CN105860856A - Leather polishing wax emulsion and preparation method thereof - Google Patents
Leather polishing wax emulsion and preparation method thereof Download PDFInfo
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- CN105860856A CN105860856A CN201610282030.5A CN201610282030A CN105860856A CN 105860856 A CN105860856 A CN 105860856A CN 201610282030 A CN201610282030 A CN 201610282030A CN 105860856 A CN105860856 A CN 105860856A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09G—POLISHING COMPOSITIONS; SKI WAXES
- C09G1/00—Polishing compositions
- C09G1/04—Aqueous dispersions
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- Dispersion Chemistry (AREA)
- Organic Chemistry (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses leather polishing wax emulsion and a preparation method thereof and belongs to the technical field of leather processing. The leather polishing wax emulsion is prepared from, by weight, 1.4-3.6% of carnauba wax, 2-5% of polyester wax, 1.6-3.8% of paraffin, 1.2-3.2% of non-ionic surfactant, 0.5-1.2% of glycerol, 0.6-1.2% of thickener and the balance water. The wax emulsion can be used for improving the polishing effect and water resistance of finished leather, excellent polishing and scorching effects are achieved, and the leather will obtain the finishing style of a comfortable hand feeling and a fine surface after being ironed at high temperature. Moreover, the wax emulsion contains no benzene compounds, is quite environmentally friendly in use, and has good application prospects and high economic value.
Description
Technical field
The present invention relates to leather processing technique field, particularly to a kind of leather buffing wax emulsion and preparation side thereof
Method.
Background technology
Wax emulsion in leather industry mainly as leather finish auxiliary agent, for the end, in, top coat, have relatively
Good performance.Wax had both had the general character of water proofing property and lubricity, have again such as oiliness, viscosity, fragility,
Characteristic in terms of toughness, fusibleness and gloss, is very different to each other.In actual applications, a kind of wax
Can not have all character met required for a certain special-purpose.Therefore, leather buffing wax breast is being selected
During the raw material of liquid, the serviceability of wax to be considered, improves the effect of leather polishing.
Chinese patent application CN102041325A discloses a kind of EFFECTS OF LEATHER FINISHING wax emulsion, including this EFFECTS OF LEATHER FINISHING
The composition of wax emulsion and preparation method.It is made up of following raw materials according (wt%): polyester wax 21.00～49.00, river
Wax 9.00～21.00, peregal 0-200.88～2.04, Arlacel-80 0.32～0.76, distilled water 28.8～
67.20.This wax emulsion adds at the bottom of leather, in, the slurry of top finishing uses, have antiseized, smooth,
The several functions such as waterproof, soft, filling, glazing.But this EFFECTS OF LEATHER FINISHING wax emulsion is after leather finish
Feel is the most puckery, and polishing effect is poor.
Chinese patent application CN103666280B discloses a kind of buffing wax emulsion for leather finish and system thereof
Preparation Method, leather buffing wax emulsion and preparation method thereof: it is made up of following raw materials according (wt%): oxidized paraffin wax
3.5%～4.6%, lignite wax 1.4%～1.9%, rice bran wax 3.3%～4.8%, paraffin 5.5%～
6.5%, comprehensive wax emulsifying agent 8.4%～10.8%, assistant for emulsifying agent 0.5%～1.5%, sodium hydroxide solution
1.0%～1.5%.This leather buffing wax emulsion emulsion has the gloss improving leather, improves leather hand feeling,
Strengthen leather wearability advantage.But the emulsifying agent used in this wax emulsion formulations and the weight of paraffin percentage
Ratio is between 1: 1～2: 1, and too much emulsifier can cause the wax emulsion permeability of preparation too by force,
Reduce the water proofing property of leather simultaneously, easily cause wetness sensation after covering with paint, lacquer, colour wash, etc. leather, have impact on the quality of leather.
Summary of the invention
The polishing effect existing for leather buffing wax emulsion is it is an object of the invention to overcome in prior art to pay no attention to
Think, the deficiency of poor water resistance, it is provided that a kind of leather buffing wax emulsion and preparation method thereof.This wax emulsion can
The effect of polishing and resistance to water after improving leather finish, it is thus achieved that remarkable polishing, burn effect, and
Comfortable feel can be obtained, the covering with paint style that surface is fine and smooth after hot iron.
In order to realize foregoing invention purpose, the invention provides techniques below scheme:
A kind of leather buffing wax emulsion, including the component of following weight percentage: include following weight percentage
Component: Brazil wax 1.4～3.6%, polyester wax 2～5%, paraffin 1.6～3.8%, nonionic table
Face activating agent 1.2～3.2%, glycerine 0.5～1.2%, thickener 0.6～1.2%, surplus is water.
