CN105902445B - A kind of plant antiseptic agent composition for cosmetics and preparation method thereof - Google Patents
A kind of plant antiseptic agent composition for cosmetics and preparation method thereof Download PDFInfo
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- CN105902445B CN105902445B CN201610421941.1A CN201610421941A CN105902445B CN 105902445 B CN105902445 B CN 105902445B CN 201610421941 A CN201610421941 A CN 201610421941A CN 105902445 B CN105902445 B CN 105902445B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
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Abstract
The invention discloses a kind of plant antiseptic agent composition for cosmetics and preparation method thereof, it is desirable to provide a kind of natural no stimulation, antiseptic property is good, and available for the plant antiseptic agent composition of cosmetics, the preservative is mainly made up of following component components：10 20 parts of prickly ash berries, 10 20 parts of the Chinese bulbul, 10 20 parts of sunglo of palpus, 5 10 parts of Magnolia bark, 5 10 parts of the coptis；Belong to cosmetic technical field.
Description
Technical field
The invention discloses a kind of plant antiseptic agent composition, is a kind of antiseptic for cosmetics specifically
Agent composition, the invention also discloses the preparation method of the plant antiseptic agent composition, belong to cosmetic technical field.
Background technology
In order to prevent microorganism from growing in the product, keep the property of skin care item not variable stably and after use of uncapping
Matter, reduce the trace of bacteria being likely to occur in products material storage, production, product bottling and corrode, in skin care item generally all
Add preservative.
It is loosely organized but excessive or inappropriate preservative can make epidermal cell developmental immaturity, so that epidermis becomes
It is thin, easily declined by environmental stimuli, phylactic power defensive power；Meeting damaging cells DNA, makes skin follow the string gradually, easily produces and relaxes, be thin
Line；And constantly defect can then be bred by the Skin Cell of preservative infringement, make skin quality worse and worse.
The content of the invention
In view of the above-mentioned problems, it is an object of the invention to provide a kind of natural no stimulation, antiseptic property it is good be used for cosmetics
Plant antiseptic agent composition and preparation method thereof.
In order to solve the above technical problems, technical scheme provided by the invention is such：
A kind of plant antiseptic agent composition for cosmetics, mainly it is made up of following component components：Prickly ash berries 10-20
Part, Chinese bulbul 10-20 parts, palpus sunglo 10-20 parts, Magnolia bark 5-10 parts, coptis 5-10 parts.
Further, the above-mentioned plant antiseptic agent composition for cosmetics, in addition to tealeaves 3-5 parts.
Further, the above-mentioned plant antiseptic agent composition in cosmetics, in addition to Herba Moslae Chinensis 1-3 parts.
Further, above-mentioned a kind of plant antiseptic agent composition for cosmetics, described plant antiseptic agent group
Compound is made up of following component components：15 parts of prickly ash berries, 15 parts of the Chinese bulbul, 8 parts of 1 Magnolia bark of palpus sunglo, 8 parts of the coptis, tealeaves 4
Part, 2 parts of Herba Moslae Chinensis.
Further, the above-mentioned plant antiseptic agent composition for cosmetics, in described plant antiseptic agent composition
Also added with the one or more in 1,2- pentanediols, 1,2- hexylene glycols, 1,3- propane diols.
Latter solution provided by the invention is such：
The preparation method of the above-mentioned plant antiseptic agent composition for cosmetics, this method comprise the steps successively：
(1) raw material is weighed according to weight described in claim 1, mixed, 40 mesh sieves are crossed after smashing；
(2) according to weight than 1:15-30 ratio mixes the mixture in step (1) with 50-70% ethanol solution,
Sealing immersion 3-6 hours；
(3) raw material obtained in step (2) is put into ultrahigh pressure vessel, pressurize 200-400MPa, pressurize extraction 5-
After 10min, feed liquid, which is crossed to filter out, takes solid residue, and extraction is concentrated under reduced pressure, and recovery ethanol is to without alcohol taste；
(4) according to weight than 1：2~1：Anti-corrosion synergy moisturizing is added in concentrate obtained by from 3 ratio to step (3)
Agent, filter, centrifuging and taking supernatant, produce.
Compared with prior art, technical scheme provided by the invention has following technological merit：
1st, in technical scheme provided by the invention, prickly ash berries, the Chinese bulbul, palpus sunglo, Magnolia bark, coptis synergy,
By being chemically reacted with each target spot in microbial cell, the metabolism of interference cell, the structure of cell is destroyed, or
The osmotic pressure that person influences microbial cell carries out anti-corrosion.
