CN106071621A - A kind of candied uctus Crataegi of vessel softening and preparation method thereof - Google Patents
A kind of candied uctus Crataegi of vessel softening and preparation method thereof Download PDFInfo
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- CN106071621A CN106071621A CN201610420133.3A CN201610420133A CN106071621A CN 106071621 A CN106071621 A CN 106071621A CN 201610420133 A CN201610420133 A CN 201610420133A CN 106071621 A CN106071621 A CN 106071621A
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- crataegi
- fructus crataegi
- candied
- vessel softening
- fructus
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- 238000002360 preparation method Methods 0.000 title abstract description 5
- 108010059892 Cellulase Proteins 0.000 claims abstract description 10
- 229940106157 cellulase Drugs 0.000 claims abstract description 10
- 235000009508 confectionery Nutrition 0.000 claims abstract description 9
- 235000012907 honey Nutrition 0.000 claims abstract description 8
- 102000008186 Collagen Human genes 0.000 claims abstract description 7
- 108010035532 Collagen Proteins 0.000 claims abstract description 7
- 235000003143 Panax notoginseng Nutrition 0.000 claims abstract description 7
- 241000180649 Panax notoginseng Species 0.000 claims abstract description 7
- 244000248825 Peltandra virginica Species 0.000 claims abstract description 7
- 235000001188 Peltandra virginica Nutrition 0.000 claims abstract description 7
- 235000008599 Poria cocos Nutrition 0.000 claims abstract description 7
- 241001506047 Tremella Species 0.000 claims abstract description 7
- 239000006071 cream Substances 0.000 claims abstract description 7
- 150000004676 glycans Chemical class 0.000 claims abstract description 7
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 7
- 239000005017 polysaccharide Substances 0.000 claims abstract description 7
- 239000000843 powder Substances 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 239000000203 mixture Substances 0.000 claims description 11
- 239000000706 filtrate Substances 0.000 claims description 9
- 238000009835 boiling Methods 0.000 claims description 6
- 238000001914 filtration Methods 0.000 claims description 6
- 239000012535 impurity Substances 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 230000007306 turnover Effects 0.000 claims description 5
- 241000251468 Actinopterygii Species 0.000 claims description 3
- 229920001817 Agar Polymers 0.000 claims description 3
- 241000256844 Apis mellifera Species 0.000 claims description 3
- 239000004698 Polyethylene Substances 0.000 claims description 3
- 239000008272 agar Substances 0.000 claims description 3
- 238000005520 cutting process Methods 0.000 claims description 3
- 238000007667 floating Methods 0.000 claims description 3
- 239000012634 fragment Substances 0.000 claims description 3
- 239000003205 fragrance Substances 0.000 claims description 3
- 239000008187 granular material Substances 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 238000001802 infusion Methods 0.000 claims description 3
- 231100000252 nontoxic Toxicity 0.000 claims description 3
- 230000003000 nontoxic effect Effects 0.000 claims description 3
- 239000004033 plastic Substances 0.000 claims description 3
- 229920003023 plastic Polymers 0.000 claims description 3
- -1 polyethylene Polymers 0.000 claims description 3
- 229920000573 polyethylene Polymers 0.000 claims description 3
- 238000007670 refining Methods 0.000 claims description 3
- 239000011550 stock solution Substances 0.000 claims description 3
- 230000000694 effects Effects 0.000 abstract description 4
- 239000002932 luster Substances 0.000 abstract description 3
- 206010030113 Oedema Diseases 0.000 abstract description 2
- 208000004880 Polyuria Diseases 0.000 abstract description 2
- 230000035619 diuresis Effects 0.000 abstract description 2
- 230000001939 inductive effect Effects 0.000 abstract description 2
- 239000004615 ingredient Substances 0.000 abstract description 2
- 239000003053 toxin Substances 0.000 abstract description 2
- 231100000765 toxin Toxicity 0.000 abstract description 2
- 235000008935 nutritious Nutrition 0.000 abstract 1
- 239000003814 drug Substances 0.000 description 9
- 108090000790 Enzymes Proteins 0.000 description 8
- 102000004190 Enzymes Human genes 0.000 description 8
- 229940088598 enzyme Drugs 0.000 description 8
- 239000001913 cellulose Substances 0.000 description 4