Preferably, a kind of leather buffing wax emulsion, including the component of following weight percentage: Brazil wax
1.6～3.4%, polyester wax 2.4～4.2%, paraffin 1.8～3.6%, nonionic surface active agent 1.4～2.8%,
Glycerine 0.6～1%, thickener 0.7～1%, surplus is water.
It is furthermore preferred that a kind of leather buffing wax emulsion, including the component of following weight percentage: babassu
Wax 1.8～3.2%, polyester wax 2.6～3.8%, paraffin 2.1～3.2%, nonionic surface active agent 1.6～
2.4%, glycerine 0.7～0.9%, thickener 0.8～1%, surplus is water.
Most preferably, a kind of leather buffing wax emulsion, including the component of following weight percentage: babassu
Wax 2.6%, polyester wax 3.2%, paraffin 2.6%, nonionic surface active agent 2.1%, glycerine 0.8%, increase
Thick dose 0.9%, surplus is water.
Preferably, above-mentioned nonionic surface active agent is sorbitan fatty acid ester-60, anhydrous sorbitol
Fatty acid ester-80, polyoxyethylene sorbitan fatty acid ester-60, polyoxyethylene sorbitan fatty acid ester
One or more in-80 and AEO-9.
Preferably, above-mentioned thickener is cellulose, cellulose gum, magnesium silicate, Arabic gum, xanthan
One or more in glue, alginates and xanthan gum.
Another object of the present invention is to provide the preparation method of a kind of leather buffing wax emulsion, including following step
Rapid:
S1 prepares oil phase dispersed mixture: Brazil wax, polyester wax and paraffin is mixed, adds hot melt
Melting, open stirring, be subsequently adding nonionic surface active agent, low whipping speed is 1000～2000rpm
Stirring condition under disperse 0.5～1h, obtain oil phase dispersed mixture；
S2 prepares Aqueous dispersions mixture: water and glycerine are sequentially added in emulsion reactor, low whipping speed
It is warming up to 60～80 DEG C under conditions of 100～200rpm, prepares Aqueous dispersions mixture；
S3 prepares wax emulsion: the mixing speed of raising emulsion reactor, to 500～800rpm, adds step S1
The oil phase dispersed mixture of preparation emulsifies, and emulsification times is 1～3h；It is 200～300rpm in speed subsequently
Mixing speed decline and warm to room temperature, add and continue stirring 10～30min after thickener, be then filtrated to get skin
Leather buffing wax emulsion.
Compared with prior art, beneficial effects of the present invention:
The leather buffing wax emulsion that the present invention provides is optimized by Surfactant type and consumption, with
Time emulsifying process is improved, the wax emulsion particle diameter of preparation is little and homogeneous, this wax emulsion can be used in improve
The effect of polishing and resistance to water after leather finish, it is thus achieved that remarkable polishing, burn effect, and press through high temperature
Comfortable feel can be obtained, the covering with paint style that surface is fine and smooth after Tanging.And, this wax emulsion not containing benezene chemical combination
Thing, uses very environmental protection, has good application prospect and economic worth.
Detailed description of the invention
Below in conjunction with test example and detailed description of the invention, the present invention is described in further detail.But should be by
This is interpreted as that the scope of the above-mentioned theme of the present invention is only limitted to below example, all real based on present invention institute
Existing technology belongs to the scope of the present invention.
Polyester wax used by the embodiment of the present invention is polyester wax-691 model that EUROCERAS company produces.
Embodiment 1
A kind of leather buffing wax emulsion, including the component of following weight percentage: Brazil wax 2.6%, poly-
Ester type waxes 3.2%, paraffin 2.6%, sorbitan fatty acid ester-80 0.9%, polyoxyethylene sorbitan fat
Fat acid esters-80 1.2%, glycerine 0.8%, xanthans 0.9%, surplus is water.
