CN105918757A - Preparation method of medicago sativa solid beverage - Google Patents
Preparation method of medicago sativa solid beverage Download PDFInfo
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- CN105918757A CN105918757A CN201610256161.6A CN201610256161A CN105918757A CN 105918757 A CN105918757 A CN 105918757A CN 201610256161 A CN201610256161 A CN 201610256161A CN 105918757 A CN105918757 A CN 105918757A
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- alfalfa
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- solid beverage
- concentrated slurry
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- 239000007787 solid Substances 0.000 title claims abstract description 73
- 235000013361 beverage Nutrition 0.000 title claims abstract description 46
- 238000002360 preparation method Methods 0.000 title claims abstract description 26
- 240000004658 Medicago sativa Species 0.000 title abstract description 10
- 235000010624 Medicago sativa Nutrition 0.000 title abstract 8
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- 238000000465 moulding Methods 0.000 claims abstract description 16
- 229920000858 Cyclodextrin Polymers 0.000 claims abstract description 14
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000002156 mixing Methods 0.000 claims abstract description 10
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- 239000002002 slurry Substances 0.000 claims description 48
- 239000007788 liquid Substances 0.000 claims description 20
- 239000003595 mist Substances 0.000 claims description 20
- 238000010438 heat treatment Methods 0.000 claims description 19
- 244000025254 Cannabis sativa Species 0.000 claims description 16
- 229930006000 Sucrose Natural products 0.000 claims description 16
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 claims description 16
- 229920002774 Maltodextrin Polymers 0.000 claims description 15
- 239000005913 Maltodextrin Substances 0.000 claims description 15
- 229940035034 maltodextrin Drugs 0.000 claims description 15
- 101710138460 Leaf protein Proteins 0.000 claims description 14
- 239000012141 concentrate Substances 0.000 claims description 14
- 239000002671 adjuvant Substances 0.000 claims description 13
- 238000000889 atomisation Methods 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 8
- 239000002245 particle Substances 0.000 claims description 8
- 238000010792 warming Methods 0.000 claims description 7
- 229920001353 Dextrin Polymers 0.000 claims description 4
- 239000004375 Dextrin Substances 0.000 claims description 4
- 235000019425 dextrin Nutrition 0.000 claims description 4
- 238000000034 method Methods 0.000 abstract description 14
- 229930182490 saponin Natural products 0.000 abstract description 10
- 150000007949 saponins Chemical class 0.000 abstract description 10
- 229930003944 flavone Natural products 0.000 abstract description 8
- 235000011949 flavones Nutrition 0.000 abstract description 8
- 238000005469 granulation Methods 0.000 abstract description 8
- 230000003179 granulation Effects 0.000 abstract description 8
- 239000001397 quillaja saponaria molina bark Substances 0.000 abstract description 8
- 238000000605 extraction Methods 0.000 abstract description 7
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 abstract description 6
- 150000002212 flavone derivatives Chemical class 0.000 abstract description 6
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 5
- 238000005507 spraying Methods 0.000 abstract description 4
- 238000001035 drying Methods 0.000 abstract description 3
- 235000015097 nutrients Nutrition 0.000 abstract description 3
- 238000001914 filtration Methods 0.000 abstract description 2
- 239000012530 fluid Substances 0.000 abstract 3
- 239000012778 molding material Substances 0.000 abstract 3
- 210000004911 serous fluid Anatomy 0.000 abstract 3
- 238000005360 mashing Methods 0.000 abstract 2
- 239000000463 material Substances 0.000 abstract 2
- 238000007493 shaping process Methods 0.000 abstract 1
- 235000018102 proteins Nutrition 0.000 description 27
- 108090000623 proteins and genes Proteins 0.000 description 27
- 102000004169 proteins and genes Human genes 0.000 description 27
- 235000017709 saponins Nutrition 0.000 description 9
- 230000008569 process Effects 0.000 description 8
- 235000016709 nutrition Nutrition 0.000 description 5
- 239000007921 spray Substances 0.000 description 5
- 238000010009 beating Methods 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 238000009413 insulation Methods 0.000 description 3
- 230000035764 nutrition Effects 0.000 description 3
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- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 108090000723 Insulin-Like Growth Factor I Proteins 0.000 description 2
- 235000019082 Osmanthus Nutrition 0.000 description 2
- 241000333181 Osmanthus Species 0.000 description 2
- 235000008331 Pinus X rigitaeda Nutrition 0.000 description 2
- 235000011613 Pinus brutia Nutrition 0.000 description 2
- 241000018646 Pinus brutia Species 0.000 description 2
- 102000013275 Somatomedins Human genes 0.000 description 2
- 235000001014 amino acid Nutrition 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- 239000002775 capsule Substances 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 150000002213 flavones Chemical class 0.000 description 2
- 229930003935 flavonoid Natural products 0.000 description 2
- 150000002215 flavonoids Chemical class 0.000 description 2
- 235000017173 flavonoids Nutrition 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 238000002372 labelling Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 108090000765 processed proteins & peptides Proteins 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 239000011573 trace mineral Substances 0.000 description 2
- 235000013619 trace mineral Nutrition 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 235000013343 vitamin Nutrition 0.000 description 2
- 229940088594 vitamin Drugs 0.000 description 2
- 229930003231 vitamin Natural products 0.000 description 2
- 150000003722 vitamin derivatives Chemical class 0.000 description 2
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 1
- UPYKUZBSLRQECL-UKMVMLAPSA-N Lycopene Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1C(=C)CCCC1(C)C)C=CC=C(/C)C=CC2C(=C)CCCC2(C)C UPYKUZBSLRQECL-UKMVMLAPSA-N 0.000 description 1
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 description 1
- 239000004472 Lysine Substances 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 150000001746 carotenes Chemical class 0.000 description 1
- 235000005473 carotenes Nutrition 0.000 description 1
- 210000000170 cell membrane Anatomy 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000004939 coking Methods 0.000 description 1
- 230000007850 degeneration Effects 0.000 description 1
- 238000004925 denaturation Methods 0.000 description 1
- 230000036425 denaturation Effects 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000012041 food component Nutrition 0.000 description 1
- 239000004459 forage Substances 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 235000021374 legumes Nutrition 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000005375 photometry Methods 0.000 description 1
- 238000012805 post-processing Methods 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 210000000582 semen Anatomy 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 235000014347 soups Nutrition 0.000 description 1
- 238000002798 spectrophotometry method Methods 0.000 description 1
- 238000001694 spray drying Methods 0.000 description 1
- NCYCYZXNIZJOKI-UHFFFAOYSA-N vitamin A aldehyde Natural products O=CC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C NCYCYZXNIZJOKI-UHFFFAOYSA-N 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/385—Concentrates of non-alcoholic beverages
- A23L2/39—Dry compositions
- A23L2/395—Dry compositions in a particular shape or form
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/72—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Fodder In General (AREA)
Abstract
The invention provides a preparation method of a medicago sativa solid beverage. The preparation method comprises the following steps of cleaning fresh medicago sativa, and then sequentially performing mashing, filtering, and concentrating so as to obtain concentrated serous fluid; adding auxiliary materials to the concentrated serous fluid, and performing uniform mixing so as to obtain molding material fluid, wherein the auxiliary materials comprise cyclodextrin; and performing spraying granulation on the molding material fluid so as to obtain the granular medicago sativa solid beverage. According to the preparation method disclosed by the invention, fixation treatment is not performed on the medicago sativa, and mashing is directly performed, so that the content of nutrient components in the concentrated serous fluid are obviously increased, particularly the content of alfalfa saponin and flavone are increased, and the extraction rate of the medicago sativa is increased. A spraying granulation method is used for drying and shaping the molding material fluid, wherein the molding temperature is low, so that zero loss of effective nutrient components in the medicago sativa is guaranteed. The moisture content is easy to control, and the percentage by mass of water of the medicago sativa solid beverage provided by the invention can be well guaranteed to be 5% or below.
Description
Technical field
The present invention relates to alfalfa technical field of beverage, particularly relate to the system of a kind of alfalfa solid beverage
Preparation Method.
Background technology
Alfalfa is universally acknowledged high-quality legume forage, is described as " King of Pasture ", " father of food ".
The multiple nutritional components such as alfalfa rich in proteins, trace element, vitamin, aminoacid, but also contain
There is unknown somatomedin.In alfalfa hay, lysine content is higher 5.7 times than Semen Maydis, in vitamin with
The content of carotene is the abundantest, in trace element with ferrum, manganese, zinc content higher.In equal plantation
Under the conditions of, alfalfa is higher than the digestible protein that graminous pasture is gathered in the crops about 2.5 times, mineral
High about 6 times, digestible nutrient is high about 2 times, the most significant UGF (unknown somatomedin)
Effect.
Directly make liquid beverage after having been reported that the fresh grass making beating of employing alfalfa at present, but need before making beating
Fresh grass completed (drift soup), during owing to completing, typically to use high temperature, high temperature make cell membrane system and
Protein denaturation encases the solable matter such as Saponin and flavone and cannot exosmose when destroying, but also may result in
Soluble protein degeneration is soluble, reduces the nutritional labeling of alfalfa.
Summary of the invention
For drawbacks described above and the problem of prior art, it is an object of the invention to provide a kind of alfalfa solid
The preparation method of beverage.During solving existing alfalfa processing and utilization, Saponin, flavone and protein
Technical problem Deng component damages.
In order to achieve the above object, the present invention provides following technical scheme:
The preparation method of the alfalfa solid beverage of the present invention, comprises the following steps:
Step one, by fresh for alfalfa grass cleaning treatment after, pull an oar successively, filter, and concentrate after
To concentrated slurry；
Step 2, addition adjuvant, mixing in concentrated slurry, obtain molding feed liquid；Described adjuvant includes ring
Dextrin；
Step 3, molding feed liquid step 2 obtained carry out mist projection granulating, obtain granular alfalfa
Solid beverage；Wherein, during mist projection granulating, add edible fine grained solid support.
In the present invention, in step one, the density of the concentrated slurry obtained after controlling to concentrate is 1.1-1.5g/cm3。
Preferably, the density of concentrated slurry is 1.1-1.2g/cm3.Concentration uses concentrate under reduced pressure at low temperature machine to carry out,
Temperature controls below 55 DEG C.
Preferably, in step 2, the mass ratio controlling cyclodextrin and concentrated slurry is 1 30-45.More preferably,
The mass ratio controlling cyclodextrin and concentrated slurry is 1 35-40.Optimally, cyclodextrin and concentrated slurry are controlled
Mass ratio be 1 36.It is precisely controlled both ratios, it is ensured that preferably embedding effect and low cost.
Further, in step 3, during mist projection granulating, control parameter as follows: hot blast temperature is 60-70
DEG C, atomization chamber temperature is 40-60 DEG C.Preferably, hot blast temperature is 60-65 DEG C, and atomization chamber temperature is 45-55
℃.Optimally, hot blast temperature is 60-65 DEG C, and atomization chamber temperature is 45-50 DEG C.
Further, in step 3, the particle diameter of described fine grained solid support is not less than 80 mesh.Be preferably, described carefully
The particle diameter of grain carrier is 80 mesh-120 mesh.More preferably, the particle diameter of described fine grained solid support is 100 mesh-110 mesh.
Further, in step 3, the weight ratio controlling fine grained solid support and concentrated slurry is 1 3-6.Preferably
Ground, the weight ratio controlling fine grained solid support and concentrated slurry is 14.
Further, described fine grained solid support uses white sugar or/and maltodextrin；When for white sugar and maltodextrin
During mixture, the mass ratio controlling white sugar and maltodextrin is 3-5 1.It is preferred that control white sugar and Fructus Hordei Germinatus
The mass ratio of dextrin is 41.
Preferably technical scheme is further, in step one, after fresh for alfalfa grass cleaning treatment, depends on
Secondary pull an oar, be filtrated to get serosity, before serosity is concentrated, increase the step to serosity heating,
Then the serosity after heating is filtered, obtains leaf protein and the filtered solution separated out, then filtered solution is concentrated,
Obtain concentrated slurry.Separate out leaf protein.Now, in concentration process, concentrate under reduced pressure at low temperature machine is used to carry out,
Temperature controls at 60-80 DEG C.
Further, in described heating steps, being heated up by serosity, controlling the highest warming temperature is 80 DEG C, so
Rear insulation 3-6min, then filters, obtains filtered solution.
Specifically, in described heating steps, serosity is warming up to 60 DEG C-80 DEG C, is incubated 3-6min, then
Filter, obtain filtered solution.
Further, in described heating steps, use staged mode of heating, be first warming up to 60 DEG C-72 DEG C,
Insulation 2-5min, filters, obtains green protein and filtered solution；Then filtered solution is again heated to 75 DEG C-80 DEG C,
Insulation 1-2min, refilters, obtains white protein and filtered solution.
The preparation method of the alfalfa solid beverage of the present invention possesses following advantage:
(1) first, in the preparation process of the concentrated slurry of the alfalfa of step one, not to alfalfa
Carry out the process that completes, directly pull an oar, filter and be concentrated to give concentrated slurry.With pull an oar again after completing, mistake
The concentrated slurry that completes filtered and be concentrated to give is compared, and the nutrition in the concentrated slurry that step one of the present invention obtains becomes
The content divided significantly improves, especially alfalfa saponin and the content of flavone；The extraction ratio of alfalfa is improved
?；The beneficially raising of the yield and quality of the alfalfa solid beverage product that the present invention obtains.Concentrated
Cheng Caiyong concentrate under reduced pressure at low temperature machine is carried out, and temperature controls below 55 DEG C.
(2) secondly, in step 2, the adjuvant of cyclodextrin is comprised to concentration by adding in concentrated slurry
Serosity is allocated, and is embedded by the careless fishy smell in concentrated slurry.And furthermore present cyclodextrin with dense
The mass ratio of contracting serosity, it is ensured that preferably embedding effect and reduction cost.
(3) it addition, in step 3, use Spray granulation method, granulation process is additionally added edible
Fine grained solid support.With fine grained solid support as core, molding feed liquid sticks on fine grained solid support, obtain granular size,
The granular solids beverage that shape is consistent, nutrition is many and reasonable mixture ratio, and is prone to dissolve, it is easy to quilt
Absorption of human body, water content less than 5%.And forming temperature is low in Spray granulation method, advantageously ensure that pale reddish brown
Effective ingredient in Herba Medicaginis does not loses.And moisture is easily controlled, the purple of the present invention can be ensured well
The content of the moisture of Herba Trigonellae Ruthenicae solid beverage is at 5% (wt.) below.And at conventional drying process (box-type drying
Method) in, concentrated slurry needs to spread the thinnest one layer out, and efficiency is the lowest；And concentrated slurry is dry below 70 DEG C
Time dry, moisture is difficult to up to standard, and i.e. less than 5%, but baking temperature is then easy to coking more than 70 DEG C；
It is difficult to control, is not suitable for the molding feed liquid of step 2 of the present invention.
(4) simultaneously, in step 3, by the procedure parameter of Comprehensive Control mist projection granulating, and it is used for spraying
The density of the concentrated slurry of pelletize, and the parameter such as the ratio of concentrated slurry and fine grained solid support, it is achieved preferably
Control mist projection granulating molding.
(5) in preferred technical scheme, before serosity is concentrated, by heating by the long-chained protein in serosity
Separate out, obtain leaf protein and filtered solution, filtered solution eliminates the long-chained protein being difficult to be absorbed by the body, protect
The short chain albumen enriched, small peptide, aminoacid etc. has been stayed easily to absorb composition so that the solid beverage finally given
Middle active constituent content is high, and proportioning is more reasonable, and instant capacity is more preferable, is more easy to be absorbed by the body.Separate out
To leaf protein can process and obtain leaf protein product, e.g., leaf protein sheet, leaf protein capsule etc..Excellent at this
In the concentration process of the technical scheme of choosing, using concentrate under reduced pressure at low temperature machine to carry out, temperature controls at 60-80 DEG C i.e.
Can.
By further preferred gradient-heated mode, green protein and white protein is made to separate out respectively, thus
Easily green protein and white protein are carried out different post processings, obtain different protein products.
(6) the alfalfa solid beverage that the preparation method of the present invention obtains, is that granular size, shape are consistent
Granular solids beverage, it is easy to dissolve, it is easy to be absorbed by the body, water content less than 5%.Wherein contain more
High alfalfa saponin and flavone, have good quality.The present invention is preferably to obtaining after serosity heat treated
Solid beverage, removes long-chained protein, and nutritional labeling proportioning is more reasonable, and instant capacity is more preferable simultaneously, it is easier to
It is absorbed by the body.
