CN1844275A - Digital-printing ink-jet ink made of nano pigment and its making process - Google Patents
Digital-printing ink-jet ink made of nano pigment and its making process Download PDFInfo
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- CN1844275A CN1844275A CN 200610026595 CN200610026595A CN1844275A CN 1844275 A CN1844275 A CN 1844275A CN 200610026595 CN200610026595 CN 200610026595 CN 200610026595 A CN200610026595 A CN 200610026595A CN 1844275 A CN1844275 A CN 1844275A
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- printing ink
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- 239000000049 pigment Substances 0.000 title claims abstract description 41
- 238000000034 method Methods 0.000 title claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 16
- 239000008367 deionised water Substances 0.000 claims abstract description 14
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 14
- 238000004519 manufacturing process Methods 0.000 claims abstract description 12
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 10
- 239000011347 resin Substances 0.000 claims abstract description 8
- 229920005989 resin Polymers 0.000 claims abstract description 8
- 239000000976 ink Substances 0.000 claims description 37
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 18
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 12
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 6
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 6
- 239000013543 active substance Substances 0.000 claims description 6
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 6
- HNJBEVLQSNELDL-UHFFFAOYSA-N pyrrolidin-2-one Chemical compound O=C1CCCN1 HNJBEVLQSNELDL-UHFFFAOYSA-N 0.000 claims description 6
- 229960004418 trolamine Drugs 0.000 claims description 6
- 239000000080 wetting agent Substances 0.000 claims description 6
- 239000012467 final product Substances 0.000 claims description 5
- 238000005374 membrane filtration Methods 0.000 claims description 5
- 229920002803 thermoplastic polyurethane Polymers 0.000 claims description 5
- RFQOPUYDLCMQCE-UHFFFAOYSA-N 1-(2-hydroxyethyl)-5-nitropyrrole-2-carboxamide Chemical compound NC(=O)C1=CC=C([N+]([O-])=O)N1CCO RFQOPUYDLCMQCE-UHFFFAOYSA-N 0.000 claims description 4
- 239000004925 Acrylic resin Substances 0.000 claims description 4
- 229920000178 Acrylic resin Polymers 0.000 claims description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 4
- ZBCBWPMODOFKDW-UHFFFAOYSA-N diethanolamine Chemical compound OCCNCCO ZBCBWPMODOFKDW-UHFFFAOYSA-N 0.000 claims description 4
- HZAXFHJVJLSVMW-UHFFFAOYSA-N 2-Aminoethan-1-ol Chemical compound NCCO HZAXFHJVJLSVMW-UHFFFAOYSA-N 0.000 claims description 2
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 2
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 claims description 2
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 2
- 239000004372 Polyvinyl alcohol Substances 0.000 claims description 2
- 229910052804 chromium Inorganic materials 0.000 claims description 2
- 239000011651 chromium Substances 0.000 claims description 2
- 229910052802 copper Inorganic materials 0.000 claims description 2
- 239000010949 copper Substances 0.000 claims description 2
- 229910052742 iron Inorganic materials 0.000 claims description 2
- 229910021645 metal ion Inorganic materials 0.000 claims description 2
- 229910017604 nitric acid Inorganic materials 0.000 claims description 2
- 229920002451 polyvinyl alcohol Polymers 0.000 claims description 2
- 239000006185 dispersion Substances 0.000 abstract description 4
- 238000003756 stirring Methods 0.000 abstract description 4
- 239000011259 mixed solution Substances 0.000 abstract 6
- 239000012190 activator Substances 0.000 abstract 2
- 239000003899 bactericide agent Substances 0.000 abstract 2
- 239000003906 humectant Substances 0.000 abstract 2
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000000227 grinding Methods 0.000 abstract 1
- 239000012528 membrane Substances 0.000 abstract 1
- 239000007921 spray Substances 0.000 description 6
- 239000004753 textile Substances 0.000 description 6
- 239000012752 auxiliary agent Substances 0.000 description 5
- 239000000975 dye Substances 0.000 description 3
- 239000004744 fabric Substances 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- -1 D-7 Chemical compound 0.000 description 2
- 238000004040 coloring Methods 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 229920000742 Cotton Polymers 0.000 description 1