The preparation method of above-mentioned wax emulsion, comprises the following steps:
S1 prepares oil phase dispersed mixture: the Brazil wax of above-mentioned formula ratio, polyester wax and paraffin are mixed
Uniformly, it is heated to 90 DEG C and melts, open stirring, be subsequently adding sorbitan fatty acid ester-80 and polyoxy second
Alkene sorbitan fatty acid ester-80, low whipping speed be 1500rpm stirring condition under disperse 1h, obtain
Oil phase dispersed mixture；
S2 prepares Aqueous dispersions mixture: water and glycerine are sequentially added in emulsion reactor, low whipping speed
It is warming up to 75 DEG C under conditions of 150rpm, prepares Aqueous dispersions mixture；
S3 prepares wax emulsion: the mixing speed improving emulsion reactor is prepared to 700rpm, addition step S1
Oil phase dispersed mixture emulsify, emulsification times is 2h；It is the mixing speed of 250rpm in speed subsequently
Decline warms to room temperature, and continues stirring 20min, be then filtrated to get leather buffing wax emulsion after adding xanthans.
Embodiment 2
A kind of leather buffing wax emulsion, including the component of following weight percentage: Brazil wax 1.4%, poly-
Ester type waxes 2.2%, paraffin 1.6%, sorbitan fatty acid ester-80 0.6%, polyoxyethylene sorbitan fat
Fat acid esters-80 0.6%, glycerine 0.5%, hydroxyethyl cellulose 0.6%, surplus is water.
The preparation method of above-mentioned wax emulsion, comprises the following steps:
S1 prepares oil phase dispersed mixture: Brazil wax, polyester wax and paraffin is mixed, is heated to
85 DEG C melt, and open stirring, are subsequently adding sorbitan fatty acid ester-80 and polyoxyethylene sorbitan
Fatty acid ester-80, low whipping speed be 1000rpm stirring condition under disperse 0.5h, obtain oil phase dispersion mixed
Compound；
S2 prepares Aqueous dispersions mixture: water and glycerine are sequentially added in emulsion reactor, low whipping speed
It is warming up to 60 DEG C under conditions of 100rpm, prepares Aqueous dispersions mixture；
S3 prepares wax emulsion: the mixing speed improving emulsion reactor is prepared to 500rpm, addition step S1
Oil phase dispersed mixture emulsify, emulsification times is 1h；It is the mixing speed of 200rpm in speed subsequently
Decline warms to room temperature, and continues stirring 10min, be then filtrated to get leather buffing wax after adding hydroxyethyl cellulose
Emulsion.
Embodiment 3
A kind of leather buffing wax emulsion, including the component of following weight percentage: Brazil wax 3.6%, poly-
Ester type waxes 4.4%, paraffin 3.8%, sorbitan fatty acid ester-80 1.6%, polyoxyethylene sorbitan fat
Fat acid esters-80 1.6%, glycerine 1.2%, xanthan gum 1.2%, surplus is water.
S1 prepares oil phase dispersed mixture: the Brazil wax of above-mentioned formula ratio, polyester wax and paraffin are mixed
Uniformly, it is heated to 92 DEG C and melts, open stirring, be subsequently adding sorbitan fatty acid ester-80 and polyoxy second
Alkene sorbitan fatty acid ester-80, low whipping speed be 1500rpm stirring condition under disperse 1h, obtain
Oil phase dispersed mixture；
S2 prepares Aqueous dispersions mixture: water and glycerine are sequentially added in emulsion reactor, low whipping speed
It is warming up to 75 DEG C under conditions of 150rpm, prepares Aqueous dispersions mixture；
S3 prepares wax emulsion: the mixing speed improving emulsion reactor is prepared to 700rpm, addition step S1
Oil phase dispersed mixture emulsify, emulsification times is 2h；It is the mixing speed of 250rpm in speed subsequently
Decline warms to room temperature, and continues stirring 20min, be then filtrated to get leather buffing wax emulsion after adding xanthan gum.
Embodiment 4
A kind of leather buffing wax emulsion, including the component of following weight percentage: Brazil wax 2.8%, poly-
Ester type waxes 3.6%, paraffin 3.2%, sorbitan fatty acid ester-60 1.6%, polyoxyethylene sorbitan fat
Fat acid esters-60 1.6%, glycerine 0.8%, sodium hydroxide solution 1.8%, xanthans 0.9%, surplus is water.
The preparation method of above-mentioned wax emulsion, comprises the following steps:
S1 prepares oil phase dispersed mixture: the Brazil wax of above-mentioned formula ratio, polyester wax and paraffin are mixed
Uniformly, it is heated to 88 DEG C and melts, open stirring, be subsequently adding sorbitan fatty acid ester-60 and polyoxy second
Alkene sorbitan fatty acid ester-60, low whipping speed be 1000rpm stirring condition under disperse 0.5h,
To oil phase dispersed mixture；
S2 prepares Aqueous dispersions mixture: water and glycerine are sequentially added in emulsion reactor, low whipping speed
It is warming up to 85 DEG C under conditions of 100rpm, prepares Aqueous dispersions mixture；
S3 prepares wax emulsion: the mixing speed improving emulsion reactor is prepared to 500rpm, addition step S1
Oil phase dispersed mixture emulsify, emulsification times is 1h；It is the mixing speed of 200rpm in speed subsequently
Decline warms to room temperature, and continues stirring 10min, be then filtrated to get leather buffing wax emulsion after adding xanthans.
