CN105918361A - Pesticide containing aloe extract and preparation method thereof - Google Patents
Pesticide containing aloe extract and preparation method thereof Download PDFInfo
- Publication number
- CN105918361A CN105918361A CN201610276230.XA CN201610276230A CN105918361A CN 105918361 A CN105918361 A CN 105918361A CN 201610276230 A CN201610276230 A CN 201610276230A CN 105918361 A CN105918361 A CN 105918361A
- Authority
- CN
- China
- Prior art keywords
- extract
- aloe
- parts
- aloe extract
- content
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
- A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
- A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
- A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/10—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds
- A01N57/14—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-oxygen bonds or phosphorus-to-sulfur bonds containing aromatic radicals
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/02—Sulfur; Selenium; Tellurium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/42—Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Environmental Sciences (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Pest Control & Pesticides (AREA)
- Mycology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Microbiology (AREA)
- Biotechnology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention relates to a pesticide containing aloe extract. The pesticide comprises, by weight, 13 to 17 parts of phoxim, 5 to 9 parts of an emulsifier, 14 to 18 parts of an organic solvent, 2 to 6 parts of a cosolvent, 1 to 4 parts of aloe extract, 1 to 4 parts of Celastrus orbiculatus extract, 1 to 4 parts of validamycin, 1 to 4 parts of tea tree oil and 1 to 4 parts of ammonium sulfate. A preparation method for the pesticide containing the aloe extract comprises the following steps: preparation of the aloe extract; preparation of the Celastrus orbiculatus extract; weighing; and mixing. The pesticide has the following advantages: (1) high prevention effect on rice hoppers, rice gall midges, diamondback moths and aphids; (2) no side effect and high security; (3) improvement of the yield of paddy rice and cauliflower per mu; (4) improvement of the quality of paddy rice and cauliflower; and (5) reduction in the disease incidence rates of paddy rice and cauliflower.
Description
Technical field
The present invention relates to a kind of insecticide containing Aloe extract, specifically, relate to a kind of killing containing Aloe extract
Worm agent and preparation method thereof, belongs to agricultural plantation technology field.
Background technology
Aloe (formal name used at school: Aloe vera) Aloe, for Liliaceae perennial evergreen herbaceous plant, leafage is raw, fertile greatly
Thickness, in seat shape or be born in stem top, the normal lanceolar of leaf or the short width of leaf, edge has sharp tooth to sting.Inflorescence is umbrella shape, total shape, spike, circle
Tapers etc., color is red, yellow or tool redness of the skin or complexion speckle, six, petal, gynoecium six pieces.The many Colaesces of perianth base portion become tubular.Aloe is collection
Edible, medicinal, improve looks, view and admire plant nova.It secretes thing (principle active component is the Herba Alii fistulosi quinones substances such as aloin)
Have been widely used in medicine and daily use chemicals.Aloe folks of china just by as beauty treatment, take care of hair and treat the natural of dermatosis
Medicine.Aloe glue has certain itching-relieving action to mosquito bite.
Crops are all had a certain degree of Side effect by existing chemical pesticide, can cause in various degree soil,
The environmental pollutions such as water source, the improper meeting of Pesticide use causes crops to produce poisoning, causes crop growth abnormal, suppresses it photosynthetic
Effect, affects crop yield, and second stubble crop will also result in certain murder by poisoning.
Pesticide is liquid or solid form and gas.The own physical property of all kinds of and pesticide according to insect or disease
Difference, uses different usages.Dispense as made powder, make aqueous solution, suspension, emulsion injection, or make steam or
Gas fumigation etc..
The defect that existing chemical pesticide exists is as follows:
(1) existing chemical pesticide, the application during Rice Cropping: spray after rice transplanting, this kind of process side
Method, undesirable to the prevention effect of insect given birth to after rice transplanting, specific aim is the strongest；
Application in Brassica oleracea L. var. botrytis L. planting process: spray after Brassica oleracea L. var. botrytis L. is emerged, this kind of processing method, to Brassica oleracea L. var. botrytis L. Tanaka
The prevention effect of insect is undesirable, and specific aim is the strongest；
(2) existing chemical pesticide is applied to Oryza sativa L., Brassica oleracea L. var. botrytis L. pest control, and Oryza sativa L., Brassica oleracea L. var. botrytis L. are had certain side effect, safety
Property poor, its growth is had certain inhibitory action, and then reduces crop yield；
(3) existing chemical pesticide, only has preventive and therapeutic effect to the insect of Oryza sativa L., Brassica oleracea L. var. botrytis L., to Oryza sativa L., Brassica oleracea L. var. botrytis L. disease without make
With.
Summary of the invention
The technical problem to be solved in the present invention is for above not enough, it is provided that a kind of insecticide containing Aloe extract:
(1) this contains the insecticide of Aloe extract, and planthopper, pachydiplosis oryzae, diamondback moth, aphid are had higher preventive effect；
(2) this contains the insecticide of Aloe extract, without any side effects, and safety is high；
(3) this contains the insecticide of Aloe extract, improves the per mu yield of Oryza sativa L. and Brassica oleracea L. var. botrytis L.；
(4) this contains the insecticide of Aloe extract, improves the quality of Oryza sativa L. and Brassica oleracea L. var. botrytis L.；
(5) this contains the insecticide of Aloe extract, reduces the sickness rate of Oryza sativa L. and cauliflower disease.
For solve above technical problem, the present invention by the following technical solutions: a kind of insecticide containing Aloe extract, its
It is characterised by: the described insecticide containing Aloe extract, mould including phoxim, Aloe extract, Celastrus orbiculatus Thunb. Extract, well ridge
Element, tea tree oil and ammonium sulfate.
The scheme of a kind of optimization, the described insecticide containing Aloe extract, in parts by weight, content is: phoxim 13-17
Part, emulsifying agent 5-9 part, organic solvent 14-18 part, cosolvent 2-6 part, Aloe extract 1-4 part, Celastrus orbiculatus Thunb. Extract 1-4 part,
Jingganmycin 1-4 part, tea tree oil 1-4 part, ammonium sulfate 1-4 part.
Further, the described insecticide containing Aloe extract, in parts by weight, content is: phoxim 15 parts, emulsifying agent
7 parts, organic solvent 16 parts, cosolvent 4 parts, Aloe extract 2 parts, Celastrus orbiculatus Thunb. Extract 2 parts, jingganmycin 3 parts, tea tree oil 3
Part, 3 parts of ammonium sulfate.
Further, the weight/mass percentage composition of described phoxim effective ingredient is 98%.
Further, described emulsifying agent is phenol polyoxyethylene ether；
Described organic solvent is dimethylbenzene, and the density of described dimethylbenzene is 0.87g/cm3；
Described cosolvent is n-butyl alcohol.
Further, containing aloe-emodin, Aloe chrysophanol, aloe saponaria glycosides and Aloe in described Aloe extract
Rather, the content of described aloe-emodin be 96%, the content of Aloe chrysophanol be 1%, the content of aloe saponaria glycosides be 1%, Aloearbonaside
Content be 1%；
Containing tripterine, pristimerin, dihydroagarofuran type sesquiterpene in described Celastrus orbiculatus Thunb. Extract, described Radix Tripterygii Wilfordii
The content of red pigment is 90%, the content of pristimerin is 1%, the content of dihydroagarofuran type sesquiterpene is 1%.
A kind of method for producing insecticide containing Aloe extract, it is characterised in that: comprise the following steps: Aloe carries in preparation
Take thing；Prepare Celastrus orbiculatus Thunb. Extract；Weigh；Mixing.
The scheme of a kind of optimization, prepares Aloe extract, comprises the following steps:
(1) take Aloe, pulverize；
(2) reflux, extract, 3 times after soaking with 10 times amount 80% ethanol waters, extracts 4h every time, filters, obtain ethanol extract and
Filtering residue, merges ethanol extract, stands 50h, filters off precipitation, and recycling design obtains crude extract；
(3) water-soluble crude extract, upper macroporous adsorptive resins, after washing desaccharide, with 82% ethanol water eluting, collect ethanol and wash
De-liquid, recycling design obtains extract；
(4) water-soluble extract, successively with 15 times amount dichloromethane, ethyl acetate, n-butanol extraction；
(5) concentrating remaining aqueous phase after extraction, being washed till concentrate with methanol can not be dissolved again, obtains final extract.
Further, weigh, comprise the following steps: according to a kind of formula containing Aloe extract, weigh each respectively former
Material.
Further, mixing, comprise the following steps:
(1) by phoxim, dimethylbenzene, n-butyl alcohol, Celastrus orbiculatus Thunb. Extract, Aloe extract, jingganmycin, tea tree oil, ammonium sulfate
Mixing, stirs；
(2) gained mixture is put into the drying room of band water leg, and the temperature controlling water leg is 78-80 DEG C, is mixed by gained in (1)
Polymer melt becomes liquid, under nitrogen protection stirring 60 minutes；
(3) in the mixing liquid of gained, add phenol polyoxyethylene ether to stir 20 minutes, obtain the parasite killing containing Aloe extract
Agent；Obtained insecticide is emulsifiable concentrate.
After the present invention uses above technical scheme, compared with prior art, have the advantage that
(1) this contains the insecticide of Aloe extract, and planthopper, pachydiplosis oryzae, diamondback moth, the preventive effect of aphid are respectively reached 98-
99.5%、99-99.5%、97-98%、97-99%；
(2) yield of the Oryza sativa L. effect of being significantly improved, per mu yield reaches 850-910 kilogram, and in Oryza sativa L., the content of protein has significantly
Raising, in Oryza sativa L. fat content be significantly reduced, in Oryza sativa L., the content of protein is 10.6-9.9 g/100g, Oryza sativa L.
The content of middle fat is 1.5-1.7 g/100g；
(3) reducing the sickness rate of rice disease, the sickness rate of the false smut of Oryza sativa L. is 2%-3%, the sickness rate of rice blast is 2%-
3%, the sickness rate of rice leaf smut be 1%-2%, the sickness rate of bakanae disease of rice be 3%-4%, the sickness rate of rice sheath blight disease be
1%-2%；
(4) yield of the Brassica oleracea L. var. botrytis L. effect of being significantly improved, per mu yield reaches 5500-6000 jin, vitamin C, vitamin in Brassica oleracea L. var. botrytis L.
The content of E has had significant raising, and in Brassica oleracea L. var. botrytis L., ascorbic content is 76-92 mg/100g, and the content of vitamin E is
0.8-1.1 mg /100g；
(5) reducing the sickness rate of cauliflower disease, the sickness rate of the black rot of Brassica oleracea L. var. botrytis L. is the sickness rate of 1%-3%, melasma
For the sickness rate of 2%-5%, balck shank be 0.5%-1%, the sickness rate of downy mildew be 2%-7%.
Below in conjunction with embodiment, the present invention is described in detail.
Detailed description of the invention
Below by way of specific embodiment, the present invention is described, but the present invention is not merely defined in these embodiments.
The embodiment 1 one kinds insecticide containing Aloe extract
Described insecticide includes the component of following weight portion:
Phoxim 13 parts, emulsifying agent 5 parts, organic solvent 14 parts, cosolvent 2 parts, Celastrus orbiculatus Thunb. Extract 1 part, Aloe extract 1
Part, jingganmycin 1 part, tea tree oil 1 part, 1 part of ammonium sulfate；
The weight/mass percentage composition of described phoxim effective ingredient is 98%；
Described emulsifying agent is phenol polyoxyethylene ether；
Described organic solvent is dimethylbenzene, and the density of described dimethylbenzene is 0.87g/cm3；
Described cosolvent is n-butyl alcohol；
Containing aloe-emodin, Aloe chrysophanol, aloe saponaria glycosides and Aloearbonaside, described Aloe Radix Et Rhizoma Rhei in described Aloe extract
The content of element is 96%, the content of Aloe chrysophanol is 1%, the content of aloe saponaria glycosides is 1%, the content of Aloearbonaside is 1%.
Containing tripterine, pristimerin, dihydroagarofuran type sesquiterpene in described Celastrus orbiculatus Thunb. Extract, described thunder
The content of celastrol is 90%, the content of pristimerin is 1%, the content of dihydroagarofuran type sesquiterpene is 1%.
The embodiment 2 one kinds insecticide containing Aloe extract
Described insecticide includes the component of following weight portion:
Phoxim 15 parts, emulsifying agent 7 parts, organic solvent 16 parts, cosolvent 4 parts, Celastrus orbiculatus Thunb. Extract 2 parts, Aloe extract 2
Part, jingganmycin 3 parts, tea tree oil 3 parts, 3 parts of ammonium sulfate；
The weight/mass percentage composition of described phoxim effective ingredient is 98%；
Described emulsifying agent is phenol polyoxyethylene ether；
Described organic solvent is dimethylbenzene, and the density of described dimethylbenzene is 0.87g/cm3；
Described cosolvent is n-butyl alcohol；
Containing aloe-emodin, Aloe chrysophanol, aloe saponaria glycosides and Aloearbonaside, described Aloe Radix Et Rhizoma Rhei in described Aloe extract
The content of element is 96%, the content of Aloe chrysophanol is 1%, the content of aloe saponaria glycosides is 1%, the content of Aloearbonaside is 1%.
Containing tripterine, pristimerin, dihydroagarofuran type sesquiterpene in described Celastrus orbiculatus Thunb. Extract, described thunder
The content of celastrol is 90%, the content of pristimerin is 1%, the content of dihydroagarofuran type sesquiterpene is 1%.
The embodiment 3 one kinds insecticide containing Aloe extract
Described insecticide includes the component of following weight portion:
Phoxim 17 parts, emulsifying agent 9 parts, organic solvent 18 parts, cosolvent 6 parts, Celastrus orbiculatus Thunb. Extract 4 parts, Aloe extract 4
Part, jingganmycin 4 parts, tea tree oil 4 parts, 4 parts of ammonium sulfate；
The weight/mass percentage composition of described phoxim effective ingredient is 98%；
Described emulsifying agent is phenol polyoxyethylene ether；
Described organic solvent is dimethylbenzene, and the density of described dimethylbenzene is 0.87g/cm3；
Described cosolvent is n-butyl alcohol；
Containing aloe-emodin, Aloe chrysophanol, aloe saponaria glycosides and Aloearbonaside, described Aloe Radix Et Rhizoma Rhei in described Aloe extract
The content of element is 96%, the content of Aloe chrysophanol is 1%, the content of aloe saponaria glycosides is 1%, the content of Aloearbonaside is 1%.
Containing tripterine, pristimerin, dihydroagarofuran type sesquiterpene in described Celastrus orbiculatus Thunb. Extract, described thunder
The content of celastrol is 90%, the content of pristimerin is 1%, the content of dihydroagarofuran type sesquiterpene is 1%.
The embodiment 4 one kinds method for producing insecticide containing Aloe extract
Step 1, prepare Aloe extract
(1) take Aloe, pulverize；
(2) reflux, extract, 3 times after soaking with 10 times amount 80% ethanol waters, extracts 4h every time, filters, obtain ethanol extract and
Filtering residue, merges ethanol extract, stands 50h, filters off precipitation, and recycling design obtains crude extract；
(3) water-soluble crude extract, upper macroporous adsorptive resins, after washing desaccharide, with 82% ethanol water eluting, collect ethanol and wash
De-liquid, recycling design obtains extract；
(4) water-soluble extract, successively with 15 times amount dichloromethane, ethyl acetate, n-butanol extraction；
(5) concentrating remaining aqueous phase after extraction, being washed till concentrate with methanol can not be dissolved again, obtains final extract.
Step 2, prepare Celastrus orbiculatus Thunb. Extract
Step 3, weighing
According to a kind of formula containing Aloe extract, weigh each raw material respectively.
Step 4, mixing
(1) by phoxim, dimethylbenzene, n-butyl alcohol, Celastrus orbiculatus Thunb. Extract, Aloe extract, jingganmycin, tea tree oil, ammonium sulfate
Mixing, stirs；
(2) gained mixture is put into the drying room of band water leg, and the temperature controlling water leg is 78-80 DEG C, is mixed by gained in (1)
Polymer melt becomes liquid, under nitrogen protection stirring 60 minutes；
(3) in the mixing liquid of gained, add phenol polyoxyethylene ether to stir 20 minutes, obtain the parasite killing containing Aloe extract
Agent；
Obtained insecticide is emulsifiable concentrate.
Percent in above-described embodiment, in addition to specified otherwise, for mass percent.
The application of the embodiment 5 one kinds insecticide containing Aloe extract
This product 2500--3000 times of liquid of dilution sprays, and emphasis insect happening part squirts and do not drips for degree.
Test effect:
Planthopper, pachydiplosis oryzae, diamondback moth, the preventive effect of aphid are respectively reached by the insecticide containing Aloe extract prepared by the present invention
98-99.5%, 99-99.5%, 97-98%, 97-99%, specific targets are shown in Table 1
Table 1 contains the insecticide of the Aloe extract prevention effect to insect for the present invention
2) insecticide containing Aloe extract prepared by the present invention is not only good to the prevention effect of planthopper, diamondback moth, the most right
Pachydiplosis oryzae, control of aphids effect might as well；
This insecticide containing Aloe extract is without any side effects, and safety is high, also obtains beyond thought effect:
Apply during Rice Cropping:
1. the yield of the Oryza sativa L. effect of being significantly improved, per mu yield reaches 850-910 kilogram, and in Oryza sativa L., the content of protein has significantly
Improving, in Oryza sativa L., the content of fat is significantly reduced, and in Oryza sativa L., the content of protein is 10.6-9.9 g/100g, in Oryza sativa L.
The content of fat is 1.5-1.7 g/100g, is specifically shown in Table 2；
Table 2 is the per mu yield of protein, fat content and Oryza sativa L. in Oryza sativa L.
2. reducing the sickness rate of rice disease, the sickness rate of the false smut of Oryza sativa L. is 2%-3%, the sickness rate of rice blast is 2%-
3%, the sickness rate of rice leaf smut be 1%-2%, the sickness rate of bakanae disease of rice be 3%-4%, the sickness rate of rice sheath blight disease be
1%-2%, is specifically shown in Table 3；
Table 3 is the sickness rate of the false smut of Oryza sativa L., rice blast, rice leaf smut, bakanae disease of rice, rice sheath blight disease；
Brassica oleracea L. var. botrytis L. planting process is applied:
1. the yield of the Brassica oleracea L. var. botrytis L. effect of being significantly improved, per mu yield reaches 5500-6000 jin, vitamin C, vitamin E in Brassica oleracea L. var. botrytis L.
Content had significant raising, in Brassica oleracea L. var. botrytis L., ascorbic content is 76-92 mg/100g, and the content of vitamin E is
0.8-1.1 mg/100g, is specifically shown in Table 4；
Table 4 is the per mu yield of vitamin C, content of vitamin E and Brassica oleracea L. var. botrytis L. in Brassica oleracea L. var. botrytis L.
2. reducing the sickness rate of cauliflower disease, the sickness rate of the black rot of Brassica oleracea L. var. botrytis L. is 1%-3%, the sickness rate of melasma is
2%-5%, the sickness rate of balck shank are 0.5%-1%, the sickness rate of downy mildew is 2%-7%, are specifically shown in Table 5；
Table 5 is the sickness rate of the black rot of Brassica oleracea L. var. botrytis L., melasma, balck shank, downy mildew
Comparison: do not use of the present invention containing Flos Caryophylli extract insecticide, use clear water to spray.
Above-mentioned detailed description of the invention is exemplary, is to enable those skilled in the art to be better understood from this
Summary of the invention, should not be understood as limiting the scope of the invention, as long as according to changing that technical solution of the present invention is made
Enter, each fall within protection scope of the present invention.
Claims (10)
1. the insecticide containing Aloe extract, it is characterised in that: the described insecticide containing Aloe extract, including pungent sulfur
Phosphorus, Aloe extract, Celastrus orbiculatus Thunb. Extract, jingganmycin, tea tree oil and ammonium sulfate.
A kind of insecticide containing Aloe extract, it is characterised in that: described containing Aloe extract
Insecticide, in parts by weight, content is: phoxim 13-17 part, emulsifying agent 5-9 part, organic solvent 14-18 part, cosolvent 2-6
Part, Aloe extract 1-4 part, Celastrus orbiculatus Thunb. Extract 1-4 part, jingganmycin 1-4 part, tea tree oil 1-4 part, ammonium sulfate 1-4 part.
A kind of insecticide containing Aloe extract, it is characterised in that: described containing Aloe extract
Insecticide, in parts by weight, content is: phoxim 15 parts, emulsifying agent 7 parts, organic solvent 16 parts, cosolvent 4 parts, Aloe are extracted
Thing 2 parts, Celastrus orbiculatus Thunb. Extract 2 parts, jingganmycin 3 parts, tea tree oil 3 parts, 3 parts of ammonium sulfate.