Accompanying drawing explanation
In order to be illustrated more clearly that the embodiment of the present invention or technical scheme of the prior art, below will be to enforcement
In example or description of the prior art, the required accompanying drawing used is briefly described, it should be apparent that, describe below
In accompanying drawing be only some embodiments of the present invention, for those of ordinary skill in the art, do not paying
On the premise of going out creative work, it is also possible to obtain other accompanying drawing according to these accompanying drawings.
Fig. 1 is the FB(flow block) of the preparation method of the alfalfa solid beverage of the embodiment of the present invention 1；
Fig. 2 is the FB(flow block) of the preparation method of the alfalfa solid beverage of the embodiment of the present invention 4.
Detailed description of the invention
Below in conjunction with embodiments of the invention, technical scheme is clearly and completely described,
Obviously, described embodiment is only a part of embodiment of the present invention rather than whole embodiments.Base
Embodiment in the present invention, those of ordinary skill in the art are obtained under not making creative work premise
The every other embodiment obtained, broadly falls into the scope of protection of the invention.
Embodiment 1
Shown in Fig. 1, the preparation method of the alfalfa solid beverage of the embodiment of the present invention 1 is described, bag
Include following steps:
Step one, by fresh for alfalfa grass remove impurity, cleaning treatment after, pull an oar successively, filter (e.g.,
Filter pressing), obtain serosity；Concentrated slurry is obtained after being concentrated by serosity again；Concentration uses concentrate under reduced pressure at low temperature
Machine is carried out, and temperature controls at 45 DEG C-50 DEG C.
Step 2, addition adjuvant, mixing in concentrated slurry, obtain molding feed liquid；Described adjuvant includes ring
Dextrin；Utilize the careless fishy smell of cyclodextrin embedding concentrated slurry.
Step 3, molding feed liquid step 2 obtained carry out mist projection granulating, obtain granular alfalfa
Solid beverage；Wherein, during mist projection granulating, add edible fine grained solid support.
In the present invention, using Spray granulation method, with fine grained solid support as core, molding feed liquid sticks to particulate and carries
On body, obtain granular size, granular solids beverage that shape is consistent, water content less than 5%.And in spray
In mist granulation process, forming temperature is low, advantageously ensures that the effective ingredient in alfalfa does not loses.And
Moisture is easily controlled, and can ensure that the moisture of alfalfa solid beverage of the present invention is 5% well
(wt.) below.
In the step one of the present invention, to obtain after fresh for alfalfa grass is directly pulled an oar, filtered by step one
The dried object (i.e. extract) filtering serosity is measured, and alfalfa saponins measures and uses uv-spectrophotometric
Method (Wang Songbai, 2005, the Chinese Academy of Agricultural Sciences's Master's thesis)；Herba Medicaginis Determination of Total Flavonoids uses spectrophotography (osmanthus
Sturdy pines, 2009, Heilungkiang medical science).Measurement result is as shown in table 1.
Alfalfa saponin in extraction yield that the fresh grass of table 1 is directly pulled an oar and extract and flavones content
*: the dry rate 15.1% that Radix Glycyrrhizae weight measures from large sample calculates.
Three parallel mensuration are carried out after *: three sample extraction thing mixing.
As a comparison, in the present invention to fresh for alfalfa grass is completed after, then carry out pulling an oar, filter after obtain
Complete filter serosity dried object (i.e. extract) be measured, alfalfa saponins measure use ultraviolet divide
Light photometry (Wang Songbai, 2005, the Chinese Academy of Agricultural Sciences's Master's thesis)；Herba Medicaginis Determination of Total Flavonoids uses light splitting light
Degree method (osmanthus sturdy pines, 2009, Heilungkiang medical science).Measurement result is as shown in table 2.
The fresh grass of table 2 complete after making beating extraction yield and extract in alfalfa saponin and flavones content
*: the dry rate 15.1% that Radix Glycyrrhizae weight measures from large sample calculates.
Three parallel mensuration are carried out after *: three sample extraction thing mixing.
Visible, compared with the serosity obtained of pulling an oar again after completing, the present invention uses the side of the directly making beating that do not completes
The content of the effective ingredient in the serosity that formula obtains significantly improves, especially alfalfa saponin and the content of flavone；
The extraction ratio of alfalfa is improve；The beneficially product of the alfalfa solid beverage product that the present invention obtains
Amount and the raising of quality.
