CN107740289A - A kind of anhydrous printing with reactive dye ink and preparation method thereof - Google Patents
A kind of anhydrous printing with reactive dye ink and preparation method thereof Download PDFInfo
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- CN107740289A CN107740289A CN201710980406.4A CN201710980406A CN107740289A CN 107740289 A CN107740289 A CN 107740289A CN 201710980406 A CN201710980406 A CN 201710980406A CN 107740289 A CN107740289 A CN 107740289A
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- reactive dye
- dye ink
- printing
- anhydrous printing
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/38—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using reactive dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/32—Inkjet printing inks characterised by colouring agents
- C09D11/328—Inkjet printing inks characterised by colouring agents characterised by dyes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/38—Inkjet printing inks characterised by non-macromolecular additives other than solvents, pigments or dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/445—Use of auxiliary substances before, during or after dyeing or printing
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
- D06P1/48—Derivatives of carbohydrates
- D06P1/50—Derivatives of cellulose
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/30—Ink jet printing
Abstract
The invention discloses a kind of anhydrous printing with reactive dye ink and preparation method thereof, the anhydrous printing with reactive dye ink is made up of the raw material of following parts by weight：10 20 parts of reactive dye, 37 parts of surfactant, 26 parts of pH adjusting agent, 13 parts of softening agent, 24 parts of wetting agent, 12 parts of defoamer, 24 parts of bactericide, 0.2 0.4 parts of graphene, 35 parts of hydroxymethyl cellulose, 20 30 parts of deionized water.The anhydrous printing with reactive dye ink high colour-fast rate of the present invention, low colourity reusing sewage, effectively reduces sewage discharge.The anhydrous printing with reactive dye ink of the present invention, manufacturing process is simple to operation, and low in raw material price easily obtains, and nontoxic, and volatility is low, and human body is not stimulated.
Description
Technical field
The invention belongs to ink-jet printed technical field, specifically relates to a kind of anhydrous printing with reactive dye ink.
Background technology
The production process of digit printing be exactly briefly by various digitlization means such as：Scanning, digital photo, image
Or computing mechanism deal with various digitlization patterns input computer, then by computer color splitting printing system handle after, by special
RIP softwares by its sprayed printed system by various dedicated dyes (active, scattered, acid main coating) directly spray printing to various
On fabric or other media, then after processing, required various high-precision stamps are obtained on various weaving face fabrics
Product.
Printing ink is configured by dyestuff, at present the most frequently used active dyestuff of dyestuff, acid dyes and scattered
Dyestuff.
Some printing inks currently used in the market need to evaporate by wet-hot steam in use, then pass through
Washing, could complete stamp process.This process needs substantial amounts of industrial water, discharges substantial amounts of industrial wastewater, while evaporate,
Washing, stoving process long flow path are, it is necessary to which equipment is more, and space-consuming is big, and equipment investment is big.Some conventional printing inks make in addition
It is not water-fastness, it is necessary to add color fixing agent and adhesive with poor color fastness afterwards, influence the quality of product.
The content of the invention
It is an object of the invention to provide a kind of anhydrous reactive dye digit printing ink and preparation method thereof, with solution
State the problem of being proposed in background technology.
To achieve the above object, the present invention provides following technical scheme：
A kind of anhydrous printing with reactive dye ink, according to important number, including following components：Reactive dye 10-20 parts, table
Face activating agent 3-7 parts, pH adjusting agent 2-6 parts, softening agent 1-3 parts, wetting agent 2-4 parts, defoamer 1-2 parts, bactericide 2-4 parts,
Graphene 0.2-0.4 parts, hydroxymethyl cellulose 3-5 parts, deionized water 20-30 parts.
Preferably, described surfactant is one or more than one kinds of in anhydrous sorbitol, sucrose ester.
Preferably, described pH adjusting agent is one or more than one kinds of in sodium hydroxide, triethanolamine.
Preferably, described softening agent is one or more than one kinds of in vinegar, sodium carbonate, borax.
