CN105970681B - A kind of environment-friendly type brown digit printing ink and preparation method thereof - Google Patents
A kind of environment-friendly type brown digit printing ink and preparation method thereof Download PDFInfo
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- CN105970681B CN105970681B CN201610452351.5A CN201610452351A CN105970681B CN 105970681 B CN105970681 B CN 105970681B CN 201610452351 A CN201610452351 A CN 201610452351A CN 105970681 B CN105970681 B CN 105970681B
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- 238000007639 printing Methods 0.000 title claims abstract description 53
- 238000002360 preparation method Methods 0.000 title claims description 13
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 19
- 244000268590 Euryale ferox Species 0.000 claims abstract description 19
- 235000006487 Euryale ferox Nutrition 0.000 claims abstract description 18
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 18
- 229910021389 graphene Inorganic materials 0.000 claims abstract description 17
- 230000000855 fungicidal effect Effects 0.000 claims abstract description 16
- 239000000417 fungicide Substances 0.000 claims abstract description 16
- 235000013311 vegetables Nutrition 0.000 claims abstract description 16
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical compound [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 19
- 239000008367 deionised water Substances 0.000 claims description 17
- 229910021641 deionized water Inorganic materials 0.000 claims description 17
- 239000002270 dispersing agent Substances 0.000 claims description 14
- 239000003002 pH adjusting agent Substances 0.000 claims description 14
- 239000004094 surface-active agent Substances 0.000 claims description 14
- 239000004034 viscosity adjusting agent Substances 0.000 claims description 14
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical group OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 12
- 239000000706 filtrate Substances 0.000 claims description 12
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical group [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 10
- 238000001914 filtration Methods 0.000 claims description 10
- 238000002137 ultrasound extraction Methods 0.000 claims description 9
- 238000003756 stirring Methods 0.000 claims description 8
- 235000011187 glycerol Nutrition 0.000 claims description 6
- 239000010903 husk Substances 0.000 claims description 6
- 239000004615 ingredient Substances 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- 238000010792 warming Methods 0.000 claims description 6
- 239000000975 dye Substances 0.000 claims description 5
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 5
- 235000015112 vegetable and seed oil Nutrition 0.000 claims description 5
- 239000008158 vegetable oil Substances 0.000 claims description 5
- 238000000605 extraction Methods 0.000 claims description 4
- 239000000843 powder Substances 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims 2
- 235000013411 Alpinia speciosa Nutrition 0.000 claims 1
- 244000060696 Alpinia speciosa Species 0.000 claims 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 239000000284 extract Substances 0.000 claims 1
- 239000010773 plant oil Substances 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 239000004408 titanium dioxide Substances 0.000 claims 1
- 239000004744 fabric Substances 0.000 abstract description 11
- 238000004040 coloring Methods 0.000 abstract description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 4
- 239000003795 chemical substances by application Substances 0.000 abstract description 3
- 238000003912 environmental pollution Methods 0.000 abstract description 3
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 abstract description 2
- 239000004202 carbamide Substances 0.000 abstract description 2
- 230000005802 health problem Effects 0.000 abstract description 2
- 230000019612 pigmentation Effects 0.000 abstract description 2
- 238000005516 engineering process Methods 0.000 description 7
- 238000000034 method Methods 0.000 description 5
- 239000000835 fiber Substances 0.000 description 4
- 238000007641 inkjet printing Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 239000007921 spray Substances 0.000 description 4
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000004043 dyeing Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 239000004753 textile Substances 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 208000030961 allergic reaction Diseases 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 229910052796 boron Inorganic materials 0.000 description 1
- -1 boron alkene Chemical class 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 150000001721 carbon Chemical group 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000005189 flocculation Methods 0.000 description 1
- 230000016615 flocculation Effects 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 238000002203 pretreatment Methods 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000009955 starching Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000012780 transparent material Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/30—Ink jet printing
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
A kind of environment-friendly type brown digit printing ink, using the brown pigmentation extracted from Gorgon fruit shell as vegetable colour, instead of the synthetic dyestuffs being often used in the digit printing ink of the prior art, the problem of environmental pollution and health problem that synthetic dyestuffs are brought are substantially reduced；It uses nano-titanium dioxide instead and makees fungicide, it is more environmentally-friendly；And graphene is added during preparing ink, therefore urea need not be added can also obtain the ideal fabric of color fastness as color fixing agent, saved production cost, enhanced coloring.