In the step one of the embodiment of the present invention 1, the fresh grass of alfalfa directly pull an oar filter after serosity need into
Row concentration, processes to certain proportion, to adapt to follow-up atomizing granulating technology.Preferably control to concentrate
After the density of concentrated slurry that obtains be 1.1-1.5g/cm3.The concentrated pulp obtained after more preferably controlling to concentrate
The density of liquid is 1.1-1.2g/cm3。
In step 2, add the adjuvant comprising cyclodextrin, the careless fishy smell in concentrated slurry can be embedded.
According to the characteristic of the fresh grass of alfalfa, the mass ratio preferably controlling cyclodextrin and concentrated slurry is 1 30-45.
It is precisely controlled both ratios, it is ensured that preferably embedding effect and reduction cost.
Certainly, in the adjuvant added in concentrated slurry in step 2, it is also possible to include other some adjuvants
Raw material, such as Sorbitol, or the adjuvant such as citric acid, it is also possible to add some functional components, so that
Final alfalfa solid beverage possesses corresponding function.
During the mist projection granulating of step 3, need to control hot blast temperature and atomization chamber temperature, to ensure atomization
Granulation outcome, it is ensured that grain forming, and better control over the water content of alfalfa solid beverage less than 5%.
Therefore, for the viscosity high characteristic of the molding feed liquid of alfalfa, during mist projection granulating, preferably control
Parameter is as follows: hot blast temperature is 60-70 DEG C, and atomization chamber temperature is 40-60 DEG C.It is highly preferred that hot blast temperature
For 60-65 DEG C, atomization chamber temperature is 45-55 DEG C.
In step 3, the particle diameter of described fine grained solid support is not less than 80 mesh.
The ratio of described fine grained solid support and concentrated slurry grain forming rate, taste and mouth to solid beverage
Sense has an impact.It is therefore preferred that the weight ratio controlling fine grained solid support and concentrated slurry is 1 3-6.
Specifically, described fine grained solid support uses edible particulate, it is preferred to use white sugar is or/and maltodextrin；
When for the mixture of white sugar and maltodextrin, the mass ratio controlling white sugar and maltodextrin is 3-5 1.
In the embodiment of the present invention 1, the concrete mist projection granulating using PLG spray-drying pelleting machine to complete step 3,
Concentrated liquid enters atomization chamber by spray gun, and fine grained solid support is first put in bottom atomization chamber before spraying.
Embodiment 2
The preparation method of the alfalfa solid beverage of the embodiment of the present invention 2, comprises the following steps:
Step one, by fresh for alfalfa grass remove impurity, cleaning treatment after, pull an oar successively, filter (e.g.,
Filter pressing), obtain serosity；Concentrated slurry is obtained after being concentrated by serosity again；The density controlling concentrated slurry is
1.1-1.2g/cm3.Concentration uses concentrate under reduced pressure at low temperature machine to carry out, and temperature controls at 45 DEG C-50 DEG C.
Step 2, in concentrated slurry add adjuvant, blending and mixing, obtain molding feed liquid；Described accessory package
Include cyclodextrin；The mass ratio controlling cyclodextrin and concentrated slurry is 1 36.
Step 3, molding feed liquid step 2 obtained carry out mist projection granulating, obtain granular alfalfa
Solid beverage；Wherein, during mist projection granulating, add edible fine grained solid support；Described fine grained solid support
The mass ratio using white sugar and the mixture of maltodextrin, white sugar and maltodextrin is 41.Described particulate carries
In body, the particle diameter of white sugar and maltodextrin is 100 mesh；The weight ratio controlling fine grained solid support and concentrated slurry is 1
4.
And during mist projection granulating, control parameter as follows: hot blast temperature is 60-65 DEG C, atomization chamber temperature
For 45-50 DEG C.
In the embodiment of the present invention 2, the fine grained solid support of 100 mesh particle diameters and step one Midst density are 1.1-1.2g/cm3
Concentrated slurry there is more preferable matching degree so that ratio of briquetting is higher.
Embodiment 3
The preparation method of the alfalfa solid beverage of the embodiment of the present invention 3, comprises the following steps:
Step one, by fresh for alfalfa grass cleaning treatment after, pull an oar successively, filter (e.g., filter pressing),
Obtain serosity；Concentrated slurry is obtained after being concentrated by serosity again；The density controlling concentrated slurry is 1.5g/cm3。
Concentration uses concentrate under reduced pressure at low temperature machine to carry out, and temperature controls at 45 DEG C-50 DEG C.
Step 2, in concentrated slurry add adjuvant, blending and mixing, obtain molding feed liquid；Described accessory package
Include cyclodextrin；The mass ratio controlling cyclodextrin and concentrated slurry is 1 35-40.
Step 3, molding feed liquid step 2 obtained carry out mist projection granulating, obtain granular alfalfa
Solid beverage；Wherein, during mist projection granulating, add edible fine grained solid support；Described fine grained solid support
The mass ratio using white sugar and the mixture of maltodextrin, white sugar and maltodextrin is 3-5 1.Described particulate
In carrier, the particle diameter of white sugar and maltodextrin is 80 mesh；The weight ratio controlling fine grained solid support and concentrated slurry is 1
3-6.
And during mist projection granulating, control parameter as follows: hot blast temperature is 60-65 DEG C, atomization chamber temperature
For 45-55 DEG C.
Embodiment 4
On the basis of above-described embodiment 1 to embodiment 3, the improvement that step one is carried out.Specifically, such as
Shown in Fig. 2, in step one, after fresh for alfalfa grass cleaning treatment, pull an oar successively, be filtrated to get
Serosity, before concentrating serosity, increases the step to serosity heating, and heating-up temperature is up to 80 DEG C,
Then the serosity after heating is filtered, obtains leaf protein and the filtered solution separated out, then filtered solution is concentrated,
Obtain concentrated slurry.Now, in concentration process, using concentrate under reduced pressure at low temperature machine to carry out, temperature controls
60-80 DEG C.
Specifically, in heating steps, serosity is warming up to 60 DEG C-80 DEG C, is incubated 3-6min, then mistake
Filter, obtains filtered solution.
Long-chained protein in serosity is difficult to be absorbed by the body, and can affect the water-soluble of alfalfa solid beverage
Property, it is therefore preferable that separated out by the long-chained protein in serosity by heating, obtain leaf protein and filtered solution, filter
Cross and liquid eliminates the long-chained protein being difficult to be absorbed by the body, remain abundant short chain albumen, small peptide, ammonia
Base acid etc. easily absorbs composition so that in the solid beverage finally given, active constituent content is high, and nutrition becomes
Distribution ratio is reasonable, is more easy to be absorbed by the body；Instant capacity is more preferable simultaneously.
The leaf protein that precipitation obtains can be processed and obtain leaf protein product, e.g., and leaf protein sheet, leaf protein capsule
Deng.
Long-chained protein in serosity exists green protein and white protein, in above-mentioned mode of heating, is
Whole green proteins and part long-chain white protein are separated out simultaneously, to follow-up albumen is carried out deep processing time
Making troubles, therefore, in the embodiment of the present invention 4, preferred technical scheme is, uses staged heating side
Formula, separates out respectively by green protein and long-chain white protein, and concrete staged mode of heating is as follows:
First it is warming up to 60 DEG C-72 DEG C, is incubated 2-5min, filter, obtain green protein and filtered solution；Then will filter
Liquid is again heated to 75 DEG C-80 DEG C, is incubated 1-2min, refilters, obtain white protein and filtered solution.
The above, the only detailed description of the invention of the present invention, but protection scope of the present invention is not limited to
This, any those familiar with the art, in the technical scope that the invention discloses, can readily occur in
Change or replacement, all should contain within protection scope of the present invention.Therefore, protection scope of the present invention should
Described it is as the criterion with scope of the claims.
Claims (10)
1. the preparation method of an alfalfa solid beverage, it is characterised in that comprise the following steps:
Step one, by fresh for alfalfa grass cleaning treatment after, pull an oar successively, filter, and concentrate after
To concentrated slurry；
Step 2, addition adjuvant, mixing in concentrated slurry, obtain molding feed liquid；Described adjuvant includes ring
Dextrin；
Step 3, molding feed liquid step 2 obtained carry out mist projection granulating, obtain granular alfalfa
Solid beverage；Wherein, during mist projection granulating, add edible fine grained solid support.
