CN105995916A - Making method of ampelopsis sinica bamboo salt - Google Patents
Making method of ampelopsis sinica bamboo salt Download PDFInfo
- Publication number
- CN105995916A CN105995916A CN201610307242.4A CN201610307242A CN105995916A CN 105995916 A CN105995916 A CN 105995916A CN 201610307242 A CN201610307242 A CN 201610307242A CN 105995916 A CN105995916 A CN 105995916A
- Authority
- CN
- China
- Prior art keywords
- ampelopsis
- caulis
- salt
- bamboo
- seu folium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000017166 Bambusa arundinacea Nutrition 0.000 title claims abstract description 119
- 235000017491 Bambusa tulda Nutrition 0.000 title claims abstract description 119
- 235000015334 Phyllostachys viridis Nutrition 0.000 title claims abstract description 119
- 241001330002 Bambuseae Species 0.000 title claims abstract description 118
- 239000011425 bamboo Substances 0.000 title claims abstract description 118
- 150000003839 salts Chemical class 0.000 title claims abstract description 108
- 238000000034 method Methods 0.000 title abstract description 14
- 241001034521 Ampelopsis sinica Species 0.000 title abstract 7
- KJXSIXMJHKAJOD-LSDHHAIUSA-N (+)-dihydromyricetin Chemical compound C1([C@@H]2[C@H](C(C3=C(O)C=C(O)C=C3O2)=O)O)=CC(O)=C(O)C(O)=C1 KJXSIXMJHKAJOD-LSDHHAIUSA-N 0.000 claims abstract description 68
- 229930003944 flavone Natural products 0.000 claims abstract description 60
- 235000011949 flavones Nutrition 0.000 claims abstract description 60
- KQILIWXGGKGKNX-UHFFFAOYSA-N dihydromyricetin Natural products OC1C(=C(Oc2cc(O)cc(O)c12)c3cc(O)c(O)c(O)c3)O KQILIWXGGKGKNX-UHFFFAOYSA-N 0.000 claims abstract description 34
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 claims abstract description 28
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 claims abstract description 28
- 150000002212 flavone derivatives Chemical class 0.000 claims abstract description 27
- 238000010438 heat treatment Methods 0.000 claims abstract description 19
- 239000013078 crystal Substances 0.000 claims abstract description 13
- 238000001816 cooling Methods 0.000 claims abstract description 11
- 238000002156 mixing Methods 0.000 claims abstract description 11
- 238000003756 stirring Methods 0.000 claims abstract description 3
- 235000009388 Parthenocissus quinquefolia Nutrition 0.000 claims description 143
- 241000563984 Ampelopsis Species 0.000 claims description 124
- 150000002213 flavones Chemical class 0.000 claims description 32
- 238000002360 preparation method Methods 0.000 claims description 25
- 239000000203 mixture Substances 0.000 claims description 24
- 238000001354 calcination Methods 0.000 claims description 23
- 239000000284 extract Substances 0.000 claims description 18
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 18
- 238000003837 high-temperature calcination Methods 0.000 claims description 16
- 159000000007 calcium salts Chemical class 0.000 claims description 14
- 159000000003 magnesium salts Chemical class 0.000 claims description 14
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 13
- 235000013305 food Nutrition 0.000 claims description 13
- 239000000419 plant extract Substances 0.000 claims description 12
- 238000000605 extraction Methods 0.000 claims description 9
- 235000013311 vegetables Nutrition 0.000 claims description 9
- RSWGJHLUYNHPMX-ONCXSQPRSA-N abietic acid Chemical compound C([C@@H]12)CC(C(C)C)=CC1=CC[C@@H]1[C@]2(C)CCC[C@@]1(C)C(O)=O RSWGJHLUYNHPMX-ONCXSQPRSA-N 0.000 claims description 7
- 238000004587 chromatography analysis Methods 0.000 claims description 6
- 239000011833 salt mixture Substances 0.000 claims description 6
- 150000002576 ketones Chemical class 0.000 claims description 4
- 238000002844 melting Methods 0.000 claims description 4
- 230000008018 melting Effects 0.000 claims description 4
- 239000002537 cosmetic Substances 0.000 claims description 2
- 241000219099 Parthenocissus quinquefolia Species 0.000 claims 20
- 235000002639 sodium chloride Nutrition 0.000 abstract description 94
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract description 11
- 239000011780 sodium chloride Substances 0.000 abstract description 11
- 239000011575 calcium Substances 0.000 abstract description 8
- 229910052791 calcium Inorganic materials 0.000 abstract description 8
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract description 7
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 abstract description 7
- 239000011777 magnesium Substances 0.000 abstract description 7
- 229910052749 magnesium Inorganic materials 0.000 abstract description 7
- 239000000843 powder Substances 0.000 description 21
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Natural products CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 14
- 241001018563 Nekemias grossedentata Species 0.000 description 11
- 239000000047 product Substances 0.000 description 9
- 241000196324 Embryophyta Species 0.000 description 8
- 238000010792 warming Methods 0.000 description 8
- 229960005069 calcium Drugs 0.000 description 7
- 230000000694 effects Effects 0.000 description 7
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 239000000706 filtrate Substances 0.000 description 6
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 4
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 4
- TWRXJAOTZQYOKJ-UHFFFAOYSA-L Magnesium chloride Chemical compound [Mg+2].[Cl-].[Cl-] TWRXJAOTZQYOKJ-UHFFFAOYSA-L 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 4
