CN106087432A - 一种棉纤维的柔化处理工艺 - Google Patents

一种棉纤维的柔化处理工艺 Download PDF

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CN106087432A
CN106087432A CN201610543114.XA CN201610543114A CN106087432A CN 106087432 A CN106087432 A CN 106087432A CN 201610543114 A CN201610543114 A CN 201610543114A CN 106087432 A CN106087432 A CN 106087432A
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cotton fiber
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严建民
沈泽平
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Changxing Xintianlong Printing And Dyeing Co Ltd
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Abstract

一种棉纤维的柔化处理工艺，在传统的棉纤维的柔化工艺的基础上，加入桑叶微粉和异构醇聚氧乙烯，将桑叶微粉有效地分散在织物表面的有机硅连续薄膜中，具有良好的抗菌作用，同时还有非常好的耐黄变性能；处理过程中使用天然染料和植物型抗菌剂，环保、健康。

Description

一种棉纤维的柔化处理工艺
技术领域
本发明涉及棉纺织技术领域，尤其涉及一种棉纤维的柔化处理工艺。
背景技术
目前棉色纺纱生产主要采用碱处理，这种方法存在不少问题，主要表现棉纤维的前处理、染色是色纺工艺过程的关键工序。棉纤维中除了含有９４％的纤维素纤维外，还存在６％的杂质（果胶、腊质、灰分等纤维素共生物）。这些杂质的存在，使棉纤维吸湿性差，后道染色困难。传统工艺采用碱处理，在去除棉纤维中的果胶和蜡质等杂质的同时，不仅使部分纤维素分子链氧化断裂、聚合度降低、纤维强力下降，而且对环境污染严重。因此，棉纤维绿色环保的处理方法代替传统的碱处理是必然趋势。
发明内容
为了解决背景技术中的问题，本发明提供一种棉纤维的柔化处理工艺。
一种棉纤维的柔化处理工艺，包括以下步骤：
A、预处理：将棉纤维在pH为7-8的碱性溶液中煮沸，降低温度至40-50℃，加入碱性果胶酶进行脱胶10-15min，再煮沸使酶失活；
B、漂白：将水温降低至30-40℃，加入5-10g/L的25%双氧水、3-5g/L的漂白稳定剂、3-5g/L的壳聚糖，保温25-35min；
C、染色：将棉面料取出并简单冲洗后，放入天然染料染液中进行染色，其中天然染料的加入量为5-15g/L，匀染剂1-2g/L，浴比为1:20-45，浸泡20-30min；
D、柔化处理：用柔化剂溶液浸泡棉纤维，所述的柔化剂溶液包括9-11g/Ｌ有机硅柔软剂、60-80g/L丙三醇、3-5g/L润湿剂、2-5g/L EDTA、0.2-0.5g/L 桑叶粉，浴比为1:20-30，温度50-55℃，处理时间90-120min，然后以0.5-0.8℃/min的速度升温至80℃；
E、将棉纤维烘干到含水率8-10%；对棉纤维进行开清棉、梳棉、精梳、纺粗纱、纺细纱，得到高强度柔化纱线产品。
优选的，所述的步骤B中，所述的漂白稳定剂为硅酸钠。
优选的，所述的步骤C中，所述的匀染剂为平平加。
优选的，所述的步骤D中，所述的有机硅柔软剂为氨基类有机硅柔软剂。
优选的，所述的步骤D中，所述的润湿剂为异构醇聚氧乙烯醚。
优选的，所述的步骤D中，所述的桑叶粉粒径为50μm以下，粒径小易于分散。
桑叶是桑叶科落叶乔木植物桑的叶。味苦、甘、性寒。桑叶中营养成分特别丰富，干桑叶中约含粗蛋白 24.0克，粗脂肪4.0克，含食物纤维52.9克，钙2699毫克，桑叶含有人体所需的18种氨基酸，含神经传递物质及降压物质γ——酪氨酸，每百克桑叶中平均有226毫克，谷氨酸高达2323毫克，天冬氨酸2049毫克，可见桑叶是氨基酸的宝库。
药用作用：消水肿、降血脂、排毒：桑叶富含优质蛋白质、粗纤维、糖类，以及钙、磷、铁、锰等营养，具有促进新陈代谢、清血、通便等功用，另外还可以使积在细胞中多余的水分排走，改善水肿现象。
美容：美白、治色斑、亮泽肤色、保持弹性：桑叶富含黄酮、酚类、氨基酸、有机酸、胡萝卜素、维生素及多种人体必需的微量元素，这对改善和调节皮肤组织的新陈代谢，特别是抑制色素沉着的发生和发展均有积极作用，所以面部有色斑或者皱纹者经常使用桑叶，具有明显的美容功效。
有机硅柔软剂的原理为：有机硅柔软剂含有硅氧键，由于硅氧键的键角在外力作用下可以伸缩，使得织物的表面形成了有机硅连续薄膜，这样就改善了成品的爽滑感。
