CN105860641A - Waterproof interior wall putty powder and preparation method thereof - Google Patents
Waterproof interior wall putty powder and preparation method thereof Download PDFInfo
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- CN105860641A CN105860641A CN201610300447.XA CN201610300447A CN105860641A CN 105860641 A CN105860641 A CN 105860641A CN 201610300447 A CN201610300447 A CN 201610300447A CN 105860641 A CN105860641 A CN 105860641A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/34—Filling pastes
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Abstract
The invention provides waterproof interior wall putty powder, prepared mainly from the following materials according to parts by weight: 8-13 parts of sodium polyacrylate, 9-14 parts of polyvinyl acetate, 38-45 parts of ash calcium powder, 15-21 parts of hydroxypropyl methyl cellulose, 20-25 parts of sepiolite, 94-102 parts of heavy calcium carbonate, 7-13 parts of polyvinylidene chloride, 15-22 parts of soluble starch, 0.5-1.5 parts of a defoaming agent, and 0.4-0.8 part of a leveling agent. The waterproof interior wall putty powder obtained herein is easy to construct, highly waterproof, anti-cracking, dusting-proof, high in adhesive strength, safe and environment-friendly and excellent in comprehensive performance.
Description
Technical field
The present invention relates to paint field, particularly relate to water-fast inner wall putty powder and preparation method thereof.
Background technology
Putty is a kind of material decorating character of smooth surface of wall, is a kind of thick slurry coating material, is requisite a kind of product before coating paints.Painting imposes on priming paint or is directly coated with and imposes on object, in order to remove rugged defect on coated article surface.The further raising required home decoration along with people, the development of putty also tends to middle and high end, does not require nothing more than and has good water proofing property, splitting resistance and the more preferable affinity of finish coat etc., to its aspect proposition requirements at the higher level such as safe and environment-friendly.
Publication No. CN 104250466 A(application number 201410501645.3) Chinese patent literature disclose a kind of water-resistant type inner wall putty powder, this powder of lacquer putty for use on is made up of the raw material of following weight portion: white cement 15-25 part, sierozem power 20-30 part, re-dispersible glue powder 1-2 part, cellulose ether 0.2-0.4 part, lignocellulose 0.3-0.5 part, thixotropic lubricant 0.1-0.3 part, Pulvis Talci 5-10 part, calcium carbonate 45-60 part.Publication No. CN 103086664 A(application number 201310004742.7) Chinese patent literature disclose a kind of inner wall putty and production technology thereof, by weight, including following components: white cement 150-300 part；Dicalcium powder 500-900 part；Ash calcium 10-50 part；Cellulose ether 1-8 part；Polymer emulsion powder 7-30 part；Hydrophober 1-10 part；Starch ether 0.05-3 part；Wood fiber 0.5-7 part.Publication No. CN 103351696 A(application number 201310254637.9) Chinese patent literature disclose a kind of Waterproof corrosion inner wall putty, described inner wall putty is made up of following component in parts by weight: sierozem power 35-45 part, attapulgite 12-14 part, sepiolite powder 6-8 part, nano oxidized zinc powder 3-5 part, titanium dioxide 10-14 part, HPMC 2-4 part, polyvinyl alcohol 5-8 part, Oleum Ricini 1-2 part, salad oil 1-3 part, latex dry powder 2-3 part, moistening auxiliary agent 1-2 part.
At present major part putty the most on the market, its resistance to water is poor, peeling after making moist, mouldy, affects attractive in appearance, it is impossible to meet the demand in market, therefore should strengthen research in this respect, strives for developing a kind of water-fast inner wall putty powder.
Summary of the invention
For problem of the prior art, it is an object of the invention to provide a kind of water-fast effective, water-fast inner wall putty powder using safety and stability and preparation method thereof.
The technical scheme is that
Water-fast inner wall putty powder, mainly it is prepared from by following raw materials according, is mass parts: sodium polyacrylate 8-13, polyvinyl acetate 9-14, sierozem power 38-45, hydroxypropyl methyl cellulose 15-21, meerschaum 20-25, ground calcium carbonate 94-102, polyvinylidene chloride 7-13, soluble starch 15-22, defoamer 0.5-1.5, levelling agent 0.4-0.8.
Preferred version is, sodium polyacrylate 9-12, polyvinyl acetate 10-13, sierozem power 40-43, hydroxypropyl methyl cellulose 17-19, meerschaum 21-24, ground calcium carbonate 96-100, polyvinylidene chloride 9-11, soluble starch 17-20, defoamer 0.8-1.2, levelling agent 0.5-0.7.
