CN105878118A - Method for extracting cedrela sinensis extract from cedrela sinensis leaves and application of method - Google Patents
Method for extracting cedrela sinensis extract from cedrela sinensis leaves and application of method Download PDFInfo
- Publication number
- CN105878118A CN105878118A CN201610348442.4A CN201610348442A CN105878118A CN 105878118 A CN105878118 A CN 105878118A CN 201610348442 A CN201610348442 A CN 201610348442A CN 105878118 A CN105878118 A CN 105878118A
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- CN
- China
- Prior art keywords
- extract
- sinensis
- cedrela sinensis
- folium toonae
- tonnae
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Abstract
The invention relates to the technical field of plant application research, in particular to a method for extracting a cedrela sinensis extract from cedrela sinensis leaves and an application of the method. The method comprises the following steps: removing surface impurities of the cedrela sinensis leaves by clean water, airing the cedrela sinensis leaves in the shade and crushing the cedrela sinensis leaves to form cedrela sinensis leaves powder; adding 30%-50% year extract solution to the cedrela sinensis leaves powder to soak for 2-3 hours, fishing out the cedrela sinensis leaves powder by distilled water, drying the cedrela sinensis leaves powder by an inert gas and coating the cedrela sinensis leaves powder with salicylic acid; extracting the cedrela sinensis leaves powder treated in the step 2 by 50%-60% organic solvent, carrying out vacuum evaporation at 50-70 DEG C under the vacuum degree of 0.05-0.07Mpa to obtain a crude extract; adding butylated hydroxytoluene to the obtained crude extract and transferring the butylated hydroxytoluene and the crude extract to a small derivatization bottle, inserting silanized quartz fiber, reacting at 60-70 DEG C for over 8 hours, pulling out the polymerized quartz fiber for ageing; and eluting and removing template molecules on the quartz fiber coating by an ethanol-acetic acid solution to prepare the cedrela sinensis extract. The extracted cedrela sinensis extract has sunscreen and anti-aging functions.
Description
Technical field
The present invention relates to plant application studying technological domain, be specially a kind of extraction from Folium toonae sinensis
The method of Tonnae Sinensis extract and application thereof.
Background technology
Tonnae Sinensis is a kind of perennial woody plant belonging to Meliaceae, originates in the ground, middle part of China
District, mainly have red Tonnae Sinensis, brown Tonnae Sinensis, red autumnal leaves Chinese toon, the green Tonnae Sinensis of red bud, dirty oil Chinese toon, chilli oil Chinese toon,
Blue or green oil Chinese toon and tongue Chinese toon seven kinds, at China's cultivation history of existing more than 2000 year.Tonnae Sinensis timber is normal
It is used to make various top-grade furniture and plant as ornamental trees.Tonnae Sinensis whole plants all can quilt
Utilize, be the high seeds of an economic worth.Tonnae Sinensis tender shoots is nutritious, comprehensive, equilibrium,
Rich in proteins, aminoacid, various volatile oil, multivitamin and trace element, can be direct
Eat or make various series flavor food.Toona sinensis seed oil is colourless, taste is fragrant, edible, richness
Containing necessary fatty acid, there is higher nutritive value.Chinese toon old leaf aminoacid composition is relatively comprehensive, is
The feedstuff of high-quality.Tonnae Sinensis is not only a kind of good woody good vegetables, and is that medicine food is same
The environmental protective hygienic food in source, all has corresponding medicine in Tang Materia Medica, Compendium of Material Medica
With record.Fructus Tonnae Sinensis cures mainly gastric duodenal ulcer, chronic gastritis etc..Folium toonae sinensis has clearly
Thermal detoxification, astringing to arrest bleeding, pain relieving of drying, stomach invigorating are regulated the flow of vital energy, blood sugar lowering, parasite killing, enhancing sperm
The effect such as vigor, antitumor.Being found by research, Tonnae Sinensis extract has the strongest antioxygen
Change activity, and Folium toonae sinensis is the Main By product in Tonnae Sinensis industry, enormous amount, fully studies
Development and utilization Chinese toon old leaf has important practical significance.
Prior art Tonnae Sinensis extracts the application as preparation treatment goat medicine of the Tonnae Sinensis extract
(CN201110057129.2), extract uses decocting, polyamide to cross the steps such as post and obtain Huang
The Tonnae Sinensis extract of ketone content 90%, then by Tonnae Sinensis extract in gout two kinds of key enzymes:
Xanthine oxidase and COX-2 carry out body outer suppressioning test.The invention provides Tonnae Sinensis
The preparation of extract and the application on gout, antiphlogistic effects, disclose Tonnae Sinensis extract
Purposes in prevention and treatment gout, this extract is=95 to the IC50 of xanthine oxidase
μ g/mL, the IC50=77 μ g/mL to COX-2, two kinds of enzymes are all had by Tonnae Sinensis extract
Significantly inhibitory action, has preferable gout, antiphlogistic effects, can be used for preparation treatment pain
Double target drugs of wind.