- 229920002678 cellulose Polymers 0.000 description 4
- 229940079593 drug Drugs 0.000 description 4
- 230000008901 benefit Effects 0.000 description 3
- 238000006555 catalytic reaction Methods 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- 108010093096 Immobilized Enzymes Proteins 0.000 description 2
- 108010091086 Recombinases Proteins 0.000 description 2
- 102000018120 Recombinases Human genes 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 241000411851 herbal medicine Species 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 101001035465 Arabidopsis thaliana Endoglucanase 3 Proteins 0.000 description 1
- 241001523405 Limax Species 0.000 description 1
- 208000032023 Signs and Symptoms Diseases 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 210000002249 digestive system Anatomy 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000006911 enzymatic reaction Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000001727 in vivo Methods 0.000 description 1
- 239000002440 industrial waste Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000010534 mechanism of action Effects 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 230000008506 pathogenesis Effects 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000008844 regulatory mechanism Effects 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 230000035899 viability Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Non-Alcoholic Beverages (AREA)
- Jellies, Jams, And Syrups (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of candied uctus Crataegi of vessel softening and preparation method thereof, be made up of following raw materials in part by weight: Fructus Crataegi 50 60, collagen protein powder 13 15, tremella polysaccharide 13 15, cellulase 56, natural honey 80 90, yellow wine 25 30, Oleum Camelliae 78, Fructus Corni 10 12, Radix Notoginseng seed 67, Exocarpium Benincasae 89, tuckahoe cream 10 12, Petiolus nelumbinis 10 12.The candied uctus Crataegi of a kind of vessel softening of the present invention, size is uniform, and color and luster temperature is yellow, and sweet mouthfeel is nutritious, drinks conveniently, and contained effective ingredient has the health-care effects such as vessel softening, inducing diuresis to remove edema, heat clearing away, toxin expelling.
Description
Technical field
The present invention relates to prepared slices of Chinese crude drugs technical field, particularly relate to a kind of candied uctus Crataegi of vessel softening and preparation side thereof
Method.
Background technology
The prepared slices of Chinese crude drugs are under guidance of traditional Chinese medicine theory, according to determination for the treatment of based on pathogenesis obtained through differentiation of symptoms and signs principle and the needs of formulation dispensing, to Chinese medicine
The finished product of material Processing methods is tcm clinical practice medication, play dialectical plus-minus, embody the basis of personalized medicine principle.Chinese medicine is drunk
Sheet is one of big pillar of Chinese herbal medicine industry three, the important component part of Ye Shi China traditional medicine, diseases prevention, cure the disease in play
Important effect.Therefore the quality of The Quality of Sliced Herbal Medicine is by directly influencing the effect of tcm clinical practice treatment, has influence on the people
Masses' life and health and the safety of medication.
Cellulose is the regenerated resources that on the earth, quantity is maximum, be plant cell wall mainly comprise composition.At present, natural
Cellulose major part in boundary is not utilized, and causes the huge wasting of resources, even environmental pollution, and cellulase can be by richness
The agricultural byproducts of cellulose and industrial waste etc. effectively convert.From the Digestive system of Limax, fiber is found from 1996
Since element enzyme, people have carried out substantial amounts of research, for fiber to cellulose enzyme viability, mechanism of action and industrial applications thereof etc.
Production and the application of element enzyme are had laid a good foundation, especially for expanding raw materials for food industry and the comprehensive utilization of plant resources
With, improve raw material availability, environment purification and aspect tools such as opening up new forms of energy and be of great significance.
