CN106083325A - A kind of preparation method of vegetables slow-release compound fertilizer - Google Patents

A kind of preparation method of vegetables slow-release compound fertilizer Download PDF

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Publication number
CN106083325A
CN106083325A CN201610409604.0A CN201610409604A CN106083325A CN 106083325 A CN106083325 A CN 106083325A CN 201610409604 A CN201610409604 A CN 201610409604A CN 106083325 A CN106083325 A CN 106083325A
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parts
acid
dreg
compound fertilizer
preparation
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CN201610409604.0A
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Chinese (zh)
Inventor
王明
韩小飞
陈建萍
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Jurong Houbai Improved Variety Farm
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Jurong Houbai Improved Variety Farm
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Priority to CN201610409604.0A priority Critical patent/CN106083325A/en
Publication of CN106083325A publication Critical patent/CN106083325A/en
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/90Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Soil Sciences (AREA)
  • Fertilizers (AREA)

Abstract

The invention provides the preparation method of a kind of vegetables slow-release compound fertilizer, first take dreg, dry, pulverize, add to NaOH solution extracts, regulate leaching liquor pH to 7.5~8.5, add trypsase, enzymolysis, filter, obtain digesting dreg;Again PLGA, sodium citrate, lecithin are added in deionized water, add vegetable oil, microcrystalline cellulose and stearic acid, high speed dispersion, obtain carrier solution;Then four water-calcium nitrate, potassium nitrate, diammonium hydrogen phosphate, epsom salt, manganese sulfate, B family vitamin, shitosan, niacinamide, amino acid, sodium alginate, urea, glucose, organic acid, the mixing of enzymolysis dreg are taken, adding in carrier solution, heat up stirring, cooling, filter, to obtain final product.The vegetables of present invention slow-release compound fertilizer can be effectively improved vegetable growth situation, significantly improve yield, improves fruit quality.