- -1 flavone compound Chemical class 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 3
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 3
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 3
- 239000008280 blood Substances 0.000 description 3
- 210000004369 blood Anatomy 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 2
- ZCYVEMRRCGMTRW-UHFFFAOYSA-N 7553-56-2 Chemical compound [I] ZCYVEMRRCGMTRW-UHFFFAOYSA-N 0.000 description 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- 238000007445 Chromatographic isolation Methods 0.000 description 2
- LCGLNKUTAGEVQW-UHFFFAOYSA-N Dimethyl ether Chemical group COC LCGLNKUTAGEVQW-UHFFFAOYSA-N 0.000 description 2
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- 241000218922 Magnoliophyta Species 0.000 description 2
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 description 2
- 241000727556 Nekemias cantoniensis Species 0.000 description 2
- 239000004952 Polyamide Substances 0.000 description 2
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 2
- 241000219094 Vitaceae Species 0.000 description 2
- 235000009392 Vitis Nutrition 0.000 description 2
- 241000219095 Vitis Species 0.000 description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 description 2
- 235000008429 bread Nutrition 0.000 description 2
- BTANRVKWQNVYAZ-UHFFFAOYSA-N butan-2-ol Chemical compound CCC(C)O BTANRVKWQNVYAZ-UHFFFAOYSA-N 0.000 description 2
- 239000001110 calcium chloride Substances 0.000 description 2
- 229910001628 calcium chloride Inorganic materials 0.000 description 2
- 239000004227 calcium gluconate Substances 0.000 description 2
- 235000013927 calcium gluconate Nutrition 0.000 description 2
- 229960004494 calcium gluconate Drugs 0.000 description 2
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 2
- NEEHYRZPVYRGPP-UHFFFAOYSA-L calcium;2,3,4,5,6-pentahydroxyhexanoate Chemical compound [Ca+2].OCC(O)C(O)C(O)C(O)C([O-])=O.OCC(O)C(O)C(O)C(O)C([O-])=O NEEHYRZPVYRGPP-UHFFFAOYSA-L 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 238000005520 cutting process Methods 0.000 description 2
- YMWUJEATGCHHMB-UHFFFAOYSA-N dichloromethane Natural products ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 150000002148 esters Chemical class 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 229910052740 iodine Inorganic materials 0.000 description 2
- 239000011630 iodine Substances 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- ZXEKIIBDNHEJCQ-UHFFFAOYSA-N isobutanol Chemical compound CC(C)CO ZXEKIIBDNHEJCQ-UHFFFAOYSA-N 0.000 description 2
- 229910001629 magnesium chloride Inorganic materials 0.000 description 2
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 description 2
- 239000000347 magnesium hydroxide Substances 0.000 description 2
- 229910001862 magnesium hydroxide Inorganic materials 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 229920002647 polyamide Polymers 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 2
- 241001233863 rosids Species 0.000 description 2
- 238000007789 sealing Methods 0.000 description 2
- 238000010187 selection method Methods 0.000 description 2
- 229910052711 selenium Inorganic materials 0.000 description 2
- 239000011669 selenium Substances 0.000 description 2
- 239000000243 solution Substances 0.000 description 2
- 238000010025 steaming Methods 0.000 description 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 description 2
- 239000003053 toxin Substances 0.000 description 2
- 231100000765 toxin Toxicity 0.000 description 2
- REZQBEBOWJAQKS-UHFFFAOYSA-N triacontan-1-ol Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCO REZQBEBOWJAQKS-UHFFFAOYSA-N 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- 229910052725 zinc Inorganic materials 0.000 description 2
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 1
- 241000209128 Bambusa Species 0.000 description 1
- 240000002779 Cayratia japonica Species 0.000 description 1
- 239000003390 Chinese drug Substances 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- BZLVMXJERCGZMT-UHFFFAOYSA-N Methyl tert-butyl ether Chemical compound COC(C)(C)C BZLVMXJERCGZMT-UHFFFAOYSA-N 0.000 description 1
- 208000019695 Migraine disease Diseases 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 241001529246 Platymiscium Species 0.000 description 1
- 241000219000 Populus Species 0.000 description 1
- QOSMNYMQXIVWKY-UHFFFAOYSA-N Propyl levulinate Chemical compound CCCOC(=O)CCC(C)=O QOSMNYMQXIVWKY-UHFFFAOYSA-N 0.000 description 1
- 240000002503 Vitis amurensis Species 0.000 description 1
- 235000004283 Vitis amurensis Nutrition 0.000 description 1
- 239000003463 adsorbent Substances 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 235000001014 amino acid Nutrition 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000003957 anion exchange resin Substances 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 235000015241 bacon Nutrition 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 150000001669 calcium Chemical class 0.000 description 1
- FUFJGUQYACFECW-UHFFFAOYSA-L calcium hydrogenphosphate Chemical compound [Ca+2].OP([O-])([O-])=O FUFJGUQYACFECW-UHFFFAOYSA-L 0.000 description 1
- MKJXYGKVIBWPFZ-UHFFFAOYSA-L calcium lactate Chemical compound [Ca+2].CC(O)C([O-])=O.CC(O)C([O-])=O MKJXYGKVIBWPFZ-UHFFFAOYSA-L 0.000 description 1
- 239000001527 calcium lactate Substances 0.000 description 1
- 229960002401 calcium lactate Drugs 0.000 description 1
- 235000011086 calcium lactate Nutrition 0.000 description 1
- ZFXVRMSLJDYJCH-UHFFFAOYSA-N calcium magnesium Chemical compound [Mg].[Ca] ZFXVRMSLJDYJCH-UHFFFAOYSA-N 0.000 description 1