A kind of insecticide containing Aloe extract, it is characterised in that: described phoxim effective ingredient
Weight/mass percentage composition be 98%.
A kind of insecticide containing Aloe extract, it is characterised in that: described emulsifying agent is that phenol gathers
Oxygen vinyl Ether；
Described organic solvent is dimethylbenzene, and the density of described dimethylbenzene is 0.87g/cm3；
Described cosolvent is n-butyl alcohol.
A kind of insecticide containing Aloe extract, it is characterised in that: described Aloe extract contains
Having aloe-emodin, Aloe chrysophanol, aloe saponaria glycosides and Aloearbonaside, the content of described aloe-emodin is 96%, Aloe Radix Et Rhizoma Rhei
The content of phenol is 1%, the content of aloe saponaria glycosides is 1%, the content of Aloearbonaside is 1%；
Containing tripterine, pristimerin, dihydroagarofuran type sesquiterpene in described Celastrus orbiculatus Thunb. Extract, described Radix Tripterygii Wilfordii
The content of red pigment is 90%, the content of pristimerin is 1%, the content of dihydroagarofuran type sesquiterpene is 1%.
7. the method for producing insecticide containing Aloe extract, it is characterised in that: comprise the following steps: Aloe is extracted in preparation
Thing；Prepare Celastrus orbiculatus Thunb. Extract；Weigh；Mixing.
A kind of method for producing insecticide containing Aloe extract, it is characterised in that: preparation Aloe
Extract, comprises the following steps:
(1) take Aloe, pulverize；
(2) reflux, extract, 3 times after soaking with 10 times amount 80% ethanol waters, extracts 4h every time, filters, obtain ethanol extract and
Filtering residue, merges ethanol extract, stands 50h, filters off precipitation, and recycling design obtains crude extract；
(3) water-soluble crude extract, upper macroporous adsorptive resins, after washing desaccharide, with 82% ethanol water eluting, collect ethanol and wash
De-liquid, recycling design obtains extract；
(4) water-soluble extract, successively with 15 times amount dichloromethane, ethyl acetate, n-butanol extraction；
(5) concentrating remaining aqueous phase after extraction, being washed till concentrate with methanol can not be dissolved again, obtains final extract.
A kind of method for producing insecticide containing Aloe extract, it is characterised in that: weigh, bag
Include following steps: according to a kind of formula containing Aloe extract, weigh each raw material respectively.
A kind of method for producing insecticide containing Aloe extract, it is characterised in that: mixing, bag
Include following steps:
(1) by phoxim, dimethylbenzene, n-butyl alcohol, Celastrus orbiculatus Thunb. Extract, Aloe extract, jingganmycin, tea tree oil, ammonium sulfate
Mixing, stirs；
(2) gained mixture is put into the drying room of band water leg, and the temperature controlling water leg is 78-80 DEG C, is mixed by gained in (1)
Polymer melt becomes liquid, under nitrogen protection stirring 60 minutes；
(3) in the mixing liquid of gained, add phenol polyoxyethylene ether to stir 20 minutes, obtain the parasite killing containing Aloe extract
Agent；Obtained insecticide is emulsifiable concentrate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610276230.XA CN105918361A (en) | 2016-04-29 | 2016-04-29 | Pesticide containing aloe extract and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610276230.XA CN105918361A (en) | 2016-04-29 | 2016-04-29 | Pesticide containing aloe extract and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105918361A true CN105918361A (en) | 2016-09-07 |
Family
ID=56836719
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610276230.XA Pending CN105918361A (en) | 2016-04-29 | 2016-04-29 | Pesticide containing aloe extract and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105918361A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106070371A (en) * | 2016-08-16 | 2016-11-09 | 惠安县科联农业科技有限公司 | Rhizoma Smilacis Glabrae extract application in preventing and treating Radix Raphani black rot |
| CN106490043A (en) * | 2016-10-12 | 2017-03-15 | 云南万绿生物股份有限公司 | A kind of plant source insect-proof agent with aloe barbadensis Miller as raw material and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1263708A (en) * | 2000-02-23 | 2000-08-23 | 武予清 | 'Xinbei' emulsified oil as agricultural chemical for preventing and eliminating beet noctuids |