Enzyme immobilizatio is or to be limited to enzyme constraint in certain area with solid material, can still provide for its distinctive catalysis
Reaction, and a recyclable and reusable class technology.Compared with resolvase, immobilized enzyme is keeping it efficient, single-minded and warm
While the enzymic catalytic reaction characteristic of sum, also present that bin stability is high, separation and recovery easily, can repeatedly use, operate
The series of advantages such as the most controlled, simple process.Enzyme immobilizatio and enzymatic reaction research thereof are biologies most with prospects
One of frontline technology field, it has important value, simultaneously to illustrating enzyme model of action, action rule and regulatory mechanism in vivo
Having opened up wide prospect for enzyme preparation in the application of the aspects such as biological engineering, biomedicine, environmental conservation, it will be in mankind society
The strategy of sustainable development can be played a significant role.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of candied uctus Crataegi of vessel softening.
The present invention is achieved by the following technical solutions:
A kind of candied uctus Crataegi of vessel softening, is made up of following raw materials in part by weight:
Fructus Crataegi 50-60, collagen protein powder 13-15, tremella polysaccharide 13-15, cellulase 5-6, natural honey 80-90, yellow wine 25-
30, Oleum Camelliae 7-8, Fructus Corni 10-12, Radix Notoginseng seed 6-7, Exocarpium Benincasae 8-9, tuckahoe cream 10-12, Petiolus nelumbinis 10-12.
The described candied uctus Crataegi of a kind of vessel softening, is made up of the following step:
1), Fructus Crataegi is cleaned, remove woody stems, undesirable root and impurity, clean Fructus Crataegi is loaded in Turnround basket, cleans end；
2), with microtome, Fructus Crataegi being cut into the thick Fructus Crataegi slice of 5-7mm, the Fructus Crataegi after cutting loads in Turnover Box；
3), by Fructus Corni, Radix Notoginseng seed, Exocarpium Benincasae, tuckahoe cream, Petiolus nelumbinis, yellow wine mixing, 20-25 times amount water, slow fire infusion 3-are added
5 hours, make decoction be concentrated into the 1/5-3 of stock solution, filtering and impurity removing, collect filtrate；
4), step 3 gained filtering residue is rubbed, add the extremely boiling of 5-10 times amount decocting in water, stop heating, be cooled to 60-70 DEG C, regulation
PH value, in 4.0-6.0, is subsequently adding the agar immobilized cellulase granule that mass fraction is 5-10%, sends out in 55-60 DEG C of constant temperature
Ferment 3-5 hour, filters, and separates and recovers immobilized cellulase, collects filtrate；
5), natural honey is put in inclinable jacketed kettle, mix with step 3, step 4 gained filtrate, after being heated to slowly seething with excitement,
Using slow fire instead, keep the waxiness of micro-boiling, scumming and floating and dead honeybee, temperature is maintained at 116-118 DEG C, and refining to panful plays fish
Bubble eye, adds collagen protein powder, tremella polysaccharide, mixing, with the toughness of hands sth. made by twisting, there is no white silk when occurring, take the dish out of the pot rapidly between referring to；
6), take step 5 gained mixture and step 2 gained Fructus Crataegi slice and mix vexed 30-40 minute, be then placed in hot pot, turn over rapidly
Dynamic, fry to surface color with slow fire and deepen, tack-free take out constantly, airing；
7), surface buff is selected, micro-glossy, somewhat stickiness, there is sweet fragrance, the sweetened haw that taste is sweet, remove and stick with paste sheet fragment, use
Non-toxic polyethylene plastic, transparent bag is packed, and seals up for safekeeping.
The invention have the advantage that
1, the candied uctus Crataegi of a kind of vessel softening of the present invention, boils natural honey so that it is flavour is stronger, makes
Herba Ephedrae mouthfeel is more sweet, and color and luster is more glossy, plays increase pliability simultaneously for Herba Ephedrae decoction pieces, prevents from crushing.