- 239000003729 cation exchange resin Substances 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 235000014510 cooky Nutrition 0.000 description 1
- 239000012043 crude product Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 235000019700 dicalcium phosphate Nutrition 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 230000029087 digestion Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 150000002170 ethers Chemical class 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000001815 facial effect Effects 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000010408 film Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000012041 food component Nutrition 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- WBJINCZRORDGAQ-UHFFFAOYSA-N formic acid ethyl ester Natural products CCOC=O WBJINCZRORDGAQ-UHFFFAOYSA-N 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 229930182478 glucoside Natural products 0.000 description 1
- 150000008131 glucosides Chemical class 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 230000012010 growth Effects 0.000 description 1
- 235000013402 health food Nutrition 0.000 description 1
- 230000002443 hepatoprotective effect Effects 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 239000010977 jade Substances 0.000 description 1
- 210000003734 kidney Anatomy 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- CSNNHWWHGAXBCP-UHFFFAOYSA-L magnesium sulphate Substances [Mg+2].[O-][S+2]([O-])([O-])[O-] CSNNHWWHGAXBCP-UHFFFAOYSA-L 0.000 description 1
- 235000019341 magnesium sulphate Nutrition 0.000 description 1
- 235000013622 meat product Nutrition 0.000 description 1
- VUZPPFZMUPKLLV-UHFFFAOYSA-N methane;hydrate Chemical compound C.O VUZPPFZMUPKLLV-UHFFFAOYSA-N 0.000 description 1
- 206010027599 migraine Diseases 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- 230000001338 necrotic effect Effects 0.000 description 1
- 235000012149 noodles Nutrition 0.000 description 1
- 235000008935 nutritious Nutrition 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 231100000614 poison Toxicity 0.000 description 1
- 239000003495 polar organic solvent Substances 0.000 description 1
- 229920002401 polyacrylamide Polymers 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 235000013324 preserved food Nutrition 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 238000010850 salt effect Methods 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 208000006379 syphilis Diseases 0.000 description 1
- 238000002560 therapeutic procedure Methods 0.000 description 1
- 238000004809 thin layer chromatography Methods 0.000 description 1
- 230000017423 tissue regeneration Effects 0.000 description 1
- 229940034610 toothpaste Drugs 0.000 description 1
- 239000000606 toothpaste Substances 0.000 description 1
- 239000003440 toxic substance Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/20—Halogens; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Nutrition Science (AREA)
- Inorganic Chemistry (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Dermatology (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention provides ampelopsis sinica bamboo salt and a making method of the ampelopsis sinica bamboo salt. Table salt and bamboo are calcined together at high temperature, temperature is then lowered, crystal bamboo salt is separated out, the active component, namely dihydromyricetin, of ampelopsis sinica plant or general flavone extracted from ampelopsis sinica plant is added, stirring, mixing and heating are conducted at a temperature of 245 DEG C+/-10 DEG C, cooling is conducted so dihydromyricetin or general flavone evenly wraps the calcined bamboo salt. The invention further provides the ampelopsis sinica bamboo salt with calcium and magnesium added and the making method of the ampelopsis sinica bamboo salt.
Description
Technical field
The invention belongs to health food production field, particularly bamboo salt manufacture field, it is provided that Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant effectively becomes one
Bamboo salt of divisional processing and preparation method thereof.
Background technology
It is that the Multiple components contained by bamboo is attached in salt that the Multiple components utilizing salt and bamboo to contain combines the bamboo salt of preparation.
The processing technology of bamboo salt has the history of more than 1300 year.Bamboo salt is initially the folkd therapy of the Buddhist monk's initiative in mausoleum, the most incoming among the people.
The mode that tradition prepares bamboo salt is unique and fastidious.Require, by loading in thick bamboo tube containing the natural sea salt of abundant mineral, to use loess
Sealing, puts in iron still, and calcining iron still heats, and makes bamboo glue fuse into completely in natural sea salt and becomes salt block, obtains for the first time
The bamboo salt block of calcining.Being broken into pieces by the bamboo salt block obtained, again carry out calcining heating in putting thick bamboo tube into, such process is repeated several times,
Finally, the salt block obtained after fusing cooling is pulverized, sieved, the most just can make finished product bamboo salt powder and grain.Owing to bamboo salt is being given birth to
Raw material used in the process of product and the uniqueness of technique so that bamboo salt have removing interior free yl, Balancing, solution toxin expelling,
Superpower reduction, rich in features such as high-energy.
