CN1058696C - 精制甲缩醛的方法 - Google Patents
精制甲缩醛的方法 Download PDFInfo
- Publication number
- CN1058696C CN1058696C CN95195524A CN95195524A CN1058696C CN 1058696 C CN1058696 C CN 1058696C CN 95195524 A CN95195524 A CN 95195524A CN 95195524 A CN95195524 A CN 95195524A CN 1058696 C CN1058696 C CN 1058696C
- Authority
- CN
- China
- Prior art keywords
- methylal
- weight
- gas
- water
- methyl alcohol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
- C07C41/48—Preparation of compounds having groups
- C07C41/58—Separation; Purification; Stabilisation; Use of additives
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP6243662A JP2786823B2 (ja) | 1994-10-07 | 1994-10-07 | メチラ−ルの精製法 |
| JP243662/94 | 1994-10-07 | ||
| JP243662/1994 | 1994-10-07 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1160392A CN1160392A (zh) | 1997-09-24 |
| CN1058696C true CN1058696C (zh) | 2000-11-22 |
Family
ID=17107144
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN95195524A Expired - Lifetime CN1058696C (zh) | 1994-10-07 | 1995-09-28 | 精制甲缩醛的方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US6160185A (enExample) |
| EP (1) | EP0785182B1 (enExample) |
| JP (1) | JP2786823B2 (enExample) |
| CN (1) | CN1058696C (enExample) |
| DE (1) | DE69514535T2 (enExample) |
| WO (1) | WO1996011178A1 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101302143B (zh) * | 2007-05-10 | 2012-05-23 | 南京林业大学 | 工业级甲缩醛的提纯方法 |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6379507B1 (en) * | 1998-08-03 | 2002-04-30 | Asahi Kasei Kabushiki Kaisha | Process for producing methylal |
| DE102004059334A1 (de) * | 2004-12-09 | 2006-06-22 | Ticona Gmbh | Verfahren zur Herstellung von Acetalen |
| CN100383099C (zh) * | 2006-02-15 | 2008-04-23 | 江阴市华凤化工植绒有限公司 | 将低浓度甲缩醛脱除杂质获得高纯度甲缩醛的方法 |
| CN101597117B (zh) * | 2009-06-23 | 2011-08-03 | 南京大学 | 一种工业甲醛废水的治理及资源化回收工艺 |
| CN101857534A (zh) * | 2010-06-03 | 2010-10-13 | 濮阳市普天化工有限公司 | 一种合成甲缩醛的工艺 |
| CN104447241A (zh) * | 2014-11-20 | 2015-03-25 | 赛鼎工程有限公司 | 一种甲缩醛与甲醇分离的工艺 |
| CN112225650B (zh) * | 2019-07-15 | 2023-06-06 | 中国石油化工股份有限公司 | 工业级甲缩醛提纯获得高纯度甲缩醛的精制方法 |
| CN110776403A (zh) * | 2019-11-06 | 2020-02-11 | 重庆云天化天聚新材料有限公司 | 一种生产高纯度甲缩醛的方法 |
| CN113457193B (zh) * | 2021-06-25 | 2023-01-17 | 济南大学 | 一种分离甲醇-甲缩醛-甲酸甲酯混合物的装置及方法 |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58103331A (ja) * | 1981-11-28 | 1983-06-20 | ヘミツシエ・ウエルケ・ヒユ−ルス・アクチエンゲゼルシヤフト | 純粋なメチラ−ルの取得方法 |
| JPH0356134A (ja) * | 1990-06-28 | 1991-03-11 | Asahi Chem Ind Co Ltd | 反応蒸留装置 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1127339B (de) * | 1960-11-22 | 1962-04-12 | Wacker Chemie Gmbh | Verfahren zur Gewinnung von alkohol- und wasserfreien Acetalen durch extraktive Destillation |
| JPS56147739A (en) * | 1980-04-17 | 1981-11-16 | Seitetsu Kagaku Co Ltd | Purification of methylal |
| US4421535A (en) * | 1982-05-03 | 1983-12-20 | El Paso Hydrocarbons Company | Process for recovery of natural gas liquids from a sweetened natural gas stream |
-
1994
- 1994-10-07 JP JP6243662A patent/JP2786823B2/ja not_active Expired - Lifetime
-
1995
- 1995-09-28 DE DE69514535T patent/DE69514535T2/de not_active Expired - Lifetime
- 1995-09-28 US US08/831,285 patent/US6160185A/en not_active Expired - Lifetime
- 1995-09-28 CN CN95195524A patent/CN1058696C/zh not_active Expired - Lifetime
- 1995-09-28 EP EP95932927A patent/EP0785182B1/en not_active Expired - Lifetime
- 1995-09-28 WO PCT/JP1995/001974 patent/WO1996011178A1/ja not_active Ceased
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS58103331A (ja) * | 1981-11-28 | 1983-06-20 | ヘミツシエ・ウエルケ・ヒユ−ルス・アクチエンゲゼルシヤフト | 純粋なメチラ−ルの取得方法 |
| JPH0356134A (ja) * | 1990-06-28 | 1991-03-11 | Asahi Chem Ind Co Ltd | 反応蒸留装置 |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101302143B (zh) * | 2007-05-10 | 2012-05-23 | 南京林业大学 | 工业级甲缩醛的提纯方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| EP0785182A4 (enExample) | 1997-08-27 |
| CN1160392A (zh) | 1997-09-24 |
| EP0785182A1 (en) | 1997-07-23 |
| US6160185A (en) | 2000-12-12 |
| DE69514535T2 (de) | 2000-08-10 |
| DE69514535D1 (de) | 2000-02-17 |
| JPH08104659A (ja) | 1996-04-23 |
| JP2786823B2 (ja) | 1998-08-13 |
| EP0785182B1 (en) | 2000-01-12 |
| WO1996011178A1 (en) | 1996-04-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CX01 | Expiry of patent term |
Granted publication date: 20001122 |
|
| EXPY | Termination of patent right or utility model |