix Ophiopogonis Lonicera japonica
Thunb. dry flower or the first flower opened of band.
Flos Lonicerae main chemical compositions has volatile oil, flavonoid, organic acid, glycoside etc., and its Content of Chlorogenic Acid composition contains
Amount be Flos Lonicerae more than 1 times (see [1] Li Hongxia, Wang Xueqin, Li Zhenguo, Liu Naiqiang, model. different sources Flos Lonicerae and mountain
The comparision contents of Flos Lonicerae main component, China Dispensary, 2011,22 (31): 2935-2937. [2] Zhang little Na, Xue Qiang, Li Ye, slowly
Dawn is beautiful. Henan Flos Lonicerae and the comparison of Xiushan Mountain Flos Lonicerae main component, and Chinese Chemical Society cooperation by production, study and research seminar,
2013), another such as largeflower-like honeysuckle flower saponin second, asperosaponin the second grade Han active component.
" Chinese Pharmacopoeia " version in 2015 thinks Flos Lonicerae sweet in the mouth cold in nature, returns lung, the heart, stomach warp, has heat clearing away solution to stroll, dispelling wind and heat pathogens
Effect, and for stewing the treatment of the diseases such as swollen furuncle, sore throat, erysipelas, toxic-heat and blood stasis, anemopyretic cold, epidemic febrile disease heating.
Flos Lonicerae was appended the plant into food and medicament dual-purpose in 2015.The dry processing of its fresh plants and flowers is typically dried in the air
Dry or dry, it is dried after separately having the fresh process of stir-fry, steam is dried after processing, be dried after sulphuring, bright solid carbon dioxide divides directly with the machine that completes
Drying etc. is carried out again after completing.Flos Lonicerae has an effective component extracting for deep processing, or Flos Lonicerae with other medical material through carrying
Pharmaceutical formulation, teabag drink etc. is made after taking.
The processing method of Flos Lonicerae decoction pieces is generally now, after flower is gathered, selects the removing impurity such as stem, leaf, then with roasting
Case is dried;Or after frying fresh process, it is dried that (steam is dried after processing, is dried after sulphuring, bright solid carbon dioxide divides and directly kills with the machine that completes
Dry again after green grass or young crops), then it is packaged into finished product.Such as Chinese invention patent application number is " the one of CN201110175689.8
Plant the wild honeysuckle flower tea processing method reducing chlorogenic acid loss ", disclose a kind of wild honeysuckle flower tea processing side reducing chlorogenic acid loss
Method, directly quickly completes with high-temperature steam, more quickly cool down with cold gas after harvesting, final high temperature hot blast flash baking,
Rear cooling is sealed up for safekeeping.
1, baking box is dried: general baking time all needs more than tens of hours, and the time is long, and energy waste is big, and cost is high;
2, being dried after frying fresh process: the temperature of process is not easily controlled, batch can not be excessive, can only be handicraft workshop behaviour
Make.
3, being dried after steam processes: general moisture the most after treatment is high, the bad flower fair of automatic steam control is wet soft and adhesion, shadow
Ring quality;
4, sulphuring post-drying: sulfur residual quantity typically can be made defective;
5, the process post-drying that completes is a shade better, and the major part that completes microwave deactivation of enzyme does not meets traditional Chinese medicine processing method,
Flos Lonicerae effective ingredient may be made to be destroyed from molecular level simultaneously, affect quality.
6, dried Flos Lonicerae is directly packaged into finished product, can give user use on inconvenience and consumption on not
Accurately.
7, when Instant Drinks, usually Flos Lonicerae whole flower brews, and composition leaches relatively slow, and brewing time is long, does not meets the modern times
The fast joint of people gathers life.