Preferably, described wetting agent is one or more than one kinds of in glycerine, polyethylene glycol, glycerine, diethylene glycol (DEG).
Preferably, described defoamer is water-based silicone oil.
Preferably, described bactericide is one or more than one kinds of in citric acid, chitosan, nano titanium oxide.
Preferably, described anhydrous printing with reactive dye ink, according to parts by weight, including following components：Reactive dye
10 parts, 3 parts of surfactant, 2 parts of pH adjusting agent, 1 part of softening agent, 2 parts of wetting agent, 1 part of defoamer, 2 parts of bactericide, graphene
0.2 part, 3 parts of hydroxymethyl cellulose, 20 parts of deionized water.
Preferably, described anhydrous printing with reactive dye ink, according to parts by weight, including following components：Reactive dye
15 parts, 5 parts of surfactant, 4 parts of pH adjusting agent, 2 parts of softening agent, 3 parts of wetting agent, 1.5 parts of defoamer, 3 parts of bactericide, graphite
0.3 part of alkene, 4 parts of hydroxymethyl cellulose, 25 parts of deionized water.
Preferably, described anhydrous printing with reactive dye ink, according to parts by weight, including following components：Reactive dye
20 parts, 7 parts of surfactant, 6 parts of pH adjusting agent, 3 parts of softening agent, 4 parts of wetting agent, 2 parts of defoamer, 4 parts of bactericide, graphene
0.4 part, 5 parts of hydroxymethyl cellulose, 30 parts of deionized water.
Preferably, the preparation method of described anhydrous printing with reactive dye ink, specific steps include：
Step 1, deionized water 20-30 parts are added in a kettle, and rise temperature is to 60-70 DEG C；
Step 2, reactive dye 10-20 parts, surfactant 3-7 parts are added, 500-1000 revs/min, stirring 20-30 divides
Clock；
Step 3, softening agent 1-3 parts, wetting agent 2-4 parts, bactericide 2-4 parts, graphene 0.2-0.4 parts, methylol are added
Cellulose 3-5 parts, 500-1000 revs/min, stir 20-30 minutes；
Step 4, pH adjusting agent 2-6 parts, defoamer 1-2 parts are added, 500-1000 revs/min, stirs 20-30 minutes；
Step 5, stirring is closed down, reduces temperature to normal temperature；
Step 6, the liquid that step 5 obtains is filtered with the filter membrane of 0.5 μm and 0.22 μm, you can described to obtain
Anhydrous printing with reactive dye ink.
Compared with prior art, the beneficial effects of the invention are as follows：
1st, anhydrous printing with reactive dye ink of the invention, manufacturing process is simple to operation, and low in raw material price easily obtains,
And it is nontoxic, volatility is low, and human body is not stimulated.
2nd, mutual compatibility, synergy between various raw materials used in anhydrous printing with reactive dye ink of the invention, jointly
The excellent product of component property.
3rd, anhydrous printing with reactive dye ink of the invention does not produce poisonous gas or solids in application process
Matter.
4th, anhydrous printing with reactive dye ink of the invention is high with up to more than 95% upper rate, color fastness.
5th, anhydrous printing with reactive dye ink of the invention can significantly reduce sewage discharge.
6th, anhydrous printing with reactive dye ink of the invention has high chroma, high brightness, high enhancing.
7th, anhydrous printing with reactive dye ink items fastness ability of the invention is excellent.
8th, anhydrous printing with reactive dye ink of the invention can under conditions of alkali-free is salt-free with it is not surface treated
Cotton, hair, silk spinning fabric combine, and dyeing does not hydrolyze with reactive dye in storing process, and dye-uptake is high, the ink storage-stable time
It is long, non-wastewater discharge dyeing is realized, reduces water consume and the pollution of printing with reactive dye.
9th, technique is simplified, safe operation is simple, is easy to industrialized production.
10th, use of the invention can receive good economic benefit.