It is more preferable that sodium polyacrylate 10.5, polyvinyl acetate 11.5, sierozem power 41.5, hydroxypropyl methyl cellulose 18, meerschaum 22.5, ground calcium carbonate 98, polyvinylidene chloride 10, soluble starch 18.5, defoamer 1.0, levelling agent 0.6.
The preparation method of described water-fast inner wall putty powder, step is as follows:
(1) taking sierozem power, meerschaum and ground calcium carbonate to be placed in grinder, attrition grinding 25-45 minute is (preferably: attrition grinding 30-40 minute；More preferably: attrition grinding 35 minutes), taking-up is sieved, and makes raw material powder；
(2) hydroxypropyl methyl cellulose and polyvinylidene chloride are placed in blender, add defoamer and levelling agent, high-speed stirred 20-36 minute, make compound；
(3) sodium polyacrylate and polyvinyl acetate are mixed, add to step (2) gained compound, stir 40-60 minute, add step (1) gained raw material powder and soluble starch, clockwise stirring 15 minutes, counterclockwise stirring 15 minutes, discharging after mix homogeneously, it is dried 24 hours, packs, obtain water-fast inner wall putty powder.
The preparation method of described water-fast inner wall putty powder, step (1) took out 300-400 mesh sieve (preferably: took out 330-370 mesh sieve；More preferably: took out 350 mesh sieves).
The preparation method of described water-fast inner wall putty powder, step (2) stirs 24-32 minute (preferably: stir 28 minutes).
The preparation method of described water-fast inner wall putty powder, step (2) mixing speed is 600-800 rev/min (preferably: mixing speed is 650-750 rev/min；More preferably: mixing speed is 700 revs/min).
The preparation method of described water-fast inner wall putty powder, step (3) mixing speed is 200-320 rev/min (preferably: mixing speed is 240-280 rev/min；More preferably: mixing speed is 260 revs/min).
The preparation method of described water-fast inner wall putty powder, step (3) stirs 45-55 minute (preferably: stir 50 minutes).
The preparation method of described water-fast inner wall putty powder, the temperature that step (3) is dried is 60-80 DEG C (preferably: the temperature being dried is 65-75 DEG C；More preferably: the temperature being dried is 70 DEG C).
The water-fast inner wall putty powder preparation science that the present invention provides, technique is simple.In addition, the excellent results of the present invention is also manifested by: products obtained therefrom easy construction of the present invention, water-tolerant, crack resistence, anti-dry linting, and adhesion strength is high, and safety and environmental protection, combination property is superior.
Detailed description of the invention
Describe technical scheme in detail below in conjunction with embodiment and experimental example, but protection domain is not limited to this.
Embodiment 1Water-fast inner wall putty powder, mainly it is prepared from (every part of 5kg) by following raw materials according: sodium polyacrylate 8 parts, polyvinyl acetate 9 parts, sierozem power 38 parts, hydroxypropyl methyl cellulose 15 parts, meerschaum 20 parts, ground calcium carbonate 94 parts, polyvinylidene chloride 7 parts, soluble starch 15 parts, defoamer 0.5 part, levelling agent 0.4 part.The preparation method of above-mentioned water-fast inner wall putty powder is:
(1) take sierozem power, meerschaum and ground calcium carbonate to be placed in grinder, attrition grinding 25 minutes, took out 300 mesh sieves, and made raw material powder；
(2) hydroxypropyl methyl cellulose and polyvinylidene chloride being placed in blender, add defoamer and levelling agent, stir 20 minutes, mixing speed is 600 revs/min, makes compound；
(3) sodium polyacrylate and polyvinyl acetate are mixed, add to step (2) gained compound, stirring 40 minutes, mixing speed is 200 revs/min, adds step (1) gained raw material powder and soluble starch, stirring 15 minutes clockwise, stirring 15 minutes counterclockwise, discharging after mix homogeneously, it is dried 24 hours under the conditions of 60 DEG C, pack, obtain water-fast inner wall putty powder.