本发明中，有机硅乳液、桑叶微粉在异构醇聚氧乙烯的作用下，相容性非常好，织物表面附着有桑叶微粉，不但有良好的抗菌效果，而且由于桑叶微粉中含有大量的黄酮、酚类等不饱和化学物，对有机硅柔软剂的氨基具有一定的保护作用，防止在高温下氨基，特别是伯氨基在高温下被氧化分解形成发色基团（偶氮基和氧化偶氮基），这种双胺型结构具有协同效应，加速氧化作用，造成织物易于泛黄。
加入EDTA，降低各种金属离子对有机硅柔软剂的影响；加入丙三醇有利于提高分散效果。
本发明的棉纤维的柔化处理工艺，在传统的棉纤维的柔化工艺的基础上，加入桑叶微粉和异构醇聚氧乙烯，将桑叶微粉有效地分散在织物表面的有机硅连续薄膜中，具有良好的抗菌作用，同时还有非常好的耐黄变性能；处理过程中使用天然染料和植物型抗菌剂，环保、健康。
具体实施方法
实施例1
一种棉纤维的柔化处理工艺，包括以下步骤：
A、预处理：将棉纤维在pH为7-8的碱性溶液中煮沸，降低温度至45℃，加入碱性果胶酶进行脱胶12min，再煮沸使酶失活；
B、漂白：将水温降低至35℃，加入8g/L的25%双氧水、4g/L的漂白稳定剂、5g/L的壳聚糖，保温30min；
C、染色：将棉面料取出并简单冲洗后，放入天然染料染液中进行染色，其中天然染料的加入量为12g/L，匀染剂1.5g/L，浴比为1:30，浸泡25min；
D、柔化处理：用柔化剂溶液浸泡棉纤维，所述的柔化剂溶液包括10g/Ｌ有机硅柔软剂、70g/L丙三醇、4g/L润湿剂、3g/L EDTA、0.5g/L 桑叶粉，浴比为1:25，温度52℃，处理时间100min，然后以0.6℃/min的速度升温至80℃；
E、将棉纤维烘干到含水率8.5%；对棉纤维进行开清棉、梳棉、精梳、纺粗纱、纺细纱，得到高强度柔化纱线产品；
所述的步骤B中，所述的漂白稳定剂为硅酸钠；
所述的步骤C中，所述的匀染剂为平平加；
所述的步骤D中，所述的有机硅柔软剂为氨基类有机硅柔软剂；
所述的步骤D中，所述的润湿剂为异构醇聚氧乙烯醚；
所述的步骤D中，所述的桑叶粉粒径为50μm以下。
实施例2
一种棉纤维的柔化处理工艺，包括以下步骤：
A、预处理：将棉纤维在pH为7-8的碱性溶液中煮沸，降低温度至40℃，加入碱性果胶酶进行脱胶15min，再煮沸使酶失活；
B、漂白：将水温降低至30℃，加入10g/L的25%双氧水、5g/L的漂白稳定剂、3g/L的壳聚糖，保温25min；
C、染色：将棉面料取出并简单冲洗后，放入天然染料染液中进行染色，其中天然染料的加入量为15g/L，匀染剂1g/L，浴比为1:45，浸泡20min；
D、柔化处理：用柔化剂溶液浸泡棉纤维，所述的柔化剂溶液包括11g/Ｌ有机硅柔软剂、60g/L丙三醇、5g/L润湿剂、2g/L EDTA、0.5g/L 桑叶粉，浴比为1:20，温度55℃，处理时间90min，然后以0.8℃/min的速度升温至80℃；
E、将棉纤维烘干到含水率8%；对棉纤维进行开清棉、梳棉、精梳、纺粗纱、纺细纱，得到高强度柔化纱线产品；
所述的步骤B中，所述的漂白稳定剂为硅酸钠；
所述的步骤C中，所述的匀染剂为平平加；
所述的步骤D中，所述的有机硅柔软剂为氨基类有机硅柔软剂；
所述的步骤D中，所述的润湿剂为异构醇聚氧乙烯醚；
所述的步骤D中，所述的桑叶粉粒径为50μm以下。
实施例3
一种棉纤维的柔化处理工艺，包括以下步骤：
A、预处理：将棉纤维在pH为7-8的碱性溶液中煮沸，降低温度至50℃，加入碱性果胶酶进行脱胶10min，再煮沸使酶失活；
B、漂白：将水温降低至40℃，加入5g/L的25%双氧水、5g/L的漂白稳定剂、3g/L的壳聚糖，保温35min；
C、染色：将棉面料取出并简单冲洗后，放入天然染料染液中进行染色，其中天然染料的加入量为5g/L，匀染剂2g/L，浴比为1:20，浸泡30min；
D、柔化处理：用柔化剂溶液浸泡棉纤维，所述的柔化剂溶液包括9g/Ｌ有机硅柔软剂、80g/L丙三醇、3g/L润湿剂、5g/L EDTA、0.2g/L 桑叶粉，浴比为1:30，温度50℃，处理时间120min，然后以0.5℃/min的速度升温至80℃；
E、将棉纤维烘干到含水率10%；对棉纤维进行开清棉、梳棉、精梳、纺粗纱、纺细纱，得到高强度柔化纱线产品；
所述的步骤B中，所述的漂白稳定剂为硅酸钠；
所述的步骤C中，所述的匀染剂为平平加；
所述的步骤D中，所述的有机硅柔软剂为氨基类有机硅柔软剂；
所述的步骤D中，所述的润湿剂为异构醇聚氧乙烯醚；
所述的步骤D中，所述的桑叶粉粒径为50μm以下。
经检测，经过本发明工艺处理后的样品，水洗50次以后，其对金黄色葡萄球菌、大肠杆菌、白色念珠菌的抑菌率菌达到85%以上。
经检测，经过本发明工艺处理后的样品，水洗50次以后，未发现明显的黄变现象。
以上所述，仅为本发明较佳的具体实施方式，但本发明的保护范围并不局限于此，任何熟悉本技术领域的技术人员在本发明揭露的技术范围内，根据本发明的技术方案及其发明构思加以等同替换或改变，都应涵盖在本发明的保护范围之内。

