CN105919074B - A kind of processing method and its brewed powder of brewed powder - Google Patents

A kind of processing method and its brewed powder of brewed powder Download PDF

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CN105919074B
CN105919074B CN201610256957.1A CN201610256957A CN105919074B CN 105919074 B CN105919074 B CN 105919074B CN 201610256957 A CN201610256957 A CN 201610256957A CN 105919074 B CN105919074 B CN 105919074B
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parts
brewed powder
processing method
starch
emulsion
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CN105919074A (en
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陈洁
孟春雨
何志勇
曾茂茂
秦昉
张爽
陶冠军
王林祥
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Jiangnan University
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Jiangnan University
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Abstract

The invention discloses a kind of processing method of brewed powder and its brewed powder, the processing method of brewed powder includes that the preparation of W/O emulsion, the preparation of W/O/W emulsion and spray drying obtain the brewed powder of low-glycemic.Product of the present invention not only avoids the Excess free enthalpy of xylitol but also improves product mouthfeel using oligofructose and xylitol as composite sweetener.Product of the present invention meets the energy and nutritional need of needed by human body, and many of function of blood sugar reduction factor synergistic effect has the effect of slowly increasing blood glucose, can become the first choice of hyperglycemia population meal replacing food after intake.

Description

A kind of processing method and its brewed powder of brewed powder
Technical field
The invention belongs to food processing technology fields, are related to a kind of packed processing and fabricating side for delaying glycemic full nutrition brewed powder Method and slow blood glucose increasing product.
Background technique
Currently, the product for being suitble to the hyperglycemia populations such as diabetes edible is broadly divided into three categories: plant extracts, vitamin Inorganic salts health product and sugar-free starch product.First two product has improvement diabetic symptom, reduces postprandial blood sugar function Effect, but diabetes patient's normal energetic requirements are unable to satisfy, dinner accesary foods can only be used as.Sugar-free starch product main feature It is high dietary-fiber, high protein, the easily blood glucose increasing raw-food material such as sucrose, glucose is replaced with sugar alcohol, such as sugar-free biscuit, sugar-free Bread, sugar-free soybean milk etc., but the Excess free enthalpy of sugar alcohol easily leads to abdominal distension, diarrhea.
Tea polysaccharide (Tea Polysaccharides, TPS) is a kind of more with the combined acidity of protein in tealeaves Sugared or a kind of acidoglycoprotein has strengthen immunity, reducing blood lipid, hypoglycemic, anti-radiation, anticoagulant, antithrombotic and other effects, In function most outstanding be it is hypoglycemic, another main physiologically active ingredient is tea polyphenols, at present both at home and abroad about tea polysaccharide, There are many hypoglycemic report of tea polyphenols.It, can serious shadow when adding excessive in food but due to the bitter taste of tea polyphenols etc. itself Ringing taste of food causes mouthfeel bad, and on the other hand, when tea polyphenols additive amount is very few in food, what can be reached is specific Effect is very little.
Summary of the invention
The purpose of this section is to summarize some aspects of the embodiment of the present invention and briefly introduce some preferable implementations Example.It may do a little simplified or be omitted to avoid our department is made in this section and the description of the application and the title of the invention Point, the purpose of abstract of description and denomination of invention it is fuzzy, and this simplification or omit and cannot be used for limiting the scope of the invention.
In view of above-mentioned and/or existing full nutrition and can be hypoglycemic reconstitute present in powder, preparation method thereof and its brewed powder Problem proposes the present invention.
Therefore, it is an object of the invention to improve the brew of starch material, a kind of processing system of brewed powder is provided Make method, a kind of full nutrition is especially provided and can be hypoglycemic brewed powder preparation method.
In order to solve the above technical problems, the present invention provides the following technical scheme that a kind of processing method of brewed powder, It includes the preparation of W/O emulsion: 45~55 parts of starch and 5~15 parts of amylomaizes are dispersed in water be made it is cold 0.03~0.07 part of sucrose ester and 0.03~0.07 part of molecule distillating monoglyceride composite emulsifier are dissolved in 10~15 by starch solution In part sunflower oil, and 0.1~0.3 part of conjugated linoleic acid is added under nitrogen protection, 45~55 DEG C of 20~40min of stirring are formed Oil-based system adds to the cold starch solution in the oil-based system dropwise, and 20~40min of stirring forms stable W/O cream Shape liquid;The preparation of W/O/W emulsion: 10~20 parts of lactalbumins are added to the water, and stirring is to being completely dissolved to obtain whey egg The prepared W/O emulsion is slowly added in the aqueous whey protein solution by white water solution, homogeneous after lasting stirring; Spray drying:, 65~75 DEG C of outlet temperature, being dried W/O/W emulsion by 130 DEG C~170 DEG C of inlet temperature, will be spraying dry Dry gained powder with 4~5 parts of oligofructose, 3.5~4 parts of xylitol, soybean powdery phosphatidase 1 .5~2.5 part, potassium chloride 1~1.5 Part, 1~1.5 part of calcium carbonate, 1~1.2 part of magnesium sulfate, 0.1~0.8 part of konjac glucomannan, 0.1~0.2 part of sodium chloride, casein calcium peptide 0.1~0.3 part, 0.4~0.8 part of tea polyphenols, 0.4~0.8 part of tea polysaccharide, 0.1~0.3 part of multi-vitamins, arabo-ascorbic acid 0.1~0.3 part of sodium, 0.01~0.05 part of taurine, 0.01~0.05 part of ascorbyl palmitate, ferrous sulfate 0.01~ 0.05 part, 0.01~0.02 part of zinc sulfate, 0.003~0.007 part of manganese sulfate, 0.001~0.005 part of chromium picolinate, phosphoric acid 0.001~0.005 part of trisodium mixing and bag distribution packaging after microwave disinfection, products obtained therefrom is the brewed powder of low-glycemic.