Embodiment 2Water-fast inner wall putty powder, mainly it is prepared from (every part of 5kg) by following raw materials according: sodium polyacrylate 13 parts, polyvinyl acetate 14 parts, sierozem power 45 parts, hydroxypropyl methyl cellulose 21 parts, meerschaum 25 parts, ground calcium carbonate 102 parts, polyvinylidene chloride 13 parts, soluble starch 22 parts, defoamer 1.5 parts, levelling agent 0.8 part.The preparation method of above-mentioned water-fast inner wall putty powder is:
(1) take sierozem power, meerschaum and ground calcium carbonate to be placed in grinder, attrition grinding 45 minutes, took out 400 mesh sieves, and made raw material powder；
(2) hydroxypropyl methyl cellulose and polyvinylidene chloride being placed in blender, add defoamer and levelling agent, stir 36 minutes, mixing speed is 800 revs/min, makes compound；
(3) sodium polyacrylate and polyvinyl acetate are mixed, add to step (2) gained compound, stirring 60 minutes, mixing speed is 320 revs/min, adds step (1) gained raw material powder and soluble starch, stirring 15 minutes clockwise, stirring 15 minutes counterclockwise, discharging after mix homogeneously, it is dried 24 hours under the conditions of 80 DEG C, pack, obtain water-fast inner wall putty powder.
Embodiment 3Water-fast inner wall putty powder, mainly it is prepared from (every part of 5kg) by following raw materials according: sodium polyacrylate 9 parts, polyvinyl acetate 10 parts, sierozem power 40 parts, hydroxypropyl methyl cellulose 17 parts, meerschaum 21 parts, ground calcium carbonate 96 parts, polyvinylidene chloride 9 parts, soluble starch 17 parts, defoamer 0.8 part, levelling agent 0.5 part.The preparation method of above-mentioned water-fast inner wall putty powder is:
(1) take sierozem power, meerschaum and ground calcium carbonate to be placed in grinder, attrition grinding 30 minutes, took out 330 mesh sieves, and made raw material powder；
(2) hydroxypropyl methyl cellulose and polyvinylidene chloride being placed in blender, add defoamer and levelling agent, stir 24 minutes, mixing speed is 650 revs/min, makes compound；
(3) sodium polyacrylate and polyvinyl acetate are mixed, add to step (2) gained compound, stirring 45 minutes, mixing speed is 240 revs/min, adds step (1) gained raw material powder and soluble starch, stirring 15 minutes clockwise, stirring 15 minutes counterclockwise, discharging after mix homogeneously, it is dried 24 hours under the conditions of 65 DEG C, pack, obtain water-fast inner wall putty powder.
Embodiment 4Water-fast inner wall putty powder, mainly it is prepared from (every part of 5kg) by following raw materials according: sodium polyacrylate 12 parts, polyvinyl acetate 13 parts, sierozem power 43 parts, hydroxypropyl methyl cellulose 19 parts, meerschaum 24 parts, ground calcium carbonate 100 parts, polyvinylidene chloride 11 parts, soluble starch 20 parts, defoamer 1.2 parts, levelling agent 0.7 part.The preparation method of above-mentioned water-fast inner wall putty powder is:
(1) take sierozem power, meerschaum and ground calcium carbonate to be placed in grinder, attrition grinding 40 minutes, took out 370 mesh sieves, and made raw material powder；
(2) hydroxypropyl methyl cellulose and polyvinylidene chloride being placed in blender, add defoamer and levelling agent, stir 32 minutes, mixing speed is 750 revs/min, makes compound；
(3) sodium polyacrylate and polyvinyl acetate are mixed, add to step (2) gained compound, stirring 55 minutes, mixing speed is 280 revs/min, adds step (1) gained raw material powder and soluble starch, stirring 15 minutes clockwise, stirring 15 minutes counterclockwise, discharging after mix homogeneously, it is dried 24 hours under the conditions of 75 DEG C, pack, obtain water-fast inner wall putty powder.
