CN105919074A - Processing and making method of brewing powder and brewing powder processed and made by processing and making method - Google Patents

Processing and making method of brewing powder and brewing powder processed and made by processing and making method Download PDF

Info

Publication number
CN105919074A
CN105919074A CN201610256957.1A CN201610256957A CN105919074A CN 105919074 A CN105919074 A CN 105919074A CN 201610256957 A CN201610256957 A CN 201610256957A CN 105919074 A CN105919074 A CN 105919074A
Authority
CN
China
Prior art keywords
parts
powder
emulsion
starch
brewing powder
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201610256957.1A
Other languages
Chinese (zh)
Other versions
CN105919074B (en
Inventor
陈洁
孟春雨
何志勇
曾茂茂
秦昉
张爽
陶冠军
王林祥
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangnan University
Original Assignee
Jiangnan University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiangnan University filed Critical Jiangnan University
Priority to CN201610256957.1A priority Critical patent/CN105919074B/en
Publication of CN105919074A publication Critical patent/CN105919074A/en
Application granted granted Critical
Publication of CN105919074B publication Critical patent/CN105919074B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Landscapes

  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The invention discloses a processing and making method of brewing powder and brewing powder processed and made by the processing and making method. The processing and making method of the brewing powder comprises the following steps of preparing W/O emulsion, preparing W/O/W emulsion, and performing spray drying so as to obtain the brewing powder with a low blood sugar index. According to the brewing powder disclosed by the invention, fructo-oligosaccharide and xylitol are used as a composite sweetening agent, so that excessive absorption of the xylitol is avoided, and the mouth feel of the brewing powder is improved. The brewing powder disclosed by the invention meets the requirements of human bodies for energy and nutrition, wherein various function factors for reducing blood sugar are in synergistic reaction, after the function factors are absorbed, the efficacy of slowly raising the blood sugar is achieved, and the brewing powder can become the first choice of meal replacement foods for crowds suffering from high blood sugar.

