CN106011195A - Preparation method of prodigiosin for silk fabric dyeing - Google Patents
Preparation method of prodigiosin for silk fabric dyeing Download PDFInfo
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- CN106011195A CN106011195A CN201610534058.3A CN201610534058A CN106011195A CN 106011195 A CN106011195 A CN 106011195A CN 201610534058 A CN201610534058 A CN 201610534058A CN 106011195 A CN106011195 A CN 106011195A
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- prodigiosin
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- silk fabric
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
- C12P17/00—Preparation of heterocyclic carbon compounds with only O, N, S, Se or Te as ring hetero atoms
- C12P17/16—Preparation of heterocyclic carbon compounds with only O, N, S, Se or Te as ring hetero atoms containing two or more hetero rings
- C12P17/165—Heterorings having nitrogen atoms as the only ring heteroatoms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
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- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Zoology (AREA)
- Wood Science & Technology (AREA)
- Biotechnology (AREA)
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- General Chemical & Material Sciences (AREA)
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Abstract
Provided is a preparation method of prodigiosin for silk fabric dyeing. An original prodigiosin culture process is adjusted, so that the effect of the cultured prodigiosin applied to silk fabrics is good. Especially under the situation of severe dyeing, the usage amount of the added prodigiosin and the time required by dyeing are greatly improved, a mordant and other chemical reagents are not needed to be added in the dyeing process, the cost is low, and the preparation method is healthy and environmentally friendly.
Description
Technical field
The present invention relates to technical field of textile printing, particularly relate to a kind of for silk fabric dyeing
The preparation method of prodigiosin.
Background technology
In recent years, due to environmental problem and the impact of energy problem, people tend to pursuing sustainable
, eco-friendly and human health advantageous approach is produced dyestuff.Exploitation natural dye
Being the general trend of world's application dyestuff development, natural dye refers to provide from plant, animal or mineral products
Obtain, the little or no dyestuff through chemical process in source, a lot of natural dyes have peace
Complete reliable, tone is natural, and close to advantages such as natural materials, natural, multi-functional is dyestuff development
Trend.Therefore from natural resources, filter out the microorganism that can produce natural dye, and then
The natural dye of developing new product variety, especially has functional natural dye, has wide
Prospect.Along with the development of biotechnology, utilize biotechnology to produce natural dye and open up for people
Wide field.Biofermentation product stability is high, and specificity is strong, pollution-free, produces
Journey is to people's fanout free region, and therefore, biological fermentation process is a kind of method of good synthetic dyestuffs.
The methoxypyrrole framing structure that bacterial dye prodigiosin is made up of three pyrrole rings
Natural pigment, be the secondary metabolite of some actinomycetes, Serratieae and other antibacterials,
There is the multiple biological activitys such as immunosuppressant, antibacterium, antifungal and malaria.Therefore, carefully
Bacterium dyestuff prodigiosin just has antibacterial function as its dyed fabric after dyeing, and
There is anticancer effect.
Donghua University discloses prodigiosin to sheep in four patents of 2010 and 2011 applications
Hair, the colouring method of acrylon, but the colouring method of silk fiber is not studied.
Summary of the invention
In order to solve the problem in background technology, the present invention provides a kind of and dyes for silk fabric
The preparation method of prodigiosin.
The preparation method of a kind of prodigiosin for silk fabric dyeing, comprises the following steps:
Step one: (Serratia marcesens, purchased from Chinese medicine antibacterial preservation by the strain of purchase
Administrative center) be diluted, after the antibacterial after dilution is coated and puts into perseverance on plating medium
Temperature incubator is cultivated；
Step 2: picking red pigment and the deeper bacterial strain of color are coated on plating medium, and
This bacterial strain is preserved under conditions of 4 DEG C；
Step 3: the bacterial strain screened is cultivated 6-8h in seed culture medium, accesses afterwards
Fermentation medium cultivates 15h；
Step 4: respectively supernatant and thalline are separated；Supernatant directly uses ethyl acetate
Being extracted from aqueous solution by prodigiosin, flocculate concentrates by rotary evaporator after being first centrifuged
After in acidic methanol extract.