Another prior art metal surface detergent based on Tonnae Sinensis Folium toonae sinensis extract and preparation thereof
Method (CN201510939616.X), including: by grey and organic molten to Folium toonae sinensis, bamboo charcoal nano
Agent mixes and carries out heat treatment, then crosses leaching filtrate；By filtrate, quaternary ammonium salt, citronellol,
Nano imvite, sodium pyrophosphate, cocoyl glucoside, calcium alginate, DBSA
Sodium, glycerol, sulfadiazine, ketopyrrolidine, tripropylene glycol butyl ether and ethanol mix with prepared base
Metal surface detergent in Folium toonae sinensis extract.The metal surface prepared by the method is cleaned
Agent has the cleaning effect of excellence.
Currently available technology is applied to field of medicaments Tonnae Sinensis extract mostly, how from Tonnae Sinensis
Extract more rich extract and to apply it to other field be the problem to be solved in the present invention.
Summary of the invention
In view of this, the present invention provide a kind of from Folium toonae sinensis extract Tonnae Sinensis extract method and
Its application, extracts Tonnae Sinensis extract from Folium toonae sinensis, can turn waste into wealth, and is a kind of green product
Industry, the Tonnae Sinensis extract extracted has sun-proof and defying age function, can being widely applied to
In cosmetic field.
To achieve these goals, the present invention is by the following technical solutions:
According to the first aspect of the invention, it is provided that a kind of from Folium toonae sinensis, extract Tonnae Sinensis extract
Method, comprising:
Step 1: dry at shady and cool after Folium toonae sinensis clear water is sloughed surface impurity, pulverize,
Cross 30～50 mesh sieves, form Folium toonae sinensis powder；
Step 2: add the yeast extract that concentration is 30～50 in Folium toonae sinensis powder, soak
2～3h, pull out and use distilled water flushing, then dry up with noble gas, be coated with in Folium toonae sinensis powder afterwards
One layer of salicylic acid of stain；
Step 3: with 50～60% the Folium toonae sinensis that processed of organic solvent extraction step 2, so
After under conditions of 50～70 DEG C, be evaporated under reduced pressure slightly under vacuum 0.05～0.07Mpa
Extract；
Step 4: in the crude extract of step 3 gained, adds butylated hydroxytoluene and proceeds to derive
Change in bottle, insert the quartz fibre after silanization, react more than 8h in 60-70 DEG C, then
Quartz fibre after polymerization is extracted, aging；
Step 5: remove the template molecule in quartz fibre coating with Ethanol-Acetic Acid eluant solution,
Prepare Tonnae Sinensis extract.
Further, in step 2, the preferred helium of described noble gas, neon, argon, krypton or
Its synthetic.
Further, in step 2, described salicylic preparation method is phenol and hydroxide
Sodium reaction generates sodium phenate, and after distillation dehydration, logical carbon dioxide carries out carboxylation reaction, prepares
Salicylic acid sodium salt, then be acidified with sulphuric acid, and obtaining crude product, crude product obtains finished product through sublimation purifying.
Further, in step 3, described organic solvent be ethanol, acetone, methanol, third
Alcohol, isopropanol, ethyl acetate.
Further, in step 3, described organic solvent is ethanol or methanol.
Further, in step 4, the preparation method of described butylated hydroxytoluene be by paracresol,
Tert-butyl alcohol 1:1.1 in molar ratio puts into reactor heating for dissolving, under catalyst phosphatizing,
Under 65～70 DEG C of strong agitation react, after completion of the reaction, product first with 10% hydrogen-oxygen
Change sodium solution and be washed till alkalescence, be washed with water to neutrality, remove solvent, with ethyl alcohol recrystallization and get final product.
According to the second aspect of the invention, it is provided that a kind of from Folium toonae sinensis, extract Tonnae Sinensis extract
Application, is applied to cosmetic field by Tonnae Sinensis extract so that it is have sun-proof, anti-senescence function.
Further, according to said extracted method, Tonnae Sinensis extract is applied to sunscreen cream, sun-proof
In breast, suntan lotion, emulsion, facial cream and milky lotion.