- 101100074998 Neurospora crassa (strain ATCC 24698 / 74-OR23-1A / CBS 708.71 / DSM 1257 / FGSC 987) nmp-2 gene Proteins 0.000 description 1
- 239000000980 acid dye Substances 0.000 description 1
- 150000004982 aromatic amines Chemical class 0.000 description 1
- 238000003556 assay Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000000795 conjunctiva Anatomy 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000005562 fading Methods 0.000 description 1
- 238000005189 flocculation Methods 0.000 description 1
- 230000016615 flocculation Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000002093 peripheral effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 239000000985 reactive dye Substances 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention relates to a nanopigment digital printing ink-jet ink, which consists of the following components: nanopigment dispersion color paste; humectant; descaling agent; bactericidal agent; control agent for PH value; surface activator; resin and deionized water. The manufacturing technique includes the following steps: (A) predispersing and grinding the pigment according to the fineness requirement to less than 200 nanometers of D90 to prepare nanopigment dispersion color paste; (B) mixing humectant, descaling agent; bactericidal agent, control agent for PH value, surface activator, resin and deionized water at the normal temperature and sufficiently stirring to obtain the mixed solution; (C) adding the nanopigment dispersion color paste into the mixed solution obtained by step (B) and sufficiently stirring to obtain mixed solution; (D) stewing and curing the mixed solution obtained by step (C) to obtain the aged mixed solution; (E) filtering the aged mixed solution obtained by step (D) by filter membrane to obtain the end product.
Description
Technical field
The present invention relates to a kind of digital ink-jet ink and production method thereof, especially a kind of digital-printing ink-jet ink made of nano pigment and production technique thereof.
Background technology
Textiles digital ink-jet printed in textile industry by more and more widely application.This method can be saved the printing stencil operation, shortens Production Flow Chart; Can realize the direct spray printing of digital pattern, novel convenient; Can reduce amount of pigment, not discarded dyestuff produces, and shortens the aftertreatment flow process simultaneously, becomes a kind of low cost, oligosaprobic printing in textiles production method.
The digital ink-jet printed main cotton class of reactive dye ink spray printing, acid dye ink spray printing silk and woolen cloth, the dispersed dye ink spray printing chemical ﹠ blended fabric of being suitable for.Yet the blending often of existing lining, independent a kind of ink can't be finished spray printing, therefore just is necessary to develop a kind of ink that is applicable to all linings.In addition, ink for ink-jet print is applied in the industrial textile, the granularity of ink, stability, colour fastness, crock fastness, washing fastness and hydrolysis fastness all need to satisfy higher requirement.
(ink for ink-jet print that D90 (200nm) dispersible pigment dispersion is made can pass through nozzle ejection safely, avoids big particle to cause spray nozzle clogging to select nano level for use.Pigment has stronger fast light ability of fading and waterproof ability with respect to dyestuff.In addition, need to add certain auxiliary agent in nano pigment ink, this auxiliary agent can prevent that pigment is rotten, solids precipitation, form macrobead, and by auxiliary agent, can form flexible conjunctiva on different fabrics, makes ink be applicable to all linings.
In the existing product, as No. the 5603756th, United States Patent (USP) and No. 6015454 disclosed two kinds of textile inkjet inks, all because of there not being well to solve the problem that ink adds auxiliary agent, thereby cause colouring dynamics and colour fastness not good, or can't preserve for a long time and easy deficiency such as infringement shower nozzle.
Summary of the invention
The objective of the invention is to exist colouring dynamics, fastness not good at existing digital ink-jet ink, and deficiency such as the perishable easy infringement shower nozzle of ink, a kind of novel nano pigment digit printing ink-jet writing ink and the production technique thereof of auxiliary agent to address the above problem of adding is provided.