A kind of preferred embodiment of processing method as brewed powder of the present invention, in which: described spraying dry It after dry step, further include being pulverized to the brewed powder, so that being crushed to the subparticle that partial size is 15~20 μm.
A kind of preferred embodiment of processing method as brewed powder of the present invention, in which: the starch includes One or more of cornstarch, pea starch, green starch.
A kind of preferred embodiment of processing method as brewed powder of the present invention, in which: the spray drying In, charging rate is 7.5ml/min~8.5ml/min.
A kind of preferred embodiment of processing method as brewed powder of the present invention, in which: the W/O emulsion Preparation in, 0.05 part of sucrose ester and 0.05 part of molecule distillating monoglyceride composite emulsifier are dissolved in 13 portions of sunflower oils.
A kind of preferred embodiment of processing method as brewed powder of the present invention, in which: the W/O/W emulsus In the preparation of liquid, in terms of mass parts, wherein 0.4 part of tea polyphenols, 0.4 part of tea polysaccharide.
It is a further object to provide a kind of according to the packed processing method for delaying glycemic full nutrition brewed powder The slow blood glucose increasing product of preparation.
In order to solve the above technical problems, the present invention provides the following technical scheme that a kind of brewed powder is wrapped in terms of mass parts It includes, 45~55 parts of pea starch, 5~15 parts of amylomaize, 0.03~0.07 part of sucrose ester, molecule distillating monoglyceride are multiple With 0.03~0.07 part of emulsifier, 10~15 parts of sunflower oil, 0.1~0.3 part of conjugated linoleic acid, 10~20 parts of lactalbumin, 4~5 parts of oligofructose, 3.5~4 parts of xylitol, soybean powdery phosphatidase 1 .5~2.5 part, 1~1.5 part of potassium chloride, calcium carbonate 1~ 1.5 parts, 1~1.2 part of magnesium sulfate, 0.1~0.8 part of konjac glucomannan, 0.1~0.2 part of sodium chloride, 0.1~0.3 part of casein calcium peptide, 0.4~0.6 part of tea polyphenols, 0.4~0.6 part of tea polysaccharide, 0.1~0.3 part of multi-vitamins, sodium isoascorbate 0.1~0.3 Part, 0.01~0.05 part of taurine, 0.01~0.05 part of ascorbyl palmitate, 0.01~0.05 part of ferrous sulfate, sulfuric acid 0.01~0.02 part of zinc, 0.003~0.007 part of manganese sulfate, 0.001~0.005 part of chromium picolinate, tertiary sodium phosphate 0.001~ 0.005 part.
A kind of preferred embodiment of processing method as brewed powder of the present invention, in which: use high-efficient liquid phase color Content containing catechin and the arabinose measured with the gas chromatography of silicon ether derivant in the brewed powder of spectrometry measurement The ratio of content is 0.56~0.80.
Product of the present invention both avoids the Excess free enthalpy of xylitol using oligofructose and xylitol as composite sweetener Product mouthfeel is improved again.Product of the present invention meets the energy and nutritional need of needed by human body, many of function of blood sugar reduction because Son synergistic effect has the effect of slowly increasing blood glucose after intake, can become the first choice of hyperglycemia population meal replacing food.
Specific embodiment
In order to make the foregoing objectives, features and advantages of the present invention clearer and more comprehensible, right combined with specific embodiments below A specific embodiment of the invention is described in detail.
In the following description, numerous specific details are set forth in order to facilitate a full understanding of the present invention, but the present invention can be with Implemented using other than the one described here other way, those skilled in the art can be without prejudice to intension of the present invention In the case of do similar popularization, therefore the present invention is not limited by the specific embodiments disclosed below.