Example is embodied
The invention discloses a kind of anhydrous printing with reactive dye ink, according to important number, including following components：Activity dye
Expect 10-20 parts, surfactant 3-7 parts, pH adjusting agent 2-6 parts, softening agent 1-3 parts, wetting agent 2-4 parts, defoamer 1-2 parts,
Bactericide 2-4 parts, graphene 0.2-0.4 parts, hydroxymethyl cellulose 3-5 parts, deionized water 20-30 parts.
Present invention also offers a kind of preparation method of anhydrous printing with reactive dye ink, specific steps include：
Step 1, deionized water 20-30 parts are added in a kettle, and rise temperature is to 60-70 DEG C；
Step 2, reactive dye 10-20 parts, surfactant 3-7 parts are added, 500-1000 revs/min, stirring 20-30 divides
Clock；
Step 3, softening agent 1-3 parts, wetting agent 2-4 parts, bactericide 2-4 parts, graphene 0.2-0.4 parts, methylol are added
Cellulose 3-5 parts, 500-1000 revs/min, stir 20-30 minutes；
Step 4, pH adjusting agent 2-6 parts, defoamer 1-2 parts are added, 500-1000 revs/min, stirs 20-30 minutes；
Step 5, stirring is closed down, reduces temperature to normal temperature；
Step 6, the liquid that step 5 obtains is filtered with the filter membrane of 0.5 μm and 0.22 μm, you can described to obtain
Anhydrous printing with reactive dye ink.
Embodiment 1
The invention discloses a kind of anhydrous printing with reactive dye ink, according to important number, including following components：Activity dye
10 parts of material, 3 parts of surfactant, 2 parts of pH adjusting agent, 1 part of softening agent, 2 parts of wetting agent, 1 part of defoamer, 2 parts of bactericide, graphite
0.2 part of alkene, 3 parts of hydroxymethyl cellulose, 20 parts of deionized water.
Present invention also offers a kind of preparation method of anhydrous printing with reactive dye ink, specific steps include：
Step 1,20 parts of deionized water is added in a kettle, and rise temperature is to 60 DEG C；
Step 2,10 parts of reactive dye, 3 parts of surfactant are added, 800 revs/min, is stirred 20 minutes；
Step 3,1 part of softening agent, 2 parts of wetting agent, 2 parts of bactericide, 0.2 part of graphene, 3 parts of hydroxymethyl cellulose are added,
900 revs/min, stir 20 minutes；
Step 4,2 parts of pH adjusting agent, 1 part of defoamer are added, 500 revs/min, is stirred 30 minutes；
Step 5, stirring is closed down, reduces temperature to normal temperature；
Step 6, the liquid that step 5 obtains is filtered with the filter membrane of 0.5 μm and 0.22 μm, you can described to obtain
Anhydrous printing with reactive dye ink.
Embodiment 2
The invention discloses a kind of anhydrous printing with reactive dye ink, according to important number, including following components：Activity dye
15 parts of material, 5 parts of surfactant, 4 parts of pH adjusting agent, 2 parts of softening agent, 3 parts of wetting agent, 1.5 parts of defoamer, 3 parts of bactericide, stone
Black 0.3 part of alkene, 4 parts of hydroxymethyl cellulose, 25 parts of deionized water.
Present invention also offers a kind of preparation method of anhydrous printing with reactive dye ink, specific steps include：
Step 1,25 parts of deionized water is added in a kettle, and rise temperature is to 65 DEG C；
Step 2,15 parts of reactive dye, 5 parts of surfactant are added, 800 revs/min, is stirred 25 minutes；
Step 3,2 parts of softening agent, 3 parts of wetting agent, 3 parts of bactericide, 0.3 part of graphene, 4 parts of hydroxymethyl cellulose are added,
800 revs/min, stir 25 minutes；
Step 4,4 parts of pH adjusting agent, 1.5 parts of defoamer are added, 800 revs/min, is stirred 25 minutes；
Step 5, stirring is closed down, reduces temperature to normal temperature；
Step 6, the liquid that step 5 obtains is filtered with the filter membrane of 0.5 μm and 0.22 μm, you can described to obtain
Anhydrous printing with reactive dye ink.