In consideration of it, be necessary to develop a kind of new Flos Lonicerae breaking cellular wall tea bubble decoction pieces, to make up the deficiencies in the prior art.This
Bright is to dry for Flos Lonicerae raw material or drying time is long, quality is wayward and Flos Lonicerae decoction pieces brewing time is long,
Composition is not easy dissolution and each takes the not accurate enough shortcoming of dosage and the production technology side of a kind of Flos Lonicerae decoction pieces that improves
Method.After selecting, processing, the modern Chinese medicine production technology of recycling by Flos Lonicerae carry out vibration drying, coarse pulverization, breaking cellular wall
Pulverize, pelletize, the operation of the operation such as packaging, make that packaging quantity is clear and definite, dosage accurate, taking convenience, composition is readily soluble when brewing
Go out, exquisite Tea containing traditional Chinese medicine that brewing time is short bubble decoction pieces.
Summary of the invention
Present invention aim to address the deficiencies in the prior art, it is provided that the production method of a kind of Flos Lonicerae breaking cellular wall decoction pieces.This
The Flos Lonicerae breaking cellular wall decoction pieces of invention, uses the form of teabag, i.e. steeps and i.e. drink, easy to use;Product uses vibrating dryer to dry
Dry, drying materials is uniform, and drying time is short;Material is after wall breaking pulverization, and plant cell wall framework is destroyed, so that product exists
Obtain composition rapid dissolution when brewing, and dissolved element content is gone out high than general wild honeysuckle flower tea bubble.
The technical scheme is that the production method of a kind of Flos Lonicerae breaking cellular wall decoction pieces, bag
Include following steps:
(1) raw material selection: take fresh Flos Lonicerae, removes stem, leaf, obtains clean Flos Lonicerae;
(2) it is dried: the clean Flos Lonicerae that step (1) is obtained, uses vibrating dryer, be dried to moisture content 5~12%, institute
The frequency of vibration stating vibrating dryer is 30~38Hz, and time of vibration is 40 seconds, baking temperature 100~105 DEG C, obtains dry mountain silver
Flower;
(3) pulverize, sieve: dry Flos Lonicerae step (2) obtained is pulverized, and sieves, obtains Flos Lonicerae powder;
(4) wall breaking pulverization: Flos Lonicerae powder step (3) obtained, carries out wall breaking pulverization, obtains Flos Lonicerae wall cell disruption powder;
(5) pelletize: the Flos Lonicerae wall cell disruption powder that step (4) is obtained, by Flos Lonicerae wall cell disruption powder and purified water weight ratio 100:
20~22, add purified water, mix homogeneously, then pelletize, sieve, dry to moisture content≤6%, obtain Flos Lonicerae granule;
(6) packaging: the Flos Lonicerae granule that step (5) is obtained, packaging, obtain packaged Flos Lonicerae granule;
(7) storage: packaged Flos Lonicerae granule step (5) obtained, loads in foil laminated film bag, evacuation
After, put in shady and cool storehouse, and hide with gobo, i.e. obtain described Flos Lonicerae breaking cellular wall decoction pieces.
The Flos Lonicerae breaking cellular wall decoction pieces of the present invention uses the form of teabag, i.e. steeps and i.e. drinks, easy to use;Material uses vibration
Drying machine, can make material dry while quickly completing, and drying time is short, and material component is destroyed hardly, thus protects
Hold former feature of plant.Further, since material is vibration drying, dry evenly;Material after wall breaking pulverization, plant cell ledge
Structure is destroyed, so that product obtains the rapid dissolution of composition when brewing, and dissolved element content is than general wild honeysuckle flower tea bubble punching
Go out to want height.
Wherein, the effect of step (1) is the quality controlling raw material, from Sources controlling quality, it is ensured that final products
Quality.
On the basis of technique scheme, the present invention can also do following improvement.
Further, the mesh number sieved described in step (3) is 24 mesh.
Use and above-mentioned further provide the benefit that: use and pulverize, sieve, make the plant framework of Flos Lonicerae be destroyed, from
And when brewing, beneficiating ingredient is more easy to settle out, brewing time is short.
The aperture of above-mentioned 24 mesh sieves is 850 ± 29 μm.
Further, the mesh number sieved described in step (5) is 16~18 mesh, and described drying uses vibrating dryer, dries temperature
Degree is 100~105 DEG C.