Preferably, the plating medium in described step one, including following main component: ferment
Female powder 10g/L, peptone 20g/L, glucose 2g/L, agar powder 20g/L, constant volume to 1L,
Surplus is water.
Preferably, the described seed culture medium in step 3, including following main component: sugarcane
Sugar 15g/L, yeast extract 0.5g/L, sodium chloride 0.2g/L, magnesium sulfate 1g/L, constant volume arrive
1L, surplus is water.
Preferably, the prodigiosin for silk fabric dyeing of the present invention, it is applied to dye
The concrete grammar of color, comprises the following steps:
A, dissolve the prodigiosin by by ethyl acetate, and add Elymus nutans extract, so
After be added to the water, make staining solution；
B, using above-mentioned staining solution to dye silk fabric, the consumption of prodigiosin is
The 0.1-0.5% of silk fabric mass fraction, dye bath ratio is 1: 10-20, regulation dye liquor
PH value is 4.0-6.0, and dyeing temperature is 60-70 DEG C, and temperature retention time is 15-25min；
After C, dyeing terminate, by fabric washing, 120 DEG C of drying 3-5min after insulation is terminated,
?.
Described silk fabric needs before use through sterilization processing, described sterilization processing side
Method is: 150 DEG C of high temperature sterilize 10min.
Elymus nutans is Perennual herbaceous plant, high50-70 centimetres, cultigen
80-120 centimetre.Rhizome dredges plexi, and well developed root system, in palpus shape.Stalk is upright, and 3-4 saves, base
It is bent that portion saves slightly knee joint.Blade is flat, long 6-8Centimetre, wide 3-5 millimeter, the micro-preesed grass in both sides or under
Portion smooths, and dredges raw pubescence above, and sheath is in addition to base portion person, and remaining is all shorter than internode.Tip of a leaf pole
Short, it is about 0.5 millimeter.Spike arrangement is relatively tight, the side of the many relatively cobs of small ear,
Generally curved, tip is sagging, long 5-12 centimetre, and cob often saves typically two pieces of small ears；Close
Top end respectively saves only one piece of small ear of tool, and base portion has sterile small ear, and small ear obstructs short or nothing；Small ear is green
Color, maturation zone purple, long 12-15 millimeter, every small ear little Hua Han 3-4, the most only 2-3 flower
Can educate.Grain husk, in Long Circle, has 3-4 arteries and veins, long 4-5 millimeter, the short awns that tool 1-4 millimeter is long；
The long lanceolar of lemma, has 5 arteries and veins；Awn length 12-20 millimeter, coarse, outside contrary flexure or slightly launch,
Glumelle and lemma have 5 arteries and veins, isometric, tip blunt circle or truncated.Turn black after flower pesticide maturation.Grain husk
Really, seed lanceolar, puce, mass of 1000 kernel 2.85-3.2 gram.
Elymus nutans is internal containing flavone compound after deliberation, adds the fringe that hangs down and drape over one's shoulders in the present invention
Alkali grass, on the one hand can improve Color, on the other hand can promote silk fabric after dyeing
Anti-microbial property.
The preparation method of the prodigiosin for silk fabric dyeing of the present invention, have adjusted
The culture process of original prodigiosin, makes the prodigiosin of cultivation be applied to silk fabric effect
More preferably, particularly dye heavier in the case of, the consumption of the prodigiosin of addition and dyeing institute
The time needed all has greatly improved, without adding the chemical reagent such as mordant in dyeing course,
Low cost, health environment-friendly.
Detailed description of the invention
Embodiment 1
The preparation method of a kind of prodigiosin for silk fabric dyeing, comprises the following steps:
Step one: (Serratia marcesens, purchased from Chinese medicine antibacterial preservation by the strain of purchase
Administrative center) be diluted, after will dilution after antibacterial coat plating medium (yeast powder
10g/L, peptone 20g/L, glucose 2g/L, agar powder 20g/L, constant volume are to 1L, remaining
Amount is for water) on put in constant incubator and cultivate；
Step 2: picking red pigment and the deeper bacterial strain of color are coated on plating medium, and
This bacterial strain is preserved under conditions of 4 DEG C.