The invention has the beneficial effects as follows: the present invention extracts Tonnae Sinensis extract from Folium toonae sinensis, permissible
Turn waste into wealth, be a kind of pollution-free industry, and technique is relatively simple, need not bigger equipment investment,
It is suitable for large-scale industrialized production, establishes for developing Tonnae Sinensis extract functional product further
Determine basis；The Tonnae Sinensis extract extracted has sun-proof and defying age function, can extensively answer
Use in cosmetic field.
Detailed description of the invention
The present invention provides a kind of method extracting Tonnae Sinensis extract from Folium toonae sinensis and application thereof, from
Folium toonae sinensis extracts Tonnae Sinensis extract, can turn waste into wealth, be a kind of pollution-free industry, extracted
Tonnae Sinensis extract there is sun-proof and defying age function, cosmetic field can be widely applied to
In.
To achieve these goals, the present invention is by the following technical solutions:
According to the first aspect of the invention, it is provided that a kind of from Folium toonae sinensis, extract Tonnae Sinensis extract
Method, comprising:
Step 1: dry at shady and cool after Folium toonae sinensis clear water is sloughed surface impurity, pulverize,
Cross 30～50 mesh sieves, form Folium toonae sinensis powder；
Step 2: add the yeast extract that concentration is 30～50 in Folium toonae sinensis powder, soak
2～3h, pull out and use distilled water flushing, then dry up with noble gas, be coated with in Folium toonae sinensis powder afterwards
One layer of salicylic acid of stain；
Step 3: with 50～60% the Folium toonae sinensis that processed of organic solvent extraction step 2, so
After under conditions of 50～70 DEG C, be evaporated under reduced pressure slightly under vacuum 0.05～0.07Mpa
Extract；
Step 4: in the crude extract of step 3 gained, adds butylated hydroxytoluene and proceeds to derive
Change in bottle, insert the quartz fibre after silanization, react more than 8h in 60-70 DEG C, then
Quartz fibre after polymerization is extracted, aging；
Step 5: remove the template molecule in quartz fibre coating with Ethanol-Acetic Acid eluant solution,
Prepare Tonnae Sinensis extract.
Further, in step 2, the preferred helium of described noble gas, neon, argon, krypton or
Its synthetic.
Further, in step 2, described salicylic preparation method is phenol and hydroxide
Sodium reaction generates sodium phenate, and after distillation dehydration, logical carbon dioxide carries out carboxylation reaction, prepares
Salicylic acid sodium salt, then be acidified with sulphuric acid, and obtaining crude product, crude product obtains finished product through sublimation purifying.
Further, in step 3, described organic solvent be ethanol, acetone, methanol, third
Alcohol, isopropanol, ethyl acetate.
Further, in step 3, described organic solvent is ethanol or methanol.
Further, in step 4, the preparation method of described butylated hydroxytoluene be by paracresol,
Tert-butyl alcohol 1:1.1 in molar ratio puts into reactor heating for dissolving, under catalyst phosphatizing,
Under 65～70 DEG C of strong agitation react, after completion of the reaction, product first with 10% hydrogen-oxygen
Change sodium solution and be washed till alkalescence, be washed with water to neutrality, remove solvent, with ethyl alcohol recrystallization and get final product.
According to the second aspect of the invention, it is provided that a kind of from Folium toonae sinensis, extract Tonnae Sinensis extract
Application, is applied to cosmetic field by Tonnae Sinensis extract so that it is have sun-proof, anti-senescence function.
Further, according to said extracted method, Tonnae Sinensis extract is applied to sunscreen cream, sun-proof
In breast, suntan lotion, emulsion, facial cream and milky lotion.
For the technical scheme making those skilled in the art be better understood from the application, below
To come technical scheme is clearly and completely described in conjunction with the embodiments, it is clear that
Described embodiment is only a part of embodiment of the application, based on the enforcement in the application
Example, it is all that those of ordinary skill in the art are obtained under not making creative work premise
Other embodiments, all should belong to the scope of the application protection.
A kind of method extracting Tonnae Sinensis extract from Folium toonae sinensis, comprising: by Folium toonae sinensis with clear
Water dries at shady and cool after sloughing surface impurity, pulverizes, and crosses 30～50 mesh sieves, forms Tonnae Sinensis
Ye Fen；In Folium toonae sinensis powder, add the yeast extract that concentration is 30～50, soak 2～3h,
Pull out with distilled water flushing, then dry up with noble gas, in Folium toonae sinensis powder coated one layer afterwards
Salicylic acid；With 50～60% the Folium toonae sinensis that processed of organic solvent extraction step 2, then
Under conditions of 50～70 DEG C, it is evaporated under reduced pressure slightly to carry under vacuum 0.05～0.07Mpa
Take thing；In the crude extract of gained, add butylated hydroxytoluene and proceed in derivatization bottle, inserting
Enter the quartz fibre after silanization, react more than 8h in 60-70 DEG C, then by the stone after polymerization
English spike protein gene is aging；The mould in quartz fibre coating is removed with Ethanol-Acetic Acid eluant solution
Plate molecule, prepares Tonnae Sinensis extract.