Comparative example 1
A kind of leather buffing wax emulsion, including the component of following weight percentage: Brazil wax 2.6%, stone
Wax 2.6%, sorbitan fatty acid ester-80 0.9%, polyoxyethylene sorbitan fatty acid ester-80 1.2%,
Glycerine 0.8%, xanthans 0.9%, surplus is water.
The preparation method of above-mentioned wax emulsion, comprises the following steps:
S1 prepares oil phase dispersed mixture: Brazil wax and the paraffin of above-mentioned formula ratio is mixed, adds
Heat melts to 90 DEG C, opens stirring, is subsequently adding sorbitan fatty acid ester-80 and polyoxyethylene sorbitan mountain
Pears alcohol fatty acid ester-80, low whipping speed be 1500rpm stirring condition under disperse 1h, obtain oil phase dispersion
Mixture；
S2 prepares Aqueous dispersions mixture: water and glycerine are sequentially added in emulsion reactor, low whipping speed
It is warming up to 75 DEG C under conditions of 150rpm, prepares Aqueous dispersions mixture；
S3 prepares wax emulsion: the mixing speed improving emulsion reactor is prepared to 700rpm, addition step S1
Oil phase dispersed mixture emulsify, emulsification times is 2h；It is the mixing speed of 250rpm in speed subsequently
Decline warms to room temperature, and continues stirring 20min, be then filtrated to get leather buffing wax emulsion after adding xanthans.
Comparative example 2
A kind of leather buffing wax emulsion, including the component of following weight percentage: Brazil wax 5.6%, poly-
Ester type waxes 7.4%, paraffin 5.2%, sorbitan fatty acid ester-80 3.2%, polyoxyethylene sorbitan fat
Fat acid esters-80 3.2%, glycerine 3.6%, Arabic gum 1.8%, surplus is water.
The preparation method of above-mentioned wax emulsion, comprises the following steps:
S1 prepares oil phase dispersed mixture: the Brazil wax of above-mentioned formula ratio, polyester wax and paraffin are mixed
Uniformly, it is heated to 90 DEG C and melts, open stirring, be subsequently adding sorbitan fatty acid ester-80 and polyoxy second
Alkene sorbitan fatty acid ester-80, low whipping speed be 1500rpm stirring condition under disperse 1h, obtain
Oil phase dispersed mixture；
S2 prepares Aqueous dispersions mixture: water and glycerine are sequentially added in emulsion reactor, low whipping speed
It is warming up to 75 DEG C under conditions of 150rpm, prepares Aqueous dispersions mixture；
S3 prepares wax emulsion: the mixing speed improving emulsion reactor is prepared to 700rpm, addition step S1
Oil phase dispersed mixture emulsify, emulsification times is 2h；It is the mixing speed of 250rpm in speed subsequently
Decline warms to room temperature, and continues stirring 20min, be then filtrated to get leather buffing wax emulsion after adding Arabic gum.
Wax emulsion embodiment 1-4 prepared allocates pulping by top coat formula consumption and other leather finish auxiliary agents
Material, after covering with paint, lacquer, colour wash, etc. ox-hide leather, leather hand feeling is comfortable, and surface is fine and smooth, and after polishing, gloss becomes clear, and haftplatte does not occurs
Phenomenon, leather has the water proofing property burning effect with excellence simultaneously.And the wax emulsion of comparative example 1 preparation is by phase
After being deployed into slurry with application formula ratio ratio, after covering with paint, lacquer, colour wash, etc. ox-hide leather, leather hand feeling comfort level is poor, surface
Rougher, though leather has and burns effect after polishing, but brightness is inadequate, and the wax breast of comparative example 2 preparation
After liquid is deployed into slurry, after covering with paint, lacquer, colour wash, etc. ox-hide leather, there is haftplatte phenomenon after leather polishing and there is poor water resistance simultaneously
Problem.
Claims (7)
1. a leather buffing wax emulsion, it is characterised in that include the component of following weight percentage: babassu
Wax 1.4～3.6%, polyester wax 2～5%, paraffin 1.6～3.8%, nonionic surface active agent 1.2～3.2%,
Glycerine 0.5～1.2%, thickener 0.6～1.2%, surplus is water.