Embodiment 3
The invention discloses a kind of anhydrous printing with reactive dye ink, according to important number, including following components：Activity dye
20 parts of material, 7 parts of surfactant, 6 parts of pH adjusting agent, 3 parts of softening agent, 4 parts of wetting agent, 2 parts of defoamer, 4 parts of bactericide, graphite
0.4 part of alkene, 5 parts of hydroxymethyl cellulose, 30 parts of deionized water.
Present invention also offers a kind of preparation method of anhydrous printing with reactive dye ink, specific steps include：
Step 1,30 parts of deionized water is added in a kettle, and rise temperature is to 70 DEG C；
Step 2,20 parts of reactive dye, 7 parts of surfactant are added, 1000 revs/min, is stirred 30 minutes；
Step 3,3 parts of softening agent, 4 parts of wetting agent, 4 parts of bactericide, 0.4 part of graphene, 5 parts of hydroxymethyl cellulose are added,
1000 revs/min, stir 30 minutes；
Step 4,6 parts of pH adjusting agent, 2 parts of defoamer are added, 1000 revs/min, is stirred 30 minutes；
Step 5, stirring is closed down, reduces temperature to normal temperature；
Step 6, the liquid that step 5 obtains is filtered with the filter membrane of 0.5u μm and 0.22 μm, you can described to obtain
Anhydrous printing with reactive dye ink.
Embodiment 4
The invention discloses a kind of anhydrous printing with reactive dye ink, according to important number, including following components：Activity dye
15 parts of material, 7 parts of surfactant, 3 parts of pH adjusting agent, 2 parts of softening agent, 2 parts of wetting agent, 1 part of defoamer, 3 parts of bactericide, graphite
0.2 part of alkene, 3 parts of hydroxymethyl cellulose, 30 parts of deionized water.
Present invention also offers a kind of preparation method of anhydrous printing with reactive dye ink, specific steps include：
Step 1,30 parts of deionized water is added in a kettle, and rise temperature is to 70 DEG C；
Step 2,15 parts of reactive dye, 7 parts of surfactant are added, 1000 revs/min, is stirred 20 minutes；
Step 3,2 parts of softening agent, 2 parts of wetting agent, 3 parts of bactericide, 0.2 part of graphene, 3 parts of hydroxymethyl cellulose are added,
800 revs/min, stir 25 minutes；
Step 4,3 parts of pH adjusting agent, 1 part of defoamer are added, 900 revs/min, is stirred 20 minutes；
Step 5, stirring is closed down, reduces temperature to normal temperature；
Step 6, the liquid that step 5 obtains is filtered with the filter membrane of 0.5 μm and 0.22 μm, you can described to obtain
Anhydrous printing with reactive dye ink.
The above-mentioned various embodiments enumerated, under the premise of reconcilable, can be mutually combined implementation, those skilled in the art
The explanation to embodiment above can be combined, as the foundation being combined to the technical characteristic in different embodiments.
Test case 1
Using embodiment 1,2,3,4 dye liquors → stamp → drying (110-140 DEG C, 2min) → decatize/hot melt → washing →
Drying, obtained printing textile is subjected to fastness test, test result is as follows：
| Embodiment | Fastness to rubbing | Washing fastness | Against weather |
| 1 | 3-4 | 3-4 | 3 |
| 2 | 4 | 4 | 3-4 |
| 3 | 4-5 | 4-5 | 4-5 |
| 4 | 4-5 | 4-5 | 4 |
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (8)
- A kind of 1. anhydrous printing with reactive dye ink, it is characterised in that：The anhydrous printing with reactive dye ink includes following weight Measure the raw material of number：Reactive dye 10-20 parts, surfactant 3-7 parts, pH adjusting agent 2-6 parts, softening agent 1-3 parts, wetting agent 2-4 parts, defoamer 1-2 parts, bactericide 2-4 parts, graphene 0.2-0.4 parts, hydroxymethyl cellulose 3-5 parts, deionized water 20-30 Part.