Patent application CN104223000A discloses the preparation method of a kind of bamboo salt treating migraine, patent application
CN104256502A individually discloses the preparation method of the bamboo salt of a kind of hepatoprotective kidney tonifying, is all to be fried into by Traditional Chinese drug mixture slow fire
Make dry powder after juice, it is put into together with salt high-temperature calcination in bamboo section.The defect of this method is that calcination stage temperature is too high,
Destroy Effective Component of Chinese Medicine so that it can not play its effect well.
Ampelopsis, Latin plant name is Ampelopsis grossedentata, is Angiospermae
(Magnoliophyta) the planting of Rosidae (Rosidae) Vitaceae (Vitaceae) Ampelopsis (Ampelopsis Michx.)
Thing, is the endemic plant of China.It includes the trace of abundant flavone, aminoacid, glucoside, vitamin and some needed by human body
Element.Originate in the ground such as Fujian, Jiangxi, Hunan, Guangxi, Guizhou, Yunnan.It is grown in height above sea level 800-1500 rice Yunwu Mountain.
Its growing environment soil, water source, air, it is necessary to be not affected by any pollution, for real pure natural, ecosystem, nothing dirt
The wild plant of dye.Ampelopsis contains abundant flavone compound.From 20 century 70s, to Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae)
Platymiscium the effective ingredient particularly extraction purification of monomer effective ingredient, isolation identification etc. have more comprehensively research.Up to now,
There are no and ampelopsis effect is combined with bamboo salt, with abundant bamboo salt effect, it is provided that the report of the bamboo salt of multiple efficacies.
Summary of the invention
It is an object of the invention to provide a kind of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt with multiple nutritional components and preparation method thereof.The present invention's
Purpose is realized by techniques below scheme: the preparation method of a kind of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt, is characterised by edible salt and bamboo
Together high-temperature calcination, then reduces temperature, isolates crystal bamboo salt, pulverizes, and adds Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) vegetable active composition dihydromyricetin
Element or from the total flavones of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant extract, at a temperature of 245 DEG C ± 10 DEG C stir Hybrid Heating, cooling, make dihydro poplar
Syphilis or total flavones are wrapped on the bamboo salt of calcining.
The Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt being prepared by the method for the present invention, product is uniform, and steady quality does not pollute, and physical aspect and outward appearance are good,
Nutritious.Because by Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) vegetable active composition dihydromyricetin or the total flavones from Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant extract are dried
Powder is mixed together heating with the bamboo salt through calcining, dihydromyricetin or equal from the total flavones dried powder of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant extract
Outside the even bamboo salt being wrapped in through calcining, and part is had to penetrate into.Heating and temperature control is planted at dihydromyricetin or from Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae)
Near the total flavones dried powder fusing point of thing extract, Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant effect is retained very well, the Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt pair obtained
In blood sugar lowering, blood fat reducing, nourishing and protecting liver, raising immunity, there is assosting effect, accomplish effective, directly improve, be modern
One of flavoring agent of ideal of life.Antiinflammatory that bamboo salt originally has, sterilize, permeate, except disliking tissue regeneration promoting, removing toxic substances, toxin expelling, clean blood
Etc. effect, and Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant extract anti-inflammation, the effect of removing the necrotic tissue and promoting granulation, this allows for Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt and is improving looks, subtracting
Fertile aspect has beyond thought effect.Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt prepared by the inventive method can be as nutrient table salt, it is also possible to be used for
Food processing field, is used for preparing food, includes but not limited to beverage, meat products, such as intestinal, bacon, canned food etc., cake,
Such as cookies etc., staple food, such as bread, steamed bread, noodles etc..Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt prepared by the inventive method can be also used for U.S.
Appearance field, is used for preparing cosmetics and skincare product, includes but not limited to toothpaste, facial film, soap, bath salt, foot bath product etc..
Magnesium salt and the calcium salt that food can add can be added in the preparation process of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt of the present invention.As required, it is also possible to
Add selenium, zinc and/or iodine.For high-melting-point magnesium salt and calcium salt, together can calcine with edible salt and bamboo, such as magnesium chloride,
Calcium chloride, calcium sulfate etc., then carry out dihydromyricetin or the total flavones from Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant extract is coated technique.For low
Fusing point magnesium salt and calcium salt, can be with Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) vegetable active composition dihydromyricetin or (excellent from the total flavones of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant extract
Select dried powder) together add heating, such as magnesium hydroxide etc..When middle food described herein can add magnesium salt, calcium salt, institute
State high-melting-point to refer to higher than 500 DEG C；Described low melting point refers to less than 500 DEG C.Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) vegetable active composition dihydromyricetin or from Serpentis
The total flavones parcel of mattae extract is after bamboo salt step completes, can by physical mixing processes add selenium, zinc, iodine and/or
The nutrients such as activated calcium.Activated calcium includes but not limited to calcium gluconate, calcium hydrogen phosphate, calcium lactate etc..