The preparation method of a kind of alfalfa solid beverage the most according to claim 1, it is characterised in that
In step one, the density of the concentrated slurry obtained after controlling to concentrate is 1.1-1.5g/cm3。
3., according to the preparation method of a kind of alfalfa solid beverage described in claims 1 or 2, it is special
Levying and be, the mass ratio controlling cyclodextrin and concentrated slurry is 1 30-45.
4., according to the preparation method of a kind of alfalfa solid beverage described in claims 1 or 2, it is special
Levy and be, during mist projection granulating, control parameter as follows: hot blast temperature is 60-70 DEG C, and atomization chamber temperature is
40-60℃。
5., according to the preparation method of a kind of alfalfa solid beverage described in claims 1 or 2, it is special
Levying and be, in step 3, the particle diameter of described fine grained solid support is not less than 80 mesh.
6., according to the preparation method of a kind of alfalfa solid beverage described in claims 1 or 2, it is special
Levying and be, in step 3, the weight ratio controlling fine grained solid support and concentrated slurry is 1 3-6.
7., according to the preparation method of a kind of alfalfa solid beverage described in claims 1 or 2, it is special
Levying and be, in step 3, described fine grained solid support uses white sugar or/and maltodextrin；When described fine grained solid support is adopted
During with the mixture of white sugar and maltodextrin, the mass ratio controlling white sugar and maltodextrin is 3-5 1.
8., according to the preparation method of a kind of alfalfa solid beverage described in claims 1 or 2, it is special
Levy and be, in step one, after fresh for alfalfa grass cleaning treatment, pull an oar successively, be filtrated to get slurry
Liquid, before concentrating serosity, increases the step to serosity heating, is then filtered by the serosity after heating,
Obtain leaf protein and the filtered solution separated out, then filtered solution is concentrated, obtain concentrated slurry.
The preparation method of a kind of alfalfa solid beverage the most according to claim 8, it is characterised in that
In described heating steps, being heated up by serosity, controlling the highest warming temperature is 80 DEG C, is then incubated 3-6min,
Then filter, obtain filtered solution.
The preparation method of a kind of alfalfa solid beverage the most according to claim 9, its feature exists
In, in described heating steps, use staged mode of heating, be first warming up to 60 DEG C-72 DEG C, be incubated 2-5min,
Filter；Then it is again heated to 75 DEG C-80 DEG C, is incubated 1-2min, refilters, obtain filtered solution.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105685708A (en) * | 2016-02-04 | 2016-06-22 | 河南农业大学 | Compound alfalfa herbal functional beverage and preparation method thereof |
| CN106820113A (en) * | 2016-12-28 | 2017-06-13 | 陕西天宝大豆食品技术研究所 | Full clover peptide nutrient food and preparation method thereof |
| CN108056344A (en) * | 2017-12-18 | 2018-05-22 | 福建农林大学 | A kind of clover celestial being fruit beverage and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1961759A (en) * | 2006-11-29 | 2007-05-16 | 辽宁大学 | Clover health beverage |
| CN103610205A (en) * | 2013-11-28 | 2014-03-05 | 刘菊 | Method for preparing bitter gourd instant beverage |
| CN103999936A (en) * | 2014-05-06 | 2014-08-27 | 大连民族学院 | Medicago sativa yoghourt and preparation method thereof |
-
2016
- 2016-04-22 CN CN201610256161.6A patent/CN105918757B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1961759A (en) * | 2006-11-29 | 2007-05-16 | 辽宁大学 | Clover health beverage |
| CN103610205A (en) * | 2013-11-28 | 2014-03-05 | 刘菊 | Method for preparing bitter gourd instant beverage |
| CN103999936A (en) * | 2014-05-06 | 2014-08-27 | 大连民族学院 | Medicago sativa yoghourt and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105685708A (en) * | 2016-02-04 | 2016-06-22 | 河南农业大学 | Compound alfalfa herbal functional beverage and preparation method thereof |
| CN106820113A (en) * | 2016-12-28 | 2017-06-13 | 陕西天宝大豆食品技术研究所 | Full clover peptide nutrient food and preparation method thereof |
| CN108056344A (en) * | 2017-12-18 | 2018-05-22 | 福建农林大学 | A kind of clover celestial being fruit beverage and preparation method thereof |
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