Step 3: (sucrose 15g/L, yeast soak at seed culture medium by the bacterial strain that screens
Cream 0.5g/L, sodium chloride 0.2g/L, magnesium sulfate 1g/L, constant volume to 1L, surplus is water, adjusts
Whole pH value 7.0-7.5) the middle 6h that cultivates, the rear fermentation medium that accesses cultivates 15h；
Step 4: respectively supernatant and thalline are separated；Supernatant directly uses ethyl acetate
Being extracted from aqueous solution by prodigiosin, flocculate concentrates by rotary evaporator after being first centrifuged
After in acidic methanol extract.
The described prodigiosin for silk fabric dyeing, is applied to the concrete grammar of dyeing,
Comprise the following steps:
A, dissolve the prodigiosin by by ethyl acetate, and add Elymus nutans extract, so
After be added to the water, make staining solution；
B, using above-mentioned staining solution to dye silk fabric, the consumption of prodigiosin is
The 0.4% of silk fabric mass fraction, dye bath ratio is 1: 15, and the pH value of regulation dye liquor is
4.0-6.0, dyeing temperature is 65 DEG C, and temperature retention time is 20min.
After C, dyeing terminate, by fabric washing, 120 DEG C of drying 4min after insulation is terminated,
?.
Described silk fabric needs before use through sterilization processing, described sterilization processing side
Method is: 150 DEG C of high temperature sterilize 10min.
Embodiment 2
The preparation method of a kind of prodigiosin for silk fabric dyeing, comprises the following steps:
Step one: (Serratia marcesens, purchased from Chinese medicine antibacterial preservation by the strain of purchase
Administrative center) be diluted, after will dilution after antibacterial coat plating medium (yeast powder
10g/L, peptone 20g/L, glucose 2g/L, agar powder 20g/L, constant volume are to 1L, remaining
Amount is for water) on put in constant incubator and cultivate；
Step 2: picking red pigment and the deeper bacterial strain of color are coated on plating medium, and
This bacterial strain is preserved under conditions of 4 DEG C；
Step 3: (sucrose 15g/L, yeast soak at seed culture medium by the bacterial strain that screens
Cream 0.5g/L, sodium chloride 0.2g/L, magnesium sulfate 1g/L, constant volume to 1L, surplus is water, adjusts
Whole pH value 7.0-7.5) the middle 7h that cultivates, the rear fermentation medium that accesses cultivates 15h；
Step 4: respectively supernatant and thalline are separated；Supernatant directly uses ethyl acetate
Being extracted from aqueous solution by prodigiosin, flocculate concentrates by rotary evaporator after being first centrifuged
After in acidic methanol extract.
The described prodigiosin for silk fabric dyeing, is applied to the concrete grammar of dyeing,
Comprise the following steps:
A, dissolve the prodigiosin by by ethyl acetate, and add Elymus nutans extract, so
After be added to the water, make staining solution；
B, using above-mentioned staining solution to dye silk fabric, the consumption of prodigiosin is
The 0.5% of silk fabric mass fraction, dye bath ratio is 1: 20, and the pH value of regulation dye liquor is
4.0-5.0, dyeing temperature is 65 DEG C, and temperature retention time is 25min；
After C, dyeing terminate, by fabric washing, 120 DEG C of drying 3min after insulation is terminated,
?.
Described silk fabric needs before use through sterilization processing, described sterilization processing side
Method is: 150 DEG C of high temperature sterilize 10min.
Embodiment 3
The preparation method of a kind of prodigiosin for silk fabric dyeing, comprises the following steps:
Step one: (Serratia marcesens, purchased from Chinese medicine antibacterial preservation by the strain of purchase
Administrative center) be diluted, after will dilution after antibacterial coat plating medium (yeast powder
10g/L, peptone 20g/L, glucose 2g/L, agar powder 20g/L, constant volume are to 1L, remaining
Amount is for water) on put in constant incubator and cultivate；
Step 2: picking red pigment and the deeper bacterial strain of color are coated on plating medium, and
This bacterial strain is preserved under conditions of 4 DEG C；
Step 3: (sucrose 15g/L, yeast soak at seed culture medium by the bacterial strain that screens
Cream 0.5g/L, sodium chloride 0.2g/L, magnesium sulfate 1g/L, constant volume to 1L, surplus is water, adjusts
Whole pH value 7.0-7.5) the middle 8h that cultivates, the rear fermentation medium that accesses cultivates 15h；
Step 4: respectively supernatant and thalline are separated；Supernatant directly uses ethyl acetate
Being extracted from aqueous solution by prodigiosin, flocculate concentrates by rotary evaporator after being first centrifuged
After in acidic methanol extract.
