CN106106524A - A kind of compositions preventing and treating beet armyworm and preparation method thereof - Google Patents
A kind of compositions preventing and treating beet armyworm and preparation method thereof Download PDFInfo
- Publication number
- CN106106524A CN106106524A CN201610450174.7A CN201610450174A CN106106524A CN 106106524 A CN106106524 A CN 106106524A CN 201610450174 A CN201610450174 A CN 201610450174A CN 106106524 A CN106106524 A CN 106106524A
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- CN
- China
- Prior art keywords
- parts
- isopropyl palmitate
- copper sulfate
- synergist
- quinoxyfen
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
- A01N59/20—Copper
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
- A01N43/42—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings condensed with carbocyclic rings
Abstract
The invention discloses a kind of compositions preventing and treating beet armyworm and preparation method thereof, including the raw material of following weight portion: quinoxyfen, 15～25 parts；Aconitine, 10～20 parts；Ethanol, 120～140 parts；Water, 440～480 parts；Totally 7～9 parts of synergist isopropyl palmitate and copper sulfate, the weight ratio of isopropyl palmitate and copper sulfate is 6～8:1.The compositions that the present invention provides can prevent and treat beet armyworm, the pesticide of preventing and treating beet armyworm can be developed into, prevention effect is relevant with the weight ratio of synergist isopropyl palmitate and copper sulfate in raw material, and when the weight ratio of isopropyl palmitate and copper sulfate is 6～8:1, prevention effect is best.
Description
Technical field
The invention belongs to pesticide field, be specifically related to a kind of compositions preventing and treating beet armyworm and preparation method thereof.
Background technology
Quinoxyfen is interior absorption, protective fungicide, powdery mildew prevention is had specially good effect, and it is mutually active to have steam, move
Dynamic property is good, appresorium can be suppressed to grow, do not have eradicant action.It is drawn to top, transmits to base portion in passing through；And pass through steam
Phase shift, it is achieved medicament reallocation in plant.It acts on the preinfective growth stage of powdery mildew, can effectively prevent and treat corn
Powdery mildew, beet powdery mildew, cucurbits powdery mildew, Fructus Capsici and Fructus Lycopersici esculenti powdery mildew, uncinula necator, peach tree powdery mildew and Fructus Fragariae Ananssae and
Fols lupuli powdery mildew etc..
Aconitine is present in the main toxic substance in the plants such as Radix Aconiti, Radix Aconiti Kusnezoffii, Radix Aconiti Lateralis Preparata.It mainly makes vagus nerve emerging
Put forth energy, to peripheral lesion.Poisoning symptom is based on nervous system and blood circulation, next to that gastrointestinal symptom.Clinical
Mainly showing as dispute and numb limbs and tense tendons, whole body tightly restraints sense etc., is reduced the self-disciplining of sinuatrial node by excited vagus, draws
The self-disciplining playing transposition pacemaker increases and causes each arrhythmia, infringement cardiac muscle.
Have not yet to see quinoxyfen and work in coordination with the report preventing and treating beet armyworm with aconitine.
Summary of the invention
It is an object of the invention to provide the preventing and treating beet armyworm of a kind of Quinoxyfen-containinsterilization and aconitine compositions and
Application in pesticide.
The above-mentioned purpose of the present invention is achieved by techniques below scheme:
A kind of compositions preventing and treating beet armyworm, including the raw material of following weight portion: quinoxyfen, 15～25 parts；Aconitum carmichjaelii Debx.
Alkali, 10～20 parts；Ethanol, 120～140 parts；Water, 440～480 parts；Totally 7～9 parts of synergist isopropyl palmitate and copper sulfate,
The weight ratio of isopropyl palmitate and copper sulfate is 6～8:1.
Further, the compositions of described preventing and treating beet armyworm includes the raw material of following weight portion: quinoxyfen, 20
Part；Aconitine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Totally 8 parts of synergist isopropyl palmitate and copper sulfate, Palmic acid isopropyl
The weight ratio of ester and copper sulfate is 7:1.
Further, the compositions of described preventing and treating beet armyworm includes the raw material of following weight portion: quinoxyfen, 15
Part；Aconitine, 10 parts；Ethanol, 120 parts；Water, 440 parts；Totally 7 parts of synergist isopropyl palmitate and copper sulfate, Palmic acid isopropyl
The weight ratio of ester and copper sulfate is 6:1.
Further, the compositions of described preventing and treating beet armyworm includes the raw material of following weight portion: quinoxyfen, 25
Part；Aconitine, 20 parts；Ethanol, 140 parts；Water, 480 parts；Totally 9 parts of synergist isopropyl palmitate and copper sulfate, Palmic acid isopropyl
The weight ratio of ester and copper sulfate is 8:1.
