CN105951208A - Modified polyester fiber and preparation method thereof - Google Patents
Modified polyester fiber and preparation method thereof Download PDFInfo
- Publication number
- CN105951208A CN105951208A CN201610542389.1A CN201610542389A CN105951208A CN 105951208 A CN105951208 A CN 105951208A CN 201610542389 A CN201610542389 A CN 201610542389A CN 105951208 A CN105951208 A CN 105951208A
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- parts
- nano
- polyester fiber
- modified polyester
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Classifications
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- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/88—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds
- D01F6/92—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polycondensation products as major constituent with other polymers or low-molecular-weight compounds of polyesters
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
- D01F1/106—Radiation shielding agents, e.g. absorbing, reflecting agents
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Artificial Filaments (AREA)
Abstract
The invention belongs to the technical field of a textile material, and particularly relates to modified polyester fiber and a preparation method thereof. The polyester fiber is prepared from the following materials in percentage by weight: 90 to 95% of polyester chips and 5 to 10% of far infrared anion nano functional slurry, wherein the far infrared anion nano functional slurry is prepared from the following materials in parts by mass: 5 to 15 parts of nano titania, 5 to 15 parts of nano zinc oxide, 20 to 30 parts of ethyl alcohol, 20 to 35 parts of far infrared ceramic powder, 20 to 35 parts of tourmaline powder and 10 to 20 parts of hydroxymethyl cellulose ether. The modified polyester fibers prepared by the formula and the preparation method which are provided by the invention are developed for meeting the requirement of people for high-end textures; the obtained polyester fiber has functions of good far infrared effect, anion physiotherapy, excellent antibacterial property, heat insulation, ultraviolet resistance and the like.
Description
Technical field
The invention belongs to textile material technical field, be specifically related to a kind of modified polyester fiber and preparation method thereof.
Background technology
Existing textile material is divided into multiple, and more conventional mostly is cotton and various chemical synthetic fiber, by respectively
The making of kind of fiber, for allowing fabric have warming, good hand touch, bibulous function, even can use special fibre
Dimension allows fabric have special effect, such as physical therapy, antibacterial, the most military shellproof.But existing various weaving
Material while its advantage represents, existence performance shortcomings more or less, e.g., cotton good warmth retention effect, inhale
Aqueous is strong, but the most mouldy, acid resistance is poor, and its fabric is fluffy too fat to move；Flaxen fiber is comfortable and easy to wear but outward appearance is coarse；
Fine animal fibre is comfortable and easy to wear, and warmth retention property is good, but expensive and easy shrinking deformation；Various chemical fibers are general
Store-through is comfortable and easy to wear, and warming good still water absorption is poor, and without physical therapy efficacy.
Anion is the material that modern is indispensable, can provide energy indirectly by air to human body.Bear from
Son is a kind of electronegative gas ion in air.Anion can not only facilitate human body synthesis and vitamin storage,
Strengthening and the physiological activity of human activin, have highly important impact to the vital movement of human body and other biological,
Therefore it is otherwise known as " air vitamin ".In medical circle, anion is identified it is to have to kill pathogenic bacteria and purification
The effective means of air.Medical research shows, in air, electronegative microgranule makes oxygen content in blood increase, favorably
In the conveying of blood oxygen, absorb and utilize, there is promotion human metabolism, improving human body immunity, strengthening people
Body flesh energy, the effect of regulation human body function balance.According to textual criticism, anion system multiple to human body (is such as breathed
System, nervous system, cardiovascular system, digestive system, hormonal system, metabolic system, blood system etc.),
Nearly more than 30 kinds of diseases have suppression, alleviate and auxiliary therapeutic action, especially the brightest to the health-care effect of human body
Aobvious.It is said that in general, people needs about 13,000,000,000 anion every day, and our room, office, public place of entertainment
The environment such as institute, can only provide about 1～2,000,000,000.Far infrared has stronger penetration and radiant force, has
Significantly temperature control effect and resonance effect, after being absorbed by the body, can make internal water produce resonance, make moisture
Son activation, strengthens its intermolecular adhesion, improves the oxygen content of health, cell thus can rejuvenate.This
Plant action intensity, make telangiectasis, improve microcirculqtory system, blood circulation promoting, strengthen each tissue
Metabolism, increases the regeneration capacity of tissue, improves the immunocompetence of body, balances the acid-base value of health, from
And play the effect of health care.
And far infrared has the effect to central nervous system to the health of people, blood circulation can be accelerated, improve
Cerebral tissue microcirculation situation, makes brain cell be able to sufficient oxygen and nutriment supply, adds excitometabolic, make big
Cortex out-of-balance conditions is changed, and deepens process of inhibition, plays calmness, soporific function.
More than for, how by the improvement of prior art, obtain one and there is antibiotic and sterilizing, and also one
The new modified polyester fiber of fixed physical therapy efficacy.
Summary of the invention
It is an object of the invention to provide a kind of new modified polyester fiber and preparation method thereof.
The technical scheme realizing the object of the invention is: a kind of modified polyester fiber, by weight percentage, including
Polyester slice 90～95%, far infrared negative ion nano function slurry 5～10%.
Preferably, described far infrared negative ion nano function slurry, according to the mass fraction, and including: nanometer two
Titanium oxide 5～15 parts, nano zine oxide 5～15 parts, ethanol 20～30 parts, far-infrared ceramic powder 20～
35 parts, tourmaline powder 20～35 parts, hydroxymethyl cellulose ether 10～20 parts.
It is furthermore preferred that described far infrared negative ion nano function slurry is prepared by following steps: 1) by nanometer
Titanium dioxide, nano zine oxide join in alcohol solvent, ultrasonic disperse, prepare nano titanium oxide/nanometer
Zinc oxide fluid dispersion；2) far-infrared ceramic powder, tourmaline powder and hydroxymethyl cellulose ether are placed in sand milling
Carrying out being mixed to prepare composite powder in machine, the particle diameter of described composite powder is 10～30 μm；3) at stirring condition
Under, composite powder is mixed with nano titanium oxide/nano zinc oxide fluid dispersion, prepared far-infrared negative-ion is received
Meter Gong Neng slurry.
The preparation method of a kind of modified polyester fiber of the present invention, preparation process is: be heated to melting by polyester slice
State, is subsequently adding far infrared negative ion nano function slurry and pelletize is blended obtains masterbatch, masterbatch is carried out Wet-spinning
Silk, is carried out spinning, is dried, winds, and obtains far infrared and anion modified polyester fiber.Wherein,
Described winding speed is 50～100m/min.
The technological merit of the present invention is:
By the modified polyester fiber obtained by inventive formulation and preparation method, it is to meet people to high-end fabric
Demand and develop, gained polyester fiber has that far-infrared effect is good, negative ion physiotherapeutic, good antibiotic property,
The functions such as heat insulation and uvioresistant.The preparation technology of the present invention is the most relatively simple.Heretofore described composite powder
Size controlling have important in 10～30 μm for the stability of the nano functional slurry system in inventive formulation
Effect, it is to avoid particle diameter is too small is susceptible to particle aggregation.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1
10kg polyester slice (PETP fiber) is heated to molten state, is subsequently adding 0.5kg
Far infrared negative ion nano function slurry is blended pelletize and obtains masterbatch, masterbatch is carried out wet spinning, enters spinning
Row cleans, is dried, winds, and winding speed is 50m/min, obtains the function containing far infrared with anion and gathers
Ester fiber.
Wherein, far infrared negative ion nano function slurry is prepared by following methods: by nano titanium oxide 5 parts,
Nano zine oxide 5 parts joins in 20 parts of alcohol solvents, ultrasonic disperse, prepares nano titanium oxide/nano oxygen
Change zinc dispersion liquid；By far-infrared ceramic powder 20 parts, tourmaline powder 20 parts and hydroxymethyl cellulose ether 10
Part is placed in sand mill and carries out being mixed to prepare composite powder, the particle diameter of described composite powder about 10 μm；In stirring
Under the conditions of, composite powder is mixed with nano titanium oxide/nano zinc oxide fluid dispersion, prepared far infrared bear from
Sub-nano functional slurry.
Embodiment 2
10kg polyester slice (PETP fiber) is heated to molten state, is subsequently adding 0.75kg
The nano functional slurry of far-infrared negative-ion is blended pelletize and obtains masterbatch, masterbatch is carried out wet spinning, to spinning
Being carried out, be dried, wind, winding speed is 80m/min, obtains the function containing far infrared Yu anion
Polyester fiber.
Wherein, far infrared negative ion nano function slurry is prepared by following methods: by nano titanium oxide 10 parts,
Nano zine oxide 10 parts joins in 30 parts of alcohol solvents, ultrasonic disperse, prepares nano titanium oxide/nanometer
Zinc oxide fluid dispersion；By far-infrared ceramic powder 30 parts, tourmaline powder 35 parts and hydroxymethyl cellulose ether
15 parts are placed in sand mill and carry out being mixed to prepare composite powder, the particle diameter of described composite powder about 20 μm；Stirring
Under the conditions of mixing, composite powder is mixed with nano titanium oxide/nano zinc oxide fluid dispersion, prepare far infrared and bear
Ion nano functional slurry.
Embodiment 3
10kg polyester slice (PETP fiber) is heated to molten state, is subsequently adding 1kg
Far infrared negative ion nano function slurry is blended pelletize and obtains masterbatch, masterbatch is carried out wet spinning, enters spinning
Row cleans, is dried, winds, and winding speed is 100m/min, obtains far-infrared negative-ion functional polyester fiber.
Wherein, far infrared negative ion nano function slurry is prepared by following methods: by nano titanium oxide 15 parts,
Nano zine oxide 15 parts joins in 25 parts of alcohol solvents, ultrasonic disperse, prepares nano titanium oxide/nanometer
Zinc oxide fluid dispersion；By far-infrared ceramic powder 35 parts, tourmaline powder 30 parts and hydroxymethyl cellulose ether
20 parts are placed in sand mill and carry out being mixed to prepare composite powder, the particle diameter of described composite powder about 30 μm；Stirring
Under the conditions of mixing, composite powder is mixed with nano titanium oxide/nano zinc oxide fluid dispersion, prepare far infrared and bear
Ion nano functional slurry.
Embodiment 1～3 is measured, the far infrared emissivity about 80～85% of gained polyester fiber, anti-
Ultraviolet rate 100%, anion sum about 2600～2800/cubic centimetre that fiber is dynamic and static.
Claims (5)
1. a modified polyester fiber, it is characterised in that: by weight percentage, including polyester slice 90～95%,
Far infrared negative ion nano function slurry 5～10%.
Modified polyester fiber the most according to claim 1, it is characterised in that: described far-infrared negative-ion
Nano functional slurry, according to the mass fraction, including: nano titanium oxide 5～15 parts, nano zine oxide 5～
15 parts, ethanol 20～30 parts, far-infrared ceramic powder 20～35 parts, tourmaline powder 20～35 parts, hydroxyl
Methyl cellulose ether 10～20 parts.
Modified polyester fiber the most according to claim 2, it is characterised in that: described far-infrared negative-ion
Nano functional slurry is prepared by following steps: 1) by nano titanium oxide, that nano zine oxide joins ethanol is molten
In agent, ultrasonic disperse, prepare nano titanium oxide/nano zinc oxide fluid dispersion；2) by far-infrared ceramic powder,
Tourmaline powder and hydroxymethyl cellulose ether are placed in sand mill and carry out being mixed to prepare composite powder, described composite powder
The particle diameter of material is 10～30 μm；3) under agitation, by composite powder and nano titanium oxide/nano oxygen
Change the mixing of zinc dispersion liquid, prepare far infrared negative ion nano function slurry.
4. the preparation method of modified polyester fiber as described in any one of claims 1 to 3, it is characterised in that:
Preparation process is: polyester slice is heated to molten state, is subsequently adding far infrared negative ion nano function slurry altogether
Mixed pelletize obtains masterbatch, and masterbatch is carried out wet spinning, is carried out spinning, is dried, winds, and obtains remote
Infrared with anion modified polyester fiber.
The preparation method of modified polyester fiber the most according to claim 4, it is characterised in that: described volume
It is 50～100m/min around speed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610542389.1A CN105951208A (en) | 2016-07-12 | 2016-07-12 | Modified polyester fiber and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610542389.1A CN105951208A (en) | 2016-07-12 | 2016-07-12 | Modified polyester fiber and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105951208A true CN105951208A (en) | 2016-09-21 |
Family
ID=56899757
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610542389.1A Pending CN105951208A (en) | 2016-07-12 | 2016-07-12 | Modified polyester fiber and preparation method thereof |
Country Status (1)
| Country | Link |
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| CN (1) | CN105951208A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107254730A (en) * | 2017-07-04 | 2017-10-17 | 江苏占姆士纺织有限公司 | A kind of production method of heat-insulated uvioresistant antibacterial permeation-proof fabric yarn |
| CN107268112A (en) * | 2017-07-04 | 2017-10-20 | 江苏占姆士纺织有限公司 | A kind of heat-insulated uvioresistant antibacterial permeation-proof imitates the production method of cotton polyester staple fibers |
| CN107385534A (en) * | 2017-08-16 | 2017-11-24 | 河北卓达建材研究院有限公司 | A kind of anion environmental protection health fiber and preparation method thereof |
| CN109487359A (en) * | 2018-08-14 | 2019-03-19 | 岑锴林 | A kind of health care far-infrared negative-ion polyester fiber |
| CN110331574A (en) * | 2019-07-09 | 2019-10-15 | 杨震源 | Energy sustained release anion, family's textile of energy element and its preparation method and application |
| CN111925198A (en) * | 2020-08-10 | 2020-11-13 | 桂林新竹大自然生物材料有限公司 | Tourmaline far infrared functional powder material and preparation method thereof |
| CN114457454A (en) * | 2022-03-04 | 2022-05-10 | 苏州世祥生物纤维有限公司 | Functional stock solution coloring fiber and preparation method and application thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1299889A (en) * | 2000-12-27 | 2001-06-20 | 东华大学 | Additive material for preparing efficient nanometer negative-oxygen ion health fiber |
| CN102345184A (en) * | 2011-08-02 | 2012-02-08 | 苏州东胜化纤纺织有限公司 | Functional polyester fiber and its manufacture method |
| CN102826834A (en) * | 2012-09-19 | 2012-12-19 | 张永利 | Low-temperature far infrared body and preparation thereof, and method for preparing far infrared anion powder using low-temperature far infrared body |
| CN102943314A (en) * | 2012-11-22 | 2013-02-27 | 吴江江旭纺织有限公司 | Method for preparing far-infrared textile through full granulation method |
| CN103570360A (en) * | 2012-07-30 | 2014-02-12 | 伯鑫科技有限公司 | Far infrared heat-radiation ceramic slurry, fiber cloth, thin film and preparation methods thereof |
| CN103849955A (en) * | 2014-02-25 | 2014-06-11 | 浙江慧德新材料有限公司 | Production process of novel health fiber containing various functional elements |
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2016
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Patent Citations (6)
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| CN1299889A (en) * | 2000-12-27 | 2001-06-20 | 东华大学 | Additive material for preparing efficient nanometer negative-oxygen ion health fiber |
| CN102345184A (en) * | 2011-08-02 | 2012-02-08 | 苏州东胜化纤纺织有限公司 | Functional polyester fiber and its manufacture method |
| CN103570360A (en) * | 2012-07-30 | 2014-02-12 | 伯鑫科技有限公司 | Far infrared heat-radiation ceramic slurry, fiber cloth, thin film and preparation methods thereof |
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| CN102943314A (en) * | 2012-11-22 | 2013-02-27 | 吴江江旭纺织有限公司 | Method for preparing far-infrared textile through full granulation method |
| CN103849955A (en) * | 2014-02-25 | 2014-06-11 | 浙江慧德新材料有限公司 | Production process of novel health fiber containing various functional elements |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107254730A (en) * | 2017-07-04 | 2017-10-17 | 江苏占姆士纺织有限公司 | A kind of production method of heat-insulated uvioresistant antibacterial permeation-proof fabric yarn |
| CN107268112A (en) * | 2017-07-04 | 2017-10-20 | 江苏占姆士纺织有限公司 | A kind of heat-insulated uvioresistant antibacterial permeation-proof imitates the production method of cotton polyester staple fibers |
| CN107385534A (en) * | 2017-08-16 | 2017-11-24 | 河北卓达建材研究院有限公司 | A kind of anion environmental protection health fiber and preparation method thereof |
| CN109487359A (en) * | 2018-08-14 | 2019-03-19 | 岑锴林 | A kind of health care far-infrared negative-ion polyester fiber |
| CN110331574A (en) * | 2019-07-09 | 2019-10-15 | 杨震源 | Energy sustained release anion, family's textile of energy element and its preparation method and application |
| CN111925198A (en) * | 2020-08-10 | 2020-11-13 | 桂林新竹大自然生物材料有限公司 | Tourmaline far infrared functional powder material and preparation method thereof |
| CN114457454A (en) * | 2022-03-04 | 2022-05-10 | 苏州世祥生物纤维有限公司 | Functional stock solution coloring fiber and preparation method and application thereof |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160921 |