2nd, also include the coptis, tealeaves, Herba Moslae Chinensis in technical scheme provided by the invention, while also add 1,2- pentanediols,
1,2- hexylene glycol, 1,3-PD etc., further increase antiseptic property, and experiment confirms to include large intestine to various harmful bacteria species
A variety of gram-positive bacterias such as the Gram-negative bacterias such as bacillus, hay bacillus and streptococcus and fungi have inhibitory action.
Plant antiseptic agent raw material sources provided by the invention are daily conventional natural plants, with safe and harmless natural
Plant is the chemical preservative that raw material replaces chemical industry synthesis, the infringement to human skin cell is minimized, non-stimulated or mistake
Quick reaction.
Plant antiseptic agent provided by the invention has favorable compatibility, has biodegradability.
Embodiment
The claim of the present invention is described in further detail with reference to specific embodiment, but not formed to this hair
Bright any restrictions, anyone changes in the limited number of time of the claims in the present invention protection domain, still the claim in the present invention
In protection domain.
Embodiment 1
A kind of plant antiseptic agent composition for cosmetics provided by the invention, it is characterised in that by following component systems
Into：Prickly ash berries 20g, Chinese bulbul 10g, must sunglo 20g, Magnolia bark 5g, coptis 10g.
Embodiment 2
A kind of plant antiseptic agent composition for cosmetics provided by the invention, it is characterised in that by following component systems
Into：Prickly ash berries 10g, Chinese bulbul 20g, must sunglo 10g, Magnolia bark 10g, coptis 5g.
The preparation method of Examples 1 and 2 is as follows：
(1) raw material is weighed, is mixed, 40 mesh sieves are crossed after smashing；
(2) according to weight than 1:15 ratio mixes the mixture in step (1) with 70% ethanol solution, sealing leaching
Bubble 6 hours；
(3) raw material obtained in step (2) is put into ultrahigh pressure vessel, pressurize 200MPa, pressurize extraction 10min
Afterwards, feed liquid, which is crossed to filter out, takes solid residue, and extraction is concentrated under reduced pressure, and recovery ethanol is to without alcohol taste；
(4) according to weight than 1：1,2- pentanediols are added in concentrate obtained by from 2 ratio to step (3), are filtered, from
The heart takes supernatant, produces.
Embodiment 3
A kind of plant antiseptic agent composition for cosmetics provided by the invention, it is characterised in that by following component systems
Into：Prickly ash berries 12g, Chinese bulbul 12g, must sunglo 13g, Magnolia bark 7g, coptis 8g, tealeaves 5g.
Embodiment 4
A kind of plant antiseptic agent composition for cosmetics provided by the invention, it is characterised in that by following component systems
Into：Prickly ash berries 10g, Chinese bulbul 16g, must sunglo 16g, Magnolia bark 8g, coptis 8g, tealeaves 3g.
The preparation method of embodiment 3 and 4 is as follows：
(1) raw material is weighed, is mixed, 40 mesh sieves are crossed after smashing；
(2) according to weight than 1:20 ratio mixes the mixture in step (1) with 60% ethanol solution, sealing leaching
Bubble 4.5 hours；
(3) raw material obtained in step (2) is put into ultrahigh pressure vessel, pressurize 300MPa, after pressurize extraction 7min,
Feed liquid, which is crossed to filter out, takes solid residue, and extraction is concentrated under reduced pressure, and recovery ethanol is to without alcohol taste；
(4) according to weight than 1：1,2- hexylene glycols are added in concentrate obtained by from 2.5 ratio to step (3), are filtered,
Centrifuging and taking supernatant, is produced.
Embodiment 5
A kind of plant antiseptic agent composition for cosmetics provided by the invention, it is characterised in that by following component systems
Into：Prickly ash berries 18g, Chinese bulbul 18g, must sunglo 15g, Magnolia bark 6g, coptis 6g, Herba Moslae Chinensis 1g.
Embodiment 6
A kind of plant antiseptic agent composition for cosmetics provided by the invention, it is characterised in that by following component systems
Into：Prickly ash berries 15g, Chinese bulbul 15g, must sunglo 12g, Magnolia bark 8g, coptis 8g, tealeaves 4g, Herba Moslae Chinensis 2g.
The preparation method of embodiment 5 and 6 is as follows：
(1) raw material is weighed, is mixed, 40 mesh sieves are crossed after smashing；
(2) according to weight than 1:25 ratio mixes the mixture in step (1) with 70% ethanol solution, sealing leaching
Bubble 3 hours；
(3) raw material obtained in step (2) is put into ultrahigh pressure vessel, pressurize 400MPa, after pressurize extraction 5min,
Feed liquid, which is crossed to filter out, takes solid residue, and extraction is concentrated under reduced pressure, and recovery ethanol is to without alcohol taste；
(4) according to weight than 1：1,3-PD is added in concentrate obtained by from 3 ratio to step (3), is filtered, from
The heart takes supernatant, produces.
