CN105948961A - Insecticide-fertilizer particulate agent and preparation method thereof - Google Patents

Insecticide-fertilizer particulate agent and preparation method thereof Download PDF

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Publication number
CN105948961A
CN105948961A CN201610283053.8A CN201610283053A CN105948961A CN 105948961 A CN105948961 A CN 105948961A CN 201610283053 A CN201610283053 A CN 201610283053A CN 105948961 A CN105948961 A CN 105948961A
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China
Prior art keywords
powder
fertilizer
fertilizer granules
sulfate
mesh
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CN201610283053.8A
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Chinese (zh)
Inventor
郑敬敏
张仙
韩辉
宁昭玉
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Shaanxi Sunger Road Bio Science Co Ltd
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Shaanxi Sunger Road Bio Science Co Ltd
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Priority to CN201610283053.8A priority Critical patent/CN105948961A/en
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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/60Biocides or preservatives, e.g. disinfectants, pesticides or herbicides; Pest repellants or attractants
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01CPLANTING; SOWING; FERTILISING
    • A01C1/00Apparatus, or methods of use thereof, for testing or treating seed, roots, or the like, prior to sowing or planting
    • A01C1/06Coating or dressing seed
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01CPLANTING; SOWING; FERTILISING
    • A01C21/00Methods of fertilising, sowing or planting
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C3/00Fertilisers containing other salts of ammonia or ammonia itself, e.g. gas liquor
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pest Control & Pesticides (AREA)
  • Soil Sciences (AREA)
  • Environmental Sciences (AREA)
  • Plant Pathology (AREA)
  • Fertilizers (AREA)

Abstract

The present invention discloses an insecticide-fertilizer particulate agent and a preparation method thereof. The insecticide-fertilizer particulate agent comprises an insecticide, a bactericide, a fertilizer and an auxiliary agent. The insecticide is composed of one or more components selected from diazinon, thiamethoxam, imidacloprid, clothianidin, chlopyrifos, phoxim, carbofuran and carbosulfan. The bactericide is composed of one or more components selected from azoxystrobin, pyraclostrobin, fludioxonil, metalaxyl, methylimidazole bacteria aniline, thifluzamide and mancozeb. The fertilizer is composed of one or more components selected from urea, ammonium sulfate, potassium sulfate, potassium chloride, monoammonium phosphate, diammonium phosphate, potassium dihydrogen phosphate, dipotassium hydrogen phosphate, ammonium polyphosphate, potassium nitrate, zinc sulfate, manganese sulfate, magnesium sulfate, borax, boric acid, ferrous sulfate, copper sulfate, ammonium molybdate, ethylene diamine tetraacetic acid, calcium nitrate, potassium humate, organic matter, amino acid and soybean meal. The insecticide-fertilizer particulate agent is applied during the crop sowing period and can be used for preventing and controlling crop underground pests and diseases at the rootstocks of crops.

Description

A kind of fertilizer granules and preparation method thereof
Technical field
The invention belongs to technical field of pesticide preparations, particularly relate to a kind of fertilizer granules agent and preparation method thereof and answer With.
Background technology
In recent years, under crop field, pest damage is on the rise, and brings bigger economic loss to peasant.Subterranean pest-insect kind Class is various, mainly has cutworm, Holotrichia diomphalia Bates, Gryllotalpa, wireworm etc..Its host types is complicated, how to cause harm at spring and autumn, mainly Cause harm the seed of crop, underground part and subaerial rhizome portion.Often result in and hinder root, dead Seedling, so that the disconnected ridge that is short of seedling.Under numerously Insect has more stable ecological environment, and biocycle length, animal migration are weak, also has the feature with ground temperature change Vertical movements, Hazard boom is formed in spring, season in autumn two.
Though root of the crop stem disease does not has leaf diseases kind many, but occur the most serious, such as Rhizoma Solani tuber osi in recent years Tar spot, take-all, root rot, banded sclerotial blight, Causal Organism of Maize Basal Stalk, Roots of Peanut maize ear rot, sclerotinia rot of colza etc..The work caught an illness Thing dies down in Seedling Stage growing way, dead time serious.The loss that root of the crop stem disease has serious consequences to agricultural production.
During traditional proportion of crop planting, fertilising and dispenser are carried out separately, and so considerably increase the work of peasant Measure.Fertilizing management and dispenser prevention and control do not have specific aim yet, easily cause blindly fertilising, medication, cause fertilising imbalance, worm Evil, diseases control are the best.Fertilizer granules of the present invention, provides the benefit that: 1, fertilising, insect protected are combined with diseases prevention, reaches same Shi Youxiao preventing and treating crop pest, disease and the purpose of fertilising;2, medicine fertilizer is used simultaneously, increases operation rate, and reaches to reduce dosage Purpose with fertilizer application amount;3, carry out dispenser during sowing, reach to reduce labor intensity, the purpose of time and labour saving.
Summary of the invention
The goal of the invention of the present invention is to provide a kind of fertilizer granules, its preparation method and application.
The fertilizer granules that the present invention provides has the triple function of parasite killing, sterilization and fertilizer, it is possible to pest control simultaneously, Nutritional labeling needed for disease and supplementary plant growth.The emergence rate that improve after the fertilizer granules of the application present invention, improves The situation that plant strain growth Seedling is weak, root growth is good, and cane is healthy and strong, effectively prevents subterranean pest-insect and root of the crop stem sick The generation of evil.
For achieving the above object, the present invention adopts the following technical scheme that.
The invention provides a kind of fertilizer granules, by percentage to the quality, it includes following component:
The bonding of the fertilizer of the antibacterial of insecticide, 0.001%~1%, 10%~90%, 1%~20% of 0.001%~1% Agent and the filler of surplus.Wherein:
Insecticide is in diazinon, Diacloden, imidacloprid, clothianidin, chlopyrifos, phoxim, carbofuran, carbosulfan Plant or multiple, preferably diazinon, Diacloden;
Antibacterial is in Fluoxastrobin, pyraclostrobin, CGA-173506, Metalaxyl-M, furan azoles bacterium aniline, thifluzamide, Mancozeb One or more, preferably Fluoxastrobin, pyraclostrobin, CGA-173506;
Fertilizer be carbamide, ammonium sulfate, potassium sulfate, potassium chloride, MAP, Diammonium phosphate (DAP), potassium dihydrogen phosphate, dipotassium hydrogen phosphate, APP, potassium nitrate, zinc sulfate, manganese sulfate, magnesium sulfate, Borax, boric acid, ferrous sulfate, copper sulfate, ammonium molybdate, ethylenediamine One or more in tetraacethyl disodium, calcium nitrate, potassium humate, organic matter, aminoacid, bean cake etc.;
Binding agent is in sodium hydroxyl cellulose, xanthan gum, gelatinized starch, paraffin, polyglutamic acid, methylcellulose, Colophonium etc. One or more.
Filler is one or more in Kaolin, kieselguhr, white carbon, starch, stone powder, quartz sand etc..
The dosage form of this medicine fertilizer preparation is granule, and preparation process comprises the following steps:
The antibacterial of insecticide, 0.001%~1% by 0.001%~1% and the binding agent of 1%~20% fill after being pulverized and mixed Dividing absorption, the mixture after adsorbing is crushed to 50~100 mesh through pulverizer and obtains powder A;By the fertilizer powder of 10%~90% It is broken to 50~100 mesh and obtains powder B, carry out pelletize after powder A and powder B and surplus filler being sufficiently mixed, finally make Obtain fertilizer granules.
Present invention also offers the application process of a kind of fertilizer granules, this application process is:
In crop sowing time, will fertilizer granules of the present invention mix with seed after be jointly sown in soil or individually that medicine of the present invention is fertile Granule is sowed in seed furrow, sows the most again.Use 3-8 kilogram for every mu.
Detailed description of the invention
The invention discloses a kind of fertilizer granules, its preparation method and application process.Those skilled in the art can join Examine present disclosure, it is thus achieved that this fertilizer granules, it is achieved its application, it is accordingly required in particular to it is noted that all similar replacements and change Apparent to those skilled in the art, they are considered as being included in the present invention.The preparation method of the present invention Being described by preferred embodiment, related personnel substantially can be without departing from present invention, spirit and scope This paper preparation method it is modified or suitably changes and combine, realize and apply the technology of the present invention.
A kind of fertilizer granules, its preparation method and the application process that the present invention provides, used reagent and raw material are equal Can be buied by market.
In order to make those skilled in the art better understood when technical scheme, below in conjunction with enforcement Example, is expanded on further the present invention:
Example of formulations 1 diazinon and the fertilizer granules embodiment of azoxystrobin compound.
Example of formulations 1-1
Fully absorption after 0.005% diazinon, 0.5% Fluoxastrobin, 20% sodium hydroxyl cellulose being pulverized and mixed, after absorption Mixture is crushed to 50~100 mesh through pulverizer and obtains powder A;30% carbamide, 20% ammonium sulfate, 10% kalium slfuricum powder are broken to 50~100 mesh obtain powder B, carry out pelletize, finally make after powder A and powder B and 19.495% Kaolin being sufficiently mixed Obtain 0.505% diazinon Fluoxastrobin fertilizer granules.
Example of formulations 1-2
Fully absorption after 0.2% diazinon, 0.01% Fluoxastrobin, 8% xanthan gum being pulverized and mixed, by the mixture warp after absorption Cross pulverizer to be crushed to 50~100 mesh and obtain powder A;20% APP, 20% potassium nitrate powder are broken to 50~100 mesh and obtain powdery Thing B, carries out pelletize after powder A and powder B and 51.79% white carbon being sufficiently mixed, final prepared 0.21% diazinon Fluoxastrobin fertilizer granules.
Example of formulations 1-3
Fully absorption after 0.03% diazinon, 0.05% Fluoxastrobin, 1% paraffin being pulverized and mixed, passes through the mixture after absorption Pulverizer is crushed to 50~100 mesh and obtains powder A;40% dipotassium hydrogen phosphate, 50% ammonium molybdate are crushed to 50~100 mesh and obtain powdery Thing B, carries out pelletize after powder A and powder B and 8.92% quartz sand being sufficiently mixed, and final prepared 0.08% diazinon is phonetic Bacterium ester fertilizer granules.
Example of formulations 1-4
Fully absorption after 0.1% diazinon, 0.1% Fluoxastrobin, 3% xanthan gum being pulverized and mixed, passes through the mixture after absorption Pulverizer is crushed to 50~100 mesh and obtains powder A;10% potassium dihydrogen phosphate is crushed to 50~100 mesh and obtains powder B, by powdery Thing A and powder B and 50% stone powder, 36.8% quartz sand carry out pelletize after being sufficiently mixed, and final prepare the 0.2% phonetic bacterium of diazinon Ester fertilizer granules.
Example of formulations 1-5
Fully absorption after 0.001% diazinon, 1% Fluoxastrobin, 4% polyglutamic acid being pulverized and mixed, by the mixture warp after absorption Cross pulverizer to be crushed to 50~100 mesh and obtain powder A;80% boric acid powder is broken to 50~100 mesh and obtains powder B, by powder A Pelletize is carried out, final prepared 1.001% diazinon Fluoxastrobin medicine fertilizer granule after being sufficiently mixed with powder B and 14.999% starch Agent.
Example of formulations 1-6
Fully absorption after 1% diazinon, 0.001% Fluoxastrobin, 6% Colophonium being pulverized and mixed, by the mixture after absorption through powder Broken machine is crushed to 50~100 mesh and obtains powder A;50% disodiumedetate is crushed to 50~100 mesh and obtains powder B, will Powder A and powder B and 22.999% white carbon, 20% quartz sand carry out pelletize after being sufficiently mixed, and final prepare 1.001% 2 Piperazine phosphorus Fluoxastrobin fertilizer granules.
The fertilizer granules embodiment that example of formulations 2 diazinon is compounding with pyraclostrobin.
Example of formulations 2-1
Fully absorption after 0.05% diazinon, 0.005% pyraclostrobin, 15% methylcellulose being pulverized and mixed, after adsorbing Mixture be crushed to 50~100 mesh through pulverizer and obtain powder A;10% potassium humate is crushed to 50~100 mesh and obtains powdery Thing B, carries out pelletize after powder A and powder B and 50% kieselguhr, 24.945% white carbon being sufficiently mixed, finally prepares 0.055% diazinon pyraclostrobin fertilizer granules.
Example of formulations 2-2
0.005% diazinon, 0.1% pyraclostrobin, 20% binding agent, 34.895% filler are pulverized and mixed 25% copper sulfate, 20% potassium humate is crushed to 50~100 mesh and obtains powder B, carries out pelletize, finally after being sufficiently mixed by powder A and powder B Prepare 0.105% diazinon pyraclostrobin fertilizer granules.
Example of formulations 2-3
0.19% diazinon, 0.01% pyraclostrobin, 8% Colophonium are pulverized and mixed 35% Borax be crushed to 50~100 mesh and obtain powder Shape thing B, carries out pelletize after powder A and powder B and 26.8% kieselguhr, 30% stone powder being sufficiently mixed, finally prepares 0.2% Diazinon pyraclostrobin fertilizer granules.
Example of formulations 2-4
By 0.03% diazinon, 0.05% pyraclostrobin, 1% gelatinized starch is pulverized and mixed 40% potassium nitrate, 50% Borax is crushed to 50~100 mesh obtain powder B, carry out pelletize, finally prepare after powder A and powder B and 8.92% white carbon being sufficiently mixed 0.08% diazinon pyraclostrobin fertilizer granules.
Example of formulations 2-5
By 0.001% diazinon, 1% pyraclostrobin, 4% xanthan gum is pulverized and mixed 40% manganese sulfate, 20% Diammonium phosphate (DAP) is crushed to 50~100 mesh obtain powder B, carry out pelletize, finally make after powder A and powder B and 34.999% kieselguhr being sufficiently mixed Obtain 1.001% diazinon pyraclostrobin fertilizer granules.
Example of formulations 2-6
1% diazinon, 0.001% pyraclostrobin, 6% polyglutamic acid are pulverized and mixed 20% APP, 20% organic pulverizing Obtain powder B to 50~100 mesh, after powder A and powder B and 52.999% Kaolin being sufficiently mixed, carry out pelletize, finally Prepare 1.001% diazinon pyraclostrobin fertilizer granules.
The fertilizer granules embodiment that example of formulations 3 diazinon is compounding with CGA-173506.
Example of formulations 3-1
Fully absorption after 0.005% diazinon, 0.01% CGA-173506,1% methylcellulose being pulverized and mixed, by mixing after absorption Compound is crushed to 50~100 mesh through pulverizer and obtains powder A;10% aminoacid powder is broken to 50~100 mesh and obtains powder B, will Powder A and powder B and 88.985% starch carry out pelletize after being sufficiently mixed, final prepared 0.015% diazinon CGA-173506 Fertilizer granules.
Example of formulations 3-2
Fully absorption after 0.25% diazinon, 0.005% CGA-173506,5% binding agent being pulverized and mixed, by the mixture after absorption It is crushed to 50~100 mesh through pulverizer and obtains powder A;420% calcium nitrate, 25% potassium humate are crushed to 50~100 mesh and obtain Powder B, carries out pelletize after powder A and powder B and 49.745% quartz sand being sufficiently mixed, and final prepared 0.255% 2 Piperazine phosphorus CGA-173506 fertilizer granules.
Example of formulations 3-3
Fully absorption after 0.03% diazinon, 0.05% CGA-173506,7% binding agent being pulverized and mixed, by the mixture warp after absorption Cross pulverizer to be crushed to 50~100 mesh and obtain powder A;40% carbamide, 30% copper sulfate, 20% potassium dihydrogen phosphate are crushed to 50~ 100 mesh obtain powder B, carry out pelletize, finally prepare 0.08% after powder A and powder B and 2.92% stone powder being sufficiently mixed Diazinon CGA-173506 fertilizer granules.
Example of formulations 3-4
Fully absorption after 0.1% diazinon, 0.1% CGA-173506,12% sodium hydroxyl cellulose being pulverized and mixed, by mixing after absorption Compound is crushed to 50~100 mesh through pulverizer and obtains powder A;30% boric acid, 30% aminoacid powder are broken to 50~100 mesh and obtain powder Shape thing B, carries out pelletize after powder A and powder B and 27.8% starch being sufficiently mixed, and final 0.2% diazinon for preparing is coughed up Bacterium nitrile fertilizer granules.
Example of formulations 3-5
Fully absorption after 0.001% diazinon, 1% CGA-173506,20% Colophonium being pulverized and mixed, passes through the mixture after absorption Pulverizer is crushed to 50~100 mesh and obtains powder A;20% dipotassium hydrogen phosphate is crushed to 50~100 mesh and obtains powder B, by powdery Thing A and powder B and 58.999% white carbon carry out pelletize after being sufficiently mixed, final prepared 1.001% diazinon CGA-173506 medicine Fertilizer granular formulation.
Example of formulations 3-6
Fully absorption after 1% diazinon, 0.001% CGA-173506,8% paraffin being pulverized and mixed, by the mixture after absorption through powder Broken machine is crushed to 50~100 mesh and obtains powder A;30% potassium chloride, 20% ammonium sulfate are crushed to 50~100 mesh and obtain powder B, will Powder A and powder B and 40.999% kieselguhr carry out pelletize after being sufficiently mixed, and final 1.001% diazinon for preparing coughs up bacterium Nitrile fertilizer granules.
Example of formulations 4 Diacloden and the fertilizer granules embodiment of azoxystrobin compound.
Example of formulations 4-1
Fully absorption after 0.1% Diacloden, 0.05% Fluoxastrobin, 20% xanthan gum being pulverized and mixed, by the mixture warp after absorption Cross pulverizer to be crushed to 50~100 mesh and obtain powder A;10% potassium nitrate, 10% zinc sulfate are crushed to 50~100 mesh and obtain powder B, carries out pelletize after powder A and powder B and 59.85% kieselguhr being sufficiently mixed, and final prepared 0.15% Diacloden is phonetic Bacterium ester fertilizer granules.
Example of formulations 4-2
Fully absorption after 0.004% Diacloden, 0.01% Fluoxastrobin, 8% Colophonium being pulverized and mixed, by the mixture warp after absorption Cross pulverizer to be crushed to 50~100 mesh and obtain powder A;30% ammonium molybdate, 10% ferrous sulfate are crushed to 50~100 mesh and obtain powdery Thing B, carries out pelletize after powder A and powder B and 51.986% white carbon being sufficiently mixed, final prepared 0.014% thiophene worm Piperazine Fluoxastrobin fertilizer granules.
Example of formulations 4-3
Fully absorption after 0.03% Diacloden, 0.05% Fluoxastrobin, 7% polyglutamic acid being pulverized and mixed, by the mixture after absorption It is crushed to 50~100 mesh through pulverizer and obtains powder A;35% dipotassium hydrogen phosphate, 25% APP, 30% potassium nitrate are pulverized Obtain powder B to 50~100 mesh, carry out pelletize after powder A and powder B and 2.92% kieselguhr being sufficiently mixed, finally make Obtain 0.08% Diacloden Fluoxastrobin fertilizer granules.
Example of formulations 4-4
Fully absorption after 0.04% Diacloden, 0.4% Fluoxastrobin, 12% xanthan gum being pulverized and mixed, by the mixture warp after absorption Cross pulverizer to be crushed to 50~100 mesh and obtain powder A;10% zinc sulfate is crushed to 50~100 mesh and obtains powder B, by powder A and powder B and 77.56% Kaolin carry out pelletize after being sufficiently mixed, fertile of final prepared 0.44% Diacloden Fluoxastrobin medicine Granule.
Example of formulations 4-5
Fully absorption after 0.001% Diacloden, 1% Fluoxastrobin, 4% gelatinized starch being pulverized and mixed, by the mixture warp after absorption Cross pulverizer to be crushed to 50~100 mesh and obtain powder A;15% potassium nitrate, 15% magnesium sulfate are crushed to 50~100 mesh and obtain powder B, carries out pelletize after powder A and powder B and 64.999% quartz sand being sufficiently mixed, final prepared 1.001% Diacloden Fluoxastrobin fertilizer granules.
Example of formulations 4-6
Fully absorption after 1% Diacloden, 0.001% Fluoxastrobin, 15% xanthan gum being pulverized and mixed, by the mixture warp after absorption Cross pulverizer to be crushed to 50~100 mesh and obtain powder A;20% potassium chloride, 30% APP are crushed to 50~100 mesh and obtain powdery Thing B, carries out pelletize after powder A and powder B and 33.999% stone powder being sufficiently mixed, final prepared 1.001% Diacloden Fluoxastrobin fertilizer granules.
The fertilizer granules embodiment that example of formulations 5 Diacloden is compounding with pyraclostrobin.
Example of formulations 5-1
Fully absorption after 0.01% Diacloden, 0.01% pyraclostrobin, 1% methylcellulose being pulverized and mixed, after absorption Mixture is crushed to 50~100 mesh through pulverizer and obtains powder A;15% calcium nitrate, 10% potassium humate are crushed to 50~100 Mesh obtains powder B, carries out pelletize, finally prepare 0.02% after powder A and powder B and 73.98% white carbon being sufficiently mixed Diacloden pyraclostrobin fertilizer granules.
Example of formulations 5-2
Fully absorption after 0.008% Diacloden, 0.02% pyraclostrobin, 10% paraffin being pulverized and mixed, by the mixing after absorption Thing is crushed to 50~100 mesh through pulverizer and obtains powder A;20% potassium nitrate, 30% aminoacid powder are broken to 50~100 mesh and obtain powder Shape thing B, carries out pelletize after powder A and powder B and 39.972% kieselguhr being sufficiently mixed, final prepared 0.028% thiophene worm Piperazine pyraclostrobin fertilizer granules.
Example of formulations 5-3
Fully absorption after 0.03% Diacloden, 0.05% pyraclostrobin, 8% gelatinized starch being pulverized and mixed, by mixing after absorption Compound is crushed to 50~100 mesh through pulverizer and obtains powder A;By 30% zinc sulfate, 40% organic, 20% potassium dihydrogen phosphate It is broken to 50~100 mesh and obtains powder B, carry out pelletize after powder A and powder B and 1.92% stone powder being sufficiently mixed, finally make Obtain 0.08% Diacloden pyraclostrobin fertilizer granules.
Example of formulations 5-4
Fully absorption after 0.5% Diacloden, 0.5% pyraclostrobin, 6% binding agent being pulverized and mixed, by the mixture after absorption It is crushed to 50~100 mesh through pulverizer and obtains powder A;10% APP is crushed to 50~100 mesh and obtains powder B, by powder Shape thing A and powder B and 83% kieselguhr carry out pelletize after being sufficiently mixed, and final prepared 1% Diacloden pyraclostrobin medicine is fertile Granule.
Example of formulations 5-5
Fully absorption after 0.001% Diacloden, 1% pyraclostrobin, 20% polyglutamic acid being pulverized and mixed, by mixing after absorption Compound is crushed to 50~100 mesh through pulverizer and obtains powder A;40% manganese sulfate, 20% disodiumedetate are crushed to 50~100 mesh obtain powder B, carry out pelletize, finally make after powder A and powder B and 18.999% kieselguhr being sufficiently mixed Obtain 1.001% Diacloden pyraclostrobin fertilizer granules.
Example of formulations 5-6
Fully absorption after 1% Diacloden, 0.001% pyraclostrobin, 4% gelatinized starch being pulverized and mixed, by the mixing after absorption Thing is crushed to 50~100 mesh through pulverizer and obtains powder A;40% Diammonium phosphate (DAP), 10% aminoacid powder are broken to 50~100 mesh and obtain Powder B, carries out pelletize after powder A and powder B and 44.999% Kaolin being sufficiently mixed, final prepared 1.001% thiophene Worm piperazine pyraclostrobin fertilizer granules.
The fertilizer granules embodiment that example of formulations 6 Diacloden is compounding with CGA-173506.
Example of formulations 6-1
Fully absorption after 0.01% Diacloden, 0.04% CGA-173506,5% xanthan gum being pulverized and mixed, by the mixture warp after absorption Cross pulverizer to be crushed to 50~100 mesh and obtain powder A;10% bean cake powder is broken to 50~100 mesh and obtains powder B, by powder A Pelletize is carried out, final prepared 0.05% Diacloden CGA-173506 medicine fertilizer granule after being sufficiently mixed with powder B and 84.95% quartz sand Agent.
Example of formulations 6-2
Fully absorption after 0.005% Diacloden, 0.01% CGA-173506,20% sodium hydroxyl cellulose being pulverized and mixed, after absorption Mixture is crushed to 50~100 mesh through pulverizer and obtains powder A;30% magnesium sulfate, 30% ammonium molybdate are crushed to 50~100 mesh Obtain powder B, after powder A and powder B and 19.985% stone powder being sufficiently mixed, carry out pelletize, final prepared 0.015% thiophene Worm piperazine CGA-173506 fertilizer granules.