In one embodiment of the invention, it is provided that the preparation method of a kind of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt, it is characterised by including following step
Rapid:
(1) followed the example of by water and/or alcohol extraction, extract total flavones from ampelopsis；
(2) Ampelosis general flavone obtained from (1) by chromatography extracts dihydromyricetin；
(3) by bamboo high-temperature calcination together with edible salt；
(4) above-mentioned calcined product is cooled down, isolate and become the bamboo salt that crystal is block, pulverize, the dihydro obtained with step (2)
The total flavones mixing of ampelopsin or step (1)；
(5) mixture that step (4) is obtained agitating heating 5-15 minute at a temperature of 245 DEG C ± 10 DEG C.
In another specific embodiments of the present invention, it is provided that the preparation method of a kind of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt added with calcium and magnesium, it is characterised by
Comprise the following steps:
(1) followed the example of by water and/or alcohol extraction, extract total flavones from ampelopsis；
(2) Ampelosis general flavone obtained from (1) by chromatography extracts dihydromyricetin；
(3) bamboo, edible salt, food can be added the high-temperature calcination together with calcium salt of high-melting-point magnesium salt；
(4) above-mentioned calcined product is cooled down, isolate and become the bamboo salt mixture that crystal is block, pulverize, obtain with step (2)
Dihydromyricetin or step (1) total flavones mixing；
(5) mixture that step (4) is obtained agitating heating 5-15 minute at a temperature of 245 DEG C ± 10 DEG C.
In another specific embodiments of the present invention, it is provided that the preparation method of a kind of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt added with calcium and magnesium, it is characterised by
Comprise the following steps:
(1) followed the example of by water and/or alcohol extraction, extract total flavones from ampelopsis；
(2) Ampelosis general flavone obtained from (1) by chromatography extracts dihydromyricetin；
(3) by bamboo high-temperature calcination together with edible salt；
(4) above-mentioned calcined product is cooled down, isolate and become the bamboo salt that crystal is block, pulverize, add food and can add low melting point magnesium
Salt and calcium salt, the total flavones of the dihydromyricetin obtained with step (2) or step (1) mixes；
(5) mixture that step (4) is obtained agitating heating 5-15 minute at a temperature of 245 DEG C ± 10 DEG C.
In embodiments of the invention, the growth bamboo of more than five year is preferably used.Bamboo can be cut into bamboo section, edible salt is filled
Enter in bamboo section, carry out high-temperature calcination with mud sealing, preferably seal with yellow mud；Or bamboo can be pulverized, by bamboo powder
High-temperature calcination together with edible salt, standby after preferably bamboo is ground into the bamboo powder that particle diameter is 50 mesh～100 mesh.Edible salt with
Appropriate Colophonium and/or Ramulus Pini high-temperature calcination together can be added during bamboo high-temperature calcination.Sal and the temperature of bamboo together high-temperature calcination
Degree is preferably at 500～1000 DEG C, and calcination time is preferably 2～10 hours, and as required, calcining step can repeat 3-8 time.
Edible salt is selected from, but not limited to, sea salt, lake salt, well salt, rock salt etc..
Edible salt is preferably 90-50 with the weight ratio of bamboo: 10-50.Colophonium and/or Ramulus Pini are appropriate.The weight of Colophonium preferably food
0-10% by salt weight.The weight of Ramulus Pini is preferably the 0-100% of bamboo weight.Magnesium salt that food can add and calcium salt
Gross weight be preferably the 0-50% of edible salt weight, in magnesium salt and calcium salt admixture, magnesium salt and calcium salt can be to appoint as required
What weight ratio.Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) vegetable active composition dihydromyricetin or the weight from the total flavones of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant extract are preferably warp
Bamboo salt or the 2-80% of bamboo salt mixture weight, more preferably 2-60% after calcining.Preferably, Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) vegetable active composition two
Hydrogen ampelopsin or heat, after cooling together with bamboo salt or bamboo salt mixture after calcining from the total flavones of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant extract
In final Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt product, the weight of edible salt equals to or less than 40%.The total flavones of the Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant extract added is excellent
Choosing is the powder of drying.At mixing Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) vegetable active composition dihydromyricetin or the total flavones from Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant extract
Bamboo salt after calcining or bamboo salt mixture being ground into salt fines, it is 100 mesh～the salt fines of 200 mesh that preferred powder is broken into particle diameter before.
In embodiments of the invention, it is possible to use arbitrarily ampelopsis.Ampelopsis grossedentata is preferably used
[Ampelopsis grossedentata (Hand.-Mazz.) W.T.Wang], unrooted
[Ampelopsis cantoniensis (HooK.etArm) Planch], ampelopsis cantoniensis, leaf jade Fructus Vitis viniferae, Cayratia japonica (Thunb.) Gagnep., northeast Serpentis
Fructus Vitis viniferae, Vitis Amurensis etc. extract Ampelosis general flavone.Extract according to a conventional method, decocted by solvent (water and/or organic solvent)
Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant, decocts one or many, and decoction liquor, through filtering, concentrate, cooling down, obtains extractum, is dried, obtains Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) total
Flavone powder.Gained extractum can also be filtered with after hot water dissolving, supersound extraction, merging filtrate, concentrate and steam solvent,
To refined Ampelosis general flavone.
In embodiments of the invention, Ampelosis general flavone extracts process can repeat steaming and decocting step 2-3 time as required, merges filter
Liquid, concentration and evaporation solvent, by residue vacuum or be spray-dried standby, the temperature of spray drying is preferably 100～120 DEG C, system
Obtain xeraphium.The weight adding water and/or organic solvent is preferably 1-10 times of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant weight, heats digestion time
Preferably 1-5 hour.
In embodiments of the invention, decoct Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant solvent for use and be selected from, but not limited to, water, alcohols, ketone, ethers and strong
Polar organic solvent.Preferably low-level chain triacontanol, low-grade fatty acid ester, there is the ketone of 3-12 carbon atom, there is 3-12
The ether of carbon atom and/or water.More preferably methanol, ethanol, propanol, isopropanol, n-butyl alcohol, isobutanol, sec-butyl alcohol, tertiary fourth
Alcohol, ethyl acetate, methyl acetate, acetone, methyl ethyl ketone, ether, methyl ethyl ether, methyl tertiary butyl ether(MTBE), dichloromethane
Alkane, chloroform, carbon tetrachloride, dimethyl sulfoxide, DMF and/or water etc..
In embodiments of the invention, the chromatographic isolation filler used from Ampelosis general flavone extraction dihydromyricetin includes but does not limits
In polyamide, polyacrylamide, macroporous adsorbent resin, cation exchange resin, anion exchange resin etc..Chromatographic isolation institute
The eluant used includes but not limited to aqueous lower alcoholic solutions, lower ketones aqueous solution, rudimentary ether aqueous solution, lower member ester aqueous solution,
Wherein organic solvent be preferably selected from methanol, ethanol, normal propyl alcohol, isopropanol, acetone, ethyl acetate, Ethyl formate or propyl ester,
Methyl acetate etc..It can be gradient elution.
Detailed description of the invention
Embodiment 1 prepares total flavones from Ampelopsis grossedentata
Take Ampelopsis grossedentata and be dried stem and leaf 2 kilograms, add 2000 milliliter of 95% ethanol, reflux, extract, 2 hours, be repeated twice.Close
And filtrate, it is evaporated to dryness, obtains extractum, wherein rich in Ampelopsis grossedentata total flavone.Extractum is spray-dried, obtains Ampelopsis grossedentata
Total flavones powder.
Embodiment 2 prepares total flavones from Ampelopsis grossedentata
Take Ampelopsis grossedentata and be dried stem and leaf 5 kilograms, add 5000 milliliters of water, heated and boiled 5 hours, be filtrated to get filtrate.To residual
Thing adds 5000 milliliters of water, heated and boiled 5 hours again, filters.In residue, again add 2000 milliliters of water, add
Heat is boiled 3 hours, filters.Merging filtrate, is evaporated to dryness, and obtains extractum, wherein rich in Ampelopsis grossedentata total flavone.By extractum
It is spray-dried, obtains Ampelopsis grossedentata total flavone powder.
Embodiment 3 prepares total flavones from Northeastern Caulis seu folium ampelopsis brevipedunculatae
Take Northeastern Caulis seu folium ampelopsis brevipedunculatae and be dried stem and leaf 3 kilograms, clean, dry, add 1.5 liters of ethyl acetate, decoct 1 hour, filter, to
Residue adds 1 liter of ethyl acetate, then steaming and decocting 1 hour, filters, merging filtrate, is evaporated to dryness, obtains extractum, Qi Zhongfu
Containing Northeastern Caulis seu folium ampelopsis brevipedunculatae total flavones.Extractum is spray-dried, obtains Northeastern Caulis seu folium ampelopsis brevipedunculatae total flavones powder.
The preparation of embodiment 4 dihydromyricetin
600 grams of Ampelosis general flavone extractum embodiment 1 (or embodiment 2 or 3) obtained, with 2 liters of 90 DEG C of hot water dissolvings, filter off black
Insoluble matter, filtrate separates (30-66 mesh, specification 100X1050mm) with polyamide column.First wash with water, then by 30% acetic acid second
Ester eluting, thin layer chromatography is monitored, is obtained crude product, boil off ethyl acetate, filtered while hot, only put, and precipitates, obtains white thread two
Hydrogen ampelopsin crystal.Produce filter 3%.Fusing point 245 DEG C.
The preparation of embodiment 5 Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt
Weighing 5 kilograms of sea salt, load in the ring about length 2 chi, described in each ring, volume of mixture accounts for the 60 of ring volume
About-70%, block two ends with yellow mud, be placed in high temperature-resistant vessel together with 500 grams of Colophonium, put into high temperature furnace calcining, forge
Burn temperature 600 degrees centigrade, calcination time about 4 hours, be warming up to 700 degrees Celsius, calcine 2 hours.It is warming up to 800
Degree Celsius, calcine 2 hours.It is warming up to 1000 degrees Celsius, calcines 1 hour.Then high temperature furnace is allowed to naturally cool to room temperature.From
Ring takes out and has changed into the bamboo salt that crystal is block, be ground into about 200 mesh, add the dihydromyricetin that embodiment 4 obtains
1 kilogram, mixing, in converter at a temperature of 245 DEG C ± 10 DEG C agitating heating 10 minutes.Cooling causes room temperature, is enclosed with
The Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt of dihydromyricetin.
