CN105907147A - Photocatalyst containing oil paint and preparation method thereof - Google Patents
Photocatalyst containing oil paint and preparation method thereof Download PDFInfo
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- CN105907147A CN105907147A CN201610278500.0A CN201610278500A CN105907147A CN 105907147 A CN105907147 A CN 105907147A CN 201610278500 A CN201610278500 A CN 201610278500A CN 105907147 A CN105907147 A CN 105907147A
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- photocatalyst
- kieselguhr
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/06—Artists' paints
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D105/00—Coating compositions based on polysaccharides or on their derivatives, not provided for in groups C09D101/00 or C09D103/00
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Catalysts (AREA)
Abstract
The invention mainly belongs to the field of oil paint and particularly relates to photocatalyst containing oil paint and a preparation method thereof. The photocatalyst containing oil paint is prepared from, by weight, 20-35 parts of paint powder, 10-15 parts of a dispersion stabilizer, 35-45 parts of an adhesive, 2-6 parts of a wetting agent, 10-25 parts of filler, 1-2 parts of a drier and 5-10 parts of a purificatory absorbent, wherein the purificatory absorbent comprises diatomite and a photocatalyst. Since the purificatory absorbent which contains the photocatalyst is added into the photocatalyst containing oil paint, oil paintings drawn with the photocatalyst containing oil paint have a function of air purification.
Description
Technical field
The present invention principally falls into oil colour field, is specifically related to a kind of oil colour containing photocatalyst and preparation method thereof.
Background technology
Pigment is divided into Chinese painting color, oil colour, gouache color, is the artistic drawing set commonly used, and some organic pigments and synthetic dyestuff have certain toxicity；Jointing material in some pigment even contains formaldehyde.
Development along with society, air pollution problem inside rooms is increasingly severe, and the pollutant sources of room air includes: gas with foreign flavor that the harmful gas discharged from industrial pollution diffusion, organic corrupt decomposition, plastics, coating, construction material etc. in room air and people and house pet are discharged etc.；
Photocatalyst, conversational implication is said catalyst is exactly the meaning of catalyst, and photocatalyst is as the term suggests being exactly photocatalyst.Catalyst is the chemical substance accelerating chemical reaction, and itself is also not involved in reaction.Photocatalyst is exactly the general designation of the chemical substance that can play catalytic action under the exciting of photon.In the world can be numerous as the material of photocatalyst, including titanium dioxide (TiO2), zinc oxide (ZnO), stannum oxide (SnO2), zirconium dioxide (ZrO2), the many oxide sulfide semiconductor such as cadmium sulfide (CdS), wherein titanium dioxide (Titanium Dioxide) because of its oxidability strong, stable chemical nature is nontoxic, becomes the most hot nano photocatalyst catalytic material.
Under the effect of photocatalyst, indoor polluter can be harmless, the product of odorless by photodissociation, and can kill the pathogenic microorganism in air simultaneously.
In view of the foregoing, exploitation one can adsorb harmful substance, and the pigment of environment purification is the most necessary.
Summary of the invention
For the problems referred to above, the present invention provides a kind of oil colour containing photocatalyst；Being added with absorption purifier in the described oil colour containing photocatalyst, comprise kieselguhr and photocatalyst in described absorption purifier, the oil painting obtained hence with oil colour of the present invention drawing can have Air purification.
The present invention is achieved by the following technical solutions:
A kind of oil colour containing photocatalyst, described oil colour includes pigment powder, dispersion stabilizer, adhesive, wetting agent, filler, drier and absorption purifier；Described absorption purifier includes that kieselguhr and photocatalyst, described oil colour include the component of following weight portion: pigment powder 20-35 part, dispersion stabilizer 10-15 part, adhesive 35-45 part, wetting agent 2-6 part, filler 10-25 part, drier 1-2 part and absorption purifier 5-10 part.
Further, in described absorption purifier, kieselguhr is carrier, tripolite loading photocatalyst, and described photocatalyst is titanium dioxide.
Further, described adhesive uses Fructus Pruni salicinae natural gum.