The described prodigiosin for silk fabric dyeing, is applied to the concrete grammar of dyeing,
Comprise the following steps:
A, dissolve the prodigiosin by by ethyl acetate, and add Elymus nutans extract, so
After be added to the water, make staining solution；
B, using above-mentioned staining solution to dye silk fabric, the consumption of prodigiosin is
The 0.1% of silk fabric mass fraction, dye bath ratio is 1: 10, and the pH value of regulation dye liquor is
4.0-5.5, dyeing temperature is 60 DEG C, and temperature retention time is 15min；
After C, dyeing terminate, by fabric washing, 120 DEG C of drying 5min after insulation is terminated,
?.
Described silk fabric needs before use through sterilization processing, described sterilization processing side
Method is: 150 DEG C of high temperature sterilize 10min.
The silk fabric using embodiment of the present invention 1-3 method is detected, and by dyeing
Parameter and Donghua University disclosed in the CN102493228A prodigiosin colouring method to Pilus Caprae seu Ovis
Contrast, obtain following data:
The above, the only present invention preferably detailed description of the invention, but the protection of the present invention
Scope is not limited thereto, and any those familiar with the art the invention discloses
In technical scope, according to technical scheme and inventive concept equivalent in addition thereof or change
Become, all should contain within protection scope of the present invention.
Claims (5)
1. the preparation method for the prodigiosin of silk fabric dyeing, it is characterised in that comprise the following steps:
Step one: the strain of purchase is diluted, after will dilution after antibacterial coat put on plating medium in constant incubator cultivate；
Step 2: picking red pigment and the deeper bacterial strain of color are coated on plating medium, and are preserved under conditions of 4 DEG C by this bacterial strain；
Step 3: the bacterial strain screened is cultivated in seed culture medium 6-8h, the rear fermentation medium that accesses cultivates 15h；
Step 4: respectively supernatant and thalline are separated；Prodigiosin is directly extracted from aqueous solution by supernatant by ethyl acetate, and flocculate extracts after concentrating by rotary evaporator after being first centrifuged in acidic methanol.
The preparation method of the prodigiosin for silk fabric dyeing the most according to claim 1, it is characterised in that the plating medium in described step one, including following main component: yeast powder 10g/L, peptone 20g/L, glucose 2g/L, agar powder 20g/L, constant volume are to 1L, and surplus is water.
The preparation method of the prodigiosin for silk fabric dyeing the most according to claim 1, it is characterized in that, the described seed culture medium in step 3, including following main component: sucrose 15g/L, yeast extract 0.5g/L, sodium chloride 0.2g/L, magnesium sulfate 1g/L, constant volume to 1L, surplus is water.
4., for a prodigiosin for silk fabric dyeing, it is applied to the concrete grammar of dyeing, comprises the following steps:
A, dissolve the prodigiosin by by ethyl acetate, and add Elymus nutans extract, be then added in water, make staining solution；
B, use above-mentioned staining solution that silk fabric is dyeed, the consumption of prodigiosin is the 0.1-0.5% of silk fabric mass fraction, and dye bath ratio is 1: 10-20, and the pH value of regulation dye liquor is 4.0-6.0, dyeing temperature is 60-70 DEG C, and temperature retention time is 15-25min；
After C, dyeing terminate, by fabric washing, 120 DEG C of drying 3-5min after insulation is terminated,；
Described silk fabric needs through sterilization processing before use, and described bactericidal treatments is: 150 DEG C of high temperature sterilize 10min.