Claims (7)

1.一种棉纤维的柔化处理工艺，其特征在于，包括以下步骤：
A、预处理：将棉纤维在pH为7-8的碱性溶液中煮沸，降低温度至40-50℃，加入碱性果胶酶进行脱胶10-15min，再煮沸使酶失活；
B、漂白：将水温降低至30-40℃，加入5-10g/L的25%双氧水、3-5g/L的漂白稳定剂、3-5g/L的壳聚糖，保温25-35min；
C、染色：将棉面料取出并简单冲洗后，放入天然染料染液中进行染色，其中天然染料的加入量为5-15g/L，匀染剂1-2g/L，浴比为1:20-45，浸泡20-30min；
D、柔化处理：用柔化剂溶液浸泡棉纤维，所述的柔化剂溶液包括9-11g/Ｌ有机硅柔软剂、60-80g/L丙三醇、3-5g/L润湿剂、2-5g/L EDTA、0.2-0.5g/L 桑叶粉，浴比为1:20-30，温度50-55℃，处理时间90-120min，然后以0.5-0.8℃/min的速度升温至80℃；
E、将棉纤维烘干到含水率8-10%；对棉纤维进行开清棉、梳棉、精梳、纺粗纱、纺细纱，得到高强度柔化纱线产品。
2.如权利要求1所述的棉纤维的柔化处理工艺，其特征在于，所述的步骤B中，所述的漂白稳定剂为硅酸钠。
3.如权利要求1所述的棉纤维的柔化处理工艺，其特征在于，所述的步骤C中，所述的匀染剂为平平加。
4.如权利要求1所述的棉纤维的柔化处理工艺，其特征在于，所述的步骤D中，所述的有机硅柔软剂为氨基类有机硅柔软剂。
5.如权利要求1所述的棉纤维的柔化处理工艺，其特征在于，所述的步骤D中，所述的润湿剂为异构醇聚氧乙烯醚。
6.如权利要求1所述的棉纤维的柔化处理工艺，其特征在于，所述的步骤D中，所述的桑叶粉粒径为50μm以下，粒径小易于分散。
7.如权利要求1所述的棉纤维的柔化处理工艺，其特征在于，包括以下步骤：
A、预处理：将棉纤维在pH为7-8的碱性溶液中煮沸，降低温度至45℃，加入碱性果胶酶进行脱胶12min，再煮沸使酶失活；
B、漂白：将水温降低至35℃，加入8g/L的25%双氧水、4g/L的漂白稳定剂、5g/L的壳聚糖，保温30min；
C、染色：将棉面料取出并简单冲洗后，放入天然染料染液中进行染色，其中天然染料的加入量为12g/L，匀染剂1.5g/L，浴比为1:30，浸泡25min；
D、柔化处理：用柔化剂溶液浸泡棉纤维，所述的柔化剂溶液包括10g/Ｌ有机硅柔软剂、70g/L丙三醇、4g/L润湿剂、3g/L EDTA、0.5g/L 桑叶粉，浴比为1:25，温度52℃，处理时间100min，然后以0.6℃/min的速度升温至80℃；
E、将棉纤维烘干到含水率8.5%；对棉纤维进行开清棉、梳棉、精梳、纺粗纱、纺细纱，得到高强度柔化纱线产品；
所述的步骤B中，所述的漂白稳定剂为硅酸钠；
所述的步骤C中，所述的匀染剂为平平加；
所述的步骤D中，所述的有机硅柔软剂为氨基类有机硅柔软剂；
所述的步骤D中，所述的润湿剂为异构醇聚氧乙烯醚；
所述的步骤D中，所述的桑叶粉粒径为50μm以下。
CN201610543114.XA 2016-07-12 2016-07-12 一种棉纤维的柔化处理工艺 Pending CN106087432A (zh)

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