2, the candied uctus Crataegi of a kind of vessel softening of the present invention, size is uniform, and color and luster temperature is yellow, and sweet mouthfeel, nutrition is rich
Richness, drinks conveniently, and contained effective ingredient has the health-care effects such as vessel softening, inducing diuresis to remove edema, heat clearing away, toxin expelling.
3, compared with resolvase, immobilized enzyme is keeping while its efficient, single-minded and gentle enzymic catalytic reaction characteristic,
Also present bin stability height, separation and recovery is easy, can repeatedly use, operate the advantages such as the most controlled, simple process.
Detailed description of the invention
A kind of candied uctus Crataegi of vessel softening, is made up of following raw materials in part by weight:
Fructus Crataegi 50, collagen protein powder 13, tremella polysaccharide 13, cellulase 5, natural honey 80, yellow wine 25, Oleum Camelliae 7, Fructus Corni
10, Radix Notoginseng seed 6, Exocarpium Benincasae 8, tuckahoe cream 10, Petiolus nelumbinis 10.
The described candied uctus Crataegi of a kind of vessel softening, is made up of the following step:
1), Fructus Crataegi is cleaned, remove woody stems, undesirable root and impurity, clean Fructus Crataegi is loaded in Turnround basket, cleans end；
2), with microtome, Fructus Crataegi being cut into the thick Fructus Crataegi slice of 5mm, the Fructus Crataegi after cutting loads in Turnover Box；
3), by Fructus Corni, Radix Notoginseng seed, Exocarpium Benincasae, tuckahoe cream, Petiolus nelumbinis, yellow wine mixing, adding 20 times amount water, slow fire infusion 3 is little
Time, make decoction be concentrated into the 1/3 of stock solution, filtering and impurity removing, collect filtrate；
4), by step 3 gained filtering residue rub, add 5 times amount decocting in water to boiling, stop heating, be cooled to 60 DEG C, regulation pH value in
5.0, it is subsequently adding the agar immobilized cellulase granule that mass fraction is 5%, in 55 DEG C of ferment at constant temperature 3 hours, filters, point
From reclaiming immobilized cellulase, collect filtrate；
5), natural honey is put in inclinable jacketed kettle, mix with step 3, step 4 gained filtrate, after being heated to slowly seething with excitement,
Using slow fire instead, keep the waxiness of micro-boiling, scumming and floating and dead honeybee, temperature is maintained at 116 DEG C, and refining to panful plays fish bubble
Eye, adds collagen protein powder, tremella polysaccharide, mixing, with the toughness of hands sth. made by twisting, there is no white silk when occurring, take the dish out of the pot rapidly between referring to；
6), take step 5 gained mixture and step 2 gained Fructus Crataegi slice and mix vexed 30 minutes, be then placed in hot pot, stir rapidly,
Fry to surface color with slow fire and deepen, tack-free take out constantly, airing；
7), surface buff is selected, micro-glossy, somewhat stickiness, there is sweet fragrance, the sweetened haw that taste is sweet, remove and stick with paste sheet fragment, use
Non-toxic polyethylene plastic, transparent bag is packed, and seals up for safekeeping.
Claims (2)
1. the candied uctus Crataegi of vessel softening, it is characterised in that be made up of following raw materials in part by weight:
Fructus Crataegi 50-60, collagen protein powder 13-15, tremella polysaccharide 13-15, cellulase 5-6, natural honey 80-90, yellow wine 25-
30, Oleum Camelliae 7-8, Fructus Corni 10-12, Radix Notoginseng seed 6-7, Exocarpium Benincasae 8-9, tuckahoe cream 10-12, Petiolus nelumbinis 10-12.