Secondly, " one embodiment " or " embodiment " referred to herein, which refers to, may be included at least one realization side of the invention A particular feature, structure, or characteristic in formula." in one embodiment " that different places occur in the present specification not refers both to The same embodiment, nor the individual or selective embodiment mutually exclusive with other embodiments.
Embodiment 1:
Raw material weight proportioning of soup processed be cornstarch 50g, lactalbumin 15g, sunflower oil 13g, amylomaize 10g, Oligofructose 4.45g, xylitol 3.68g, soybean powdery phosphatidase 2 g, konjac glucomannan 0.5g, conjugated linoleic acid 0.2g, casein calcium peptide 0.16g, tea polyphenols 0.6g, tea polysaccharide 0.5g, multi-vitamins 0.1g, molecular distillation type monoglyceride 0.05g, sucrose ester 0.05g, Potassium chloride 1.2g, calcium carbonate 1.2g, magnesium sulfate 1g, konjac glucomannan 0.5g, sodium chloride 0.16g, casein calcium peptide 0.2g, different Vitamin C Sour sodium 0.2g, taurine 0.03g, ascorbyl palmitate 0.03g, ferrous sulfate 0.03g, zinc sulfate 0.01g, manganese sulfate 0.005g, chromium picolinate 0.003g, tertiary sodium phosphate 0.003g.
It disperses 50g cornstarch and 10g amylomaize in 240mL water and cold starch solution is made.
0.05g sucrose ester and 0.05g molecular distillation type monoglyceride composite emulsifier are dissolved in 13g sunflower oil, and 0.2g conjugated linoleic acid is added under nitrogen protection, 50 DEG C of magnetic agitation 30min form oil-based system.
Cold starch solution (starch dispersion liquid) is added in oil-based system dropwise, magnetic agitation 30min forms stable W/O Mixing and emulsifying system.
15g lactalbumin is added in 200mL water, magnetic agitation is to being completely dissolved.It is added into W/O mixing and emulsifying In system, 2 formation W/O/W emulsion of high pressure homogenizer homogeneous are used after lasting stirring a period of time.
W/O/W emulsion is spray-dried: 130 DEG C of inlet temperature, 70 DEG C of outlet temperature carry out W/O/W emulsion It is dry, charging rate 7.5ml/min.Spray drying gained powder is subjected to sterile mix after microwave disinfection with other raw-food materials Merge bag distribution packaging, products obtained therefrom is low-glycemic brewed powder.
Embodiment 2:
Raw material weight proportioning of soup processed is pea starch 45g, lactalbumin 10g, sunflower oil 10g, and amylomaize 5g is low Fructooligosaccharides 4g, xylitol 3g, soybean powdery phosphatidase 2 g, konjac glucomannan 0.5g, conjugated linoleic acid 0.2g, casein calcium peptide 0.1g, tea Polyphenol 0.4g, tea polysaccharide 0.4g, multi-vitamins 0.1g, molecular distillation type monoglyceride 0.05g, sucrose ester 0.05g, potassium chloride 1.0g, calcium carbonate 1.5g, magnesium sulfate 1g, konjac glucomannan 0.5g, sodium chloride 0.16g, casein calcium peptide 0.2g, sodium isoascorbate 0.2g, taurine 0.03g, ascorbyl palmitate 0.03g, ferrous sulfate 0.03g, zinc sulfate 0.01g, manganese sulfate 0.002g, chromium picolinate 0.005g, tertiary sodium phosphate 0.005g.
It disperses 50g pea starch and 10g amylomaize in 240mL water and cold starch solution is made.
0.05g sucrose ester and 0.05g molecular distillation type monoglyceride composite emulsifier are dissolved in 10g sunflower oil, and 0.2g conjugated linoleic acid is added under nitrogen protection, 50 DEG C of magnetic agitation 30min form oil-based system.
Cold starch solution (starch dispersion liquid) is added in oil-based system dropwise, magnetic agitation 30min forms stable W/O Mixing and emulsifying system.
10g lactalbumin is added in 200mL water, magnetic agitation is to being completely dissolved.It is added into W/O mixing and emulsifying In system, 2 formation W/O/W emulsion of high pressure homogenizer homogeneous are used after lasting stirring a period of time.
W/O/W emulsion is spray-dried: 150 DEG C of inlet temperature, 70 DEG C of outlet temperature carry out W/O/W emulsion It is dry, charging rate 7.5ml/min.Spray drying gained powder is subjected to sterile mix after microwave disinfection with other raw-food materials Merge bag distribution packaging, products obtained therefrom is low-glycemic brewed powder.
Embodiment 3:
Raw material weight proportioning of soup processed be green starch 50g, lactalbumin 20g, sunflower oil 13g, amylomaize 10g, Oligofructose 5g, xylitol 4g, soybean powdery phosphatidase 3 g, konjac glucomannan 0.5g, conjugated linoleic acid 0.3g, casein calcium peptide 0.16g, Tea polyphenols 0.6g, tea polysaccharide 0.6g, multi-vitamins 0.1g, molecular distillation type monoglyceride 0.05g, sucrose ester 0.05g, potassium chloride 1.5g, calcium carbonate 1.2g, magnesium sulfate 1g, konjac glucomannan 0.7g, sodium chloride 0.2g, casein calcium peptide 0.5g, sodium isoascorbate 0.2g, taurine 0.03g, ascorbyl palmitate 0.03g, ferrous sulfate 0.03g, zinc sulfate 0.01g, manganese sulfate 0.007g, chromium picolinate 0.003g, tertiary sodium phosphate 0.007g.
It disperses 50g green starch and 10g amylomaize in 240mL water and cold starch solution is made.
0.05g sucrose ester and 0.05g molecular distillation type monoglyceride composite emulsifier are dissolved in 13g sunflower oil, and 0.2g conjugated linoleic acid is added under nitrogen protection, 50 DEG C of magnetic agitation 30min form oil-based system.
Cold starch solution (starch dispersion liquid) is added in oil-based system dropwise, magnetic agitation 30min forms stable W/O Mixing and emulsifying system.
20g lactalbumin is added in 200mL water, magnetic agitation is to being completely dissolved.It is added into W/O mixing and emulsifying In system, 2 formation W/O/W emulsion of high pressure homogenizer homogeneous are used after lasting stirring a period of time.
W/O/W emulsion is spray-dried: 170 DEG C of inlet temperature, 70 DEG C of outlet temperature carry out W/O/W emulsion It is dry, charging rate 7.5ml/min.Spray drying gained powder is subjected to sterile mix after microwave disinfection with other raw-food materials Merge bag distribution packaging, products obtained therefrom is low-glycemic brewed powder.
Embodiment 4:
Raw material weight proportioning of soup processed be cornstarch 50g, lactalbumin 12g, sunflower oil 13g, amylomaize 10g, Oligofructose 4.45g, xylitol 3.68g, soybean powdery phosphatidase 2 g, konjac glucomannan 0.5g, conjugated linoleic acid 0.3g, casein calcium peptide 0.16g, tea polyphenols 0.55g, tea polysaccharide 0.5g, multi-vitamins 0.1g, molecular distillation type monoglyceride 0.05g, sucrose ester 0.05g, potassium chloride 1.0g, calcium carbonate 1.5g, magnesium sulfate 1g, konjac glucomannan 0.5g, sodium chloride 0.16g, casein calcium peptide 0.2g are different Sodium ascorbate 0.2g, taurine 0.04g, ascorbyl palmitate 0.03g, ferrous sulfate 0.03g, zinc sulfate 0.01g, sulphur Sour manganese 0.002g, chromium picolinate 0.005g, tertiary sodium phosphate 0.005g.
It disperses 50g cornstarch and 10g amylomaize in 240mL water and cold starch solution is made.
0.05g sucrose ester and 0.05g molecular distillation type monoglyceride composite emulsifier are dissolved in 13g sunflower oil, and 0.2g conjugated linoleic acid is added under nitrogen protection, 50 DEG C of magnetic agitation 30min form oil-based system.
Cold starch solution (starch dispersion liquid) is added in oil-based system dropwise, magnetic agitation 30min forms stable W/O Mixing and emulsifying system.
12g lactalbumin is added in 200mL water, magnetic agitation is to being completely dissolved.It is added into W/O mixing and emulsifying In system, 2 formation W/O/W emulsion of high pressure homogenizer homogeneous are used after lasting stirring a period of time.
W/O/W emulsion is spray-dried: 150 DEG C of inlet temperature, 70 DEG C of outlet temperature carry out W/O/W emulsion It is dry, charging rate 8ml/min.Spray drying gained powder is subjected to sterile mix with other raw-food materials after microwave disinfection And bag distribution packaging, products obtained therefrom are low-glycemic brewed powder.
Embodiment 5:
Raw material weight proportioning of soup processed be cornstarch 50g, lactalbumin 13g, sunflower oil 13g, amylomaize 10g, Oligofructose 4.45g, xylitol 3.68g, soybean powdery phosphatidase 2 g, konjac glucomannan 0.5g, conjugated linoleic acid 0.2g, casein calcium peptide 0.16g, tea polyphenols 0.45g, tea polysaccharide 0.4g, multi-vitamins 0.1g, molecular distillation type monoglyceride 0.05g, sucrose ester 0.05g, potassium chloride 1.0g, calcium carbonate 1.5g, magnesium sulfate 1g, konjac glucomannan 0.5g, sodium chloride 0.16g, casein calcium peptide 0.2g are different Sodium ascorbate 0.2g, taurine 0.04g, ascorbyl palmitate 0.03g, ferrous sulfate 0.03g, zinc sulfate 0.01g, sulphur Sour manganese 0.002g, chromium picolinate 0.005g, tertiary sodium phosphate 0.005g.