Description

A kind of processing method reconstituting powder and reconstitute powder
Technical field
The invention belongs to food processing technology field, relate to a kind of packed slow glycemic full nutrition and reconstitute the processing of powder Manufacture method and slow blood glucose increasing product.
Background technology
At present, it is suitable for the edible product of the hyperglycemia population such as diabetes and is broadly divided into three major types: plant extract, Vitamin inorganic salts health promoting product and sugar-free starch based product.First two product has and improves diabetes Shape, reduction post-prandial glycemia effect, but diabetes patient's normal energetic requirements cannot be met, auxiliary only as dinner Help food.Sugar-free starch based product is mainly characterized by high dietary-fiber, high protein, by sucrose, glucose etc. Easily blood glucose increasing raw-food material sugar alcohol replaces, such as sugar-free biscuit, sugar-free bread, sugar-free soybean milk etc., but sugar alcohol Excess free enthalpy be easily caused abdominal distention, diarrhoea.
Tea polysaccharide (Tea Polysaccharides, TPS) is that tea Ye Zhongyi class is together with protein bound Acidic polysaccharose or a kind of acidoglycoprotein, have enhancing immunity, blood fat reducing, blood sugar lowering, radioprotective, resist The effect such as blood clotting, antithrombotic, the most prominent function is blood sugar lowering, and another kind of main physiologically active becomes Dividing is tea polyphenols, and the most both at home and abroad about tea polysaccharide, the hypoglycemic report of tea polyphenols is a lot.But owing to tea is many The bitterness of phenol etc. self, when adding too much in food, can have a strong impact on taste of food and cause mouthfeel not Good, and on the other hand, when in food, tea polyphenols addition is very few, its given efficacy that can reach micro-its Micro-.
Summary of the invention
The purpose of this part is summarize some aspects of embodiments of the invention and briefly introduce some relatively Good embodiment.This part and the description of the present application make a summary and denomination of invention may be done a little simplify or Omit to avoid making the purpose of this part, specification digest and denomination of invention to obscure, and this simplification or omission Cannot be used for limiting the scope of the present invention.
In view of above-mentioned and/or existing full nutrition and hypoglycemic can reconstitute powder, preparation method thereof and reconstitute in powder The problem existed, it is proposed that the present invention.
Therefore, it is an object of the invention to improve the brew of starch based material, it is provided that a kind of powder that reconstitutes Processing method, provides a kind of full nutrition especially and hypoglycemic can reconstitute the preparation method of powder.
For solving above-mentioned technical problem, the technical scheme is that a kind of processing system reconstituting powder Making method, it includes, the preparation of W/O emulsion: by 45~55 parts of starch and 5~15 parts of high straight-chain maizes Starch dispersion makes cold starch solution in water, 0.03~0.07 part of sucrose ester and 0.03~0.07 part of molecule is steamed Evaporate monoglyceride composite emulsifier to be dissolved in 10~15 portions of Oleum Helianthis, and add 0.1~0.3 under nitrogen protection Part conjugated linoleic acid, 45~55 DEG C of stirring 20~40min formation oil-based systems, by described cold starch solution dropwise Adding in described oil-based system, stirring 20~40min forms stable W/O emulsion;W/O/W emulsus The preparation of liquid: be added to the water by 10~20 parts of lactalbumins, stirs to being completely dissolved and obtains lactalbumin water Solution, is slowly added to the described W/O emulsion prepared in described aqueous whey protein solution, persistently stirs Mix rear homogenizing;It is spray-dried: inlet temperature 130 DEG C~170 DEG C, outlet temperature 65~75 DEG C, to W/O/W Emulsion is dried, general's spray drying gained powder and oligofructose 4~5 parts, xylitol 3.5~4 parts, Semen sojae atricolor powdery phosphatidase 1 .5~2.5 parts, potassium chloride 1~1.5 parts, calcium carbonate 1~1.5 parts, magnesium sulfate 1~1.2 parts, Konjac glucomannan 0.1~0.8 part, sodium chloride 0.1~0.2 part, Calcium peptide of casein 0.1~0.3 part, tea polyphenols 0.4~0.8 Part, tea polysaccharide 0.4~0.8 part, compound vitamin 0.1~0.3 part, sodium erythorbate 0.1~0.3 part, cattle Sulfonic acid 0.01~0.05 part, ascorbyl palmitate 0.01~0.05 part, ferrous sulfate 0.01~0.05 part, Zinc sulfate 0.01~0.02 part, manganese sulfate 0.003~0.007 part, chromium picolinate 0.001~0.005 part, phosphoric acid Trisodium 0.001~0.005 part of mixing bag distribution packaging after microwave disinfection, products obtained therefrom is low-glycemic Reconstitute powder.
As a kind of preferred version of the processing method reconstituting powder of the present invention, wherein: described After spray drying step, also include, the described powder that reconstitutes is carried out micronizing so that being crushed to particle diameter is The subparticle of 15~20 μm.
As a kind of preferred version of the processing method reconstituting powder of the present invention, wherein: described shallow lake Powder includes one or more in corn starch, pea starch, green starch.
As a kind of preferred version of the processing method reconstituting powder of the present invention, wherein: described spray During mist is dried, its charging rate is 7.5ml/min~8.5ml/min.
As a kind of preferred version of the processing method reconstituting powder of the present invention, wherein: described In the preparation of W/O emulsion, by 0.05 part of sucrose ester and 0.05 part of molecule distillating monoglyceride composite emulsifier It is dissolved in 13 portions of Oleum Helianthis.
As a kind of preferred version of the processing method reconstituting powder of the present invention, wherein: described In the preparation of W/O/W emulsion, in terms of mass parts, wherein tea polyphenols 0.4 part, tea polysaccharide 0.4 part.
It is a further object to provide a kind of processing system reconstituting powder according to packed slow glycemic full nutrition The slow blood glucose increasing product prepared as method.