Description
Technical field
The present invention relates to digital printing technology field more particularly to a kind of environment-friendly type brown digit printing ink and its preparations
Method.
Background technology
Digital ink-jet printed technology is that inkjet printing is expanded greatly the one of industrial application.Modern computer inkjet printing
When technology is used for printing in textiles, various input mediums such as scanner, digital camera, digital camera etc. can be used, need
The pattern wanted is with digital input computer, after the processing of various mapping software color separation in printing systems, using computer control
Printing ink is directly ejected on various fabrics by the digital inkjet printing machine of system, prints out required various patterns, this
Kind printing technique is referred to as digital inking printing.
In recent years, digital printing technology has obtained rapid development.Compared with Conventional decal, digital printing process cleaning,
Production process is flexible, can remotely be ordered goods, be included in supply chain network, is the direction of the following printing in textiles technology development.
On Vehicles Collected from Market, the dyestuff of used type of dye ink is essentially all synthetic dyestuffs, although synthetic dyestuffs
It is gorgeous with color and luster, good color fastness, can mass production the advantages that, but synthetic dyestuffs are due to complicated, various in style, biological
Degradability is low etc. to cause a large amount of environmental pollutions, while having the defects of carcinogenic, easily to cause allergic reaction.It is increasingly pursued in people
The ink of today of healthy living, exploitation high-performance, high fastness and aqueous environment protection are current digital ink-jet printing ink hair
The main trend of exhibition.
On the other hand, digit printing in a manner of contactless by the accurate spray printing of ink to the surface of fabric, therefore color fastness phase
To relatively low, therefore in the prior art, before carrying out digit printing spray printing to fabric, need to carry out starching pre-treatment to fabric,
The problems such as to help the degree of fixation and color fastness for improving vegetable colour.But the work contaminated on digit printing spray printing can be increased in this way
Sequence.
Chinese invention patent CN103966861A provides a kind of environment-friendly digital printing ink and preparation method thereof, the ink
Water dyes silk, cotton, can reach good coloring, but the invention only provides the ink system of solid color
Preparation Method, and organic bactericide is added in the ink, it is still not environmentally friendly enough.
Invention content
In order to solve the problems in background technology, a kind of environment-friendly type brown digit printing ink of present invention offer and its preparation
Method.
A kind of environment-friendly type brown digit printing ink, includes the ingredient of following weight percent：
Preferably, the viscosity modifier is glycerine.
Preferably, the surfactant is neopelex.
Preferably, the fungicide is nano-titanium dioxide.
Preferably, the pH adjusting agent is sodium carbonate.
Preferably, the dispersant is vegetable oil.
A kind of preparation method of environment-friendly type brown digit printing ink, includes the following steps：
A, Gorgon fruit husk as raw material is crushed to 80 mesh by microphyte pulverizer, after impregnating 1-3h with deionized water, then profit
Brown yellow solution is obtained with ultrasonic extraction, is filtered, filtrate obtains brownish-yellow powder, as Gorgon fruit shell through being concentrated in vacuo dry, crushing
Vegetable colour；
B, vegetable colour, viscosity modifier, surfactant, pH adjusting agent, fungicide are add to deionized water, often
(control system pH value is 6-7) is stirred evenly under temperature, then is warming up to 60-70 DEG C and continues to stir 1h, and is kept the temperature in 60-70 DEG C of curing
2-3h, after being down to room temperature, filtering；
C, graphene and dispersant are added in filtrate, disperse 3-5min under the supersonic frequency of 25-35kHz, obtains ring
Guarantor's type brown digit printing ink.
The two dimensional crystal for only one layer of atomic thickness that graphene is made of carbon atom.2004, Manchester, England
Graphene is isolated in College Physics scholar An Deliegaimu and Constantine's Nuo Woxiao loves, success from graphite, it was demonstrated that
Therefore it can also obtain Nobel Prize in physics in 2010 jointly with individualism, two people.Before the discovery of 2015 year end boron alkene,
Graphene is both most thin material, and most tough material, 200 times more taller than best steel of fracture strength.While it
There are good elasticity, stretch range that can reach the 20% of own dimensions again.It is that current nature is most thin, the highest material of intensity
Material.