Embodiment 7
A kind of plant antiseptic agent composition for cosmetics provided by the invention, it is characterised in that by following component systems
Into：Prickly ash berries 15g, Chinese bulbul 15g, must sunglo 12g, Magnolia bark 8g, coptis 8g, tealeaves 4g, Herba Moslae Chinensis 3g.
Embodiment 8
A kind of plant antiseptic agent composition for cosmetics provided by the invention, it is characterised in that by following component groups
Divide and be made：Prickly ash berries 15g, Chinese bulbul 15g, must sunglo 11g, Magnolia bark 8g, coptis 8g, tealeaves 4g, Herba Moslae Chinensis 2g.
The preparation method of embodiment 7 and 8 is as follows：
(1) raw material is weighed, is mixed, 40 mesh sieves are crossed after smashing；
(2) according to weight than 1:30 ratio mixes the mixture in step (1) with 50% ethanol solution, sealing leaching
Bubble 4 hours；
(3) raw material obtained in step (2) is put into ultrahigh pressure vessel, pressurize 400MPa, pressurize extraction 10min
Afterwards, feed liquid, which is crossed to filter out, takes solid residue, and extraction is concentrated under reduced pressure, and recovery ethanol is to without alcohol taste；
(4) according to weight than 1：1,2- pentanediols and 1,3- third are added in concentrate obtained by from 2 ratio to step (3)
Glycol, filter, centrifuging and taking supernatant, produce.
There is advantage to better illustrate the present invention, plant antiseptic agent composition effect inspection provided by the invention is given below
Survey data.
The cutaneous safety of test example 1 is evaluated
Evaluated using the experiment of human body patch.
1st, test method：Subject amounts to 30 people, and specific sex composition and age composition determine (to meet at random《Cosmetics
Contact dermatitis diagnostic criteria and treatment principle》Include, exclusion standard).Sample made from embodiment 1,2,3 is put into spot examination device
Interior (amount of samples is 0.020~0.025g), control wells are blank (not putting any material), and sample and blank control are affixed on
The forearm song side of subject, is gently pressed with palm and is allowed to equably be pasted on skin, continues 24h.Remove spot and try 30min after device,
Dermoreaction is observed after impression disappearance.As result for feminine gender, observed again once respectively in 24h and 48h.
According to《Cosmetics contact dermatitis diagnostic criteria and treatment principle》, its classify judge standard it is as shown in table 1.Comment
Sentence standard and be more than 5, or the number of 2 grades of skin adverse reactions to occur the number of 1 grade of skin adverse reaction in 30 subjects
More than 2, or occur any 13 grades or during more than 3 grades skin adverse reactions, judge that tested material has skin bad anti-to human body
Should.
Table 1
2nd, result of the test：1-8 of embodiment of the present invention human body patch test results are as shown in table 2.
Table 2
Table 2 is skin closure type patch test dermoreaction grade scale and experimental result, from table 2 it can be seen that implementing
Plant origin cosmetics anticorrosive composite prepared by example 1-8 passes through patch test, judges that it has no adverse reaction to human body skin.
The antiseptic property of test example 2 is evaluated
1st, test method：0.8% and 1.5% embodiment 1-8 composition is added respectively to basic cosmetics aqua and cream
Preservation challenge test is carried out in frost.Method American Pharmacopeia USP is carried out, and the microorganism of inoculation has staphylococcus aureus, large intestine bar
Bacterium, Pseudomonas aeruginosa, staphylococcus aureus, Candida albicans and black-koji mould, then examined respectively at the 0th, 7,14,28 day every
The amount of survival of kind bacterium, amount of survival is fewer, and its preservative antibacterial effect is better.Validity standard is to be lived when cultivating 14 days
Bacterial concentration should be less than the 0.1% of initial concentration, not be further added by；It is dense that 14 days fungi concentrations of culture should be maintained at or below starting
Degree, is not further added by.
2nd, result of the test：
Preservation challenge test result (addition 1%) of the sample of table 3 in basic cosmetics aqua
Preservation challenge test result (addition 1.5%) of the sample of table 4 in basic cosmetics cream
From table 3 it can be seen that plant antiseptic agent composition prepared by the embodiment 1-8 of addition 0.8% is added to basicization
It can be tested in cosmetic aqua formula by preservation challenge；From table 4, it can be seen that plant prepared by the embodiment 1-8 of addition 1.5%
Thing antiseptic composition is added in basic cosmetics cream formula also can be tested by preservation challenge.Pass through table 3 and table 4
As a result as can be seen that plant antiseptic agent composition prepared by the present invention has excellent antiseptic power.