For solving above-mentioned technical problem, the technical scheme is that one reconstitutes powder, with quality Part meter, including, pea starch 45~55 parts, amylomaize 5~15 parts, sucrose ester 0.03~0.07 Part, molecule distillating monoglyceride composite emulsifier 0.03~0.07 part, Oleum Helianthi 10~15 parts, the sub-oil of conjugation Acid 0.1~0.3 part, lactalbumin 10~20 parts, oligofructose 4~5 parts, xylitol 3.5~4 parts, Semen sojae atricolor Powdered phospholipid 1.5~2.5 parts, potassium chloride 1~1.5 parts, calcium carbonate 1~1.5 parts, magnesium sulfate 1~1.2 parts, evil spirit Taro glue 0.1~0.8 part, sodium chloride 0.1~0.2 part, Calcium peptide of casein 0.1~0.3 part, tea polyphenols 0.4~0.6 part, Tea polysaccharide 0.4~0.6 part, compound vitamin 0.1~0.3 part, sodium erythorbate 0.1~0.3 part, taurine 0.01~0.05 part, ascorbyl palmitate 0.01~0.05 part, ferrous sulfate 0.01~0.05 part, zinc sulfate 0.01~0.02 part, manganese sulfate 0.003~0.007 part, chromium picolinate 0.001~0.005 part, tertiary sodium phosphate 0.001~0.005 part.
As a kind of preferred version of the processing method reconstituting powder of the present invention, wherein: with efficiently The gas chromatogram reconstituting the content containing catechin in powder and use silicon ether derivant of liquid chromatography for measuring The ratio of the arabinose content that method measures is 0.56~0.80.
Product utilization oligofructose of the present invention and xylitol, as composite sweetener, had both avoided the mistake of xylitol Amount is taken in and is improved again products taste.Product of the present invention meets energy and the nutritional need of needed by human body, wherein Multiple function of blood sugar reduction factor synergism, has the effect slowly rising hyperglycemia, can become hyperglycemia after absorption The first-selection of crowd's meal replacing food.
Detailed description of the invention
Understandable for enabling the above-mentioned purpose of the present invention, feature and advantage to become apparent from, below in conjunction with concrete real Execute example the detailed description of the invention of the present invention is described in detail.
Elaborate a lot of detail in the following description so that fully understanding the present invention, but the present invention Other can also be used to be different from alternate manner described here implement, those skilled in the art can be not Doing similar popularization in the case of running counter to intension of the present invention, therefore the present invention is not by following public specific embodiment Restriction.
Secondly, " embodiment " or " embodiment " referred to herein refers to may be included in the present invention at least Special characteristic, structure or characteristic in one implementation.Different in this manual local appearance " In one embodiment " not refer both to same embodiment, it is not single or selective and other enforcements The embodiment that example is mutually exclusive.
Embodiment 1:
Raw material weight proportioning is corn starch 50g, lactalbumin 15g, Oleum Helianthi 13g, high straight-chain maize Starch 10g, oligofructose 4.45g, xylitol 3.68g, Semen sojae atricolor powdery phosphatidase 2 g, Konjac glucomannan 0.5g, altogether Conjugated linoleic acid 0.2g, Calcium peptide of casein 0.16g, tea polyphenols 0.6g, tea polysaccharide 0.5g, compound vitamin 0.1g, Molecular distillation type monoglyceride 0.05g, sucrose ester 0.05g, potassium chloride 1.2g, calcium carbonate 1.2g, magnesium sulfate 1g, Konjac glucomannan 0.5g, sodium chloride 0.16g, Calcium peptide of casein 0.2g, sodium erythorbate 0.2g, taurine 0.03g, Ascorbyl palmitate 0.03g, ferrous sulfate 0.03g, zinc sulfate 0.01g, manganese sulfate 0.005g, pyridine Chromic formate 0.003g, tertiary sodium phosphate 0.003g.
50g corn starch and 10g amylomaize are scattered in 240mL water that to make cold starch molten Liquid.
0.05g sucrose ester and 0.05g molecular distillation type monoglyceride composite emulsifier are dissolved in 13g Oleum Helianthi In, and adding 0.2g conjugated linoleic acid under nitrogen protection, 50 DEG C of magnetic agitation 30min form oil-based system.
Dropwise being added in oil-based system by cold starch solution (starch dispersion liquid), magnetic agitation 30min is formed Stable W/O mixing and emulsifying system.
Being joined by 15g lactalbumin in 200mL water, magnetic agitation is to being completely dissolved.Be added into In W/O mixing and emulsifying system, formed for 2 times with high pressure homogenizer homogenizing after continuously stirred a period of time W/O/W emulsion.
Being spray-dried by W/O/W emulsion: inlet temperature 130 DEG C, outlet temperature 70 DEG C is right W/O/W emulsion is dried, charging rate 7.5ml/min.Spray drying gained powder is killed through microwave Carrying out aseptic mixing and bag distribution packaging with other raw-food materials after bacterium, products obtained therefrom is low-glycemic and reconstitutes Powder.
Embodiment 2:
Raw material weight proportioning is pea starch 45g, lactalbumin 10g, Oleum Helianthi 10g, high straight-chain maize Starch 5g, oligofructose 4g, xylitol 3g, Semen sojae atricolor powdery phosphatidase 2 g, Konjac glucomannan 0.5g, the sub-oil of conjugation Acid 0.2g, Calcium peptide of casein 0.1g, tea polyphenols 0.4g, tea polysaccharide 0.4g, compound vitamin 0.1g, molecule Distillation type monoglyceride 0.05g, sucrose ester 0.05g, potassium chloride 1.0g, calcium carbonate 1.5g, magnesium sulfate 1g, evil spirit Taro glue 0.5g, sodium chloride 0.16g, Calcium peptide of casein 0.2g, sodium erythorbate 0.2g, taurine 0.03g, Ascorbyl palmitate 0.03g, ferrous sulfate 0.03g, zinc sulfate 0.01g, manganese sulfate 0.002g, pyridine Chromic formate 0.005g, tertiary sodium phosphate 0.005g.
50g pea starch and 10g amylomaize are scattered in 240mL water that to make cold starch molten Liquid.
0.05g sucrose ester and 0.05g molecular distillation type monoglyceride composite emulsifier are dissolved in 10g Oleum Helianthi In, and adding 0.2g conjugated linoleic acid under nitrogen protection, 50 DEG C of magnetic agitation 30min form oil-based system.
Dropwise being added in oil-based system by cold starch solution (starch dispersion liquid), magnetic agitation 30min is formed Stable W/O mixing and emulsifying system.
Being joined by 10g lactalbumin in 200mL water, magnetic agitation is to being completely dissolved.Be added into In W/O mixing and emulsifying system, formed for 2 times with high pressure homogenizer homogenizing after continuously stirred a period of time W/O/W emulsion.