It disperses 50g cornstarch and 10g amylomaize in 240mL water and cold starch solution is made.
0.05g sucrose ester and 0.05g molecular distillation type monoglyceride composite emulsifier are dissolved in 13g sunflower oil, and 0.2g conjugated linoleic acid is added under nitrogen protection, 50 DEG C of magnetic agitation 30min form oil-based system.
Cold starch solution (starch dispersion liquid) is added in oil-based system dropwise, magnetic agitation 30min forms stable W/O Mixing and emulsifying system.
13g lactalbumin is added in 200mL water, magnetic agitation is to being completely dissolved.It is added into W/O mixing and emulsifying In system, 2 formation W/O/W emulsion of high pressure homogenizer homogeneous are used after lasting stirring a period of time.
W/O/W emulsion is spray-dried: 170 DEG C of inlet temperature, 70 DEG C of outlet temperature carry out W/O/W emulsion It is dry, charging rate 8.5ml/min.Spray drying gained powder is subjected to sterile mix after microwave disinfection with other raw-food materials Merge bag distribution packaging, products obtained therefrom is low-glycemic brewed powder.
Ultramicro grinding of the present invention refers to using air-flowing type or mechanical disintegrating apparatus, is milled, is rushed to material It hits, shear, in crushing material to partial size be 15~20 μm of subparticle by partial size, the material after ultramicro grinding is more convenient for water The migration divided, is more evenly distributed in material, is convenient for the intermolecular crosslinking of heterogeneity material, and product brew is more preferable.But it is another On the one hand, it can make to topple over material when reconstituting and fly upward if product particle is meticulous, therefore experiments have shown that 15~20 μm of subparticle rushes Adjust effect best.
The discussion of each embodiment brewed powder powder instant capacity of the present invention:
(1) it reconstitutes influence of the water temperature to instant capacity: reconstituting experiment in the case where reconstituting 40~80 DEG C of water temperature, obtain punching of the present invention The optimum water temperature of powder is adjusted, as shown in the table:
Table 1 reconstitutes influence of the water temperature to brewed powder instant capacity
Conglomeration rate involved in the test method is determined by the following procedure: weighing brewed powder 50g in beaker, adds The hot water 400mL for entering 40~80 DEG C, is sufficiently stirred 10min, then observes conglomeration, lamination;Then with 20 mesh screens to molten Liquid is filtered, and is rinsed agglomeration object with clear water, is put into drying box and dries to constant weight, band sieve is weighed, and subtracting sieve weight is The weight of agglomeration object, the calculation formula of conglomeration rate are as follows: conglomeration rate (%)=(conglomeration object weight/coffee beverage powder) × 100.
From 1 test result of table it is found that reconstitute water temperature be 60 DEG C when, the instant capacity of brewed powder is best.It needs to consider to rush simultaneously It adjusts nutritional ingredient contained in powder to be easy decomposed metamorphic at high temperature, is such as dissolved in 80 DEG C of water, polyphenol content will in 10min Loss 35.4%, so under comprehensively considering, selected 60 DEG C of optimum water temperatures reconstituted for brewed powder.
(2) reconstitute influence of the water to instant capacity: reconstituting water is important one of the influence factor of brewed powder instant capacity, choosing It selects to reconstitute water and be 4 times, 6 times, 8 times, 10 times, 12 times of brewed powder quality and be tested, brewed powder is determined by subjective appreciation Most suitable water when reconstituting.Results of sensory evaluation is shown: when reconstituting water is 8 times of brewed powder quality, mouthfeel is best, and shape At conglomeration it is minimum.
(3) it influence of the addition stabilizer to brewed powder instant capacity: since to reconstitute rear property unstable for brewed powder, was reconstituting Phenomena such as being easy to happen layering in journey, uniting, sink to the bottom, so steady by addition multi-vitamins, molecular distillation type monoglyceride etc. Agent is determined to inquire into and solve the stability problem after brewed powder reconstitutes.Pass through the examination to plurality of stable agent and its dosage in the present invention It tests, reconstituting the best stabilizer of effect is multi-vitamins and molecular distillation type monoglyceride.
Efficient liquid is used after filter (aperture: 0.8 μm) filtering with the brewed powder in distilled water dilution embodiment 1 Phase chromatography, installation import the liquid chromatogram packed column L-columm of octadecylTMODS uses A liquid and B liquid at 35 DEG C of column temperature According to the catechins in gradient method measurement filtered fluid.Mobile phase A liquid is the distilled water solution containing 0.1mol/L acetic acid, B liquid is the acetonitrile solution containing 0.1mol/L acetic acid, and sample injection rate is that 20 μ L, UV detector wavelengths are 280nm.