The aperture of above-mentioned 16 mesh sieves is 1180 μm, and the aperture of 18 mesh sieves is 1000 μm.
Further, step (6) described packaging, it is the Flos Lonicerae granule that step (5) is obtained, first uses filter paper bag inner packing,
Add foil laminated film bag outer package again.
Use and above-mentioned further provide the benefit that: readily soluble effective ingredient is leached by the filter opening of filter paper bag, insoluble
Medicinal residues are stayed in filter paper bag because there being filter paper to stop so that brew liquid bright, of good quality, haze-free.
Further, the temperature < 20 DEG C in the described shady and cool storehouse of step (6).
Use and above-mentioned further provide the benefit that: the stability of product quality can be kept, extend the shelf life.
The present invention is to use modern medicines preparation technique, the technique formulated according to the characteristic of Flos Lonicerae.Process repeatability, steady
Qualitative good, workable;Product meets drug's GMP requirement, and capability and performance is excellent.Used production equipment such as pulverizer,
Wall-broken grinder, vibrating dryer, granulator, mixer, racking machine etc., be all the production equipment that pharmacy corporation is conventional.In system
Medicine enterprise need not when producing this product increase extra equipment investment expense.There are skilled process operator, medicine in medicine enterprise
Production management, quality control officer, have a reliable and stable production technology, thus the good stability of product quality.In properties of product,
Bag bubble decoction pieces, tea flavour color is aromatic various, good taste.Foil laminated film bag is packed, and product stability is good, long shelf-life.Function
Aspect, the product that this programme produces, maintain the various characteristics of crude drug, therefore, product, in effect, has as Flos Lonicerae
Have heat clearing away solution stroll, effect of dispelling wind and heat pathogens, and for stewing swollen furuncle, sore throat, erysipelas, toxic-heat and blood stasis, anemopyretic cold, epidemic febrile disease are sent out
The treatment of the diseases such as heat.
The invention has the beneficial effects as follows:
(1) the Flos Lonicerae breaking cellular wall decoction pieces of the present invention, uses the form of teabag, i.e. steeps and i.e. drink, easy to use;Product uses
Vibrating dryer is dried, and drying materials is uniform, and drying time is short;Material is after wall breaking pulverization, and plant cell wall framework is destroyed,
So that product obtains the rapid dissolution of composition when brewing, and dissolved element content is gone out high than general wild honeysuckle flower tea bubble.
(2) present invention uses the packaged of teabag, has filter paper bag to filter, and dissolution part light green, to faint yellow, becomes
Color is good, and sweet and slightly bitter taste suffuses an exquisite fragrance all around.
(3) present invention is exquisite tea bubble decoction pieces, and packaging quantity is clear and definite, and user taking dose is accurate.
(4) preparation method of the present invention is simple, wide market, is suitable for large-scale production.
Detailed description of the invention
Being described principle and the feature of the present invention below in conjunction with specific embodiment, example is served only for explaining this
Bright, it is not intended to limit the scope of the present invention.
Embodiment 1
The production method of a kind of Flos Lonicerae breaking cellular wall decoction pieces of the present embodiment, comprises the steps:
(1) raw material selection: take fresh Flos Lonicerae, removes stem, leaf, obtains clean Flos Lonicerae;
(2) it is dried: the clean Flos Lonicerae that step (1) is obtained, uses vibrating dryer, be 30Hz at frequency of vibration, be dried
Temperature is 105 DEG C, and time of vibration is 40 seconds, is dried to moisture content 5%, obtains dry Flos Lonicerae;
(3) pulverize, sieve: dry Flos Lonicerae step (2) obtained is pulverized, cross 24 mesh sieves, obtain Flos Lonicerae powder;
(4) wall breaking pulverization: Flos Lonicerae powder step (3) obtained, adds from wall-broken grinder hopper port, carries out wall cell disruption powder
Broken, obtain Flos Lonicerae wall cell disruption powder;
(5) pelletize: the Flos Lonicerae wall cell disruption powder that step (4) is obtained, by Flos Lonicerae wall cell disruption powder and purified water weight ratio 100:
20, add purified water, start trough type mixing machine, mix to after uniformly, with the wet grain of oscillating granulator system, cross 16 mesh sieves, then with shaking
Dynamic drying machine is dried, and drying temperature is 100 DEG C, dries to pellet moisture 6%, obtains Flos Lonicerae granule;
(6) packaging: Flos Lonicerae granule step (5) obtained, first uses filter paper bag inner packing, then adds outside foil laminated film bag
Packaging, obtains packaged Flos Lonicerae granule;
(7) storage: packaged Flos Lonicerae granule step (5) obtained, loads in foil laminated film bag, evacuation
After, put in the shady and cool storehouse of 19 DEG C, and hide with gobo, i.e. obtain described Flos Lonicerae breaking cellular wall decoction pieces.