Being spray-dried by W/O/W emulsion: inlet temperature 150 DEG C, outlet temperature 70 DEG C is right W/O/W emulsion is dried, charging rate 7.5ml/min.Spray drying gained powder is killed through microwave Carrying out aseptic mixing and bag distribution packaging with other raw-food materials after bacterium, products obtained therefrom is low-glycemic and reconstitutes Powder.
Embodiment 3:
Raw material weight proportioning is green starch 50g, lactalbumin 20g, Oleum Helianthi 13g, high straight-chain maize Starch 10g, oligofructose 5g, xylitol 4g, Semen sojae atricolor powdery phosphatidase 3 g, Konjac glucomannan 0.5g, the sub-oil of conjugation Acid 0.3g, Calcium peptide of casein 0.16g, tea polyphenols 0.6g, tea polysaccharide 0.6g, compound vitamin 0.1g, molecule Distillation type monoglyceride 0.05g, sucrose ester 0.05g, potassium chloride 1.5g, calcium carbonate 1.2g, magnesium sulfate 1g, evil spirit Taro glue 0.7g, sodium chloride 0.2g, Calcium peptide of casein 0.5g, sodium erythorbate 0.2g, taurine 0.03g, Ascorbyl palmitate 0.03g, ferrous sulfate 0.03g, zinc sulfate 0.01g, manganese sulfate 0.007g, pyridine Chromic formate 0.003g, tertiary sodium phosphate 0.007g.
50g green starch and 10g amylomaize are scattered in 240mL water that to make cold starch molten Liquid.
0.05g sucrose ester and 0.05g molecular distillation type monoglyceride composite emulsifier are dissolved in 13g Oleum Helianthi In, and adding 0.2g conjugated linoleic acid under nitrogen protection, 50 DEG C of magnetic agitation 30min form oil-based system.
Dropwise being added in oil-based system by cold starch solution (starch dispersion liquid), magnetic agitation 30min is formed Stable W/O mixing and emulsifying system.
Being joined by 20g lactalbumin in 200mL water, magnetic agitation is to being completely dissolved.Be added into In W/O mixing and emulsifying system, formed for 2 times with high pressure homogenizer homogenizing after continuously stirred a period of time W/O/W emulsion.
Being spray-dried by W/O/W emulsion: inlet temperature 170 DEG C, outlet temperature 70 DEG C is right W/O/W emulsion is dried, charging rate 7.5ml/min.Spray drying gained powder is killed through microwave Carrying out aseptic mixing and bag distribution packaging with other raw-food materials after bacterium, products obtained therefrom is low-glycemic and reconstitutes Powder.
Embodiment 4:
Raw material weight proportioning is corn starch 50g, lactalbumin 12g, Oleum Helianthi 13g, high straight-chain maize Starch 10g, oligofructose 4.45g, xylitol 3.68g, Semen sojae atricolor powdery phosphatidase 2 g, Konjac glucomannan 0.5g, altogether Conjugated linoleic acid 0.3g, Calcium peptide of casein 0.16g, tea polyphenols 0.55g, tea polysaccharide 0.5g, compound vitamin 0.1g, Molecular distillation type monoglyceride 0.05g, sucrose ester 0.05g, potassium chloride 1.0g, calcium carbonate 1.5g, magnesium sulfate 1g, Konjac glucomannan 0.5g, sodium chloride 0.16g, Calcium peptide of casein 0.2g, sodium erythorbate 0.2g, taurine 0.04g, Ascorbyl palmitate 0.03g, ferrous sulfate 0.03g, zinc sulfate 0.01g, manganese sulfate 0.002g, pyridine Chromic formate 0.005g, tertiary sodium phosphate 0.005g.
50g corn starch and 10g amylomaize are scattered in 240mL water that to make cold starch molten Liquid.
0.05g sucrose ester and 0.05g molecular distillation type monoglyceride composite emulsifier are dissolved in 13g Oleum Helianthi In, and adding 0.2g conjugated linoleic acid under nitrogen protection, 50 DEG C of magnetic agitation 30min form oil-based system.
Dropwise being added in oil-based system by cold starch solution (starch dispersion liquid), magnetic agitation 30min is formed Stable W/O mixing and emulsifying system.
Being joined by 12g lactalbumin in 200mL water, magnetic agitation is to being completely dissolved.Be added into In W/O mixing and emulsifying system, formed for 2 times with high pressure homogenizer homogenizing after continuously stirred a period of time W/O/W emulsion.
Being spray-dried by W/O/W emulsion: inlet temperature 150 DEG C, outlet temperature 70 DEG C is right W/O/W emulsion is dried, charging rate 8ml/min.Spray drying gained powder is killed through microwave Carrying out aseptic mixing and bag distribution packaging with other raw-food materials after bacterium, products obtained therefrom is low-glycemic and reconstitutes Powder.
Embodiment 5:
Raw material weight proportioning is corn starch 50g, lactalbumin 13g, Oleum Helianthi 13g, high straight-chain maize Starch 10g, oligofructose 4.45g, xylitol 3.68g, Semen sojae atricolor powdery phosphatidase 2 g, Konjac glucomannan 0.5g, altogether Conjugated linoleic acid 0.2g, Calcium peptide of casein 0.16g, tea polyphenols 0.45g, tea polysaccharide 0.4g, compound vitamin 0.1g, Molecular distillation type monoglyceride 0.05g, sucrose ester 0.05g, potassium chloride 1.0g, calcium carbonate 1.5g, magnesium sulfate 1g, Konjac glucomannan 0.5g, sodium chloride 0.16g, Calcium peptide of casein 0.2g, sodium erythorbate 0.2g, taurine 0.04g, Ascorbyl palmitate 0.03g, ferrous sulfate 0.03g, zinc sulfate 0.01g, manganese sulfate 0.002g, pyridine Chromic formate 0.005g, tertiary sodium phosphate 0.005g.
50g corn starch and 10g amylomaize are scattered in 240mL water that to make cold starch molten Liquid.
0.05g sucrose ester and 0.05g molecular distillation type monoglyceride composite emulsifier are dissolved in 13g Oleum Helianthi In, and adding 0.2g conjugated linoleic acid under nitrogen protection, 50 DEG C of magnetic agitation 30min form oil-based system.
Dropwise being added in oil-based system by cold starch solution (starch dispersion liquid), magnetic agitation 30min is formed Stable W/O mixing and emulsifying system.
Being joined by 13g lactalbumin in 200mL water, magnetic agitation is to being completely dissolved.Be added into In W/O mixing and emulsifying system, formed for 2 times with high pressure homogenizer homogenizing after continuously stirred a period of time W/O/W emulsion.
Being spray-dried by W/O/W emulsion: inlet temperature 170 DEG C, outlet temperature 70 DEG C is right W/O/W emulsion is dried, charging rate 8.5ml/min.Spray drying gained powder is killed through microwave Carrying out aseptic mixing and bag distribution packaging with other raw-food materials after bacterium, products obtained therefrom is low-glycemic and reconstitutes Powder.