In the present invention extracts the method for Tonnae Sinensis extract, the preferred neon of described noble gas；Described
Salicylic preparation method is that phenol reacts generation sodium phenate with sodium hydroxide, after distillation dehydration,
Logical carbon dioxide carries out carboxylation reaction, prepares salicylic acid sodium salt, then is acidified with sulphuric acid, and obtains
Crude product, crude product obtains finished product through sublimation purifying；Described organic solvent is ethanol or methanol；Described fourth
The preparation method of hydroxy toluene is that paracresol, tert-butyl alcohol 1:1.1 in molar ratio is put into reactor
Heating for dissolving, under catalyst phosphatizing, reacts, instead under 65～70 DEG C of strong agitation
After Ying, product be first washed till alkalescence with the sodium hydroxide solution of 10%, be washed with water to
Neutrality, removes solvent, with ethyl alcohol recrystallization and get final product.
Embodiment 1
Method of testing is: utilizes and can become empurpled variable color card, above after being irradiated to ultraviolet
Carry out the irradiation of a minute after coating sunscreen cream, observe its change.
Said method is used to extract the reality that Tonnae Sinensis extract is applied in cosmetics from Folium toonae sinensis
Border effect is as shown in table 1:
Table 1
Be can be seen that by table 1, use said method to extract the application of Tonnae Sinensis extract from Folium toonae sinensis
In sun care preparations, sun-proof result is optimal.
Embodiment 2
Method of testing is: is coated with on dermatine after spreading sunscreen cream and drips an oil dripping, observes oil
Whether body spreads apart, if the appearance of oil body does not changes much, just indicates this sunscreen cream
Grease resistance stronger.
Said method is used to extract the reality that Tonnae Sinensis extract is applied in cosmetics from Folium toonae sinensis
Border effect is as shown in table 2:
Table 2
Be can be seen that by table 2, use said method to extract the application of Tonnae Sinensis extract from Folium toonae sinensis
In sun care preparations, grease resistance is the strongest.
Embodiment 3
Owing to skin aging does not has a test verification method of very scientific and precise, in the present embodiment,
3 groups of ages are allowed to use this product at least 6 respectively the middle aged experiencer of 30 to 45 years old respectively
More than Yue, observe change of skin, wherein, carry using the present invention to extract Tonnae Sinensis from Folium toonae sinensis
Taking the experiencer that thing is applied in facial cream, skin is the most satisfactory.
Finally illustrating, above example is only in order to illustrate technical scheme rather than limit
System, those of ordinary skill in the art technical scheme is made other amendment or etc.
With replacing, without departing from the spirit and scope of technical solution of the present invention, all should contain at this
In the middle of bright right.
Claims (8)
1. the method extracting Tonnae Sinensis extract from Folium toonae sinensis, it is characterised in that comprising:
Step 1: dry at shady and cool after Folium toonae sinensis clear water is sloughed surface impurity, pulverize,
Cross 30～50 mesh sieves, form Folium toonae sinensis powder；
Step 2: add the yeast extract that concentration is 30～50 in Folium toonae sinensis powder, soak
2～3h, pull out and use distilled water flushing, then dry up with noble gas, be coated with in Folium toonae sinensis powder afterwards
One layer of salicylic acid of stain；
Step 3: with 50～60% the Folium toonae sinensis that processed of organic solvent extraction step 2, so
After under conditions of 50～70 DEG C, be evaporated under reduced pressure slightly under vacuum 0.05～0.07Mpa
Extract；
Step 4: in the crude extract of step 3 gained, adds butylated hydroxytoluene and proceeds to derive
Change in bottle, insert the quartz fibre after silanization, react more than 8h in 60-70 DEG C, then
Quartz fibre after polymerization is extracted, aging；
Step 5: remove the template molecule in quartz fibre coating with Ethanol-Acetic Acid eluant solution,
Prepare Tonnae Sinensis extract.
A kind of side extracting Tonnae Sinensis extract from Folium toonae sinensis the most according to claim 1
Method, it is characterised in that in step 2, the preferred helium of described noble gas, neon, argon, krypton or
Its synthetic of person.