The preparation of embodiment 6 Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt
Weighing 4 kilograms of sea salt, load in the ring about length 2 chi, described in each ring, volume of mixture accounts for the 60 of ring volume
About-70%, block two ends with yellow mud, be placed in high temperature-resistant vessel together with 600 grams of Colophonium, put into high temperature furnace calcining, forge
Burn temperature 600 degrees centigrade, calcination time about 4 hours, be warming up to 700 degrees Celsius, calcine 2 hours.It is warming up to 900
Degree Celsius, calcine 2 hours.Then high temperature furnace is allowed to naturally cool to room temperature.Take out from ring and have changed into the bamboo that crystal is block
Salt, is ground into about 100 mesh.2000 grams of Ampelosis general flavone extractum sprayings that embodiment 1 (or embodiment 2 or 3) is obtained
It is dried, obtains Ampelosis general flavone powder.Bamboo salt powder is mixed with Ampelosis general flavone powder, at 245 DEG C ± 10 DEG C in converter
At a temperature of agitating heating 10 minutes.Cooling causes room temperature, obtains the Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt of the Ampelosis general flavone being enclosed with.
The preparation of embodiment 7 Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt
3 kilograms of bamboo cutting machines are pulverized.Weigh 5 kilograms of sea salt, Colophonium 400 grams, put into together in ball mill and mix.By upper
State mixture and put into high temperature converter calcining, calcine 2 hours at about 700 DEG C, be warming up to 800 DEG C, calcine 1 hour, heat up
To 900 DEG C, calcine 1 hour.Then high temperature furnace is allowed to naturally cool to room temperature.The impurity after bamboo bits calcining is removed with wind selection method,
Being pulverized by salt block is 150 mesh.1000 grams of Ampelosis general flavone extractum spray dried that embodiment 1 (or embodiment 2 or 3) is obtained
Dry, obtain Ampelosis general flavone powder.Bamboo salt powder is mixed with Ampelosis general flavone powder, at 245 DEG C ± 10 DEG C in converter
At a temperature of agitating heating 10 minutes.Cooling causes room temperature, obtains the bamboo salt of the Ampelosis general flavone being enclosed with.
Embodiment 8 is added with the preparation of the Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt of calcium and magnesium
Weigh 3 kilograms of sea salt, 1 kilogram of magnesium chloride, 2 kilograms of calcium chloride, mix in ball mill, load the bamboo about length 2 chi
In joint, described in each ring, volume of mixture accounts for about the 50-60% of ring volume, blocks two ends with yellow mud, puts into high temperature
Stove is calcined, calcining heat 600 degrees centigrade, and calcination time about 4 hours is warming up to 700 degrees Celsius, calcines 4 hours.
Then high temperature furnace is allowed to naturally cool to room temperature.Take out from ring and have changed into the calcium and magnesium bamboo salt mixture that crystal is block, be ground into
About 150 mesh, adding the dihydromyricetin 1 kilogram that embodiment 4 obtains, mixing, in converter at a temperature of 245 DEG C ± 10 DEG C
Agitating heating 10 minutes.Cooling causes room temperature, obtains being enclosed with the calcium and magnesium Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt of dihydromyricetin.
Embodiment 9 is added with the preparation of the Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt of calcium and magnesium
2 kilograms of bamboos, 2 kilograms of Ramulus Pini cutting machines are pulverized.Weigh 5 kilograms of sea salt, put into together in ball mill and mix.By upper
State mixture and put into high temperature converter calcining, calcine 2 hours at about 700 DEG C, be warming up to 850 DEG C, calcine 2 hours, heat up
To 900 DEG C, calcine 1 hour.Then high temperature furnace is allowed to naturally cool to room temperature.After removing bamboo bits Ramulus Pini calcining with wind selection method
Impurity, by salt block pulverize be 100 mesh, add 1 kilogram of magnesium hydroxide, add embodiment 1 (or embodiment 2 or 3) obtain 1500
Gram Ampelosis general flavone extractum spray-dried powders, mixing, in converter at a temperature of 245 DEG C ± 10 DEG C agitating heating 10 minutes.
Cooling causes room temperature, adds 500 grams of calcium gluconate, mixing, obtains magnesium calcium Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt.
Claims (10)
1. a preparation method for Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt, is characterised by, by edible salt and bamboo together high-temperature calcination, then reduces temperature,
Isolate crystal bamboo salt, pulverize, add Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) vegetable active composition dihydromyricetin or from total Huang of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant extract
Ketone, stirs Hybrid Heating, cooling at a temperature of 245 DEG C ± 10 DEG C, makes dihydromyricetin or total flavones be wrapped in through calcining
On bamboo salt.
The preparation method of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt the most according to claim 1, is characterised by, adds food in the preparation process of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt
The addible magnesium salt of product and calcium salt, high-melting-point magnesium salt and calcium salt are together calcined with edible salt and bamboo；Or, low melting point magnesium salt and
Calcium salt and Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) vegetable active composition dihydromyricetin or the total flavones from Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) plant extract together add agitating heating.