Claims (3)
1. a kind of plant antiseptic agent composition for cosmetics, it is characterised in that be mainly made up of following components：Prickly ash berries
10-20 parts, Chinese bulbul 10-20 parts, palpus sunglo 10-20 parts, Magnolia bark 5-10 parts, coptis 5-10 parts；Herba Moslae Chinensis 1-3 parts, tea
Leaf 3-5 parts；
Described plant antiseptic agent composition is passed sequentially through made from following step：
(1) each raw material is weighed by above-mentioned weight, mixed, 40 mesh sieves are crossed after smashing；
(2) according to weight than 1:15-30 ratio mixes the mixture in step (1) with 50-70% ethanol solution, sealing
Soak 3-6 hours；
(3) raw material obtained in step (2) is put into ultrahigh pressure vessel, pressurize 200-400MPa, pressurize extraction 5-10min
Afterwards, feed liquid is filtered to remove solid residue, and extraction is concentrated under reduced pressure, and recovery ethanol is to without alcohol taste；
(4) according to weight than 1：2~1：Added in concentrate obtained by from 3 ratio to step (3) 1,2- pentanediols, 1,2- oneself
One or more in glycol, 1,3-PD, filter, centrifuging and taking supernatant, produce.
A kind of 2. plant antiseptic agent composition for cosmetics according to claim 1, it is characterised in that described plant
Thing antiseptic composition is made up of following components：15 parts of prickly ash berries, 15 parts of the Chinese bulbul, 1 part of sunglo of palpus, 8 parts of Magnolia bark, the coptis
8 parts, 4 parts of tealeaves, 2 parts of Herba Moslae Chinensis.
A kind of 3. preparation method of plant antiseptic agent composition for cosmetics described in claim 1, it is characterised in that according to
It is secondary to comprise the steps：
(1) raw material is weighed according to weight described in claim 1, mixed, 40 mesh sieves are crossed after smashing；
(2) according to weight than 1:15-30 ratio mixes the mixture in step (1) with 50-70% ethanol solution, sealing
Soak 3-6 hours；
(3) raw material obtained in step (2) is put into ultrahigh pressure vessel, pressurize 200-400MPa, pressurize extraction 5-10min
Afterwards, feed liquid is filtered to remove solid residue, and extraction is concentrated under reduced pressure, and recovery ethanol is to without alcohol taste；
(4) according to weight than 1：2~1：Added in concentrate obtained by from 3 ratio to step (3) 1,2- pentanediols, 1,2- oneself
One or more in glycol, 1,3-PD, filter, centrifuging and taking supernatant, produce.
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| CN106377467A (en) * | 2016-11-29 | 2017-02-08 | 佛山市芊茹化妆品有限公司 | Pomelo-peel-extract-containing anticorrosive bactericidal composition |
| CN107308064A (en) * | 2017-08-08 | 2017-11-03 | 广州蜜妆生物科技有限公司 | A kind of compound natural preservative |
| CN107669543A (en) * | 2017-10-11 | 2018-02-09 | 广州市禾基生物科技有限公司 | A kind of preservative and preparation method thereof |
| CN108078863B (en) * | 2018-01-29 | 2020-07-14 | 广州天然国度生物科技有限公司 | Bactericidal composition based on plant extracts and infant care composition |
| CN108295008A (en) * | 2018-04-07 | 2018-07-20 | 广州市索柔生物科技有限公司 | A kind of plant antiseptic agent composition |
| CN108578520B (en) * | 2018-06-20 | 2021-06-04 | 华南师范大学 | Response surface method optimized combination compound plant-derived preservative and application thereof |
| CN109350577B (en) * | 2018-12-13 | 2021-09-21 | 广州睿森生物科技有限公司 | Skin care composition and application thereof |
| CN111671688A (en) * | 2020-06-24 | 2020-09-18 | 陕西斯堪纳维亚生物科技有限公司 | Multi-effect repair essence |
| CN112156050A (en) * | 2020-11-13 | 2021-01-01 | 东晟源研究院(广州)有限公司 | Plant preservative composition suitable for cosmetics and preparation method thereof |
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| CN104840400A (en) * | 2015-05-18 | 2015-08-19 | 中山安理汇日用品有限公司 | Skin care lotion formula with self corrosion-resistant property |
| CN104825381B (en) * | 2015-05-18 | 2018-07-31 | 中山安理汇日用品有限公司 | Has the essence formula of liquid from Anticorrosive Character |
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| Title |
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| 香薷的临床应用研究;江岁等;《中医药导报》;20150531;第21卷(第9期);95-97 * |
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