Description

A kind of preparation method of vegetables slow-release compound fertilizer
Technical field
The invention belongs to vegetable fertilizer technical field, be specifically related to the preparation method of a kind of vegetables slow-release compound fertilizer.
Background technology
The reasonable employment of fertilizer is not only closely bound up with the yield of agricultural product, and the quality safety concerning agricultural product is asked Can topic, reasonable employment fertilizer be the key that high quality agricultural products produces.Practice have shown that, the most directly effectively improve the hand of crop yield Section is rationally to enrich fertilizer, and this also adjusts the most important means of farmland ecosystem balance and Nutrient Cycling.
China's fertilizer application is inefficient, and by the statistics display of a large amount of field test data, China's utilization rate of nitrogen fertilizer is 30 ~35%, fertilizer be 10~20%, potash fertilizer be 35~50%.This has the gap determining degree compared with developed countries.Not only Cause the waste of resource, and enormous pressure can be caused to ecological environment.
The features such as the nutritive peculiarity of vegetable crop is embodied in that root system is shallow, likes high rich water, weak, the luxury absorption of absorbability.Cause This vegetable crop vegetable plot dose, fertilizer requirement is of a relatively high.In recent years, many vegetable growers are for obtaining maximum economic well-being of workers and staff, pass through Chemical fertilizer is excessive to be put into pursue the high yield vegetables, and its result often leads to vegetable increase production amplitude and declines year by year, reduces fertilizer Utilization rate and be not reaching to higher economic benefit, vegetable flavor and quality decline, even severe contamination environment, causes vegetable plot The even more serious problem such as soil degradation, wherein nitrogen is particularly problematic.Therefore, in order to realize high yield that vegetables produce, excellent Produce, safety nuisance free reaches sustainable development, it is necessary to studies further for the vegetable plot rational application of fertilizer and includes novel fertilizer The research and development of material.Slow-release or control-release fertilizer has the important function improving fertilizer utilization efficiency, reducing environmental pollution, and it can realize nutrients release With Crop synchronization, reduction field ammonia volatilization amount.Numerous studies show, it is excellent that slow-release or control-release fertilizer can not only make crop reach high yield Produce, and can also reduce labour base fertilising material and topdress input, use less fertilizer amount to carry nitrogen fertilizer use simultaneously Rate, reduces the pressure bringing environment.
Content of the invention
The preparation side that it is an object of the invention to overcome the deficiencies in the prior art and a kind of vegetables slow-release compound fertilizer is provided Method, gained fertilizer can be effectively improved vegetable growth situation, significantly improve yield, improves fruit quality.
The preparation method of a kind of vegetables slow-release compound fertilizer, comprises the following steps:
Step 1, takes dreg, dries, pulverizes, and adds to extract in 1~3wt%NaOH solution, and regulation leaching liquor pH to 7.5~ 8.5, add trypsase, 35~45 DEG C of enzymolysis 1~2h, go out enzyme, filters, and obtains digesting dreg;
Poly(D,L-lactide-co-glycolide 10~20 parts, sodium citrate 3~7 parts, 0.5~2 part of lecithin are added by step 2 To deionized water 10~20 parts, be warming up to 40~50 DEG C of insulation 1~2h, add vegetable oil 2~5 parts, microcrystalline cellulose 1~ 4 parts and stearic acid 2~6 parts, high speed dispersion, it is warming up to 45~60 DEG C of insulation 2~4h, be cooled to room temperature, obtain carrier solution;
Step 3, takes four water-calcium nitrate 2~5 parts, 1~4 part of potassium nitrate, diammonium hydrogen phosphate 3~6 parts, epsom salt 2~5 Part, manganese sulfate 1~4 part, B family vitamin 2~5 parts, shitosan 0.5~3 part, niacinamide 0.1~0.7 part, amino acid 0.4~ 1.2 parts, sodium alginate 2~5 parts, 1~4 part of urea, glucose 2~6 parts, organic acid 1~4 part, enzymolysis dreg 3~7 parts mixing, Add in carrier solution 10 parts, be warming up to 45~60 DEG C of stirring 2~4h, be cooled to 5~10 DEG C, filter, to obtain final product.