Example of formulations 6-3
Fully absorption after 0.004% Diacloden, 0.004% CGA-173506,10% Colophonium being pulverized and mixed, by the mixture after absorption It is crushed to 50~100 mesh through pulverizer and obtains powder A;40% MAP is crushed to 50~100 mesh and obtains powder B, by powder Shape thing A and powder B and 49.992% starch carry out pelletize after being sufficiently mixed, final prepared 0.008% Diacloden CGA-173506 medicine Fertilizer granular formulation.
Example of formulations 6-4
Fully absorption after 0.03% Diacloden, 0.05% CGA-173506,1% methylcellulose being pulverized and mixed, by the mixing after absorption Thing is crushed to 50~100 mesh through pulverizer and obtains powder A;40% APP, 20% calcium nitrate, 30% carbamide are crushed to 50 ~100 mesh obtain powder B, carry out pelletize after powder A and powder B and 8.92% white carbon being sufficiently mixed, finally prepare 0.08% Diacloden CGA-173506 fertilizer granules.
Example of formulations 6-5
Fully absorption after 0.001% Diacloden, 1% CGA-173506,14% xanthan gum being pulverized and mixed, by the mixture warp after absorption Cross pulverizer to be crushed to 50~100 mesh and obtain powder A;25% manganese sulfate, 15% potassium humate are crushed to 50~100 mesh and obtain powdery Thing B, carries out pelletize after powder A and powder B and 44.999% kieselguhr being sufficiently mixed, final prepared 1.001% thiophene worm Piperazine CGA-173506 fertilizer granules.
Example of formulations 6-6
Fully absorption after 1% Diacloden, 0.001% CGA-173506,6% polyglutamic acid being pulverized and mixed, by the mixture warp after absorption Cross pulverizer to be crushed to 50~100 mesh and obtain powder A;20% Diammonium phosphate (DAP), 30% ferrous sulfate are crushed to 50~100 mesh and obtain powder Shape thing B, carries out pelletize after powder A and powder B and 42.999% Kaolin being sufficiently mixed, final prepared 1.001% thiophene worm Piperazine CGA-173506 fertilizer granules.
Biological Examples
Application example of formulations 1-2, the fertilizer granules thing of 2-3,3-2,4-2,5-2,6-3 use one in Different Crop sowing time Secondary, preparation dosage is 5kg/ mu.
Choosing 6 comparative examples, these 6 comparative example's dosage forms are suspension seed-coating agent, and method of application is seed pelleting. Test group and in the matched group after planting regular period investigate emergence rate.The medicine fertilizer matched group of comparative example 1-6 is raw crop The long later stage every mu imposes carbamide 20kg, the investigation preventive effect to pest and disease damage, investigation statistics output condition during results.
Wheat Diseases And Insect Pests field test results prevented and treated by table 1
Brassica campestris L pest and disease damage field test results prevented and treated by table 2
Semen arachidis hypogaeae pest and disease damage field test results prevented and treated by table 3
Potato disease insect pest field test results prevented and treated by table 4
Corn diseases and insect pests field test results prevented and treated by table 5
Above-mentioned field test results shows, the fertilizer granules of the present invention is used in crop sowing time, compared with control treatment, Crop subterranean pest-insect and rhizome portion disease had higher prevention effect.Except prevention and elimination of disease and pests, also there is effect of fertilising, After using the fertilizer granules of the present invention, crop growing state is vigorous, and leaf color is dark green, and embodiment respectively processes all than matched group growth Good.
From interpretation of result, the fertilizer granules of the present invention, on the one hand play the effect of fertilizer, promoted that plant growth is sent out Educate, improve crop yield, on the other hand enhance the prevention effect to subterranean pest-insect and other pest and disease damages, reduce dosage and Fertilizer application amount.Simultaneously, it is only necessary to dispenser once, reaches the purpose of time and labour saving.
In sum, the fertilizer granules that the present invention provides, active height, good drug efficacy, fertilizer efficiency are notable, possess medicine, fertilizer Double effects, it is possible to give full play to the effect of parasite killing, sterilization, weight gaining, is not likely to produce the features such as resistance, and to crop safety, executes By simplicity, dosage is few, and effective drug duration is long, has effectively saved the Productive statistics of peasant, has improve crop yield, in agricultural Production has a wide range of applications.
Below it is only the preferred embodiment of the present invention, it is noted that it is right that above-mentioned preferred implementation is not construed as The restriction of the present invention, protection scope of the present invention should be as the criterion with claim limited range.For the art For those of ordinary skill, without departing from the spirit and scope of the present invention, it is also possible to make some improvement, these improve and also should It is considered as protection scope of the present invention.

Claims (7)

1. fertilizer granules and preparation method thereof, it is characterised in that this fertilizer granules is by insecticide, antibacterial, fertilizer And auxiliary agent composition, insecticide is selected from diazinon, Diacloden, imidacloprid, clothianidin, chlopyrifos, phoxim, carbofuran, fourth sulfur gram One or more in Budweiser, antibacterial selected from Fluoxastrobin, pyraclostrobin, CGA-173506, Metalaxyl-M, furan azoles bacterium aniline, One or more in thifluzamide, Mancozeb, fertilizer selected from carbamide, ammonium sulfate, potassium sulfate, potassium chloride, MAP, Diammonium phosphate (DAP), potassium dihydrogen phosphate, dipotassium hydrogen phosphate, APP, potassium nitrate, zinc sulfate, manganese sulfate, magnesium sulfate, Borax, boron Acid, ferrous sulfate, copper sulfate, ammonium molybdate, disodiumedetate, calcium nitrate, potassium humate, organic matter, aminoacid, bean cake In one or more.
Fertilizer granules and preparation method thereof the most according to claim 1, it is characterised in that insecticide be preferably diazinon, One or more in Diacloden, antibacterial is preferably one or more in Fluoxastrobin, pyraclostrobin, CGA-173506.
Fertilizer granules and preparation method thereof the most according to claim 1, it is characterised in that auxiliary agent is by binding agent and filler group Becoming, wherein binding agent is in sodium hydroxyl cellulose, xanthan gum, gelatinized starch, paraffin, polyglutamic acid, methylcellulose, Colophonium One or more, one or more in Kaolin, kieselguhr, white carbon, starch, stone powder, the quartz sand etc. of filler.
Fertilizer granules and preparation method thereof the most according to claim 1, it is characterised in that by the parasite killing of 0.001%~1% The antibacterial of agent, 0.001%~1% and 1%~20% binding agent be pulverized and mixed after fully absorption, by the mixture warp after absorption Cross pulverizer to be crushed to 50~100 mesh and obtain powder A;The fertilizer of 10%~90% is crushed to 50~100 mesh and obtains powder B, will Powder A and powder B and surplus filler carry out pelletize after being sufficiently mixed, and finally prepare fertilizer granules.
Fertilizer granules and preparation method thereof the most according to claim 1, it is characterised in that this fertilizer granules is broadcast in crop The phase of kind uses.
Fertilizer granules and preparation method thereof the most according to claim 1, it is characterised in that this fertilizer granules is used for preventing and treating Crop subterranean pest-insect and rhizome portion disease.
Fertilizer granules and preparation method thereof the most according to claim 1, it is characterised in that this fertilizer granules was using Journey can use spread fertilizer over the fields, the farming mode of operation of ditch spread.
CN201610283053.8A 2016-05-03 2016-05-03 Insecticide-fertilizer particulate agent and preparation method thereof Pending CN105948961A (en)

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CN106397000A (en) * 2016-12-02 2017-02-15 河南力浮科技有限公司 Production method of special controlled release seed dressing insecticide-fertilizer for wheat
CN106916019A (en) * 2017-04-07 2017-07-04 河北德瑞化工有限公司 Tobacco special fertiliser granulates agent and its preparation method and application containing sustained-release pesticides
CN107011033A (en) * 2017-04-07 2017-08-04 河北德瑞化工有限公司 Sweet potato and potato special fertiliser granulates agent and preparation method and application containing sustained-release pesticides
CN107232246A (en) * 2017-07-27 2017-10-10 苏州星川园艺绿化有限公司 A kind of insecticide of garderning green
CN107500886A (en) * 2017-09-10 2017-12-22 惠州市欧野科技有限公司 A kind of fertilizer granules for preventing and treating radish aphid
CN107721572A (en) * 2017-10-20 2018-02-23 成都盛世光华生物科技有限公司 A kind of significant fire works of sequoia tree nutrient solution of using effect and its application
CN107805106A (en) * 2017-12-22 2018-03-16 苏州萨瑟斯兰环境科技有限公司 A kind of ecological fertilizer and preparation method thereof
CN107827624A (en) * 2017-12-20 2018-03-23 青岛住商中农肥料有限公司 A kind of Synergistic slow release urea and its preparation technology
CN107973641A (en) * 2017-11-30 2018-05-01 惠州市梦芭迪工业产品设计中心(普通合伙) A kind of Bactericide fertilizer composition
CN108077258A (en) * 2017-12-28 2018-05-29 四川省农业科学院生物技术核技术研究所 A kind of granule of biocontrol of mango bacterial disease and preparation method thereof
CN108651473A (en) * 2018-06-19 2018-10-16 陕西标正作物科学有限公司 The effectively fertilizer granules of prevention soil-borne disease and plant disease
CN110150310A (en) * 2019-05-13 2019-08-23 河南瀚斯作物保护有限公司 A kind of seed treatment compositions and its application containing imidacloprid, fludioxonil and Fluoxastrobin
CN112250508A (en) * 2020-11-03 2021-01-22 中诚国联(河南)生物科技有限公司 Preparation method and application of pesticide-fertilizer granules containing thifluzamide and azoxystrobin
CN112273392A (en) * 2020-11-03 2021-01-29 中诚国联(河南)生物科技有限公司 Application of insecticide-fertilizer granules containing clothianidin and imidacloprid in controlling peanut grubs
CN112956480A (en) * 2021-02-04 2021-06-15 四川眉山凯尔化工有限公司 Pesticide raw material formula
CN113142212A (en) * 2021-03-24 2021-07-23 河南省农业科学院粮食作物研究所 Millet compound seed dressing agent with disease resistance, growth promotion and yield increase functions and preparation method thereof
CN113558063A (en) * 2021-08-10 2021-10-29 黑龙江省大地丰农业科技开发有限公司 Seed coating agent for preventing and treating soybean root rot and soil insects and preparation method thereof
CN114230395A (en) * 2021-12-16 2022-03-25 河北安格诺农化有限公司 Slow-release pesticide-fertilizer composition and application thereof
CN114831123A (en) * 2022-06-08 2022-08-02 安徽丰乐农化有限责任公司 Pesticide fertilizer composition and application thereof

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CN103058789A (en) * 2012-12-29 2013-04-24 广东中迅农科股份有限公司 Cartap fertilizer granules and preparation method thereof
CN103058790A (en) * 2012-12-29 2013-04-24 广东中迅农科股份有限公司 Cyfluthrin drug fertilizer granules and preparation method thereof
CN103058767A (en) * 2012-12-29 2013-04-24 广东中迅农科股份有限公司 Flubendiamide drug fertilizer granules and preparation method thereof
CN103864516A (en) * 2014-03-07 2014-06-18 湖南神隆超级稻丰产工程有限公司 Special multi-resistance drug fertilizer for super rice and preparation method thereof
CN104522045A (en) * 2014-12-03 2015-04-22 联保作物科技有限公司 Pesticide composition, sustained-release pesticidal fertilizer, and preparation methods thereof
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Publication number Priority date Publication date Assignee Title
CN106397000A (en) * 2016-12-02 2017-02-15 河南力浮科技有限公司 Production method of special controlled release seed dressing insecticide-fertilizer for wheat
CN106916019A (en) * 2017-04-07 2017-07-04 河北德瑞化工有限公司 Tobacco special fertiliser granulates agent and its preparation method and application containing sustained-release pesticides
CN107011033A (en) * 2017-04-07 2017-08-04 河北德瑞化工有限公司 Sweet potato and potato special fertiliser granulates agent and preparation method and application containing sustained-release pesticides
CN107232246A (en) * 2017-07-27 2017-10-10 苏州星川园艺绿化有限公司 A kind of insecticide of garderning green
CN107500886A (en) * 2017-09-10 2017-12-22 惠州市欧野科技有限公司 A kind of fertilizer granules for preventing and treating radish aphid
CN107721572A (en) * 2017-10-20 2018-02-23 成都盛世光华生物科技有限公司 A kind of significant fire works of sequoia tree nutrient solution of using effect and its application
CN107973641A (en) * 2017-11-30 2018-05-01 惠州市梦芭迪工业产品设计中心(普通合伙) A kind of Bactericide fertilizer composition
CN107827624A (en) * 2017-12-20 2018-03-23 青岛住商中农肥料有限公司 A kind of Synergistic slow release urea and its preparation technology
CN107805106A (en) * 2017-12-22 2018-03-16 苏州萨瑟斯兰环境科技有限公司 A kind of ecological fertilizer and preparation method thereof
CN108077258A (en) * 2017-12-28 2018-05-29 四川省农业科学院生物技术核技术研究所 A kind of granule of biocontrol of mango bacterial disease and preparation method thereof
CN108651473A (en) * 2018-06-19 2018-10-16 陕西标正作物科学有限公司 The effectively fertilizer granules of prevention soil-borne disease and plant disease
CN110150310A (en) * 2019-05-13 2019-08-23 河南瀚斯作物保护有限公司 A kind of seed treatment compositions and its application containing imidacloprid, fludioxonil and Fluoxastrobin
CN112250508A (en) * 2020-11-03 2021-01-22 中诚国联(河南)生物科技有限公司 Preparation method and application of pesticide-fertilizer granules containing thifluzamide and azoxystrobin
CN112273392A (en) * 2020-11-03 2021-01-29 中诚国联(河南)生物科技有限公司 Application of insecticide-fertilizer granules containing clothianidin and imidacloprid in controlling peanut grubs
CN112956480A (en) * 2021-02-04 2021-06-15 四川眉山凯尔化工有限公司 Pesticide raw material formula
CN113142212A (en) * 2021-03-24 2021-07-23 河南省农业科学院粮食作物研究所 Millet compound seed dressing agent with disease resistance, growth promotion and yield increase functions and preparation method thereof
CN113558063A (en) * 2021-08-10 2021-10-29 黑龙江省大地丰农业科技开发有限公司 Seed coating agent for preventing and treating soybean root rot and soil insects and preparation method thereof
CN114230395A (en) * 2021-12-16 2022-03-25 河北安格诺农化有限公司 Slow-release pesticide-fertilizer composition and application thereof
CN114230395B (en) * 2021-12-16 2022-12-06 河北安格诺农化有限公司 Slow-release pesticide-fertilizer composition and application thereof
CN114831123A (en) * 2022-06-08 2022-08-02 安徽丰乐农化有限责任公司 Pesticide fertilizer composition and application thereof

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Application publication date: 20160921