Micronizing of the present invention refers to utilize air-flowing type or mechanical pulverizatio equipment, grinds material Grind, impact, shearing etc., by particle diameter at the subparticle that crushing material to particle diameter is 15~20 μm, ultra micro Material after pulverizing is more convenient for the migration of moisture, is more evenly distributed, it is simple to heterogeneity material divides in material Crosslinking between son, product brew is more preferable.But then, if the meticulous meeting of product particle makes to topple over reconstitute Time material fly upward, to reconstitute effect best for the subparticle of historical facts or anecdotes checking bright 15~20 μm.
Each embodiment of the present invention reconstitutes the discussion of powder powder instant capacity:
(1) water temperature impact on instant capacity is reconstituted: at reconstituting water temperature 40~80 DEG C, reconstitute experiment, Go out the present invention and reconstitute the optimum water temperature of powder, as shown in the table:
Table 1 reconstitutes the water temperature impact on reconstituting powder instant capacity
Conglomeration rate involved in this method of testing is determined by the following procedure: weighs and reconstitutes powder 50g in burning In Bei, add the hot water 400mL of 40~80 DEG C, be sufficiently stirred for 10min, then observe conglomeration, layering now As;Then with 20 eye mesh screens, solution is filtered, rinse caking thing with clear water, put in drying baker and dry To constant weight, band screen cloth is weighed, and deducts screen cloth weight and is the weight of caking thing, and the computing formula of conglomeration rate is such as Under: conglomeration rate (%)=(conglomeration thing weight/coffee beverage powder) × 100.
Knowable to table 1 result of the test, reconstituting water temperature when being 60 DEG C, the instant capacity reconstituting powder is best.Simultaneously Need to consider that reconstituting nutritional labeling contained in powder the most easily decomposes rotten, as being dissolved in 80 DEG C of water, In 10min, polyphenol content will lose 35.4%, so under considering, selecting 60 DEG C for reconstituting powder The optimum water temperature reconstituted.
(2) reconstitute the water yield impact on instant capacity: reconstitute the water yield be reconstitute powder instant capacity important affect because of One of element, selecting to reconstitute the water yield is to reconstitute 4 times of opaque amount, 6 times, 8 times, 10 times, 12 times to try Test, determined the suitableeest water yield reconstituted when powder reconstitutes by subjective appreciation.Results of sensory evaluation shows: when reconstituting When the water yield is reconstitute opaque amount 8 times, mouthfeel is optimal, and the conglomeration formed is minimum.
(3) stabilizer impact on reconstituting powder instant capacity is added: reconstitute rear character instability owing to reconstituting powder, Be susceptible to be layered during reconstituting, unite, the phenomenon such as sink to the bottom, thus by add compound vitamin, The stabilizers such as molecular distillation type monoglyceride are inquired into solution and are reconstituted the stability problem after powder reconstitutes.In the present invention By the test to plurality of stable agent and consumption thereof, reconstituting the best stabilizer of effect is compound vitamin and molecule Distillation type monoglyceride.
With the powder that reconstitutes in distilled water diluting embodiment 1, then after filter (aperture: 0.8 μm) filters, Use high performance liquid chromatography, the liquid chromatograph packed column L-columm importing octadecyl is installedTMODS, At column temperature 35 DEG C, A liquid and B liquid is used to measure the catechins in filtrate according to gradient method.Stream Dynamic phase A liquid is the distilled water solution containing 0.1mol/L acetic acid, and B liquid is the second containing 0.1mol/L acetic acid Nitrile solution, sample injection rate is 20 μ L, and UV detector wavelength is 280nm.
Example 1 reconstitutes powder 2g, is dissolved in 20ml distilled water, and adding ethanol to concentration of alcohol is 70% Time precipitation 24h be centrifuged.In precipitate, add 4ml 2mol/L trifluoroacetic acid make it dissolve and be transferred to glass Sealing in tube sealing, after the 8h that degrades in 100 DEG C of calorstats, glass fiber filter paper filters, in rotary evaporator Concentrating under reduced pressure repeatedly adding water is evaporated under reduced pressure again, takes off removing trifluoroacetic acid, use N to small size2Gas Being blown to without tart flavour, the 4ml that adds water dissolves the monosaccharide of degraded.Respectively take 2.0ml lysate, drip 1 ammonia and 1.0m l inositol (making internal standard), adds sodium borohydride 30mg respectively, shakes up overnight, makes monosaccharide be converted into sugar alcohol, It is separately added into Dowex 50W-X8 (H again+) ion exchange resin, it is acid with decationize to aqueous solution Property.Filtering, filtrate decompression is evaporated, and repeatedly adds methanol and borate is evaporated off totally 5 times.The a little methanol of residue It is transferred in small test tube, uses N2Air-blowing is done, and puts 2d in exsiccator, after being completely dried, adds trimethyl silicane Miaow 0.1ml, fully vibrates, and makes sugar alcohol be converted into silica-ether compound, records me as gas chromatographic analysis Uncle's sugar content.
Test determination, now reconstituting in powder the ratio containing the content of catechin and arabinose content is 0.69. Male mice 10 is selected in experiment, and often group uses high lipid diet to set up hyperglycemia mouse model, is not affecting On the premise of mice feed, then give tea polysaccharide (12g/kg normal feedstuff), tea polyphenols (12g/kg basis Feedstuff), embodiment 1 reconstitutes powder feeding equal amount and surveys blood sugar level.After feeding 30 days continuously, embodiment 1 reconstitutes powder group can make hyperglycemia mouse blood sugar value be down to (10.88 ± 0.89) by (15.52 ± 1.89) mmol/L Mmol/L, and the blood glucose value of tea polysaccharide group and tea polyphenols group hyperglycemia mice is down to (12.45 ± 2.78) respectively mmol/L、(11.38±3.67)mmol/L.Conclusion: in the present invention, embodiment 1 reconstitutes the blood sugar reducing function of powder It is significantly better than tea polysaccharide group and tea polyphenols group.
Embodiment 1~embodiment 5 test all displays: when reconstitute in powder containing the content of catechin and I When the ratio of uncle's sugar content is between 0.56~0.80, blood sugar decreasing effect becomes apparent from.
In the present invention, the selection of other components:
1, experiment show: amylomaize have anti-swelling, gelatinization point is high, film property is strong Feature, is difficult to by enzyme hydrolysis in digestion, so delaying blood glucose to raise, reducing food blood sugar Index aspect has important function.
2, experiment shows: Calcium peptide of casein (CCP) is a kind of efficient calcium absorption enhancer.In food Calcium salt under gastric juice effect, become solubility calcium, but enter neutral to time in the small intestinal of weakly alkaline environment, its Middle a part of calcium ion is combined formation insoluble calcium phosphate precipitation and cannot be absorbed by the body with phosphoric acid.Casein The existence of calcium peptide can stop the precipitation of calcium phosphate, makes calcium ion be constantly in free state, thus improves food The absorbance of middle calcium.
3, experiment shows: taurine is as a kind of nutrition enhancer, except in prevention cardiovascular disease and rush Entering fat digestion absorption aspect to play an important role, it also can be combined with Insulin receptor INSR, promote cellular uptake and Utilize glucose, accelerate glycolysis, reduce blood sugar concentration.
4, experiment shows: chromium picolinate is the product that trace element chromium necessary to human body is combined with pyridine acid Thing.Pyridine acid and chromic combination can promote effective absorption of chromium.Chromium picolinate can improve insulin Activity, makes body utilize a small amount of insulin to eliminate glucose from blood quickly.For hyperglycemia and sugar Urine patient, internal supplementary trivalent chromium element is conducive to regulating blood glucose, drops in the case of low dose of long-term taking Sugar effect becomes apparent from.
5, experiment shows: polyphenolic substance is the plant component having several phenolic hydroxyl group in molecular structure General name, mainly includes phenolic acids and flavone compound.Polyphenol compound has certain oxidation resistance, Superoxide anion and the hydroxy radical etc. that 26S Proteasome Structure and Function damages are caused freely to peroxidation can be produced Base has obvious scavenging action, and its anti-oxidation function has good result to the prevention of diabetes chronic diseases.
6, experiment shows: plant polyphenol can be by suppression carbohydrate inversion enzyme such as small intestinal glucoside Enzyme and pancreaticα-amylase postpone Starch Hydrolysis, and the release of delay glucose and absorption can make post-prandial glycemia Slowly raise, thus reach to control the effect of blood glucose.
7, experiment shows: plant polyphenol can strengthen hypoglycemic activity with other functional components synergism. Tea polyphenols and the impact on hyperglycemia mouse body index of the tea polysaccharide immixture, zoopery knot shows that tea is many Sugar and tea polyphenols synergism can reduce the blood glucose value of hyperglycemia mice, promote that glucose changes into glycogen Former, and effect is notable compared with tea polysaccharide independent role.
In addition, polyphenolic substance is attached to protein network by affinity interaction by the protein in food In structure, the polyphenol in system is had absorption, concentration and stable effect, and the complex obtained is to obesity With hyperglycemia mice, still there is significant effect of lowering blood sugar.Defatted soybean protein powder is joined the Portugal after dilution Grape juice finds along with the increase of defatted soybean protein powder content, free anthocyanidin in stock solution, procyanidin and Total phenol content reduces, and shows that this albumen network structure has enrichment to polyphenolic substance.Separation is obtained The albumen composition rich in polyphenol feed high lipid diet induction hyperglycemia mice, the post-prandial glycemia of experimental group Level significantly reduces, and shows that this complex has preferable effect of reducing blood sugar and uses.
Molecular distillation type monoglyceride forms composite emulsifier with sucrose ester, has for reconstituting the character of rear emulsion Good Stabilization.Experiment shows, monoglyceride and sucrose ester add the feelings of Walnut Milk with the mass ratio of 5:5 Under condition, sample particle diameter reduces, and centrifugal breast analysis rate reduces with rate of deposition, adds storage stability and improves wind Taste, is applied to reconstitute in powder by this composite emulsifier the character reconstituting emulsion is had improvement result.
Microwave disinfection processes the features such as time is short, penetration power strong, homogeneous heating and guarantor to food quality with it Hold important function.Now, microwave disinfection has been widely used for fluid, semisolid and pressed powder product Process of manufacture.Having experiment to show, the fresh phragmites communis non-oxidizability after microwave disinfection strengthens, and nutrition is damaged Losing few, chlorophyll loss is few, bright-colored.In the tea beverage that microwave disinfection processed, tea polyphenols loss amount is remote Less than high temperature high pressure sterilizing, therefore microwave disinfection has preferably work to the preservation of heat-sensitive substance in tea beverage With.
As can be seen here, product main component of the present invention has corn starch, lactalbumin, Oleum Helianthi etc., full Foot hyperglycemia population normal energetic requirements, conjugated linoleic acid, Konjac glucomannan, chromium picolinate, tea polyphenols etc. become Divide for stimulating insulin secretion, suppress α-amylase and alpha-glucosidase activity, reduction blood glucose liter high speed Degree has good effects.It is right that being added on of a small amount of oligofructose and xylitol is avoided while improving products taste The facilitation that blood glucose raises.This product instant is quick, rich in multiple nutritional components, it is possible to meet people Body energy requirement, is suitable for each age group consumer especially hyperglycemia population and eats.
It should be noted that above example only in order to technical scheme to be described and unrestricted, although ginseng According to preferred embodiment, the present invention is described in detail, it will be understood by those within the art that, can Technical scheme is modified or equivalent, without deviating from the essence of technical solution of the present invention God and scope, it all should be contained in the middle of scope of the presently claimed invention.