Further, after in step 1, dreg is pulverized, granularity is at 80~100 mesh.
Further, in step 1, trypsase consumption is the 0.5~1% of dreg weight.
Further, in step 1, extracting condition is 30~40 DEG C, 0.5~1h.
Further, step 2 high speed dispersion condition is 1000~2000rpm, 10~15min.
Further, in step 3, amino acid is the one in valine, methionine or isoleucine.
Further, in step 3, organic acid is indolebutyric acid, methyl α-naphthyl acetate, salicylic acid, folic acid, tartaric acid, succinic acid, corruption One in phytic acid, malic acid or nicotinic acid.
The vegetables of present invention slow-release compound fertilizer can be effectively improved vegetable growth situation, significantly improve yield, improvement fruit Real quality.
Detailed description of the invention
Embodiment 1
The preparation method of a kind of vegetables slow-release compound fertilizer, comprises the following steps:
Step 1, takes dreg, dries, pulverizes, and adds to extract in 1wt%NaOH solution, regulates leaching liquor pH to 7.5, adds Trypsase, 35 DEG C of enzymolysis 2h, go out enzyme, filters, and obtains digesting dreg;
Poly(D,L-lactide-co-glycolide 10 parts, sodium citrate 3 parts, 0.5 part of lecithin are added to deionized water by step 2 It in 10 parts, is warming up to 40 DEG C of insulation 1h, adds vegetable oil 2 parts, microcrystalline cellulose 1 part and stearic acid 2 parts, high speed dispersion, rise Temperature, to 45 DEG C of insulation 4h, is cooled to room temperature, obtains carrier solution;
Step 3, takes four water-calcium nitrate 2 parts, 1 part of potassium nitrate, diammonium hydrogen phosphate 3 parts, epsom salt 2 parts, manganese sulfate 1 Part, B family vitamin 2 parts, shitosan 0.5 part, niacinamide 0.1 part, 0.4 part of amino acid, sodium alginate 2 parts, 1 part of urea, grape Sugar 2 parts, organic acid 1 part, enzymolysis dreg 3 parts mixing, add in carrier solution 10 parts, is warming up to 45 DEG C of stirring 2h, is cooled to 5 DEG C, filter, to obtain final product.
Wherein, after in step 1, dreg is pulverized, granularity is at 80 mesh, and trypsase consumption is the 0.5% of dreg weight, extracts bar Part is 30 DEG C, 1h;Step 2 high speed dispersion condition is 1000rpm, 15min;In step 3, amino acid is valine, and organic acid is Indolebutyric acid.
Embodiment 2
The preparation method of a kind of vegetables slow-release compound fertilizer, comprises the following steps:
Step 1, takes dreg, dries, pulverizes, and adds to extract in 2wt%NaOH solution, regulates leaching liquor pH to 8.0, adds Trypsase, 40 DEG C of enzymolysis 1.5h, go out enzyme, filters, and obtains digesting dreg;
Poly(D,L-lactide-co-glycolide 15 parts, sodium citrate 4 parts, 1.2 parts of lecithin are added to deionized water by step 2 It in 16 parts, is warming up to 45 DEG C of insulation 1.5h, adds vegetable oil 4 parts, microcrystalline cellulose 3 parts and stearic acid 5 parts, high speed dispersion, It is warming up to 55 DEG C of insulation 3h, be cooled to room temperature, obtain carrier solution;
Step 3, takes four water-calcium nitrate 4 parts, 3 parts of potassium nitrate, diammonium hydrogen phosphate 5 parts, epsom salt 4 parts, manganese sulfate 2 Part, B family vitamin 4 parts, shitosan 1.5 parts, niacinamide 0.6 part, 0.7 part of amino acid, sodium alginate 4 parts, 2 parts of urea, grape Sugar 5 parts, organic acid 3 parts, enzymolysis dreg 6 parts mixing, add in carrier solution 10 parts, is warming up to 55 DEG C of stirring 3h, is cooled to 10 DEG C, filter, to obtain final product.
Wherein, after in step 1, dreg is pulverized, granularity is at 90 mesh, and trypsase consumption is the 0.8% of dreg weight, extracts bar Part is 35 DEG C, 1h;Step 2 high speed dispersion condition is 1500rpm, 15min;In step 3, amino acid is isoleucine, organic acid For salicylic acid.
Embodiment 3
The preparation method of a kind of vegetables slow-release compound fertilizer, comprises the following steps:
Step 1, takes dreg, dries, pulverizes, and adds to extract in 2wt%NaOH solution, regulates leaching liquor pH to 7.5, adds Trypsase, 35 DEG C of enzymolysis 2h, go out enzyme, filters, and obtains digesting dreg;
Poly(D,L-lactide-co-glycolide 18 parts, sodium citrate 6 parts, 0.8 part of lecithin are added to deionized water by step 2 It in 17 parts, is warming up to 40 DEG C of insulation 1h, adds vegetable oil 3 parts, microcrystalline cellulose 3 parts and stearic acid 5 parts, high speed dispersion, rise Temperature, to 45 DEG C of insulation 4h, is cooled to room temperature, obtains carrier solution;