The preparation method of above-mentioned composition, comprises the steps:
Step S1, by quinoxyfen, aconitine and synergist isopropyl palmitate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Advantages of the present invention:
The compositions that the present invention provides can prevent and treat beet armyworm, can develop into the pesticide of preventing and treating beet armyworm.
Detailed description of the invention
Further illustrate the essentiality content of the present invention below in conjunction with embodiment, but do not limit the present invention with this and protect model
Enclose.Although the present invention being explained in detail with reference to preferred embodiment, it will be understood by those within the art that, can be right
Technical scheme is modified or equivalent, without deviating from the spirit and scope of technical solution of the present invention.
Embodiment 1: the preparation of the compositions of preventing and treating beet armyworm
Parts by weight of raw materials compares:
Quinoxyfen, 20 parts；Aconitine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist isopropyl palmitate and sulfur
Acid copper totally 8 parts, the weight ratio of isopropyl palmitate and copper sulfate is 7:1.
Preparation method:
Step S1, by quinoxyfen, aconitine and synergist isopropyl palmitate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 2: the preparation of the compositions of preventing and treating beet armyworm
Parts by weight of raw materials compares:
Quinoxyfen, 15 parts；Aconitine, 10 parts；Ethanol, 120 parts；Water, 440 parts；Synergist isopropyl palmitate and sulfur
Acid copper totally 7 parts, the weight ratio of isopropyl palmitate and copper sulfate is 6:1.
Preparation method:
Step S1, by quinoxyfen, aconitine and synergist isopropyl palmitate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 3: the preparation of the compositions of preventing and treating beet armyworm
Parts by weight of raw materials compares:
Quinoxyfen, 25 parts；Aconitine, 20 parts；Ethanol, 140 parts；Water, 480 parts；Synergist isopropyl palmitate and sulfur
Acid copper totally 9 parts, the weight ratio of isopropyl palmitate and copper sulfate is 8:1.
Preparation method:
Step S1, by quinoxyfen, aconitine and synergist isopropyl palmitate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 4: the preparation of the compositions of preventing and treating beet armyworm
Parts by weight of raw materials compares:
Quinoxyfen, 20 parts；Aconitine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist isopropyl palmitate and sulfur
Acid copper totally 8 parts, the weight ratio of isopropyl palmitate and copper sulfate is 6:1.
Preparation method:
Step S1, by quinoxyfen, aconitine and synergist isopropyl palmitate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 5: the preparation of the compositions of preventing and treating beet armyworm
Parts by weight of raw materials compares:
Quinoxyfen, 20 parts；Aconitine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist isopropyl palmitate and sulfur
Acid copper totally 8 parts, the weight ratio of isopropyl palmitate and copper sulfate is 8:1.
Preparation method:
Step S1, by quinoxyfen, aconitine and synergist isopropyl palmitate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 6: comparative example, isopropyl palmitate and copper sulfate is 5:1
Parts by weight of raw materials compares:
Quinoxyfen, 20 parts；Aconitine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist isopropyl palmitate and sulfur
Acid copper totally 8 parts, the weight ratio of isopropyl palmitate and copper sulfate is 5:1.
Preparation method:
Step S1, by quinoxyfen, aconitine and synergist isopropyl palmitate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
The weight ratio of embodiment 7: comparative example, isopropyl palmitate and copper sulfate is 9:1
Parts by weight of raw materials compares:
Quinoxyfen, 20 parts；Aconitine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist isopropyl palmitate and sulfur
Acid copper totally 8 parts, the weight ratio of isopropyl palmitate and copper sulfate is 9:1.
Preparation method:
Step S1, by quinoxyfen, aconitine and synergist isopropyl palmitate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Embodiment 8: effect example
The compositions of the testing example 1～7 preparation preventing and treating effective percentage (%) to beet armyworm respectively.
During use, present composition water carries out 40 times of dilutions, and fountain height is 25 liters/mu.
Result such as following table.
| Preventing and treating effective percentage (%) | |
| Embodiment 1 | 100 |
| Embodiment 4 | 98 |
| Embodiment 5 | 98 |
| Embodiment 6 | 76 |
| Embodiment 7 | 74 |
The effect of embodiment 2,3 is basically identical with embodiment 4,5.
The above results shows, the compositions that the present invention provides can prevent and treat beet armyworm, can develop into preventing and treating Radix Betae night
The pesticide of moth, prevention effect is relevant with the weight ratio of synergist isopropyl palmitate and copper sulfate in raw material, and Palmic acid is different
When the weight ratio of propyl ester and copper sulfate is 6～8:1, prevention effect is best.