1 brewed powder 2g of Example, is dissolved in 20ml distilled water, add ethyl alcohol to concentration of alcohol be 70% when precipitating for 24 hours Centrifugation.In sediment plus 4ml 2mol/L trifluoroacetic acid makes it dissolve and is transferred in glass tube sealing and seals, 100 DEG C of insulating boxs After middle degradation 8h, glass fiber filter paper is filtered, and is concentrated under reduced pressure on rotary evaporator and is added water to be evaporated under reduced pressure again repeatedly, to remove three It is removed after fluoroacetic acid to small size, uses N2Air-blowing adds the monosaccharide of water 4ml dissolution degradation to no tart flavour.2.0ml lysate is respectively taken, 1 drop ammonium hydroxide and 1.0m l inositol (making internal standard) is added dropwise, respectively plus sodium borohydride 30mg, shakes up overnight, monosaccharide is made to be converted into sugar alcohol, It is separately added into Dowex 50W-X8 (H again+) ion exchange resin, except decationizing to aqueous solution is in acidity.Filtering, filtrate subtract Pressure is evaporated, and repeatedly plus methanol is evaporated off borate 5 times totally.Residue is transferred in small test tube with a little methanol, uses N2Air-blowing is dry, sets 2d in drier adds trimethyl silicane miaow 0.1ml after being completely dried, and sufficiently vibrates, sugar alcohol is made to be converted into silica-ether compound, Arabinose content is measured as gas chromatographic analysis.
Test measurement, the ratio of the content in brewed powder containing catechin and arabinose content is 0.69 at this time.Experiment Male mice 10 are selected, every group is established hyperglycemia mouse model using high lipid diet, under the premise of not influencing mouse feed, Give tea polysaccharide (12g/kg basal feed), tea polyphenols (12g/kg basal feed), 1 brewed powder feeding equal amount of embodiment again simultaneously Survey blood glucose level.After continuous feeding 30 days, 1 brewed powder group of embodiment can make hyperglycemia mouse blood sugar value by (15.52 ± 1.89) Mmol/L is down to (10.88 ± 0.89) mmol/L, and tea polysaccharide group and the blood glucose value of tea polyphenols group hyperglycemia mouse are down to respectively (12.45±2.78)mmol/L,(11.38±3.67)mmol/L.Conclusion: the blood sugar reducing function of 1 brewed powder of embodiment in the present invention It is significantly better than tea polysaccharide group and tea polyphenols group.
The test of 1~embodiment of embodiment 5 is shown: when the content and arabinose content in brewed powder containing catechin Ratio be 0.56~0.80 between when, blood sugar decreasing effect becomes apparent from.
In the present invention, the selection of other components:
1, experiment shows: amylomaize has the characteristics that resist that swelling, gelatinization point is high, film forming is strong, in people It is not easy in body digestive system by enzyme hydrolysis, so playing a significant role in terms of delaying blood glucose rise, reducing food blood sugar index.
2, experiment shows: casein calcium peptide (CCP) is a kind of efficient accelerating agent of calcium absorption.Calcium salt in food is in gastric juice When becoming solubility calcium under effect, but entering neutrality into the small intestine of weakly alkaline environment, a portion calcium ion and phosphoric acid knot Conjunction forms insoluble calcium phosphate precipitation and can not be absorbed by the body.The presence of casein calcium peptide can prevent the precipitating of calcium phosphate, make Calcium ion is constantly in free state, to improve the absorptivity of calcium in food.
3, experiment shows: taurine is as a kind of nutrition fortifier, in addition to disappearing in prevention cardiovascular disease and promotion fat Change absorption aspects to play an important role, it also can bind to the insulin receptor, and promotes cellular uptake and utilizes glucose, accelerates sugared ferment Solution reduces blood sugar concentration.
4, experiment shows: chromium picolinate is product of the trace element chromium necessary to human body in conjunction with pyridine acid.Pyridine The combination of acid and trivalent chromium can promote effective absorption of chromium.Chromium picolinate can be improved insulin active, make body using less The insulin of amount quickly eliminates glucose from blood.For hyperglycemia and diabetic, trivalent chromium is supplemented in vivo Be conducive to adjust blood glucose, hypoglycemic effect becomes apparent from the case that low dose is taken for a long time.
5, experiment shows: polyphenolic substance is the general name for having the plant component of several phenolic hydroxyl group in molecular structure, main It to include phenolic acid class and flavone compound.Polyphenol compound has certain oxidation resistance, is turned into that can generate peroxide With and the superoxide anion and the free radicals such as hydroxy radical that cause structure and function to be damaged has apparent scavenging effect, it is anti-oxidant Function has good result to the prevention of diabetes chronic diseases.
6, experiment shows: plant polyphenol can be by inhibiting carbohydrate inversion enzyme such as small intestine glucuroide and pancreas α- Amylase postpones Starch Hydrolysis, and the release and absorption of delay glucose can be such that postprandial blood sugar slowly increases, to reach control The effect of blood glucose processed.
7, experiment shows: plant polyphenol can act synergistically with other function ingredient enhances hypoglycemic effect.Tea polyphenols with Influence of the tea polysaccharide immixture to hyperglycemia mouse body index, zoopery knot show that tea polysaccharide and tea polyphenols act synergistically The blood glucose value of hyperglycemia mouse can be reduced, glucose is promoted to be converted to hepatic glycogen, and is imitated compared with tea polysaccharide independent role Fruit is significant.
In addition to this, polyphenolic substance is integrated to protein network structure by affinity interaction by the protein in food In, there are absorption, concentration and stable to the polyphenol in system, and obtained compound still has fat and hyperglycemia mouse There is significant effect of lowering blood sugar.De-fatted soya protein Powder is added in the grape juice after dilution and is found with skimmed soybean protein The increase of powder content, dissociate in stoste anthocyanidin, procyanidine and total phenol content reduce, and show the albumen network structure to polyphenol Compound has enrichment.The hyperglycemia for the albumen composition feeding high lipid diet induction rich in polyphenol that separation is obtained is small The level of postprandial blood sugar of mouse, experimental group significantly reduces, and shows that the compound is used with preferable effect of reducing blood sugar.
Molecular distillation type monoglyceride and sucrose ester form composite emulsifier, and the character for reconstituting rear lotion has good Stabilization.In the case that experiment shows that Walnut Milk is added with the mass ratio of 5:5 in monoglyceride and sucrose ester, sample particle diameter reduces, Being centrifuged newborn analysis rate and rate of deposition reduces, and increases storage stability and improves flavor, this composite emulsifier is applied to brewed powder In to reconstitute lotion character have improvement result.
The features such as microwave disinfection is with its short processing time, penetration power is strong, homogeneous heating and weight is maintained to food quality It acts on.Now, microwave disinfection has been widely used for the process of manufacture of fluid, semisolid and solid powder product.Have Experiment shows the fresh reed inoxidizability enhancing after microwave disinfection, and nutritive loss is few, and chlorophyll loss is few, bright-colored.It is micro- Tea polyphenols loss amount is far fewer than high temperature high pressure sterilizing in the sterile-processed tea beverage of wave, therefore microwave disinfection is to warm in tea beverage The preservation of quick property substance has preferable effect.
It can be seen that product of the present invention main component has cornstarch, lactalbumin, sunflower oil etc., meet hyperglycemia Crowd's normal energetic requirements, the ingredients such as conjugated linoleic acid, konjac glucomannan, chromium picolinate, tea polyphenols for stimulating insulin secretion, Inhibit alpha-amylase and alpha-glucosidase activity, reduce blood glucose rise speed with good effects.A small amount of oligofructose and wood The addition of sugar alcohol avoids the facilitation to blood glucose rise while improving product mouthfeel.The product is convenient quick, rich Containing multiple nutritional components, body energy demand can satisfy, be suitble to each age group consumer especially hyperglycemia population edible.
It should be noted that the above examples are only used to illustrate the technical scheme of the present invention and are not limiting, although referring to preferable Embodiment describes the invention in detail, those skilled in the art should understand that, it can be to technology of the invention Scheme is modified or replaced equivalently, and without departing from the spirit and scope of the technical solution of the present invention, should all be covered in this hair In bright scope of the claims.

Claims (8)

1. a kind of processing method of brewed powder, it is characterised in that: including,
The preparation of W/O emulsion: 45~55 parts of starch and 5~15 parts of amylomaizes are dispersed in water and cold starch is made .07 parts of molecule distillating monoglyceride composite emulsifiers of the .07 parts of sucrose esters of 0 .03~0 and 0 .03~0 are dissolved in 10~15 by solution In part sunflower oil, and the .3 parts of conjugated linoleic acid of 0 .1~0 are added under nitrogen protection, 45~55 DEG C of stirring 20~40min shapes At oil-based system, the cold starch solution is added to dropwise in the oil-based system, 20~40min of stirring forms stable W/O Emulsion;
The preparation of W/O/W emulsion: 10~20 parts of lactalbumins are added to the water, and stirring is to being completely dissolved to obtain lactalbumin The prepared W/O emulsion is slowly added in the aqueous whey protein solution by aqueous solution, homogeneous after lasting stirring;
Spray drying: 130 DEG C~170 DEG C of inlet temperature, 65~75 DEG C of outlet temperature, W/O/W emulsion is dried, will be sprayed The dry gained powder of mist with 4~5 parts of oligofructose, 3 .5~4 part of xylitol .5 parts of .5~2 of soybean powdery phosphatidase 1, chlorination 1~1 .5 parts of potassium, 1~1 .5 parts of calcium carbonate, 1~1 .2 parts of magnesium sulfate .8 parts of konjac glucomannan 0 .1~0,0 .1~0 of sodium chloride .2 part .3 parts of casein calcium peptide 0 .1~0 .6 parts of tea polyphenols 0 .4~0 .6 parts of tea polysaccharide 0 .4~0, multi-vitamins 0 .1~0 .3 parts .3 parts of sodium isoascorbate 0 .1~0 .05 parts of taurine 0 .01~0, ascorbyl palmitate 0 .01~0 .05 parts .05 parts of ferrous sulfate 0 .01~0 .02 parts of zinc sulfate 0 .01~0, manganese sulfate 0 .003~0 .007 Part, chromium picolinate 0 .001~0 .005
Part .005 parts of tertiary sodium phosphate 0 .001~0 is mixed after microwave disinfection and bag distribution packaging, and products obtained therefrom is hypoglycemia The brewed powder of index.