The preparation method of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt the most according to claim 1, is characterised by comprising the following steps:
(1) followed the example of by water and/or alcohol extraction, extract total flavones from ampelopsis；
(2) Ampelosis general flavone obtained from step (1) by chromatography extracts dihydromyricetin；
(3) by bamboo high-temperature calcination together with edible salt；
(4) above-mentioned calcined product is cooled down, isolate and become the bamboo salt that crystal is block, pulverize, the dihydro obtained with step (2)
The total flavones mixing of ampelopsin or step (1)；
(5) mixture that step (4) is obtained agitating heating 5-15 minute at a temperature of 245 DEG C ± 10 DEG C.
The preparation method of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt the most according to claim 2, is characterised by comprising the following steps:
(1) followed the example of by water and/or alcohol extraction, extract total flavones from ampelopsis；
(2) Ampelosis general flavone obtained from step (1) by chromatography extracts dihydromyricetin；
(3) bamboo, edible salt, food can be added the high-temperature calcination together with calcium salt of high-melting-point magnesium salt；
(4) above-mentioned calcined product is cooled down, isolate and become the bamboo salt mixture that crystal is block, pulverize, obtain with step (2)
Dihydromyricetin or step (1) total flavones mixing；
(5) mixture that step (4) is obtained agitating heating 5-15 minute at a temperature of 245 DEG C ± 10 DEG C.
The preparation method of Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt the most according to claim 2, is characterised by comprising the following steps:
(1) followed the example of by water and/or alcohol extraction, extract total flavones from ampelopsis；
(2) Ampelosis general flavone obtained from step (1) by chromatography extracts dihydromyricetin；
(3) by bamboo high-temperature calcination together with edible salt；
(4) above-mentioned calcined product is cooled down, isolate and become the bamboo salt that crystal is block, pulverize, add food and can add low melting point magnesium
Salt and calcium salt, the total flavones of the dihydromyricetin obtained with step (2) or step (1) mixes；
(5) mixture that step (4) is obtained agitating heating 5-15 minute at a temperature of 245 DEG C ± 10 DEG C.
6. according to the preparation method of the Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt of any one of claim 1-5, it is characterised by, edible salt and bamboo high-temperature calcination
Time can add Colophonium and/or Ramulus Pini high-temperature calcination together.
7. the Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt prepared according to the preparation method of the Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt of any one of claim 1-7.
Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt the most according to claim 8, is characterised by, in described Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt final products, and the weight etc. of edible salt
In or less than 40%.
The Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt the most according to claim 7 purposes in preparing food.
The Caulis seu folium ampelopsis brevipedunculatae (Caulis Ampelopsis Brevipedunculae) bamboo salt the most according to claim 7 purposes in preparing cosmetics and skincare product.
Priority Applications (1)
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| CN201610307242.4A CN105995916A (en) | 2016-05-06 | 2016-05-06 | Making method of ampelopsis sinica bamboo salt |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108685775A (en) * | 2018-07-04 | 2018-10-23 | 徐姣姣 | A kind of plant enzyme facial mask and its preparation method and application |
| CN112654259A (en) * | 2018-07-23 | 2021-04-13 | 杭州尤美特科技有限公司 | Functional plant salt and preparation method and application thereof |
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| CN1288892A (en) * | 1999-09-16 | 2001-03-28 | 宋新荣 | Preparation and application of dihydromyricetrin |
| CN1375289A (en) * | 2001-03-15 | 2002-10-23 | 北京美林亚科技发展有限公司 | Ampelosis general flavone composition with liver protecting function |
| CN101006860A (en) * | 2007-01-27 | 2007-08-01 | 雷昭宁 | Smoke-roasting bamboo salt and its making method |
| CN104621526A (en) * | 2015-03-09 | 2015-05-20 | 中盐国本盐业有限公司 | Method for preparing bamboo salt through temperature program |
| CN105326010A (en) * | 2015-10-29 | 2016-02-17 | 天津科技大学 | Preparation method of bamboo salt |
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1288892A (en) * | 1999-09-16 | 2001-03-28 | 宋新荣 | Preparation and application of dihydromyricetrin |
| CN1375289A (en) * | 2001-03-15 | 2002-10-23 | 北京美林亚科技发展有限公司 | Ampelosis general flavone composition with liver protecting function |
| CN101006860A (en) * | 2007-01-27 | 2007-08-01 | 雷昭宁 | Smoke-roasting bamboo salt and its making method |
| CN104621526A (en) * | 2015-03-09 | 2015-05-20 | 中盐国本盐业有限公司 | Method for preparing bamboo salt through temperature program |
| CN105326010A (en) * | 2015-10-29 | 2016-02-17 | 天津科技大学 | Preparation method of bamboo salt |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108685775A (en) * | 2018-07-04 | 2018-10-23 | 徐姣姣 | A kind of plant enzyme facial mask and its preparation method and application |
| CN112654259A (en) * | 2018-07-23 | 2021-04-13 | 杭州尤美特科技有限公司 | Functional plant salt and preparation method and application thereof |
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Application publication date: 20161012 |