Leather buffing wax emulsion the most according to claim 1, it is characterised in that include following weight percentage
Component: Brazil wax 1.6～3.4%, polyester wax 2.4～4.2%, paraffin 1.8～3.6%, nonionic
Surfactant 1.4～2.8%, glycerine 0.6～1%, thickener 0.7～1%, surplus is water.
Leather buffing wax emulsion the most according to claim 2, it is characterised in that include following weight percentage
Component: Brazil wax 1.8～3.2%, polyester wax 2.6～3.8%, paraffin 2.1～3.2%, nonionic
Surfactant 1.6～2.4%, glycerine 0.7～0.9%, thickener 0.8～1%, surplus is water.
Leather buffing wax emulsion the most according to claim 3, it is characterised in that include following weight percentage
Component: Brazil wax 2.6%, polyester wax 3.2%, paraffin 2.6%, nonionic surface active agent 2.1%,
Glycerine 0.8%, thickener 0.9%, surplus is water.
5. according to the leather buffing wax emulsion described in any one of claim 1-4, it is characterised in that described nonionic
Type surfactant is sorbitan fatty acid ester-60, sorbitan fatty acid ester-80, and polyoxyethylene loses
Water Span-60, one in polyoxyethylene sorbitan fatty acid ester-80 and AEO-9 or
Several.
Leather buffing wax emulsion the most according to claim 1, it is characterised in that described thickener is cellulose,
One or more in cellulose gum, magnesium silicate, Arabic gum, xanthans, alginates and xanthan gum.
7. according to the preparation method of the leather buffing wax emulsion described in any one of claim 1-6, it is characterised in that
Comprise the following steps:
S1 prepares oil phase dispersed mixture: Brazil wax, polyester wax and paraffin is mixed, adds heat fusing,
Opening stirring, be subsequently adding nonionic surface active agent, low whipping speed is 1000～2000rpm stirs
Disperse 0.5～1h under the conditions of mixing, obtain oil phase dispersed mixture；
S2 prepares Aqueous dispersions mixture: water and glycerine are sequentially added in emulsion reactor, low whipping speed 100～
It is warming up to 60～80 DEG C under conditions of 200rpm, prepares Aqueous dispersions mixture；
S3 prepares wax emulsion: the mixing speed of raising emulsion reactor, to 500～800rpm, adds step S1 system
Standby oil phase dispersed mixture emulsifies, and emulsification times is 1～3h；It is 200～300rpm in speed subsequently
Mixing speed decline and warm to room temperature, add and continue stirring 10～30min after thickener, be then filtrated to get skin
Leather buffing wax emulsion.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201610282030.5A CN105860856A (en) | 2016-04-29 | 2016-04-29 | Leather polishing wax emulsion and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610282030.5A CN105860856A (en) | 2016-04-29 | 2016-04-29 | Leather polishing wax emulsion and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106366920A (en) * | 2016-08-29 | 2017-02-01 | 浙江奥王服饰有限公司 | Emulsion used in leather processing process and preparation method thereof |
| CN106752760A (en) * | 2016-11-28 | 2017-05-31 | 德阳力久云智知识产权运营有限公司 | A kind of wax Emulsion for Leather containing polyester wax and preparation method thereof |
| CN114907770A (en) * | 2022-05-26 | 2022-08-16 | 清远市宏图助剂有限公司 | Aqueous emulsion type polishing brick antifouling liquid and aqueous organosilicon emulsion |
| CN115948624A (en) * | 2022-12-05 | 2023-04-11 | 温州大学 | Surface finishing wax emulsion for leather |
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|---|---|---|---|---|
| CN106366920A (en) * | 2016-08-29 | 2017-02-01 | 浙江奥王服饰有限公司 | Emulsion used in leather processing process and preparation method thereof |
| CN106752760A (en) * | 2016-11-28 | 2017-05-31 | 德阳力久云智知识产权运营有限公司 | A kind of wax Emulsion for Leather containing polyester wax and preparation method thereof |
| CN114907770A (en) * | 2022-05-26 | 2022-08-16 | 清远市宏图助剂有限公司 | Aqueous emulsion type polishing brick antifouling liquid and aqueous organosilicon emulsion |
| CN115948624A (en) * | 2022-12-05 | 2023-04-11 | 温州大学 | Surface finishing wax emulsion for leather |
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Application publication date: 20160817 |