Prodigiosin for silk fabric dyeing the most according to claim 4, is applied to the concrete grammar of dyeing, comprises the following steps:
A, dissolve the prodigiosin by by ethyl acetate, and add Elymus nutans extract, be then added in water, make staining solution；
B, using above-mentioned staining solution to dye silk fabric, the consumption of prodigiosin is the 0.5% of silk fabric mass fraction, and dye bath ratio is 1: 20, and the pH value of regulation dye liquor is 4.0-5.0, and dyeing temperature is 65 DEG C, and temperature retention time is 25min；
After C, dyeing terminate, by fabric washing, 120 DEG C of drying 3min after insulation is terminated,；
Described silk fabric needs through sterilization processing before use, and described bactericidal treatments is: 150 DEG C of high temperature sterilize 10min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610534058.3A CN106011195A (en) | 2016-07-04 | 2016-07-04 | Preparation method of prodigiosin for silk fabric dyeing |
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| CN201610534058.3A CN106011195A (en) | 2016-07-04 | 2016-07-04 | Preparation method of prodigiosin for silk fabric dyeing |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106436366A (en) * | 2016-10-16 | 2017-02-22 | 饶琼仙 | Production method of discharge prints of gambiered Canton gauze |
| CN106436365A (en) * | 2016-10-16 | 2017-02-22 | 饶琼仙 | Production method of gambiered canton gauze discharge print adopting pure natural raw materials |
| CN108411631A (en) * | 2018-04-16 | 2018-08-17 | 佛山市尚柏科技有限公司 | A kind of washable textile product inorganic agent |
| CN108720032A (en) * | 2017-04-19 | 2018-11-02 | 嘉兴学院 | A kind of natural pigment pure cellulose food and preparation method thereof |
| CN112375791A (en) * | 2020-11-26 | 2021-02-19 | 河池学院 | Preparation and dyeing method of streptomyces spectabilis haematochrome |
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| CN102493220A (en) * | 2011-12-09 | 2012-06-13 | 东华大学 | Method for dyeing acrylic fiber fabrics by utilizing bacterium dyestuff prodigiosin |
| CN102493228A (en) * | 2011-12-09 | 2012-06-13 | 东华大学 | Method for dyeing wool fabric by using bacterial dye of prodigiosin |
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2016
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|---|---|---|---|---|
| CN102493220A (en) * | 2011-12-09 | 2012-06-13 | 东华大学 | Method for dyeing acrylic fiber fabrics by utilizing bacterium dyestuff prodigiosin |
| CN102493228A (en) * | 2011-12-09 | 2012-06-13 | 东华大学 | Method for dyeing wool fabric by using bacterial dye of prodigiosin |
Non-Patent Citations (3)
| Title |
|---|
| 汤立军 等: "《黄酮类发色体的合成与应用》", 30 June 2011 * |
| 谈献和 等: "《药用植物学》", 31 May 2009 * |
| 钟绵国: "灵菌红素的合成及其染色性能研究", 《中国优秀硕士学位论文全文数据库 工程科技Ⅰ辑》 * |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106436366A (en) * | 2016-10-16 | 2017-02-22 | 饶琼仙 | Production method of discharge prints of gambiered Canton gauze |
| CN106436365A (en) * | 2016-10-16 | 2017-02-22 | 饶琼仙 | Production method of gambiered canton gauze discharge print adopting pure natural raw materials |
| CN106436366B (en) * | 2016-10-16 | 2019-07-02 | 江苏佳丝缘纺织有限公司 | A kind of Canton gauze gambiered pulls out the production method of print stamp |
| CN108720032A (en) * | 2017-04-19 | 2018-11-02 | 嘉兴学院 | A kind of natural pigment pure cellulose food and preparation method thereof |
| CN108411631A (en) * | 2018-04-16 | 2018-08-17 | 佛山市尚柏科技有限公司 | A kind of washable textile product inorganic agent |
| CN112375791A (en) * | 2020-11-26 | 2021-02-19 | 河池学院 | Preparation and dyeing method of streptomyces spectabilis haematochrome |
| CN112375791B (en) * | 2020-11-26 | 2022-04-22 | 河池学院 | Preparation and dyeing method of streptomyces spectabilis haematochrome |
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Application publication date: 20161012 |