The effect of above-described embodiment indicates that the essentiality content of the present invention, but does not limit the protection of the present invention with this
Scope.It will be understood by those within the art that, technical scheme can be modified or equivalent,
Essence and protection domain without deviating from technical solution of the present invention.
Claims (5)
1. the compositions preventing and treating beet armyworm, it is characterised in that include the raw material of following weight portion: quinoxyfen, 15～
25 parts；Aconitine, 10～20 parts；Ethanol, 120～140 parts；Water, 440～480 parts；Synergist isopropyl palmitate and copper sulfate
Totally 7～9 parts, the weight ratio of isopropyl palmitate and copper sulfate is 6～8:1.
The compositions of preventing and treating beet armyworm the most according to claim 1, it is characterised in that include the former of following weight portion
Material: quinoxyfen, 20 parts；Aconitine, 15 parts；Ethanol, 130 parts；Water, 460 parts；Synergist isopropyl palmitate and copper sulfate are altogether
8 parts, the weight ratio of isopropyl palmitate and copper sulfate is 7:1.
The compositions of preventing and treating beet armyworm the most according to claim 1, it is characterised in that include the former of following weight portion
Material: quinoxyfen, 15 parts；Aconitine, 10 parts；Ethanol, 120 parts；Water, 440 parts；Synergist isopropyl palmitate and copper sulfate are altogether
7 parts, the weight ratio of isopropyl palmitate and copper sulfate is 6:1.
The compositions of preventing and treating beet armyworm the most according to claim 1, it is characterised in that include the former of following weight portion
Material: quinoxyfen, 25 parts；Aconitine, 20 parts；Ethanol, 140 parts；Water, 480 parts；Synergist isopropyl palmitate and copper sulfate are altogether
9 parts, the weight ratio of isopropyl palmitate and copper sulfate is 8:1.
5. the preparation method of the arbitrary described compositions of Claims 1 to 4, it is characterised in that comprise the steps:
Step S1, by quinoxyfen, aconitine and synergist isopropyl palmitate ethanol and water dissolution；
Step S2, by copper sulfate water dissolution；
Step S3, slowly adds the solution of step S1 in the solution of step S2, and interpolation limit, limit is stirred, and to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610450174.7A CN106106524A (en) | 2016-06-19 | 2016-06-19 | A kind of compositions preventing and treating beet armyworm and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610450174.7A CN106106524A (en) | 2016-06-19 | 2016-06-19 | A kind of compositions preventing and treating beet armyworm and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106106524A true CN106106524A (en) | 2016-11-16 |
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ID=57470254
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610450174.7A Pending CN106106524A (en) | 2016-06-19 | 2016-06-19 | A kind of compositions preventing and treating beet armyworm and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN106106524A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113519529A (en) * | 2021-07-14 | 2021-10-22 | 湖南省林业科学院 | Composition for preventing and treating beet armyworm and preparation method and application thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102047884A (en) * | 2010-10-20 | 2011-05-11 | 华南理工大学 | Aconitine plant source insecticidal micro emulsion and preparation method thereof |
| CN103380772A (en) * | 2012-05-04 | 2013-11-06 | 中国中化股份有限公司 | Oil suspending agent containing SYP-1620 |
| CN103734149A (en) * | 2013-12-28 | 2014-04-23 | 上海艳紫化工科技有限公司 | Activated ester and quinoxyfen compound insecticidal suspending agent |
| CN103891781A (en) * | 2013-04-02 | 2014-07-02 | 徐兆焕 | Efficient pesticide with low toxicity and broad spectrum and preparation method of pesticide |
-
2016
- 2016-06-19 CN CN201610450174.7A patent/CN106106524A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102047884A (en) * | 2010-10-20 | 2011-05-11 | 华南理工大学 | Aconitine plant source insecticidal micro emulsion and preparation method thereof |
| CN103380772A (en) * | 2012-05-04 | 2013-11-06 | 中国中化股份有限公司 | Oil suspending agent containing SYP-1620 |
| CN103891781A (en) * | 2013-04-02 | 2014-07-02 | 徐兆焕 | Efficient pesticide with low toxicity and broad spectrum and preparation method of pesticide |
| CN103734149A (en) * | 2013-12-28 | 2014-04-23 | 上海艳紫化工科技有限公司 | Activated ester and quinoxyfen compound insecticidal suspending agent |
Non-Patent Citations (1)
| Title |
|---|
| 许勇华等: "乌头生物碱对甜菜夜蛾毒杀活性的测定", 《湖北农业科学》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113519529A (en) * | 2021-07-14 | 2021-10-22 | 湖南省林业科学院 | Composition for preventing and treating beet armyworm and preparation method and application thereof |
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| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
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| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20161116 |
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| RJ01 | Rejection of invention patent application after publication |