- 2. anhydrous printing with reactive dye ink according to claim 1, it is characterised in that：Described surfactant is mistake It is one or more than one kinds of in water sorbierite, sucrose ester.
- 3. anhydrous printing with reactive dye ink according to claim 1, it is characterised in that：Described pH adjusting agent is hydrogen-oxygen Change one or more than one kinds of in sodium, triethanolamine.
- 4. anhydrous printing with reactive dye ink according to claim 1, it is characterised in that：Described softening agent be vinegar, It is one or more than one kinds of in sodium carbonate, borax.
- 5. anhydrous printing with reactive dye ink according to claim 1, it is characterised in that：Described wetting agent is the third three It is one or more than one kinds of in alcohol, polyethylene glycol, glycerine, diethylene glycol (DEG).
- 6. anhydrous printing with reactive dye ink according to claim 1, it is characterised in that：Described defoamer is water-based silicon Oil.
- 7. anhydrous printing with reactive dye ink according to claim 1, it is characterised in that：Described bactericide is lemon It is one or more than one kinds of in acid, chitosan, nano titanium oxide.
- 8. the preparation method of any described anhydrous printing with reactive dye ink in a kind of 1-7 using the claims, it is special Sign is：Specific steps include：Step 1, deionized water 20-30 parts are added in a kettle, and rise temperature is to 60-70 DEG C；Step 2, reactive dye 10-20 parts, surfactant 3-7 parts are added, 500-1000 revs/min, stirs 20-30 minutes；Step 3, softening agent 1-3 parts, wetting agent 2-4 parts, bactericide 2-4 parts, graphene 0.2-0.4 parts, hydroxylmethyl cellulose are added Plain 3-5 parts, 500-1000 revs/min, stir 20-30 minutes；Step 4, pH adjusting agent 2-6 parts, defoamer 1-2 parts are added, 500-1000 revs/min, stirs 20-30 minutes；Step 5, stirring is closed down, reduces temperature to normal temperature；Step 6, the liquid that step 5 obtains is filtered with the filter membrane of 0.5 μm and 0.22 μm, you can described anhydrous to obtain Printing with reactive dye ink.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710980406.4A CN107740289A (en) | 2017-10-19 | 2017-10-19 | A kind of anhydrous printing with reactive dye ink and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710980406.4A CN107740289A (en) | 2017-10-19 | 2017-10-19 | A kind of anhydrous printing with reactive dye ink and preparation method thereof |
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| Publication Number | Publication Date |
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| CN107740289A true CN107740289A (en) | 2018-02-27 |
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| CN201710980406.4A Pending CN107740289A (en) | 2017-10-19 | 2017-10-19 | A kind of anhydrous printing with reactive dye ink and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108797152A (en) * | 2018-06-13 | 2018-11-13 | 南通强生石墨烯科技有限公司 | A kind of graphene concentrator and preparation method thereof |
| CN113354981A (en) * | 2021-06-29 | 2021-09-07 | 安徽正洁高新材料股份有限公司 | Thermal transfer ink and preparation method thereof |
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| JP2004359928A (en) * | 2002-10-24 | 2004-12-24 | Seiko Epson Corp | Inkjet ink for textile printing, and inkjet printing method |
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| JP2015183342A (en) * | 2014-03-26 | 2015-10-22 | セイコーエプソン株式会社 | Inkjet textile printing method |
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| CN108797152A (en) * | 2018-06-13 | 2018-11-13 | 南通强生石墨烯科技有限公司 | A kind of graphene concentrator and preparation method thereof |
| CN113354981A (en) * | 2021-06-29 | 2021-09-07 | 安徽正洁高新材料股份有限公司 | Thermal transfer ink and preparation method thereof |
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Application publication date: 20180227 |