Further, described dispersion stabilizer is modified castor oil；Wetting agent is any one in Semen Lini oil, Oleum Juglandis, poppy seed oil, safflower oil, Oleum Helianthi；Described filler is the mixture that calcium carbonate, Pulvis Talci and Kaolin configure according to mass ratio 1:1:1；Described drier is dibutyl tin laurate.
The preparation method of a kind of oil colour containing photocatalyst, for preparing described a kind of oil colour containing photocatalyst, it is characterised in that described preparation method specifically includes following steps:
(1) when addition 35-45 part adhesive is heated to 80-90 DEG C in a reservoir, maintain 40min in this temperature range, obtain bonding glue；
(2) bonding glue addition ball mill 10-25 part filler, 20-35 part pigment powder and step (1) prepared carries out ball milling 2-4h, controls ball milling temperature and be 25-40 DEG C, it is thus achieved that pigment premix material；
(3) 100-150 mesh sieve is crossed in the described pigment premix material that step (2) prepares, it is subsequently adding 2-6 part wetting agent, 10-15 part dispersion stabilizer, is placed in blender and stirs, control mixing speed 2000-3000 rev/min, whipping temp controls at 60-90 DEG C, stirs 30min；
(4) after step (4), add 1-2 part drier and 5-10 part absorption purifier, stir, it is thus achieved that containing the oil colour of photocatalyst；Wherein, containing photocatalyst in described absorption purifier.
Further, described absorption purifier preparation method particularly as follows:
(1) kieselguhr acidleach processes: added water by the kieselguhr that particle diameter is 800-1000um, obtain the kieselguhr slurry that mass concentration is 23-30%, adds dilute sulfuric acid and sodium dithionite, carry out acid-leaching reaction 15-20h；Described dilute sulfuric acid mass concentration is 20-35%, and dilute sulfuric acid consumption is the 0.5-1.0% of described kieselguhr slurry volume, and sodium dithionite consumption is the 1.0-1.5% of described kieselguhr slurry solid content；
(2) diatomite calcination brightens: kieselguhr slurries filtration after step (1) acidleach being processed, washes with water, dry, it is thus achieved that the diatomite powder after drying；Described diatomite powder after drying adds Linesless charcoal and sodium bicarbonate, as calcining furnace being carried out calcine to improve diatomaceous whiteness after mixing, obtains after calcining and brighten rear kieselguhr；
(3) preparation of absorption purifier: rear kieselguhr is brightened in the calcining that step (2) obtains and pulverizes, after controlling to pulverize, kieselguhr particle diameter is 700-800um, photocatalyst is mixed with kieselguhr after pulverizing, so that tripolite loading photocatalyst, prepares described absorption purifier.
Further, during step (2) diatomite calcination brightens, the condition of calcining is: calcining heat is 600-700 DEG C, and Linesless charcoal consumption is the 0.5-0.9% of the diatomite powder weight after described drying, and sodium bicarbonate consumption is the 0.5%-2.0% of the diatomite powder weight after described drying.
The Advantageous Effects of the present invention:
(1) oil colour containing photocatalyst of the present invention is added with in the described absorption purifier of absorption purifier containing photocatalyst, it is carrier loaded photocatalyst with kieselguhr, under the effect of photocatalyst, indoor polluter can be harmless, the product of odorless by photodissociation, and can kill the pathogenic microorganism in air simultaneously；Draw, hence with oil colour of the present invention, the oil painting obtained and can have Air purification.
(2) firming agent in oil colour uses Fructus Pruni salicinae natural gum, and compared with the Radix Acaciae senegalis in conventional art, the ability forming protecting film is higher.
Detailed description of the invention
In order to make the purpose of the present invention, technical scheme and advantage clearer, below in conjunction with embodiment, the present invention is explained in further detail.Should be appreciated that specific embodiment described herein is used only for explaining the present invention, be not intended to limit the present invention.
On the contrary, the present invention contains any replacement made in the spirit and scope of the present invention, amendment, equivalent method and scheme being defined by the claims.Further, in order to make the public that the present invention to be had a better understanding, in below the details of the present invention being described, detailed describe some specific detail sections.The description not having these detail sections for a person skilled in the art can also understand the present invention completely.