Technical scheme of the present invention is: a kind of digital-printing ink-jet ink made of nano pigment, and hundred parts than composed of the following components by weight:
Nano-level pigment disperses mill base 1-20%;
Wetting Agent for Printing Inks 10-15%;
Scale remover 1-5%;
Sterilant 0.2-1%;
PH value control agent 1-5%;
Tensio-active agent 0.5-5%;
Resin 5-10%;
Its surplus of deionized water.
Preferably, described wetting Agent for Printing Inks is at least a among ethylene glycol, Diethylene Glycol, glycerol, polyvinyl alcohol, the PEG.
Preferably, described scale remover is at least a among Virahol, 2-Pyrrolidone, the NMP.
Preferably, described sterilant is D-7.
Preferably, described pH value control agent is at least a in rare nitric acid, Monoethanolamine MEA BASF, diethanolamine, trolamine, the oxyammonia.
Preferably, described tensio-active agent is at least a among NP-10, the NP-15.
Preferably, described deionized water is for removing copper, iron, chromium, manganese metal ion and Cl
-, SO
4 2-After water.
Preferably, described resin is at least a in urethane resin, the acrylic resin.
The production technique of above-mentioned digital-printing ink-jet ink made of nano pigment comprises the following steps:
(A) pigment is pre-dispersed according to fineness requirement, be ground to D90＜200 nanometers, make nano-level pigment and disperse mill base;
(B) wetting Agent for Printing Inks, scale remover, sterilant, pH value control agent, tensio-active agent, deionized water, resin are mixed at normal temperatures, fully stirred 0.5-1 hour, get mixing solutions;
(C) nano-level pigment is disperseed mill base add in the step (B) in the prepared mixing solutions, and fully stirred 20-30 minute, mixing solutions;
(D) mixing solutions with gained in the step (C) leaves standstill slaking in 24-48 hour under temperature 50-70 ℃, gets the slaking mixing solutions;
(E) with the slaking mixing solutions of gained in the step (D) successively through 1 micron, 0.5 micron, 0.22 micron membrane filtration, obtain final product.
Beneficial effect of the present invention is: the textiles digit printing reactive dyestuffs ink for ink-jet print that provides among the present invention may be used on minute-pressure electricity, heat foamable printer; Granularity is below 0.22 micron, and for the contained salt of 50-100/one of the nozzle diameter impurity that grades is few, specific conductivity is low, is difficult for the infringement shower nozzle; And can keep certain pH value, and be difficult for hydrolysis and flocculation take place, can store for a long time; Its degree of fixation, washing fastness, light fastness all can reach higher technical requirements; Do not contain azoic dyestuffs such as aromatic amine,, meet national standard-GB18401 human body safety.
Embodiment
Embodiment 1:
Comprise following component by weight percentage, nano-level pigment disperses mill base (black) 18%, ethylene glycol 10%, and NMP 2%, D-70.5%, trolamine 1.5%, NP-10 1%, 5%, and all the other are deionized water.
During production, may further comprise the steps:
(A) pigment (black) is pre-dispersed according to fineness requirement, be ground to D90＜200 nanometers, make nano-level pigment and disperse mill base (black);
(B) ethylene glycol, NMP, D-7, trolamine, NP-10, urethane resin, deionized water are mixed at normal temperatures, fully stirred 0.5 hour, get mixing solutions;
(C) nano-level pigment is disperseed mill base (black) add in the step (B) in the prepared mixing solutions, and fully stirred 20 minutes, mixing solutions;
(D) mixing solutions of gained in the step (C) is left standstill slaking in 30 hours under 60 ℃ of temperature, the slaking mixing solutions;
(E) with the slaking mixing solutions of gained in the step (D) successively through 1 micron, 0.5 micron, 0.22 micron membrane filtration, obtain final product.
Embodiment 2:
Comprise following component by weight percentage, nano-level pigment disperses mill base (magenta) 7.5%, glycerol 10%, and 2-Pyrrolidone 5%, Virahol 5%, D-7 0.5%, trolamine 1%, NP-15 1.5%, acrylic resin 7%, all the other are deionized water.