| CN1483451A (en) * | 2003-07-18 | 2004-03-24 | 王舒妍 | Method for extracting 50% aloetin |
| CN102669163A (en) * | 2011-03-16 | 2012-09-19 | 秦施豪 | Phoxim-pyridaben missible oil |
-
2016
- 2016-04-29 CN CN201610276230.XA patent/CN105918361A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1263708A (en) * | 2000-02-23 | 2000-08-23 | 武予清 | 'Xinbei' emulsified oil as agricultural chemical for preventing and eliminating beet noctuids |
| CN1483451A (en) * | 2003-07-18 | 2004-03-24 | 王舒妍 | Method for extracting 50% aloetin |
| CN102669163A (en) * | 2011-03-16 | 2012-09-19 | 秦施豪 | Phoxim-pyridaben missible oil |
Non-Patent Citations (4)
| Title |
|---|
| 朱俊义等: "《中国长白山木本植物彩色图志》", 30 September 2013 * |
| 贾敏如: "《国际传统药物和天然药物》", 31 October 2006 * |
| 邹先伟: "中华芦荟叶提取物的杀虫活性研究", 《万方学位论文库》 * |
| 高文胜等: "《无公害果园首选农药100种 第3版》", 31 January 2014 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106070371A (en) * | 2016-08-16 | 2016-11-09 | 惠安县科联农业科技有限公司 | Rhizoma Smilacis Glabrae extract application in preventing and treating Radix Raphani black rot |
| CN106490043A (en) * | 2016-10-12 | 2017-03-15 | 云南万绿生物股份有限公司 | A kind of plant source insect-proof agent with aloe barbadensis Miller as raw material and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| Kaliyadasa et al. | A review on golden species of Zingiberaceae family around the world: Genus Curcuma | |
| Aćimović et al. | Cymbopogon citratus (DC.) Staph: Chemical composition, antimicrobial and antioxidant activities, use in medicinal and cosmetic purpose | |
| KR101974499B1 (en) | Cosmetic Composition For Clearing Scalp Keratin And Dandruff, And Improving Hair Using Containing Chojeong Carbonated Water | |
| Kanu et al. | A review of the multifaceted usefulness of Celosia argentea Linn | |
| CN105918361A (en) | Pesticide containing aloe extract and preparation method thereof | |
| CN105831164A (en) | Pesticide for preventing and controlling cotton diseases and insect pests and preparation method thereof | |
| Kozak et al. | Health properties of selected herbal plants | |
| CN110465040A (en) | A kind of degradation agent and its preparation and application of farm-forestry crop pesticide residue of degrading | |
| Mariod | Multiple biological activities of unconventional seed oils | |
| CN109010173A (en) | A kind of multi-functional skin care is spraying and preparation method thereof | |
| CN105831168A (en) | Botanical pesticide and preparing method thereof | |
| JP2016193882A (en) | Anti-aging agent | |
| CN105104457B (en) | A kind of microbicide compositions | |
| CN106973952A (en) | A kind of preparation method for the natural bactericidal agent for preventing and treating safron root rot | |
| CN112656716A (en) | Green healthy skin cream and preparation method thereof | |
| KR102177613B1 (en) | Cosmetic composition for slimming comprising complex extracts of Taraxacum platycarpum, Lonicera japonica and Perilla frutescens | |
| CN105875676A (en) | Pinellia ternata extract containing plant pesticide special for corns in saline and alkaline land and preparation method thereof | |
| CN107242255B (en) | Plant insecticide for repelling and killing mosquitoes and preparation method thereof | |
| CN105394106A (en) | Compound pesticide for preventing and treating oilseed rape aphids and preparation method thereof | |
| CN104547022A (en) | Traditional Chinese medicinal composition capable of clearing heat, moistening lung, relieving sore throat and detoxifying | |
| Makarova et al. | Apium graveolens L.: A phytochemical and pharmacological review | |
| CN108935538A (en) | A kind of agriculture and forestry control of insect liquid pesticidal and its making and use method | |
| CN105613634B (en) | Dendrobium candidum is special organic except spiral shell medicinal powder and preparation method thereof | |
| CN109258714A (en) | A kind of biological insecticides and preparation method thereof for preventing and treating vegetable aphid | |
| KR20190041776A (en) | Health tea composition and health tea using medicinal herbs |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160907 |
|
| RJ01 | Rejection of invention patent application after publication |