Embodiment
1
A kind of oil colour containing photocatalyst, described oil colour includes pigment powder, dispersion stabilizer, adhesive, wetting agent, filler, drier and absorption purifier；Described absorption purifier includes that kieselguhr and photocatalyst, described oil colour include the component of following weight portion: 20 parts of pigment powder, dispersion stabilizer 10 parts, adhesive 35 parts, wetting agent 2 parts, filler 10 parts, drier 1 part and absorption purifier 5 parts.
In described absorption purifier, kieselguhr is carrier, tripolite loading photocatalyst.Kieselguhr is a kind of natural material, has that porosity is big, stable chemical nature, a feature such as wear-resisting, heat-resisting, also has dehumidifying, deodorization, purifying the air of a room etc. acts on；Being carrier loaded photocatalyst with kieselguhr, under the effect of photocatalyst, indoor polluter can be harmless, the product of odorless by photodissociation, and can kill the pathogenic microorganism in air simultaneously；In sum, oil colour of the present invention adds absorption purifier；Utilize oil colour of the present invention to draw the oil painting obtained and can have Air purification.
Described adhesive uses Fructus Pruni salicinae natural gum；Why selecting particle natural gum, be based on following reason: first reason, Fructus Pruni salicinae natural gum can make the viscosity of water increase on the one hand, on the other hand forms protecting film on the surface of granules of pigments, prevents pigment particles aggregate；Other polysaccharide, such as Resina persicae and arabic gum, have the ability of these two aspects equally, and stablizing effect effect compared with Fructus Pruni salicinae natural gum are poor.
Wherein, the preparation of Fructus Pruni salicinae of the present invention natural gum is particularly as follows: put into the Fructus Pruni salicinae natural gum of collection and soak, and add soda powder, the weight of soda powder is the 0.05% of Fructus Pruni salicinae natural gum weight, soaking temperature controls at 30-35 DEG C, and soak time 4-5 hour proceeds in pressure vessel and inputs steam, when temperature reaches 110 DEG C in container, keep this temperature 60min；Turn on agitator carries out stirring at low speed 250r/min to material water mixture) 40min；Warming while stirring, when temperature rises to 115 DEG C, slowly improves the speed of agitator to 300r/min；Continuously stirred 60 min under conditions of 300r/min rotating speed, 115 DEG C of temperature；Again improve mixing speed and rise to 120 DEG C to 600r/min, temperature, be kept stirring for 120 min；Steam off, reduction mixing speed, to 300r/min, stirs 120min；Close agitator.
When container pressure is down to normal pressure, being stored in precipitation vessel after being filtered by glue solution, the solution after filtering with clean water dilutes 4 times, and allows its physics settle 24 hours.Afterwards, upper strata settled solution is carried out after filtration treatment in suction reactor, and again remove impurity in solution (color and luster deeper glue solution can bleach with bleach) with ion-exchange process.Lurid solution can be obtained through above-mentioned steps, then with the drainage screen of 5 micron pore size, solution carried out pressurizing filter (also can adopt molecular film filter method).Finally give the Fructus Pruni salicinae natural gum that purity is higher.It is noted that once 2 point during purifying: (1) Fructus Pruni salicinae natural gum is hydrophilic colloid, and insoluble in majority of organic solvents such as ethanol, glue, water separate and uses vacuum distillation mode, ethanol reusable edible, it is possible to directly utilize ethanol by colloidal precipitation.(2) colloid is pulverized with broken, disintegrating apparatus after drying, and obtain is the powder granule that can flow freely white (or light beige) Fructus Pruni salicinae natural gum.
Described dispersion stabilizer is modified castor oil；Wetting agent is any one in Semen Lini oil, Oleum Juglandis, poppy seed oil, safflower oil, Oleum Helianthi；Described filler is the mixture that calcium carbonate, Pulvis Talci and Kaolin configure according to mass ratio 1:1:1；Described drier is dibutyl tin laurate.