During production, may further comprise the steps:
(A) pigment (magenta) is pre-dispersed according to fineness requirement, be ground to D90＜200 nanometers, make nano-level pigment and disperse mill base (magenta);
(B) with glycerol, 2-Pyrrolidone, Virahol, D-7, trolamine, NP-15, acrylic resin, deionized water mixes at normal temperatures, fully stirs 1 hour, gets mixing solutions;
(C) nano-level pigment is disperseed mill base (magenta) add in the step (B) in the prepared mixing solutions, and fully stirred 20 minutes, mixing solutions;
(D) mixing solutions of gained in the step (C) is left standstill slaking in 30 hours under 50 ℃ of temperature, the slaking mixing solutions;
(E) with the slaking mixing solutions of gained in the step (D) successively through 1 micron, 0.5 micron, 0.22 micron membrane filtration, obtain final product.
Embodiment 3:
Comprise following component by weight percentage, nano-level pigment disperses mill base (blueness) 12%, glycerol 15%, and Virahol 5%, 2-Pyrrolidone 1%, diethanolamine 2%, D-7 0.7%, and NP-15 2%, urethane resin 9%, all the other are deionized water.
During production, may further comprise the steps:
(A) pigment (blueness) is pre-dispersed according to fineness requirement, be ground to D90＜200 nanometers, make nano-level pigment and disperse mill base (blueness);
(B) with glycerol, Virahol, 2-Pyrrolidone, diethanolamine, D-7, NP-15, urethane resin, deionized water mixes at normal temperatures, fully stirs 0.5 hour, gets mixing solutions;
(C) nano-level pigment is disperseed mill base (blueness) add in the step (B) in the prepared mixing solutions, and fully stirred 20 minutes, mixing solutions;
(D) mixing solutions of gained in the step (C) is left standstill slaking in 24 hours under 65 ℃ of temperature, the slaking mixing solutions;
(E) with the slaking mixing solutions of gained in the step (D) successively through 1 micron, 0.5 micron, 0.22 micron membrane filtration, obtain final product.
Each component among the above embodiment all can be bought acquisition by market.
The ink that embodiment 1-3 makes, washing fastness can reach the 4-5 level, 4 grades of light fastnesss, through the check of national computer peripheral quality supervision and test center, its every index is as shown in the table:
| Interventions Requested | Technical qualification | Assay | |||
| 1. light fastness | Answer≤40% according to preceding, back 1.5 hours colour density rate of fall-off of photograph | C | M | Y | K |
| 0.00％ | 0.00％ | 0.00％ | 0.00％ | ||
| Qualified | |||||
| 2. trace density | Should meet C 〉=1.2, M 〉=1.1, Y 〉=0.8, K 〉=1.3 | C | M | Y | K | ||
| 1.32 | 1.22 | 1.14 | 1.33 | ||||
| Qualified | |||||||
| 3. color uniformity | The relative value of pull each point colour density difference should be not less than 90% | C | M | Y | K | ||
| 99.24％ | 99.18％ | 99.12％ | 99.50％ | ||||
| Qualified | |||||||
| 4. trace sharpness | Font size is made as 2,3,4,5point, the smallest font that observation station can discern | Coated paper: 3point common paper: 3point | |||||
Claims (9)
1. a digital-printing ink-jet ink made of nano pigment is characterized in that, hundred parts than composed of the following components by weight:
Nano-level pigment disperses mill base 1-20%;
Wetting Agent for Printing Inks 10-15%;
Scale remover 1-5%;
Sterilant 0.2-1%;
PH value control agent 1-5%;
Tensio-active agent 0.5-5%;
Resin 5-10%
Its surplus of deionized water.
2. digital-printing ink-jet ink made of nano pigment according to claim 1 is characterized in that: described wetting Agent for Printing Inks is at least a among ethylene glycol, Diethylene Glycol, glycerol, polyvinyl alcohol, the PEG.
3. digital-printing ink-jet ink made of nano pigment according to claim 1 is characterized in that: described scale remover is at least a among Virahol, 2-Pyrrolidone, the NMP.
4. digital-printing ink-jet ink made of nano pigment according to claim 1 is characterized in that: described sterilant is D-7.