A kind of side extracting Tonnae Sinensis extract from Folium toonae sinensis the most according to claim 1
Method, it is characterised in that in step 2, described salicylic preparation method is phenol and hydrogen-oxygen
Changing sodium reaction and generate sodium phenate, after distillation dehydration, logical carbon dioxide carries out carboxylation reaction, system
Obtaining salicylic acid sodium salt, then be acidified with sulphuric acid, and obtain crude product, crude product obtains finished product through sublimation purifying.
A kind of side extracting Tonnae Sinensis extract from Folium toonae sinensis the most according to claim 1
Method, it is characterised in that in step 3, described organic solvent be ethanol, acetone, methanol,
Propanol, isopropanol, ethyl acetate.
A kind of side extracting Tonnae Sinensis extract from Folium toonae sinensis the most according to claim 1
Method, it is characterised in that in step 3, described organic solvent is ethanol or methanol.
A kind of side extracting Tonnae Sinensis extract from Folium toonae sinensis the most according to claim 1
Method, it is characterised in that in step 4, the preparation method of described butylated hydroxytoluene be by paracresol,
Tert-butyl alcohol 1:1.1 in molar ratio puts into reactor heating for dissolving, under catalyst phosphatizing,
Under 65～70 DEG C of strong agitation react, after completion of the reaction, product first with 10% hydrogen-oxygen
Change sodium solution and be washed till alkalescence, be washed with water to neutrality, remove solvent, with ethyl alcohol recrystallization and get final product.
7. the application extracting Tonnae Sinensis extract from Folium toonae sinensis, it is characterised in that by Tonnae Sinensis
Extract is applied to cosmetic field so that it is have sun-proof, anti-senescence function.
The most according to claim 7 a kind of from Folium toonae sinensis extract Tonnae Sinensis extract should
With, it is characterised in that according to said extracted method, Tonnae Sinensis extract is applied to sunscreen cream, anti-
Shine in breast, suntan lotion, emulsion, facial cream and milky lotion.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610348442.4A CN105878118A (en) | 2016-05-21 | 2016-05-21 | Method for extracting cedrela sinensis extract from cedrela sinensis leaves and application of method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610348442.4A CN105878118A (en) | 2016-05-21 | 2016-05-21 | Method for extracting cedrela sinensis extract from cedrela sinensis leaves and application of method |
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| CN105878118A true CN105878118A (en) | 2016-08-24 |
Family
ID=56716853
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610348442.4A Pending CN105878118A (en) | 2016-05-21 | 2016-05-21 | Method for extracting cedrela sinensis extract from cedrela sinensis leaves and application of method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107384635A (en) * | 2017-08-01 | 2017-11-24 | 河南省农业科学院 | A kind of preparation method of Chinese toon handmade soap |
| CN107823112A (en) * | 2017-12-06 | 2018-03-23 | 广州赛莱拉干细胞科技股份有限公司 | A kind of anti-oxidant skin care item containing pot marigold stem cell extract |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1289760A (en) * | 2000-09-25 | 2001-04-04 | 谢虎 | Process for preparing salicylic acid by solvent method |
| CN101099768A (en) * | 2007-07-25 | 2008-01-09 | 天津科技大学 | Method for extracting anti-oxidation active substance from overgrown leaves of Chinese toon |
| CN101912445A (en) * | 2010-08-26 | 2010-12-15 | 西北农林科技大学 | Method for extracting general flavonoids from toona sinensis leaves under assistance of surfactant |
-
2016
- 2016-05-21 CN CN201610348442.4A patent/CN105878118A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1289760A (en) * | 2000-09-25 | 2001-04-04 | 谢虎 | Process for preparing salicylic acid by solvent method |
| CN101099768A (en) * | 2007-07-25 | 2008-01-09 | 天津科技大学 | Method for extracting anti-oxidation active substance from overgrown leaves of Chinese toon |
| CN101912445A (en) * | 2010-08-26 | 2010-12-15 | 西北农林科技大学 | Method for extracting general flavonoids from toona sinensis leaves under assistance of surfactant |
Non-Patent Citations (1)
| Title |
|---|
| 张凯歌等: "《色谱》", 28 December 2012 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107384635A (en) * | 2017-08-01 | 2017-11-24 | 河南省农业科学院 | A kind of preparation method of Chinese toon handmade soap |
| CN107823112A (en) * | 2017-12-06 | 2018-03-23 | 广州赛莱拉干细胞科技股份有限公司 | A kind of anti-oxidant skin care item containing pot marigold stem cell extract |
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