A kind of preparation method of the oil colour containing photocatalyst, described preparation method is for preparing described a kind of oil colour containing photocatalyst, and described preparation method specifically includes following steps:
(1) when 35 parts of adhesives of addition are heated to 80-90 DEG C in a reservoir, maintain 40min in this temperature range, obtain bonding glue；
(2) the bonding glue addition ball mill 10 parts of fillers, 20 parts of pigment powder and step (1) prepared carries out ball milling 2-4h, controls ball milling temperature and be 25-40 DEG C, it is thus achieved that pigment premix material；
(3) 100-150 mesh sieve is crossed in the described pigment premix material that step (2) prepares, it is subsequently adding 2 parts of wetting agent, 10 portions of dispersion stabilizers, is placed in blender and stirs, control mixing speed 2000-3000 rev/min, whipping temp controls at 60-90 DEG C, stirs 30min；
(4) after step (4), add 1 part of drier and 5 parts of absorption purifiers, stir, it is thus achieved that containing the oil colour of photocatalyst；Wherein, containing photocatalyst in described absorption purifier.
The preparation method of described absorption purifier particularly as follows:
(1) kieselguhr acidleach processes: added water by the kieselguhr that particle diameter is 800-1000um, obtain the kieselguhr slurry that mass concentration is 23-30%, adds dilute sulfuric acid and sodium dithionite, carry out acid-leaching reaction 15-20h；Described dilute sulfuric acid mass concentration is 20-35%, and dilute sulfuric acid consumption is the 0.5-1.0% of described kieselguhr slurry volume, and sodium dithionite consumption is the 1.0-1.5% of described kieselguhr slurry solid content；
(2) diatomite calcination brightens: kieselguhr slurries filtration after step (1) acidleach being processed, washes with water, dry, it is thus achieved that the diatomite powder after drying；Described diatomite powder after drying adds Linesless charcoal and sodium bicarbonate, as calcining furnace being carried out calcine to improve diatomaceous whiteness after mixing, obtains after calcining and brighten rear kieselguhr；
(3) preparation of absorption purifier: rear kieselguhr is brightened in the calcining that step (2) obtains and pulverizes, after controlling to pulverize, kieselguhr particle diameter is 700-800um, photocatalyst is mixed with kieselguhr after pulverizing, so that tripolite loading photocatalyst, prepares described absorption purifier.
Embodiment
2
A kind of oil colour containing photocatalyst, described oil colour includes pigment powder, dispersion stabilizer, adhesive, wetting agent, filler, drier and absorption purifier；Described absorption purifier includes kieselguhr and photocatalyst, and described oil colour formula proportion is according to weight ratio: 35 parts of pigment powder, dispersion stabilizer 15 parts, adhesive 45 parts, wetting agent 6 parts, filler 25 parts, drier 2 parts and absorption purifier 10 parts.Preparation method is with embodiment 1.
Embodiment
3
A kind of oil colour containing photocatalyst, described oil colour includes pigment powder, dispersion stabilizer, adhesive, wetting agent, filler, drier and absorption purifier；Described absorption purifier includes kieselguhr and photocatalyst, and described oil colour formula proportion is according to weight ratio: 25 parts of pigment powder, dispersion stabilizer 13 parts, adhesive 40 parts, wetting agent 4 parts, filler 15 parts, drier 1.5 parts and absorption purifier 8 parts.Preparation method is with embodiment 1.
Claims (7)
1. the oil colour containing photocatalyst, it is characterised in that described oil colour includes pigment powder, dispersion stabilizer, adhesive, wetting agent, filler, drier and absorption purifier；Described absorption purifier includes that kieselguhr and photocatalyst, described oil colour include the component of following weight portion: pigment powder 20-35 part, dispersion stabilizer 10-15 part, adhesive 35-45 part, wetting agent 2-6 part, filler 10-25 part, drier 1-2 part and absorption purifier 5-10 part.
A kind of oil colour containing photocatalyst, it is characterised in that in described absorption purifier, kieselguhr is carrier, tripolite loading photocatalyst, and described photocatalyst is titanium dioxide.
A kind of oil colour containing photocatalyst, it is characterised in that described adhesive uses Fructus Pruni salicinae natural gum.