2. the processing method of brewed powder according to claim 1, it is characterised in that: in the spray drying step It afterwards, further include being pulverized to the brewed powder, so that being crushed to the subparticle that partial size is 15~20 μm.
3. the processing method of brewed powder according to claim 1 or 2, it is characterised in that: the starch includes corn One or more of starch, pea starch, green starch.
4. the processing method of brewed powder according to claim 1 or 2, it is characterised in that: in the spray drying, Charging rate is the .5ml/min of 7.5ml/min~8.
5. the processing method of brewed powder according to claim 1 or 2, it is characterised in that: the system of the W/O emulsion In standby, 0 .05 parts of sucrose ester and 0 .05 parts of molecule distillating monoglyceride composite emulsifier are dissolved in 13 portions of sunflower oils.
6. the processing method of brewed powder according to claim 1 or 2, it is characterised in that: in terms of mass parts, the tea 0 .4 parts of polyphenol, 0 .4 parts of the tea polysaccharide.
7. a kind of brewed powder of processing method preparation according to claim 1, it is characterised in that: in terms of mass parts, Including,
45~55 parts of starch, 5~15 parts of amylomaize .07 parts of sucrose ester 0 .03~0, molecule distillating monoglyceride are multiple With .07 parts of emulsifier 0 .03~0,10~15 parts of sunflower oil .3 parts of conjugated linoleic acid 0 .1~0, lactalbumin 10~20 Part, 4~5 parts of oligofructose, 3 .5~4 part of xylitol .5 parts of .5~2 of soybean powdery phosphatidase 1,1~1 .5 parts of potassium chloride, carbon 1~1 .5 parts of sour calcium, 1~1 .2 parts of magnesium sulfate .8 parts of konjac glucomannan 0 .1~0 .2 parts of sodium chloride 0 .1~0, calcium caseinate .3 parts of peptide 0 .1~0 .6 parts of tea polyphenols 0 .4~0 .6 parts of tea polysaccharide 0 .4~0 .3 parts of multi-vitamins 0 .1~0, 0.1~0.3 part of sodium isoascorbate, 0.01~0.05 part of taurine, 0.01~0.05 part of ascorbyl palmitate, sulfuric acid is sub- 0.01~0.05 part of iron, 0.01~0.02 part of zinc sulfate, 0.003~0.007 part of manganese sulfate, chromium picolinate 0.001~0.005 Part, 0.001~0.005 part of tertiary sodium phosphate.
8. brewed powder according to claim 7, it is characterised in that: wherein,
With the gas-chromatography of content and use silicon ether derivant in the brewed powder of high effective liquid chromatography for measuring containing catechin The ratio of the arabinose content of method measurement is 0.56~0.80.
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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004323366A (en) * 2003-04-22 2004-11-18 Taisho Pharmaceut Co Ltd W/o/w type composite emulsion
CN102511849A (en) * 2011-12-21 2012-06-27 安徽天歌鹅业有限责任公司 Preparation method of goose bone meal solid instant powder
CN104366260A (en) * 2014-11-20 2015-02-25 甘肃圣大方舟马铃薯变性淀粉有限公司 Starch-based high-dietary-fiber mixing powder and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004323366A (en) * 2003-04-22 2004-11-18 Taisho Pharmaceut Co Ltd W/o/w type composite emulsion
CN102511849A (en) * 2011-12-21 2012-06-27 安徽天歌鹅业有限责任公司 Preparation method of goose bone meal solid instant powder
CN104366260A (en) * 2014-11-20 2015-02-25 甘肃圣大方舟马铃薯变性淀粉有限公司 Starch-based high-dietary-fiber mixing powder and preparation method thereof

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