Claims (8)

1. the processing method reconstituting powder, it is characterised in that: include,
The preparation of W/O emulsion: 45~55 parts of starch and 5~15 parts of amylomaizes are scattered in water In make cold starch solution, by compounding to 0.03~0.07 part of sucrose ester and 0.03~0.07 part of molecule distillating monoglyceride breast Agent is dissolved in 10~15 portions of Oleum Helianthis, and adds 0.1~0.3 part of conjugated linoleic acid under nitrogen protection, 45~55 DEG C of stirring 20~40min formation oil-based systems, dropwise add to described oil phase body by described cold starch solution In system, stirring 20~40min forms stable W/O emulsion;
The preparation of W/O/W emulsion: be added to the water by 10~20 parts of lactalbumins, stirring is to being completely dissolved Obtain aqueous whey protein solution, the described W/O emulsion prepared is slowly added to described lactalbumin water-soluble In liquid, continuously stirred rear homogenizing;
Being spray-dried: inlet temperature 130 DEG C~170 DEG C, W/O/W emulsion is entered by outlet temperature 65~75 DEG C Row is dried, by spray drying gained powder and oligofructose 4~5 parts, xylitol 3.5~4 parts, Semen sojae atricolor powdery phosphorus Fat 1.5~2.5 parts, potassium chloride 1~1.5 parts, calcium carbonate 1~1.5 parts, magnesium sulfate 1~1.2 parts, Konjac glucomannan 0.1~0.8 Part, sodium chloride 0.1~0.2 part, Calcium peptide of casein 0.1~0.3 part, tea polyphenols 0.4~0.6 part, tea polysaccharide 0.4~0.6 Part, compound vitamin 0.1~0.3 part, sodium erythorbate 0.1~0.3 part, taurine 0.01~0.05 part, anti- Bad hematic acid cetylate 0.01~0.05 part, ferrous sulfate 0.01~0.05 part, zinc sulfate 0.01~0.02 part, sulfur Acid manganese 0.003~0.007 part, chromium picolinate 0.001~0.005 part, tertiary sodium phosphate 0.001~0.005 part are through micro- Mixing bag distribution packaging after ripple sterilization, what products obtained therefrom was low-glycemic reconstitutes powder.
The processing method reconstituting powder the most according to claim 1, it is characterised in that: in described spray After mist drying steps, also include, the described powder that reconstitutes is carried out micronizing so that being crushed to particle diameter is The subparticle of 15~20 μm.
The processing method reconstituting powder the most according to claim 1 and 2, it is characterised in that: described Starch includes one or more in corn starch, pea starch, green starch.
The processing method reconstituting powder the most according to claim 1 and 2, it is characterised in that: described In spray drying, its charging rate is 7.5ml/min~8.5ml/min.
The processing method reconstituting powder the most according to claim 1 and 2, it is characterised in that: described In the preparation of W/O emulsion, by molten to 0.05 part of sucrose ester and 0.05 part of molecule distillating monoglyceride composite emulsifier In 13 portions of Oleum Helianthis.
The processing method reconstituting powder the most according to claim 1 and 2, it is characterised in that: described In the preparation of W/O/W emulsion, in terms of mass parts, wherein tea polyphenols 0.4 part, tea polysaccharide 0.4 part.
7. what prepared by a processing method according to claim 1 reconstitutes powder, it is characterised in that: In terms of mass parts, including,
Pea starch 45~55 parts, amylomaize 5~15 parts, sucrose ester 0.03~0.07 part, molecule Distillation monoglyceride composite emulsifier 0.03~0.07 part, Oleum Helianthi 10~15 parts, conjugated linoleic acid 0.1~0.3 Part, lactalbumin 10~20 parts, oligofructose 4~5 parts, xylitol 3.5~4 parts, Semen sojae atricolor powdery phosphatidase 1 .5~2.5 Part, potassium chloride 1~1.5 parts, calcium carbonate 1~1.5 parts, magnesium sulfate 1~1.2 parts, Konjac glucomannan 0.1~0.8 part, chlorine Change sodium 0.1~0.2 part, Calcium peptide of casein 0.1~0.3 part, tea polyphenols 0.4~0.8 part, tea polysaccharide 0.4~0.8 part, Compound vitamin 0.1~0.3 part, sodium erythorbate 0.1~0.3 part, taurine 0.01~0.05 part, Vitamin C Acid cetylate 0.01~0.05 part, ferrous sulfate 0.01~0.05 part, zinc sulfate 0.01~0.02 part, manganese sulfate 0.003~0.007 part, chromium picolinate 0.001~0.005 part, tertiary sodium phosphate 0.001~0.005 part.
The most according to claim 7 reconstitute powder, it is characterised in that: wherein,
Reconstituting the content containing catechin in powder and using silicon ether derivant with high effective liquid chromatography for measuring The ratio of the arabinose content of gas chromatography determination is 0.56~0.80.
CN201610256957.1A 2016-04-23 2016-04-23 A kind of processing method and its brewed powder of brewed powder Active CN105919074B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610256957.1A CN105919074B (en) 2016-04-23 2016-04-23 A kind of processing method and its brewed powder of brewed powder