5. digital-printing ink-jet ink made of nano pigment according to claim 1 is characterized in that: described pH value control agent is at least a in rare nitric acid, Monoethanolamine MEA BASF, diethanolamine, trolamine, the oxyammonia.
6. digital-printing ink-jet ink made of nano pigment according to claim 1 is characterized in that: described tensio-active agent is at least a among NP-10, the NP-15.
7. digital-printing ink-jet ink made of nano pigment according to claim 1 is characterized in that: described deionized water is for removing copper, iron, chromium, manganese metal ion and Cl
-, SO
4 2-After water.
8. digital-printing ink-jet ink made of nano pigment according to claim 1 is characterized in that: described resin is at least a in urethane resin, the acrylic resin.
9. the production technique of the described digital-printing ink-jet ink made of nano pigment of claim 1 is characterized in that, comprises the following steps:
(A) pigment is pre-dispersed according to fineness requirement, be ground to D90＜200 nanometers, make nano-level pigment and disperse mill base;
(B) wetting Agent for Printing Inks, scale remover, sterilant, pH value control agent, tensio-active agent, deionized water, resin are mixed at normal temperatures, fully stirred 0.5-1 hour, get mixing solutions;
(C) nano-level pigment is disperseed mill base add in the step (B) in the prepared mixing solutions, and fully stirred 20-30 minute, mixing solutions;
(D) mixing solutions with gained in the step (C) leaves standstill slaking in 24-48 hour under temperature 50-70 ℃, gets the slaking mixing solutions;
(E) with the slaking mixing solutions of gained in the step (D) successively through 1 micron, 0.5 micron, 0.22 micron membrane filtration, obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200610026595 CN100532475C (en) | 2006-05-16 | 2006-05-16 | Nano-pigment digital printing inkjet ink and its production process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200610026595 CN100532475C (en) | 2006-05-16 | 2006-05-16 | Nano-pigment digital printing inkjet ink and its production process |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1844275A true CN1844275A (en) | 2006-10-11 |
| CN100532475C CN100532475C (en) | 2009-08-26 |
Family
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200610026595 Active CN100532475C (en) | 2006-05-16 | 2006-05-16 | Nano-pigment digital printing inkjet ink and its production process |
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| Country | Link |
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| CN (1) | CN100532475C (en) |
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| WO2011066669A1 (en) * | 2009-12-02 | 2011-06-09 | 青岛尤尼科技有限公司 | Digital discharging ink and preparation method thereof |
| CN101629038B (en) * | 2009-08-19 | 2011-07-20 | 郭振荣 | Production method of aqueous nanometer color past for digital ink jet and container with ultrasonic generator |
| CN101531848B (en) * | 2009-03-24 | 2011-10-05 | 深圳市墨库数码耗材有限公司 | An environment-friendly digital ink-jet direct printing textile ink and method for preparing same |
| CN102443314A (en) * | 2011-10-26 | 2012-05-09 | 日冠(福建)针纺织机械有限公司 | Cold-dyeing digital direct-injection printing ink and application process thereof |
| CN102978976A (en) * | 2012-11-20 | 2013-03-20 | 江南大学 | Method for preparing water-based UV (Ultraviolet) pigment printing paste for textile use |
| CN104746362A (en) * | 2015-04-15 | 2015-07-01 | 南京鼎科纳米技术研究所有限公司 | Water-based nano pigment ink for textile printing |
| CN104790227A (en) * | 2015-04-07 | 2015-07-22 | 山东黄河三角洲纺织科技研究院有限公司 | Reactive dye ink for inkjet printing and preparation method thereof |
| CN105256605A (en) * | 2015-10-20 | 2016-01-20 | 湖州博仁纺织品有限公司 | Novel nanoscale natural dye for digital printing and preparation method of natural dye |