Embodiment 2
The production method of a kind of Flos Lonicerae breaking cellular wall decoction pieces of the present embodiment, comprises the steps:
(1) raw material selection: take fresh Flos Lonicerae, removes stem, leaf, obtains clean Flos Lonicerae;
(2) it is dried: the clean Flos Lonicerae that step (1) is obtained, uses vibrating dryer, be 35Hz at frequency of vibration, be dried
Temperature is 103 DEG C, and time of vibration is 40 seconds, is dried to moisture content 8%, obtains dry Flos Lonicerae;
(3) pulverize, sieve: dry Flos Lonicerae step (2) obtained is pulverized, cross 24 mesh sieves, obtain Flos Lonicerae powder;
(4) wall breaking pulverization: Flos Lonicerae powder step (3) obtained, adds from wall-broken grinder hopper port, carries out wall cell disruption powder
Broken, obtain Flos Lonicerae wall cell disruption powder;
(5) pelletize: the Flos Lonicerae wall cell disruption powder that step (4) is obtained, by Flos Lonicerae wall cell disruption powder and purified water weight ratio 100:
21, add purified water, start trough type mixing machine, mix to after uniformly, with the wet grain of oscillating granulator system, cross 17 mesh sieves, then with shaking
Dynamic drying machine is dried, and drying temperature is 103 DEG C, dries to pellet moisture 5%, obtains Flos Lonicerae granule;
(6) packaging: Flos Lonicerae granule step (5) obtained, first uses filter paper bag inner packing, then adds outside foil laminated film bag
Packaging, obtains packaged Flos Lonicerae granule;
(7) storage: packaged Flos Lonicerae granule step (5) obtained, loads in foil laminated film bag, evacuation
After, put in the shady and cool storehouse of 18 DEG C, and hide with gobo, i.e. obtain described Flos Lonicerae breaking cellular wall decoction pieces.
Embodiment 3
The production method of a kind of Flos Lonicerae breaking cellular wall decoction pieces of the present embodiment, comprises the steps:
(1) raw material selection: take fresh Flos Lonicerae, removes stem, leaf, obtains clean Flos Lonicerae;
(2) it is dried: the clean Flos Lonicerae that step (1) is obtained, uses vibrating dryer, be 38Hz at frequency of vibration, be dried
Temperature is 100 DEG C, and time of vibration is 40 seconds, is dried to moisture content 12%, obtains dry Flos Lonicerae;
(3) pulverize, sieve: dry Flos Lonicerae step (2) obtained is pulverized, cross 24 mesh sieves, obtain Flos Lonicerae powder;
(4) wall breaking pulverization: Flos Lonicerae powder step (3) obtained, adds from wall-broken grinder hopper port, carries out wall cell disruption powder
Broken, obtain Flos Lonicerae wall cell disruption powder;
(5) pelletize: the Flos Lonicerae wall cell disruption powder that step (4) is obtained, by Flos Lonicerae wall cell disruption powder and purified water weight ratio 100:
22, add purified water, start trough type mixing machine, mix to after uniformly, with the wet grain of oscillating granulator system, cross 18 mesh sieves, then with shaking
Dynamic drying machine is dried, and drying temperature is 105 DEG C, dries to pellet moisture 4%, obtains Flos Lonicerae granule;
(6) packaging: Flos Lonicerae granule step (5) obtained, first uses filter paper bag inner packing, then adds outside foil laminated film bag
Packaging, obtains packaged Flos Lonicerae granule;
(7) storage: packaged Flos Lonicerae granule step (5) obtained, loads in foil laminated film bag, evacuation
After, put in the shady and cool storehouse of 17 DEG C, and hide with gobo, i.e. obtain described Flos Lonicerae breaking cellular wall decoction pieces.