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610256957.1A CN105919074B (en) 2016-04-23 2016-04-23 A kind of processing method and its brewed powder of brewed powder

Publications (2)

Publication Number Publication Date
CN105919074A true CN105919074A (en) 2016-09-07
CN105919074B CN105919074B (en) 2019-02-19

Family

ID=56836025

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610256957.1A Active CN105919074B (en) 2016-04-23 2016-04-23 A kind of processing method and its brewed powder of brewed powder

Country Status (1)

Country Link
CN (1) CN105919074B (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106954785A (en) * 2017-04-03 2017-07-18 天津农学院 A kind of black nutritive reconstitutes powder and preparation method
CN107462657A (en) * 2017-09-11 2017-12-12 夏永刚 A kind of method for detecting uronic acid and aldose simultaneously using gaschromatographic mass spectrometric analysis method
CN110352013A (en) * 2017-06-30 2019-10-18 日本食品化工株式会社 Fats and oils processing starch and its manufacturing method

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004323366A (en) * 2003-04-22 2004-11-18 Taisho Pharmaceut Co Ltd W/o/w type composite emulsion
CN102511849A (en) * 2011-12-21 2012-06-27 安徽天歌鹅业有限责任公司 Preparation method of goose bone meal solid instant powder
CN104366260A (en) * 2014-11-20 2015-02-25 甘肃圣大方舟马铃薯变性淀粉有限公司 Starch-based high-dietary-fiber mixing powder and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004323366A (en) * 2003-04-22 2004-11-18 Taisho Pharmaceut Co Ltd W/o/w type composite emulsion
CN102511849A (en) * 2011-12-21 2012-06-27 安徽天歌鹅业有限责任公司 Preparation method of goose bone meal solid instant powder
CN104366260A (en) * 2014-11-20 2015-02-25 甘肃圣大方舟马铃薯变性淀粉有限公司 Starch-based high-dietary-fiber mixing powder and preparation method thereof

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106954785A (en) * 2017-04-03 2017-07-18 天津农学院 A kind of black nutritive reconstitutes powder and preparation method
CN110352013A (en) * 2017-06-30 2019-10-18 日本食品化工株式会社 Fats and oils processing starch and its manufacturing method
CN110352013B (en) * 2017-06-30 2020-12-18 日本食品化工株式会社 Oil-and-fat processed starch and method for producing same
CN107462657A (en) * 2017-09-11 2017-12-12 夏永刚 A kind of method for detecting uronic acid and aldose simultaneously using gaschromatographic mass spectrometric analysis method
CN107462657B (en) * 2017-09-11 2020-11-03 夏永刚 Method for simultaneously detecting uronic acid and aldose by gas chromatography-mass spectrometry

Also Published As

Publication number Publication date
CN105919074B (en) 2019-02-19

Similar Documents

Publication Publication Date Title
CN103445169B (en) Instant germ mixing powder and preparation method thereof
CN104146197A (en) Jelly powder for invigorating stomach and improving digestion of infants and preparation method of jelly powder
CN102106495A (en) Konjac jelly powder and method for making jellies by using same
JPH05268919A (en) Health drink composition
KR102020586B1 (en) Healthy foods for elderly comprising animal and plant extracts and process for preparation thereof
CN102894101B (en) Functional fresh cheese with special flavor and preparation method thereof
CN101322513A (en) Liquid state dairy food and producing method thereof
CN105919074A (en) Processing and making method of brewing powder and brewing powder processed and made by processing and making method
CN107981291A (en) A kind of jelly powder, jelly and preparation method thereof
RU2676799C1 (en) Composition for preparation of nutritional bar
CN101292994B (en) Method for relieving or neutralizing the effect of alcohol, and products thereof
CN105558056A (en) Inonotus obliquus milk tea powder and preparation method thereof
CN101632409B (en) Method for preparing fat mimics taking wheat gliadin as substrate
CN108771076B (en) Preparation and redissolution method of composite curcumin myofibrillar protein solid beverage
CN103763930A (en) Acid-stable creamer or whitener composition
CN102187902A (en) Vitamin c protein beverage, and preparation method thereof
CN106070813A (en) Green tea powder nourishing medicinal granule
CN104757689A (en) Solid beverage with pine pollen, taurine and vitamins, and preparation method of the solid beverage
CN105029572B (en) A kind of black soya bean antioxidation polypeptide beverage and preparation method thereof
CN102125098B (en) Liquid dairy product containing royal jelly and preparation method thereof
CN112352962A (en) Protein medical food for improving taking compliance and preparation method thereof
CN107183190A (en) A kind of composite solid is formulated goat milk
CN107594276B (en) Sugar-free solid beverage and preparation method thereof
CN103380875B (en) Tribulus terrestris jelly and preparation process thereof
CN107259476A (en) A kind of chicken soup and preparation method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant