CN106083126A - Nixing pottery base substrate is filled the processing technology of white clay - Google Patents
Nixing pottery base substrate is filled the processing technology of white clay Download PDFInfo
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- CN106083126A CN106083126A CN201610434923.7A CN201610434923A CN106083126A CN 106083126 A CN106083126 A CN 106083126A CN 201610434923 A CN201610434923 A CN 201610434923A CN 106083126 A CN106083126 A CN 106083126A
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- base substrate
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B37/00—Joining burned ceramic articles with other burned ceramic articles or other articles by heating
- C04B37/04—Joining burned ceramic articles with other burned ceramic articles or other articles by heating with articles made from glass
- C04B37/045—Joining burned ceramic articles with other burned ceramic articles or other articles by heating with articles made from glass characterised by the interlayer used
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/24—Manufacture of porcelain or white ware
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B37/00—Joining burned ceramic articles with other burned ceramic articles or other articles by heating
- C04B37/04—Joining burned ceramic articles with other burned ceramic articles or other articles by heating with articles made from glass
- C04B37/047—Joining burned ceramic articles with other burned ceramic articles or other articles by heating with articles made from glass by means of an interlayer consisting of an organic adhesive, e.g. phenol resin or pitch
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
- C04B2235/612—Machining
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2237/00—Aspects relating to ceramic laminates or to joining of ceramic articles with other articles by heating
- C04B2237/02—Aspects relating to interlayers, e.g. used to join ceramic articles with other articles by heating
- C04B2237/04—Ceramic interlayers
- C04B2237/06—Oxidic interlayers
- C04B2237/064—Oxidic interlayers based on alumina or aluminates
Abstract
The invention discloses a kind of processing technology filling white clay on Nixing pottery base substrate, including preparing blank, blank forming, painting, carve, filler, be dried and ablating work procedure, described fillering is uniformly to spread last layer croci and one layer of amphoteric starch in the groove carved, and is then inserted in the groove carved by white clay；Described white clay is the ratio that east mud and western mud are 7～8:2～3 by weight to be mixed, and the processing technology according still further to blank processes；Described being dried is that the base substrate after fillering processes 1～5min under the conditions of 10～15Mpa, then natural air drying.The present invention can be greatly enhanced the electrostatic attraction of white clay and base substrate body by adding ferric oxide particles, and the molecule long-chain of amphoteric starch has the effect being mutually wound around and cross-linking, white clay and blank are combined closely, also there is certain water conservation uniformity, make to be dehydrated more uniform, neither ftracture and also do not fall off.
Description
Technical field
The present invention relates to the manufacture method of Nixing pottery, be specifically related to a kind of making side filling white clay on Nixing pottery base substrate
Method.
Background technology
According to Historical Data Data About, the technique of fillering of Qiezhou Nixing pottery has been formed from the Qing Dynasty, and traditional Nixing pottery fillers technique
Mainly include following step: 1) prepare blank: the earth of the Jiang Yidong that admires crossing urban district, Qiezhou selected by blank, is commonly called as east mud
(for mild-clay, color is yellow-white, containing trace quartz sand, plays adjustment plasticity to combine in the production technology of Nixing pottery
Property effect), and the earth of region to the west of river by the emperor himself, it is commonly called as western mud (containing a small amount of K2O、NaO、CaO、MgO、Fe203、TiO2、MnO2,
Being the purple mudstone that a kind of iron-holder is higher, color is aubergine, and surface layer has a small amount of irony to contaminate, for hard paste, plasticity
And associativity is poor), by east mud 40～60%, western mud 40～the percentage by weight mixing of 60%, ground, dehydration etc. is a series of
Technique makes blank；2) blank forming: use stiff-mud process or slip casting method that blank is made the base substrate of various type；3) finishing base
Body: by base substrate finishing to reach to design requirement；4) drawing: submit a written statement to a higher authority writing picture at base substrate；5) engraving: with icking tool along base substrate ink marks
Earth is chosen by both sides of the edge, and the part having ink marks is all removed the groove forming bottom even；6) filler: the mud that will fill
Groove inserted by material, then equating, compacting；Generally filling pug is clay；7) it is dried: use aeration drying that base substrate is entered
Row is dried, and makes base substrate moisture get rid of；8) firing base substrate: dry base substrate loading of kiln fired, firing temperature is 1100～1200 DEG C,
Kiln discharge after cooling；9) polishing grinding: green body polishing is polished, to obtain final product.Owing to the Nixing pottery technique process that fillers is loaded down with trivial details, and filled out
The pug filled is sucked in sintering procedure mutually with Nixing pottery body, the most easily comes off, and yield rate is extremely low, and only 20% is left
The right side, seriously hinders Qiezhou Nixing pottery and fillers the development of technique.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of manufacture method filling white clay on Nixing pottery base substrate, this work
Artistic skill be prevented effectively from filler come off and ftracture, be greatly improved yield rate.
The technical scheme that the present invention provides is a kind of manufacture method filling white clay on Nixing pottery base substrate, including preparing base
Material and white clay, blank forming, paint, carve, filler, be dried and ablating work procedure, described in filler be equal in groove carve
Even spread last layer alumina powder and one layer of carboxymethyl propyl cellulose, then white clay is inserted in the groove carved；Described
White clay is the ratio that east mud and western mud are 7～8:2～3 by weight to be mixed, and the processing technology according still further to blank processes；
Described being dried is that the base substrate after fillering processes 1～5min under the conditions of 10～15Mpa, then natural air drying.
The isoelectric pH value of alumina particle is 7.1, and the isoelectric pH value of Nixing pottery blank is 4～5, and the pH value of aqueous medium
It is between 6～7, say, that the pH value of aqueous medium is more than the isoelectric pH value of Nixing pottery blank, then blank surface is by electronegative, and
The isoelectric pH value of alumina particle is more than the pH value of aqueous medium, then Membranes On Alumina Particles Surface positively charged.White clay and the raw material of blank
Composition and preparation technology are identical, and only proportioning raw materials is different, and the isoelectric pH value of white clay is similarly less than 6.So, positively charged oxidation
Alumina particles attracts each other with electronegative blank and white clay and closely connects together, and produces firm electrostatic attraction, so may be used
To prevent coming off of white clay and the base substrate body filled in sintering procedure.
Base substrate after fillering processes 1～5min under the conditions of 10～15Mpa, and condition of high voltage can reduce alumina particle
And the hole between blank and white clay, reduce grain spacing from, contact number of particle mesh increases, and promotes the most positively charged
Alumina particle and electronegative blank and the combination of white clay, the electrostatic attraction of generation increases further, so that base
Material is tightly combined with white clay, prevents white clay in sintering procedure from coming off with base substrate body.
It is crucial that, blank and white clay are clay particle, the most in the form of sheets structure, and negative electricity worn by plate, and seamed edge band is just
Electric charge, but overall net charge is negative charge.In the presence of not pressurization and alumina particle, white clay and the knot of blank
It is combined into irregular combination, has the combination in face and face, have the combination on limit and limit, also have the combination in face and limit, face and face and limit
With limit because band identical charges, present certain repulsion, although limit attracts each other with face, but limit be less with the bonded area in face,
The electrostatic attraction produced is the least, and this is also to cause the caducous main cause of appearance of fillering.But under elevated pressure conditions, Detachable
The in-house network shelf structure of blank and white clay, makes limit and limit, the combination in limit and face is changed into the arrangement in face and face, and the adding of aluminium oxide
Enter, can be filled in the gap in face and face so that aluminium oxide is clamped by white clay and blank again while surrounding white clay and blank, pole
Big improves base substrate and the electrostatic attraction filling white clay, prevents white clay from coming off in sintering procedure.
Due to east mud be white, western mud be redness, the weight ratio of play the host mud and western mud with 7～8:2～3 modulated obtain white
Color pug.
White clay keeps consistent with the granularity of blank, and the granularity of the Nixing pottery blank that common process makes is 4～6 μm, the most in vain
The granularity of mud is also 4～6 μm.The white clay filled in sintering procedure is so conducive to shrink consistent with base substrate body, it is to avoid to open
Split and come off.
Blank and white clay are clay particle, in the form of sheets structure, and negative electricity worn by plate, due to blank and white clay granularity relatively
Little, therefore its lamellar is the thinnest.Alumina powder is circular granular, when alumina particle granularity is 1～during 2 μm, less than blank and
The granularity of pug, adsorbable multiple positively charged alumina particles on the plate face of electronegative blank and white clay so that oxygen
Change alumina particles blank and white clay tightly to be surrounded, define firm electrostatic attraction, so that blank is tied with the tight of white clay
Close.
The consumption of described alumina powder is the 1～2% of white clay dry weight, it is ensured that blank and white clay form the quiet of abundance
Electric attraction, to prevent coming off of in sintering procedure white clay.Alumina powder consumption is too high, easily causes condensed alumina, old
Change and form crystalline state aluminium oxide mineral, do not produce Electrostatic Absorption with blank and white clay.
Consumption is white clay dry weight the 0.01～0.05% of described carboxymethyl propyl cellulose, its molecular weight is 9 × 105~
1.2×106。
As preferably, the moisture content of white clay is than blank high 5～8%, and the hydrone in white clay can ooze in base substrate body
Thoroughly, also bring along the migration of a small amount of blank, promote the Electrostatic Absorption of white clay, aluminium oxide and blank, strengthen white clay and base substrate
The combination of body.
It is further preferred that described blank is east mud, western mud to be mixed by the weight ratio of 6～4:4～6, ground, de-
Water, vacuum pugging, old forming, the moisture content of blank is 20～25%.
Compared with prior art, the present invention can be greatly enhanced white by adding alumina particle in the groove carved
The electrostatic attraction of mud and base substrate body, can be substantially reduced coming off and cracking of in sintering procedure white clay.Carboxymethyl propyl group fiber
Element is macromolecular compound, has molecule long-chain, has and is mutually wound around and the effect of crosslinking, by white clay and base in sintering procedure
Material combines closely, also has certain water conservation uniformity so that dehydration is more uniform, neither ftractures and does not also fall off.
Detailed description of the invention
The present invention is further elaborated for specific examples below, but not as a limitation of the invention.
Embodiment 1
1) prepare blank: east mud, western mud are mixed by weight for 6:4, ground, dehydration, vacuum pugging, old make
Moisture content is the blank of 20%；
2) prepare white clay: east mud and western mud mixed by weight 8:2, ground, dehydration, vacuum pugging, old make
Moisture content is the white clay of 25%；
3) blank forming: blank is made teacup base substrate, a diameter of 8cm of teacup, height is 10cm；
4) finishing base substrate: by base substrate finishing to reach to design requirement；
5) drawing: submit a written statement to a higher authority writing picture at base substrate；
6) engraving: along base substrate ink marks both sides of the edge, earth is chosen with icking tool, the part having ink marks is all removed shape
Become the groove of bottom even；
7) filler: in the groove carved, uniformly spread last layer alumina powder and carboxymethyl propyl cellulose, then
White clay is inserted in the groove carved, equating, compacting；The granularity of alumina powder is 1 μm, and consumption is the 1% of white clay dry weight；
Consumption is white clay dry weight the 0.01% of described carboxymethyl propyl cellulose, its molecular weight is 9 × 105。
8) it is dried: the base substrate after fillering processes 1min, then natural air drying under the conditions of 10Mpa；
9) base substrate is fired: the base substrate loading of kiln that 100 dry fired, first to raise the programming rate of 80 DEG C per hour by kiln
After in-furnace temperature rises to 450 DEG C, then is warming up to 1100 DEG C to raise the programming rate of 140 DEG C per hour, and 1h is fired in insulation, stop
Only heating, kiln discharge after cooling.Through statistics, 100 intact, and 0 comes off.
Embodiment 2
1) prepare blank: east mud, western mud are mixed by weight for 6:4, ground, dehydration, vacuum pugging, old make
Moisture content is the blank of 22%；
2) white clay is prepared: east mud and western mud mixed by weight 7.5:2.5, ground, dehydration, vacuum pugging, old
Make the white clay of moisture content 28%；
3) blank forming: blank is made the base substrate of teapot, a diameter of 15cm of teapot, height is 10cm；
4) finishing base substrate: by base substrate finishing to reach to design requirement；
5) drawing: submit a written statement to a higher authority writing picture at base substrate；
6) engraving: along base substrate ink marks both sides of the edge, earth is chosen with icking tool, the part having ink marks is all removed shape
Become the groove of bottom even；
7) filler: in the groove carved, uniformly spread last layer alumina powder and carboxymethyl propyl cellulose, then
White clay is inserted in the groove carved, equating, compacting；The granularity of alumina powder is 1.5 μm, and consumption is white clay dry weight
1.5%；Consumption is white clay dry weight the 0.05% of described carboxymethyl propyl cellulose, its molecular weight is 1.2 × 106。
8) it is dried: the base substrate after fillering processes 3min, then natural air drying under the conditions of 12Mpa；
9) base substrate is fired: the base substrate loading of kiln that 100 dry fired, first to raise the programming rate of 80 DEG C per hour by kiln
After in-furnace temperature rises to 450 DEG C, then is warming up to 1100 DEG C to raise the programming rate of 140 DEG C per hour, and 1h is fired in insulation, stop
Only heating, kiln discharge after cooling.Through statistics, 97 intact, and 3 come off.
Embodiment 3
1) prepare blank: east mud, western mud are mixed by weight for 6:4, ground, dehydration, vacuum pugging, old make
Moisture content is the blank of 25%；
2) prepare white clay: east mud and western mud mixed by weight 7:3, ground, dehydration, vacuum pugging, old make
Moisture content is the white clay of 33%；
3) blank forming: blank is made vase base substrate, a diameter of 20cm of vase, height is 40cm；
4) finishing base substrate: by base substrate finishing to reach to design requirement；
5) drawing: submit a written statement to a higher authority writing picture at base substrate；
6) engraving: along base substrate ink marks both sides of the edge, earth is chosen with icking tool, the part having ink marks is all removed shape
Become the groove of bottom even；
7) filler: in the groove carved, uniformly spread last layer alumina powder and carboxymethyl propyl cellulose, then
White clay is inserted in the groove carved, equating, compacting；The granularity of alumina powder is 2 μm, and consumption is the 2% of white clay dry weight；
Consumption is white clay dry weight the 0.02% of described carboxymethyl propyl cellulose, its molecular weight is 1 × 106；
8) it is dried: the base substrate after fillering processes 5min, then natural air drying under the conditions of 15Mpa；
9) base substrate is fired: the base substrate loading of kiln that 100 dry fired, first to raise the programming rate of 80 DEG C per hour by kiln
After in-furnace temperature rises to 450 DEG C, then is warming up to 1100 DEG C to raise the programming rate of 140 DEG C per hour, and 1h is fired in insulation, stop
Only heating, kiln discharge after cooling.Through statistics, 94 intact, and 2 crackings, 4 come off.
Embodiment 4
1) prepare blank: east mud, western mud are mixed by weight for 6:4, ground, dehydration, vacuum pugging, old make
Moisture content is the blank of 20%；
2) prepare white clay: east mud and western mud mixed by weight 7:2, ground, dehydration, vacuum pugging, old make
The white clay of moisture content 28%；
3) blank forming: blank is made the base substrate of vase, a diameter of 30cm of vase, height is 50cm；
4) finishing base substrate: by base substrate finishing to reach to design requirement；
5) drawing: submit a written statement to a higher authority writing picture at base substrate；
6) engraving: along base substrate ink marks both sides of the edge, earth is chosen with icking tool, the part having ink marks is all removed shape
Become the groove of bottom even；
7) filler: in the groove carved, uniformly spread last layer alumina powder and carboxymethyl propyl cellulose, then
White clay is inserted in the groove carved, equating, compacting；The granularity of alumina powder is 1 μm, and consumption is the 2% of white clay dry weight；
Consumption is white clay dry weight the 0.01 of described carboxymethyl propyl cellulose, its molecular weight is 1.2 × 106；
8) it is dried: the base substrate after fillering processes 5min, then natural air drying under the conditions of 10Mpa；
9) base substrate is fired: the base substrate loading of kiln that 100 dry fired, first to raise the programming rate of 80 DEG C per hour by kiln
After in-furnace temperature rises to 450 DEG C, then is warming up to 1100 DEG C to raise the programming rate of 140 DEG C per hour, and 1h is fired in insulation, stop
Only heating, kiln discharge after cooling.Through statistics, 92 intact, and 4 crackings, 4 come off.
Comparative example 1
1) prepare blank: east mud, western mud are mixed by weight for 6:4, ground, dehydration, vacuum pugging, old make
Moisture content is the blank of 20%；
2) prepare white clay: east mud and western mud mixed by weight 7:2, ground, dehydration, vacuum pugging, old make
The white clay of moisture content 20%；
3) blank forming: blank is made the base substrate of vase, a diameter of 30cm of vase, height is 50cm；
4) finishing base substrate: by base substrate finishing to reach to design requirement；
5) drawing: submit a written statement to a higher authority writing picture at base substrate；
6) engraving: along base substrate ink marks both sides of the edge, earth is chosen with icking tool, the part having ink marks is all removed shape
Become the groove of bottom even；
7) filler: white clay is inserted in the groove carved, equating, compacting；
8) it is dried: the base substrate natural air drying after fillering；
9) base substrate is fired: the base substrate loading of kiln that 100 dry fired, first to raise the programming rate of 80 DEG C per hour by kiln
After in-furnace temperature rises to 450 DEG C, then is warming up to 1100 DEG C to raise the programming rate of 140 DEG C per hour, and 1h is fired in insulation, stop
Only heating, kiln discharge after cooling.Through statistics, 19 intact, and 47 crackings, 34 come off.
Claims (7)
1. on Nixing pottery base substrate, fill the processing technology of white clay, including prepare blank, blank forming, paint, carve, filler,
Be dried and ablating work procedure, it is characterised in that filler described in: be uniformly spread in the groove carve last layer croci with
One layer of amphoteric starch, then inserts white clay in the groove carved；Described white clay be by east mud and western mud be by weight 7～
The ratio mixing of 8:2～3, the processing technology according still further to blank processes；
Described being dried is that the base substrate after fillering processes 1～5min under the conditions of 10～15Mpa, then natural air drying.
The processing technology filling white clay on Nixing pottery base substrate the most according to claim 1, it is characterised in that: described white clay
Granularity and blank granularity keep consistent.
The processing technology filling white clay on Nixing pottery base substrate the most according to claim 2, it is characterised in that: described oxidation
The granularity of iron powder is 1～2 μm.
The processing technology filling white clay on Nixing pottery base substrate the most according to claim 1, it is characterised in that: described oxidation
The consumption of iron powder is the 1～2% of white clay dry weight.
The processing technology filling white clay on Nixing pottery base substrate the most according to claim 1, it is characterised in that: described both sexes
The consumption of starch is the 0.01～0.05% of white clay dry weight, and its viscosity is 300～600mPa s.
6., according to the processing technology filling white clay on Nixing pottery base substrate according to any one of Claims 1 to 5, its feature exists
In: the moisture content higher than the moisture content of blank 5～8% of described white clay.
The processing technology filling white clay on Nixing pottery base substrate the most according to claim 5, it is characterised in that: described blank
Moisture content be 20～25%.
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| CN108656834A (en) * | 2018-05-14 | 2018-10-16 | 南宁学院 | A kind of manufacture craft of Nixing pottery cloud carving |
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| CN108656834A (en) * | 2018-05-14 | 2018-10-16 | 南宁学院 | A kind of manufacture craft of Nixing pottery cloud carving |
| CN108656834B (en) * | 2018-05-14 | 2020-07-10 | 南宁学院 | Manufacturing process of nixing pottery cloud sculpture |
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