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| CN101531848B (en) * | 2009-03-24 | 2011-10-05 | 深圳市墨库数码耗材有限公司 | An environment-friendly digital ink-jet direct printing textile ink and method for preparing same |
| CN101629038B (en) * | 2009-08-19 | 2011-07-20 | 郭振荣 | Production method of aqueous nanometer color past for digital ink jet and container with ultrasonic generator |
| WO2011066669A1 (en) * | 2009-12-02 | 2011-06-09 | 青岛尤尼科技有限公司 | Digital discharging ink and preparation method thereof |
| CN102443314A (en) * | 2011-10-26 | 2012-05-09 | 日冠(福建)针纺织机械有限公司 | Cold-dyeing digital direct-injection printing ink and application process thereof |
| CN102978976A (en) * | 2012-11-20 | 2013-03-20 | 江南大学 | Method for preparing water-based UV (Ultraviolet) pigment printing paste for textile use |
| CN102978976B (en) * | 2012-11-20 | 2015-06-24 | 江南大学 | Method for preparing water-based UV (Ultraviolet) pigment printing paste for textile use |
| CN104790227A (en) * | 2015-04-07 | 2015-07-22 | 山东黄河三角洲纺织科技研究院有限公司 | Reactive dye ink for inkjet printing and preparation method thereof |
| CN104746362A (en) * | 2015-04-15 | 2015-07-01 | 南京鼎科纳米技术研究所有限公司 | Water-based nano pigment ink for textile printing |
| CN104746362B (en) * | 2015-04-15 | 2016-09-28 | 南京鼎科纳米技术研究所有限公司 | A kind of textile printing water nano paint ink |
| CN105256605B (en) * | 2015-10-20 | 2017-09-22 | 湖州优创科技有限公司 | A kind of natural dye of nanoscale digit printing and preparation method thereof |
| CN105256605A (en) * | 2015-10-20 | 2016-01-20 | 湖州博仁纺织品有限公司 | Novel nanoscale natural dye for digital printing and preparation method of natural dye |
| CN105694591A (en) * | 2016-04-25 | 2016-06-22 | 广州市番禺区协运来化工用品有限公司 | Digital printing ink and preparation method thereof |
| CN105970681A (en) * | 2016-06-20 | 2016-09-28 | 湖州新隆龙丝绸印花有限公司 | Environment-friendly brown digital printing ink and preparation method thereof |
| CN105970681B (en) * | 2016-06-20 | 2018-08-17 | 中山市东华印艺有限公司 | A kind of environment-friendly type brown digit printing ink and preparation method thereof |
| CN106280713A (en) * | 2016-08-17 | 2017-01-04 | 上海贝通色彩科技有限公司 | A kind of thermal transfer ink jet ink and preparation method thereof |
| CN109667167A (en) * | 2018-12-24 | 2019-04-23 | 珠海华彩新材料科技有限公司 | A kind of number garment print ink |
| CN109667167B (en) * | 2018-12-24 | 2021-10-15 | 珠海华彩新材料科技有限公司 | Ink for digital garment printing |
| CN110396838A (en) * | 2019-07-19 | 2019-11-01 | 浙江海印数码科技有限公司 | Modified ink-jet printed use coating type ink of a kind of compound particle based on multilevel structure and preparation method thereof, application |
| CN110396838B (en) * | 2019-07-19 | 2022-04-01 | 浙江海印数码科技有限公司 | Multi-stage structure based composite particle modified coating type ink for inkjet printing, and preparation method and application thereof |
| CN110982345A (en) * | 2019-12-18 | 2020-04-10 | 珠海市东昌颜料有限公司 | Pigment ink and preparation method thereof |
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| CN100532475C (en) | 2009-08-26 |
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Application publication date: 20061011 Assignee: Hongsam Digital Science & Technology Co., Ltd. Assignor: Yinneng Digit Sci.& Tech. Co., Ltd., Shanghai Contract record no.: 2010410000026 Denomination of invention: Digital-printing ink-jet ink made of nano pigment and its making process Granted publication date: 20090826 License type: Exclusive License Record date: 20100324 |
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Address after: 201611 room 6, building 261, three Bang Road, Shanghai, Songjiang District, 301 Patentee after: Yinneng Digit Sci.& Tech. Co., Ltd., Shanghai Address before: 200237 Shanghai City Jia Chuan Road No. 245 Building No. 1 101 Patentee before: Yinneng Digit Sci.& Tech. Co., Ltd., Shanghai |