A kind of candied uctus Crataegi of vessel softening the most according to claim 1, it is characterised in that be made up of the following step
:
1), Fructus Crataegi is cleaned, remove woody stems and impurity, clean Fructus Crataegi is loaded in Turnround basket, cleans end；
2), with microtome, Fructus Crataegi being cut into the thick Fructus Crataegi slice of 5-7mm, the Fructus Crataegi after cutting loads in Turnover Box；
3), by Fructus Corni, Radix Notoginseng seed, Exocarpium Benincasae, tuckahoe cream, Petiolus nelumbinis, yellow wine mixing, 20-25 times amount water, slow fire infusion 3-are added
5 hours, make decoction be concentrated into the 1/5-3 of stock solution, filtering and impurity removing, collect filtrate；
4), step 3 gained filtering residue is rubbed, add the extremely boiling of 5-10 times amount decocting in water, stop heating, be cooled to 60-70 DEG C, regulation
PH value, in 4.0-6.0, is subsequently adding the agar immobilized cellulase granule that mass fraction is 5-10%, sends out in 55-60 DEG C of constant temperature
Ferment 3-5 hour, filters, and separates and recovers immobilized cellulase, collects filtrate；
5), natural honey is put in inclinable jacketed kettle, mix with step 3, step 4 gained filtrate, after being heated to slowly seething with excitement,
Using slow fire instead, keep the waxiness of micro-boiling, scumming and floating and dead honeybee, temperature is maintained at 116-118 DEG C, and refining to panful plays fish
Bubble eye, adds collagen protein powder, tremella polysaccharide, mixing, with the toughness of hands sth. made by twisting, there is no white silk when occurring, take the dish out of the pot rapidly between referring to；
6), take step 5 gained mixture and step 2 gained Fructus Crataegi slice and mix vexed 30-40 minute, be then placed in hot pot, turn over rapidly
Dynamic, fry to surface color with slow fire and deepen, tack-free take out constantly, airing；
7), surface buff is selected, micro-glossy, somewhat stickiness, there is sweet fragrance, the sweetened haw that taste is sweet, remove and stick with paste sheet fragment, use
Non-toxic polyethylene plastic, transparent bag is packed, and seals up for safekeeping.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610420133.3A CN106071621A (en) | 2016-06-16 | 2016-06-16 | A kind of candied uctus Crataegi of vessel softening and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610420133.3A CN106071621A (en) | 2016-06-16 | 2016-06-16 | A kind of candied uctus Crataegi of vessel softening and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
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| CN106071621A true CN106071621A (en) | 2016-11-09 |
Family
ID=57846073
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610420133.3A Pending CN106071621A (en) | 2016-06-16 | 2016-06-16 | A kind of candied uctus Crataegi of vessel softening and preparation method thereof |
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| Country | Link |
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| CN (1) | CN106071621A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1919997A (en) * | 2005-08-25 | 2007-02-28 | 深圳市海川实业股份有限公司 | Hawthorn yellow wine health care drink and preparation method thereof |
| CN103355678A (en) * | 2013-08-05 | 2013-10-23 | 彭常安 | Manufacturing method for haw-licorice decoction piece |
| CN104186837A (en) * | 2014-08-19 | 2014-12-10 | 安徽孟氏中药饮片有限公司 | Crataegus pinnatifida bunge and lotus leaf gut purging tea and preparation method thereof |
| CN104304602A (en) * | 2014-11-24 | 2015-01-28 | 青岛恒波仪器有限公司 | Pagoda tree fruit tea capable of softening blood vessels and preparation method thereof |
-
2016
- 2016-06-16 CN CN201610420133.3A patent/CN106071621A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1919997A (en) * | 2005-08-25 | 2007-02-28 | 深圳市海川实业股份有限公司 | Hawthorn yellow wine health care drink and preparation method thereof |
| CN103355678A (en) * | 2013-08-05 | 2013-10-23 | 彭常安 | Manufacturing method for haw-licorice decoction piece |
| CN104186837A (en) * | 2014-08-19 | 2014-12-10 | 安徽孟氏中药饮片有限公司 | Crataegus pinnatifida bunge and lotus leaf gut purging tea and preparation method thereof |
| CN104304602A (en) * | 2014-11-24 | 2015-01-28 | 青岛恒波仪器有限公司 | Pagoda tree fruit tea capable of softening blood vessels and preparation method thereof |
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Application publication date: 20161109 |