A kind of oil colour containing photocatalyst, it is characterised in that described dispersion stabilizer is modified castor oil；Wetting agent be Semen Lini oil, Oleum Juglandis, poppy seed oil, safflower oil,
Any one in Oleum Helianthi；Described filler is the mixture that calcium carbonate, Pulvis Talci and Kaolin configure according to mass ratio 1:1:1；Described drier is dibutyl tin laurate.
5. the preparation method of oil colour containing photocatalyst, for preparing the described a kind of oil colour containing photocatalyst of one of claim 1-4, it is characterised in that described preparation method specifically includes following steps:
(1) when addition 35-45 part adhesive is heated to 80-90 DEG C in a reservoir, maintain 40min in this temperature range, obtain bonding glue；
(2) bonding glue addition ball mill 10-25 part filler, 20-35 part pigment powder and step (1) prepared carries out ball milling 2-4h, controls ball milling temperature and be 25-40 DEG C, it is thus achieved that pigment premix material；
(3) 100-150 mesh sieve is crossed in the described pigment premix material that step (2) prepares, it is subsequently adding 2-6 part wetting agent, 10-15 part dispersion stabilizer, is placed in blender and stirs, control mixing speed 2000-3000 rev/min, whipping temp controls at 60-90 DEG C, stirs 30min；
(4) after step (4), add 1-2 part drier and 5-10 part absorption purifier, stir, it is thus achieved that containing the oil colour of photocatalyst；Wherein, containing photocatalyst in described absorption purifier.
A kind of preparation method of the oil colour containing photocatalyst, it is characterised in that the preparation method of described absorption purifier particularly as follows:
(1) kieselguhr acidleach processes: added water by the kieselguhr that particle diameter is 800-1000um, obtain the kieselguhr slurry that mass concentration is 23-30%, adds dilute sulfuric acid and sodium dithionite, carry out acid-leaching reaction 15-20h；Described dilute sulfuric acid mass concentration is 20-35%, and dilute sulfuric acid consumption is the 0.5-1.0% of described kieselguhr slurry volume, and sodium dithionite consumption is the 1.0-1.5% of described kieselguhr slurry solid content；
(2) diatomite calcination brightens: kieselguhr slurries filtration after step (1) acidleach being processed, washes with water, dry, it is thus achieved that the diatomite powder after drying；Described diatomite powder after drying adds Linesless charcoal and sodium bicarbonate, as calcining furnace being carried out calcine to improve diatomaceous whiteness after mixing, obtains after calcining and brighten rear kieselguhr；
(3) preparation of absorption purifier: rear kieselguhr is brightened in the calcining that step (2) obtains and pulverizes, after controlling to pulverize, kieselguhr particle diameter is 700-800um, photocatalyst is mixed with kieselguhr after pulverizing, so that tripolite loading photocatalyst, prepares described absorption purifier.
A kind of preparation method of the oil colour containing photocatalyst, it is characterized in that, during step (2) diatomite calcination brightens, the condition of calcining is: calcining heat is 600-700 DEG C, Linesless charcoal consumption is the 0.5-0.9% of the diatomite powder weight after described drying, and sodium bicarbonate consumption is the 0.5%-2.0% of the diatomite powder weight after described drying.
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| CN201610278500.0A CN105907147A (en) | 2016-05-03 | 2016-05-03 | Photocatalyst containing oil paint and preparation method thereof |
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| CN201610278500.0A CN105907147A (en) | 2016-05-03 | 2016-05-03 | Photocatalyst containing oil paint and preparation method thereof |
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| CN106634124A (en) * | 2016-12-05 | 2017-05-10 | 钦州市钦南区生产力促进中心 | Oil painting pigment and preparation method thereof |
| CN108359300A (en) * | 2018-02-10 | 2018-08-03 | 谢新昇 | A kind of preparation method of the anti-dust suction oil colour of quick-dry type |
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| CN106634124A (en) * | 2016-12-05 | 2017-05-10 | 钦州市钦南区生产力促进中心 | Oil painting pigment and preparation method thereof |
| CN108359300A (en) * | 2018-02-10 | 2018-08-03 | 谢新昇 | A kind of preparation method of the anti-dust suction oil colour of quick-dry type |
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Application publication date: 20160831 |