Embodiment 5Water-fast inner wall putty powder, mainly it is prepared from (every part of 5kg) by following raw materials according: sodium polyacrylate 10.5 parts, polyvinyl acetate 11.5 parts, sierozem power 41.5 parts, hydroxypropyl methyl cellulose 18 parts, meerschaum 22.5 parts, ground calcium carbonate 98 parts, polyvinylidene chloride 10 parts, soluble starch 18.5 parts, defoamer 1.0 parts, levelling agent 0.6 part.The preparation method of above-mentioned water-fast inner wall putty powder is:
(1) take sierozem power (purchased from Wuhan Hong Xinkang Fine Chemical Co., Ltd), meerschaum (purchased from Wuhan Neng Ren medication chemistry company limited) and ground calcium carbonate (purchased from Hubei Bang Sheng Chemical Co., Ltd.) to be placed in grinder, attrition grinding 35 minutes, take out 350 mesh sieves, make raw material powder；
(2) hydroxypropyl methyl cellulose (purchased from Zibo Pan Ze Chemical Industry Science Co., Ltd) and polyvinylidene chloride (purchased from Zhenghai, Ningbo City Ji Yong Chemical Co., Ltd.) are placed in blender, add defoamer (be purchased from Doris and be coated with Science and Technology Ltd.) and levelling agent (purchased from Hubei Ju Sheng Science and Technology Ltd.), stir 28 minutes, mixing speed is 700 revs/min, makes compound；
(3) sodium polyacrylate (purchased from Henan Hong Jia chemical products company limited) and polyvinyl acetate (grinding Science and Technology Ltd. purchased from upper sea valley) are mixed, add to step (2) gained compound, stir 50 minutes, mixing speed is 260 revs/min, add step (1) gained raw material powder and soluble starch (purchased from Shanghai Bang Jing cause company limited), stirring 15 minutes clockwise, stirring 15 minutes counterclockwise, discharging after mix homogeneously, it is dried 24 hours under the conditions of 70 DEG C, pack, obtain water-fast inner wall putty powder.
Primary raw material used by the present invention:
Sodium polyacrylate: a kind of new functional macromolecule material, plays peptizaiton, plays slurry peptizaiton in textile auxiliary in water paint, Ceramic manufacturing auxiliary agent plays peptizaiton, as washing assisant in detergent, play peptizaiton, dirt-proof resedimentation and thickening power etc..
Polyvinyl acetate: be the polymer of vinyl acetate (vinylacetate).For colourless viscous fluid or pale yellow transparent glass particles, odorless, tasteless, flexible and plasticity.Can not dissolve each other with fat and water, can dissolve each other with ethanol, acetic acid, acetone, ethyl acetate.Purposes: chewing gum base material can be made；Can be used as coating, adhesive, paper, chewing gum base and fabric finishing agent, it is possible to as polyvinyl alcohol and the raw material of Pioloform, polyvinyl acetal.
Sierozem power: main component is Ca (OH)2, CaO and a small amount of CaCO3Mixture, be the intensely processed products of Calx.It is mainly used in building coating to improve the resistance to water of coating, abrasion resistance, has the highest using value.
Hydroxypropyl methyl cellulose: be the gossypin selecting high purity as raw material, prepare, for white or off-white powder through special etherificate in the basic conditions.There is thickening capabilities, the feature such as the low ashes of salt tolerance, pH stability, water-retaining property, dimensional stability, excellent film property and the most resistance to enzyme, dispersibility and caking property.Purposes: mortar can be made to have pumping as the water-retaining agent of cement mortar, retarder in building industry.In coatings industry as thickening agent, dispersant and stabilizer, water or organic solvent all have good intermiscibility.As paint stripper.
Meerschaum: be a kind of have layer chain structure containing Shuifu County's magnesium silicate clay mineral, there is extremely strong absorption, decolour and the performance such as dispersion, also have high heat stability, heat-resisting quantity is up to 1500 ~ 1700 DEG C, and formative nature, insulating properties, anti-salinity are good.Can be used as building field sound insulation, heat-barrier material.
Ground calcium carbonate: be called for short triple superphosphate, be to be ground formed by natural carbonate mineral such as calcite, marble, limestone.Have that chemical purity is high, inertia big, be difficult to chemical reaction, Heat stability is good, will not decompose less than 400 DEG C, whiteness height, oil absorbency is low, index of refraction is low, matter is soft, dry, without advantages such as water of crystallization, the low wearing valve of hardness little, nontoxic, tasteless, odorless, good dispersions, be mainly used as powdery inorganic filler.
Polyvinylidene chloride: prepared through radical polymerization with peroxide or azo-compound for initiator by vinylidene chloride, for white nonflammable porous powder shape, intermolecular cohesiveness is strong, and degree of crystallinity is high, there is excellent oxygen barrier and resistance is moist, and its oxygen barrier is not affected by ambient humidity.
Soluble starch: be a kind of white or off-white powder, odorless, tasteless, 100 mesh percent of pass 100%.Soluble starch does not dissolves in cold water, is dissolved in boiling water.
Test example 1 The performance test of gained of the present invention is water-fast inner wall putty powder (embodiment 5):
1. choose the water-fast inner wall putty powder of gained of the present invention to be uniformly mixed according to the ratio of 1:0.5 with water, then scratch；Carrying out basic property test according to the requirement of JG/T298-2010 N-type, its testing standard is as shown in table 1:
Table 1 test index
The whole conformance with standard of basic property of gained putty of the present invention, and drying time is 40min, water-fast 60h is abnormal without foaming, cracking and obvious dry linting etc., adhesion strength under standard state is 0.86 MPa, adhesion strength after immersion is 0.47 MPa, being substantially better than the level of national standard, illustrate that products obtained therefrom crack resistence of the present invention and water-fast effect are more preferable, performance is more superior.