Step 3, takes four water-calcium nitrate 4 parts, 3 parts of potassium nitrate, diammonium hydrogen phosphate 5 parts, epsom salt 4 parts, manganese sulfate 2 Part, B family vitamin 4 parts, shitosan 2.4 parts, niacinamide 0.6 part, 0.9 part of amino acid, sodium alginate 4 parts, 3 parts of urea, grape Sugar 5 parts, organic acid 2 parts, enzymolysis dreg 6 parts mixing, add in carrier solution 10 parts, is warming up to 45 DEG C of stirring 2h, is cooled to 5 DEG C, filter, to obtain final product.
Wherein, after in step 1, dreg is pulverized, granularity is at 80 mesh, and trypsase consumption is the 0.5% of dreg weight, extracts bar Part is 30 DEG C, 1h;Step 2 high speed dispersion condition is 1000rpm, 15min;In step 3, amino acid is valine, and organic acid is Humic acid.
Embodiment 4
The preparation method of a kind of vegetables slow-release compound fertilizer, comprises the following steps:
Step 1, takes dreg, dries, pulverizes, and adds to extract in 3wt%NaOH solution, regulates leaching liquor pH to 8.5, adds Trypsase, 45 DEG C of enzymolysis 1h, go out enzyme, filters, and obtains digesting dreg;
Poly(D,L-lactide-co-glycolide 20 parts, sodium citrate 7 parts, 2 parts of lecithin are added to deionized water 20 by step 2 It in Fen, is warming up to 50 DEG C of insulation 2h, adds vegetable oil 5 parts, microcrystalline cellulose 4 parts and stearic acid 6 parts, high speed dispersion, heat up It to 60 DEG C of insulation 2h, is cooled to room temperature, obtains carrier solution;
Step 3, takes four water-calcium nitrate 5 parts, 4 parts of potassium nitrate, diammonium hydrogen phosphate 6 parts, epsom salt 5 parts, manganese sulfate 4 Part, B family vitamin 5 parts, shitosan 3 parts, niacinamide 0.7 part, amino acid/11 .2 part, sodium alginate 5 parts, 4 parts of urea, glucose 6 Part, organic acid 4 parts, enzymolysis dreg 7 parts mixing, add in carrier solution 10 parts, is warming up to 60 DEG C of stirring 4h, is cooled to 10 DEG C, Filter, to obtain final product.
Wherein, after in step 1, dreg is pulverized, granularity is at 100 mesh, and trypsase consumption is the 1% of dreg weight, extracts bar Part is 40 DEG C, 0.5h;Step 2 high speed dispersion condition is 2000rpm, 10min;In step 3, amino acid is methionine, organic acid For tartaric acid.
Compare with Common compound fertilizer, capsicum pot experiment is carried out to embodiment 1 to 4 gained slow release fertilizer.Every kind of fertilizer If 3 repetitions, random alignment.5 kilograms of every basin dress soil, is carried out by amount of nitrogen 270mg/kg in soil, and fertilising point is carried out, i.e. for 3 times Topdress for 2 times of base manure, florescence and the best fruiting period.Base manure by executing the 50% of total amount, topdress respectively by execute N total amount the 30%th, 20%, Carry out and then the Nitrogen Application amount of polishing and slow-release fertilizer.Eggplant seedling two strain transplanted by every basin, adds every day deionized water to make soil Earth reaches the 60% of field capacity.Pepper seedling two strain transplanted by every basin, adds every day deionized water to make soil reach field Water-holding capacity.Capsicum carries out receiving according to its concrete condition after starting result and detects its yield and quality, and potted plant After off-test, plant, soil sample etc. are analyzed.
Compare with Common compound fertilizer, eggplant pot experiment is carried out to embodiment 1 to 4 gained slow release fertilizer.Every kind of fertilizer If 3 repetitions, random alignment.5 kilograms of every basin dress soil, is carried out by amount of nitrogen 225mg/kg in soil, and fertilising point is carried out, i.e. for 3 times Topdress for 2 times of base manure, florescence and the best fruiting period.Base manure by executing the 50% of total amount, topdress respectively by execute N total amount the 30%th, 20%, Carry out and then the Nitrogen Application amount of polishing and slow-release fertilizer.Eggplant seedling two strain transplanted by every basin, adds every day deionized water to make soil Earth reaches the 60% of field capacity.Eggplant carries out receiving according to its concrete condition after starting result and carries out its yield and quality Detection, and after pot experiment terminates, plant, soil sample etc. are analyzed.
From result above, the slow release fertilizer of the present invention can be effectively improved the upgrowth situation of capsicum and eggplant, significantly carry High yield, improve fruit quality.