Graphene is added in the present invention to have the advantage that：
First, having two-dimensional structure using graphene, in pattern-printing and dyeing, the contact surface of bigger can be provided to vegetable colour
Product, can reach good coloring it is not necessary that color fixing agent is added；
Second is that due to increasing contact area, nano-titanium dioxide can partly penetrate into fabric fibre in pattern-printing and dyeing
Surface and inside increase the antibacterial effect of fabric；
Third, graphene is colourless transparent material, will not have an impact to the color of fabric, be removed when subsequent fabric is handled
Also relatively simple, after high-speed stirred, it is easy flocculation.
The environment-friendly type brown digit printing ink of the present invention, using the brown pigmentation extracted from Gorgon fruit shell as plant
Object dyestuff substantially reduces synthetic dyestuffs and brings instead of the synthetic dyestuffs being often used in the digit printing ink of the prior art
Problem of environmental pollution and health problem；It uses nano-titanium dioxide instead and makees fungicide, it is more environmentally-friendly；And prepare the process of ink
Middle addition graphene, therefore urea need not be added can also obtain the ideal fabric of color fastness as color fixing agent, save production
Cost enhances coloring.
Specific implementation mode
Embodiment 1
A kind of environment-friendly type brown digit printing ink, includes the ingredient of following weight percent：
The viscosity modifier is glycerine；
The surfactant is neopelex；
The fungicide is nano-titanium dioxide；
The pH adjusting agent is sodium carbonate；
The dispersant is vegetable oil；
A kind of preparation method of environment-friendly type brown digit printing ink, includes the following steps：
A, Gorgon fruit husk as raw material is crushed to 80 mesh by microphyte pulverizer, after impregnating 2h with deionized water, Gorgon fruit shell
Weight ratio with deionized water is 1:30；Ultrasonic extraction is recycled to obtain brown yellow solution, the frequency of ultrasonic extraction is
50kHz, Extracting temperature are 70 DEG C, extraction time 25min；Filtering, filtrate obtain pale brown toner through being concentrated in vacuo dry, crushing
End, as Gorgon fruit shell vegetable colour；
B, vegetable colour, viscosity modifier, surfactant, pH adjusting agent, fungicide are add to deionized water, often
(control system pH value is 6-7) is stirred evenly under temperature, then is warming up to 65 DEG C and continues to stir 1h, and is kept the temperature and cured 2.5h in 65 DEG C,
After being down to room temperature, filtering；
C, graphene and dispersant are added in filtrate, disperse 4min under the supersonic frequency of 30kHz, obtain environment-friendly type palm fibre
Chromatic number code printing ink.
Embodiment 2
A kind of environment-friendly type brown digit printing ink, includes the ingredient of following weight percent：
The viscosity modifier is glycerine；
The surfactant is neopelex；
The fungicide is nano-titanium dioxide；
The pH adjusting agent is sodium carbonate；
The dispersant is vegetable oil；
A kind of preparation method of environment-friendly type brown digit printing ink, includes the following steps：
A, Gorgon fruit husk as raw material is crushed to 80 mesh by microphyte pulverizer, after impregnating 3h with deionized water, Gorgon fruit shell
Weight ratio with deionized water is 1:20；Ultrasonic extraction is recycled to obtain brown yellow solution, the frequency of ultrasonic extraction is
40kHz, Extracting temperature are 65 DEG C, extraction time 35min；Filtering, filtrate obtain pale brown toner through being concentrated in vacuo dry, crushing
End, as Gorgon fruit shell vegetable colour；
B, vegetable colour, viscosity modifier, surfactant, pH adjusting agent, fungicide are add to deionized water, often
(control system pH value is 6-7) is stirred evenly under temperature, then is warming up to 60 DEG C and continues to stir 1h, and is kept the temperature and cured 3h, drop in 60 DEG C
To room temperature, filtering；
C, graphene and dispersant are added in filtrate, disperse 3min under the supersonic frequency of 35kHz, obtain environment-friendly type palm fibre
Chromatic number code printing ink.
Embodiment 3
A kind of environment-friendly type brown digit printing ink, includes the ingredient of following weight percent：
The viscosity modifier is glycerine；
The surfactant is neopelex；
The fungicide is nano-titanium dioxide；
The pH adjusting agent is sodium carbonate；
The dispersant is vegetable oil；
A kind of preparation method of environment-friendly type brown digit printing ink, includes the following steps：
A, Gorgon fruit husk as raw material is crushed to 80 mesh by microphyte pulverizer, after impregnating 1h with deionized water, Gorgon fruit shell
Weight ratio with deionized water is 1:40；Ultrasonic extraction is recycled to obtain brown yellow solution, the frequency of ultrasonic extraction is
55kHz, Extracting temperature are 75 DEG C, extraction time 15min；Filtering, filtrate obtain pale brown toner through being concentrated in vacuo dry, crushing
End, as Gorgon fruit shell vegetable colour；
B, vegetable colour, viscosity modifier, surfactant, pH adjusting agent, fungicide are add to deionized water, often
(control system pH value is 6-7) is stirred evenly under temperature, then is warming up to 70 DEG C and continues to stir 1h, and is kept the temperature and cured 2h, drop in 70 DEG C
To room temperature, filtering；
C, graphene and dispersant are added in filtrate, disperse 5min under the supersonic frequency of 25kHz, obtain environment-friendly type palm fibre
Chromatic number code printing ink.
Comparative example 1
By the graphene removal in embodiment 1, other preparation conditions are constant, obtain environment-friendly type brown digit printing ink.
Silk spray printing, test fabric are carried out to the environment-friendly type brown digit printing ink of embodiment 1-3 and comparative example 1
Fastness to soaping, colour fastness to rubbing, fastness to light tested, the results are shown in Table 1.
Table 1：
Test data it is recognised that printing ink made of the present invention, color fastness is high, even across being cleaned multiple times, still
Energy is colour-fast, fades, and keeps original color and vividness.
The foregoing is only a preferred embodiment of the present invention, but scope of protection of the present invention is not limited thereto,
Any one skilled in the art in the technical scope disclosed by the present invention, according to the technique and scheme of the present invention and its
Inventive concept is subject to equivalent substitution or change, should be covered by the protection scope of the present invention.
Claims (8)
1. a kind of environment-friendly type brown digit printing ink, which is characterized in that include the ingredient of following weight percent：
Gorgon fruit shell vegetable colour 5-20%
Viscosity modifier 5-12%
Surfactant 2-5%
PH adjusting agent 0.5-2%
Fungicide 0.2-0.5%
Dispersant 0.2-0.5%
Graphene 0.05-0.08%
Deionized water surplus.
2. environment-friendly type brown digit printing ink according to claim 1, which is characterized in that the viscosity modifier is
Glycerine.
3. environment-friendly type brown digit printing ink according to claim 1, which is characterized in that the surfactant is
Neopelex.
4. environment-friendly type brown digit printing ink according to claim 1, which is characterized in that the fungicide is nanometer
Titanium dioxide.
5. environment-friendly type brown digit printing ink according to claim 1, which is characterized in that the pH adjusting agent is carbon
Sour sodium.
6. environment-friendly type brown digit printing ink according to claim 1, which is characterized in that the dispersant is plant
Oil.
7. environment-friendly type brown digit printing ink according to claim 1, which is characterized in that preparation method, including with
Lower step：
A, Gorgon fruit husk as raw material is crushed to 80 mesh by microphyte pulverizer, after impregnating 1-3h with deionized water, recycled super
Sound extracts to obtain brown yellow solution, filtering, and filtrate obtains brownish-yellow powder, as Gorgon fruit shell plant through being concentrated in vacuo dry, crushing
Dyestuff；
B, vegetable colour, viscosity modifier, surfactant, pH adjusting agent, fungicide are add to deionized water, under room temperature
It is 6-7 to stir evenly and adjust pH value, then is warming up to 60-70 DEG C and continues to stir 1h, and keeps the temperature and cure 2-3h, drop in 60-70 DEG C
To room temperature, filtering；
C, graphene and dispersant are added in filtrate, disperse 3-5min under the supersonic frequency of 25-35kHz, obtains environment-friendly type
Brown digit printing ink.
8. environment-friendly type brown digit printing ink according to claim 7, which is characterized in that preparation method, including with
Lower step：
A, Gorgon fruit husk as raw material is crushed to 80 mesh by microphyte pulverizer, with deionized water impregnate 2h after, Gorgon fruit shell with go
The weight ratio of ionized water is 1:30；Ultrasonic extraction is recycled to obtain brown yellow solution, the frequency of ultrasonic extraction is 50kHz, is carried
It is 70 DEG C to take temperature, extraction time 25min；Filtering, filtrate obtain brownish-yellow powder, as Gorgon euryale through being concentrated in vacuo dry, crushing
Real shell vegetable colour；
B, vegetable colour, viscosity modifier, surfactant, pH adjusting agent, fungicide are add to deionized water, under room temperature
It is 6-7 to stir evenly and adjust pH value, then is warming up to 65 DEG C and continues to stir 1h, and keeps the temperature and cure 2.5h in 65 DEG C, is down to room temperature
Afterwards, it filters；
C, graphene and dispersant are added in filtrate, disperse 4min under the supersonic frequency of 30kHz, obtain environment-friendly type brown number
Code printing ink；
The environment-friendly type brown digit printing ink, includes the ingredient of following weight percent：
Vegetable colour 18%
Viscosity modifier 10%
Surfactant 3.5%
PH adjusting agent 1%
Fungicide 0.35%
Dispersant 0.4%
Graphene 0.06%
Deionized water surplus；
The viscosity modifier is glycerine；
The surfactant is neopelex；
The fungicide is nano-titanium dioxide；
The pH adjusting agent is sodium carbonate；
The dispersant is vegetable oil.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610452351.5A CN105970681B (en) | 2016-06-20 | 2016-06-20 | A kind of environment-friendly type brown digit printing ink and preparation method thereof |
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| CN201610452351.5A CN105970681B (en) | 2016-06-20 | 2016-06-20 | A kind of environment-friendly type brown digit printing ink and preparation method thereof |
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| CN105970681B true CN105970681B (en) | 2018-08-17 |
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| CN106835672A (en) * | 2017-01-11 | 2017-06-13 | 郑宋滨 | Graphene printed textile and preparation method |
| CN107740288A (en) * | 2017-10-19 | 2018-02-27 | 无锡嘉加科技有限公司 | A kind of wool anhydrous printing ink and preparation method thereof |
| CN107740289A (en) * | 2017-10-19 | 2018-02-27 | 无锡嘉加科技有限公司 | A kind of anhydrous printing with reactive dye ink and preparation method thereof |
| CN107881807A (en) * | 2017-10-19 | 2018-04-06 | 无锡嘉加科技有限公司 | A kind of environmentally friendly anhydrous printing ink and preparation method thereof |
| CN108797152A (en) * | 2018-06-13 | 2018-11-13 | 南通强生石墨烯科技有限公司 | A kind of graphene concentrator and preparation method thereof |
| CN112267310A (en) * | 2020-10-26 | 2021-01-26 | 山东众和新材料科技有限公司 | Cinnamomum camphora pulp pigment printing paste and printing method thereof on pure cotton fabric |
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| CN102501673A (en) * | 2011-11-08 | 2012-06-20 | 哈尔滨工业大学 | Method for preparing nano composite absorption material for print |
| CN103447013A (en) * | 2013-09-23 | 2013-12-18 | 青岛大学 | Method for preparing graphene/chitosan adsorbent and application method thereof |
| CN103694794A (en) * | 2013-12-26 | 2014-04-02 | 济南蓝贝思特科技有限公司 | Water whiteboard ink and preparation method thereof |
| CN103952922A (en) * | 2014-05-19 | 2014-07-30 | 常州美胜生物材料有限公司 | Plant dye digital printing ink and preparation method thereof |
| CN103966861A (en) * | 2014-05-19 | 2014-08-06 | 常州美胜生物材料有限公司 | Environment-friendly digital printing ink and preparation method thereof |
| CN105315773A (en) * | 2015-11-04 | 2016-02-10 | 桐城市人和包装有限公司 | Water-based printing ink and preparation method thereof |
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