The foregoing is only presently preferred embodiments of the present invention, not in order to limit the present invention, all spirit in the present invention and
Within principle, any modification, equivalent substitution and improvement etc. made, should be included within the scope of the present invention.
Claims (4)
1. the production method of a Flos Lonicerae breaking cellular wall decoction pieces, it is characterised in that comprise the steps:
(1) raw material selection: take fresh Flos Lonicerae, removes stem, leaf, obtains clean Flos Lonicerae;
(2) be dried: the clean Flos Lonicerae that step (1) is obtained, use vibrating dryer, be dried to moisture content 5~12%, described in shake
The frequency of vibration of dynamic drying machine is 30~38Hz, and time of vibration is 40 seconds, baking temperature 100~105 DEG C, obtains dry Flos Lonicerae;
(3) pulverize, sieve: dry Flos Lonicerae step (2) obtained is pulverized, and sieves, obtains Flos Lonicerae powder;
(4) wall breaking pulverization: Flos Lonicerae powder step (3) obtained, carries out wall breaking pulverization, obtains Flos Lonicerae wall cell disruption powder;
(5) pelletize: the Flos Lonicerae wall cell disruption powder that step (4) is obtained, by Flos Lonicerae wall cell disruption powder and purified water weight ratio 100:20~
22, add purified water, mix homogeneously, then pelletize, sieve, dry to moisture content≤6%, obtain Flos Lonicerae granule;
(6) packaging: the Flos Lonicerae granule that step (5) is obtained, packaging, obtain packaged Flos Lonicerae granule;
(7) storage: packaged Flos Lonicerae granule step (5) obtained, loads in foil laminated film bag, after evacuation, puts
Enter in shady and cool storehouse, and hide with gobo, i.e. obtain described Flos Lonicerae breaking cellular wall decoction pieces.
The production method of a kind of Flos Lonicerae breaking cellular wall decoction pieces the most according to claim 1, it is characterised in that step (3) is described
The mesh number sieved is 24 mesh.
The production method of a kind of Flos Lonicerae breaking cellular wall decoction pieces the most according to claim 1, it is characterised in that step (5) is described
The mesh number sieved is 16~18 mesh, and described drying uses vibrating dryer, and drying temperature is 100~105 DEG C.
The production method of a kind of Flos Lonicerae breaking cellular wall decoction pieces the most according to claim 1, it is characterised in that step (6) is described
Packaging, is Flos Lonicerae granule step (5) obtained, first uses filter paper bag inner packing, then add foil laminated film bag outer package.
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Cited By (1)
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CN107441123A (en) * | 2017-08-09 | 2017-12-08 | 芜湖振龙齐欣药业有限公司 | A kind of preparation method of the broken wall prepared slices of Chinese crude drugs |
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2016
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CN102204603A (en) * | 2011-05-24 | 2011-10-05 | 安徽立顿生物药业有限公司 | Chrysanthemum and honeysuckle heat clearing tea bag |
CN105344428A (en) * | 2015-09-22 | 2016-02-24 | 陕西年青保药业有限公司 | Wall-breaking and superfine grinding process and device for better ground traditional Chinese medicine decoction piece |
Non-Patent Citations (1)
Title |
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赵新先主编: "《中药注射剂学》", 30 November 2000, 广东科技出版社 * |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107441123A (en) * | 2017-08-09 | 2017-12-08 | 芜湖振龙齐欣药业有限公司 | A kind of preparation method of the broken wall prepared slices of Chinese crude drugs |
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