Claims (7)

1. the preparation method of a vegetables slow-release compound fertilizer, it is characterised in that: comprise the following steps:
Step 1, takes dreg, dries, pulverizes, and adds to extract in 1~3wt% NaOH solution, regulates leaching liquor pH to 7.5~8.5, Adding trypsase, 35~45 DEG C of enzymolysis 1~2h, go out enzyme, filters, and obtains digesting dreg;
Poly(D,L-lactide-co-glycolide 10~20 parts, sodium citrate 3~7 parts, 0.5~2 part of lecithin are added to by step 2 It in ionized water 10~20 parts, is warming up to 40~50 DEG C of insulation 1~2h, adds vegetable oil 2~5 parts, microcrystalline cellulose 1~4 part It with stearic acid 2~6 parts, high speed dispersion, is warming up to 45~60 DEG C of insulation 2~4h, is cooled to room temperature, obtains carrier solution;
Step 3, take four water-calcium nitrate 2~5 parts, 1~4 part of potassium nitrate, diammonium hydrogen phosphate 3~6 parts, epsom salt 2~5 parts, Manganese sulfate 1~4 part, B family vitamin 2~5 parts, shitosan 0.5~3 part, niacinamide 0.1~0.7 part, amino acid 0.4~1.2 Part, sodium alginate 2~5 parts, 1~4 part of urea, glucose 2~6 parts, organic acid 1~4 part, enzymolysis dreg 3~7 parts mixing, add It to carrier solution 10 parts, is warming up to 45~60 DEG C of stirring 2~4h, is cooled to 5~10 DEG C, filters, to obtain final product.
2. the preparation method of vegetables slow-release compound fertilizer according to claim 1, it is characterised in that: dreg in step 1 After pulverizing, granularity is at 80~100 mesh.
3. the preparation method of vegetables slow-release compound fertilizer according to claim 1, it is characterised in that: pancreas egg in step 1 White enzyme dosage is the 0.5~1% of dreg weight.
4. the preparation method of vegetables slow-release compound fertilizer according to claim 1, it is characterised in that: step 1 extracts Condition is 30~40 DEG C, 0.5~1h.
5. the preparation method of vegetables slow-release compound fertilizer according to claim 1, it is characterised in that: step 2 high speed Dispersion condition is 1000~2000rpm, 10~15min.
6. the preparation method of vegetables slow-release compound fertilizer according to claim 1, it is characterised in that: amino in step 3 Acid is the one in valine, methionine or isoleucine.
7. the preparation method of vegetables slow-release compound fertilizer according to claim 1, it is characterised in that: organic in step 3 Acid is the one in indolebutyric acid, methyl α-naphthyl acetate, salicylic acid, folic acid, tartaric acid, succinic acid, humic acid, malic acid or nicotinic acid.
CN201610409604.0A 2016-06-12 2016-06-12 A kind of preparation method of vegetables slow-release compound fertilizer Pending CN106083325A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107235812A (en) * 2017-08-11 2017-10-10 句容市白兔镇张峰良品家庭农场 A kind of wine-growing organic fertilizer and preparation method thereof
CN107739259A (en) * 2017-12-05 2018-02-27 定远县英华种植家庭农场 A kind of non-irrigated lotus root special fertilizer preparation method for improving soil regime
CN108947625A (en) * 2017-05-17 2018-12-07 四川施邦威生物科技发展有限公司 A kind of fertilizer additive increasing disease-resistant crops, insect pest ability

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102206118A (en) * 2011-03-10 2011-10-05 山东省农业科学院农业资源与环境研究所 Nuisanceless organic fertilizer prepared from edible fungus slag, preparation method thereof and application thereof
CN103058757A (en) * 2012-12-26 2013-04-24 施可丰化工股份有限公司 Preparation method for special slow-release long-acting compound fertilizer for vegetable
CN104591835A (en) * 2015-02-14 2015-05-06 孟红琳 Preparation method of mushroom residue organic fertilizer for scutellaria baicalensis planting

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102206118A (en) * 2011-03-10 2011-10-05 山东省农业科学院农业资源与环境研究所 Nuisanceless organic fertilizer prepared from edible fungus slag, preparation method thereof and application thereof
CN103058757A (en) * 2012-12-26 2013-04-24 施可丰化工股份有限公司 Preparation method for special slow-release long-acting compound fertilizer for vegetable
CN104591835A (en) * 2015-02-14 2015-05-06 孟红琳 Preparation method of mushroom residue organic fertilizer for scutellaria baicalensis planting

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108947625A (en) * 2017-05-17 2018-12-07 四川施邦威生物科技发展有限公司 A kind of fertilizer additive increasing disease-resistant crops, insect pest ability
CN107235812A (en) * 2017-08-11 2017-10-10 句容市白兔镇张峰良品家庭农场 A kind of wine-growing organic fertilizer and preparation method thereof
CN107739259A (en) * 2017-12-05 2018-02-27 定远县英华种植家庭农场 A kind of non-irrigated lotus root special fertilizer preparation method for improving soil regime

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