It should be pointed out that, the detailed description of the invention more representational example that is the present invention, it is clear that technical scheme is not limited to above-described embodiment, it is also possible to have many variations.Those of ordinary skill in the art, with the present invention undoubted the obtaining of clearly disclosed or according to file written description, be all considered as this patent scope of the claimed.
Claims (10)
- The most water-fast inner wall putty powder, it is characterised in that be mainly prepared from by following raw materials according, it is mass parts: sodium polyacrylate 8-13, polyvinyl acetate 9-14, sierozem power 38-45, hydroxypropyl methyl cellulose 15-21, meerschaum 20-25, ground calcium carbonate 94-102, polyvinylidene chloride 7-13, soluble starch 15-22, defoamer 0.5-1.5, levelling agent 0.4-0.8.
- Water-fast inner wall putty powder the most as claimed in claim 1, it is characterized in that, sodium polyacrylate 9-12, polyvinyl acetate 10-13, sierozem power 40-43, hydroxypropyl methyl cellulose 17-19, meerschaum 21-24, ground calcium carbonate 96-100, polyvinylidene chloride 9-11, soluble starch 17-20, defoamer 0.8-1.2, levelling agent 0.5-0.7.
- Water-fast inner wall putty powder the most as claimed in claim 1, it is characterized in that, sodium polyacrylate 10.5, polyvinyl acetate 11.5, sierozem power 41.5, hydroxypropyl methyl cellulose 18, meerschaum 22.5, ground calcium carbonate 98, polyvinylidene chloride 10, soluble starch 18.5, defoamer 1.0, levelling agent 0.6.
- 4. the preparation method of the water-fast inner wall putty powder as described in claim 1-3 is arbitrary, it is characterised in that step is as follows:(1) taking sierozem power, meerschaum and ground calcium carbonate to be placed in grinder, attrition grinding 25-45 minute is (preferably: attrition grinding 30-40 minute；More preferably: attrition grinding 35 minutes), taking-up is sieved, and makes raw material powder；(2) hydroxypropyl methyl cellulose and polyvinylidene chloride are placed in blender, add defoamer and levelling agent, high-speed stirred 20-36 minute, make compound；(3) sodium polyacrylate and polyvinyl acetate are mixed, add to step (2) gained compound, stir 40-60 minute, add step (1) gained raw material powder and soluble starch, clockwise stirring 15 minutes, counterclockwise stirring 15 minutes, discharging after mix homogeneously, it is dried 24 hours, packs, obtain water-fast inner wall putty powder.
- The preparation method of water-fast inner wall putty powder the most as claimed in claim 4, it is characterised in that step (1) took out 300-400 mesh sieve (preferably: took out 330-370 mesh sieve；More preferably: took out 350 mesh sieves).
- The preparation method of water-fast inner wall putty powder the most as claimed in claim 4, it is characterised in that step (2) stirs 24-32 minute (preferably: stir 28 minutes).
- The preparation method of water-fast inner wall putty powder the most as claimed in claim 4, it is characterised in that step (2) mixing speed is 600-800 rev/min (preferably: mixing speed is 650-750 rev/min；More preferably: mixing speed is 700 revs/min).
- The preparation method of water-fast inner wall putty powder the most as claimed in claim 4, it is characterised in that step (3) mixing speed is 200-320 rev/min (preferably: mixing speed is 240-280 rev/min；More preferably: mixing speed is 260 revs/min).
- The preparation method of water-fast inner wall putty powder the most as claimed in claim 4, it is characterised in that step (3) stirs 45-55 minute (preferably: stir 50 minutes).
- The preparation method of water-fast inner wall putty powder the most as claimed in claim 4, it is characterised in that the temperature that step (3) is dried is 60-80 DEG C (preferably: the temperature being dried is 65-75 DEG C；More preferably: the temperature being dried is 70 DEG C).
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106634140A (en) * | 2016-10-08 | 2017-05-10 | 深圳市富粤新材料有限公司 | Outer wall natural stone paint coating and preparation technology thereof |
| CN107189516A (en) * | 2017-07-14 | 2017-09-22 | 合肥威斯伏新材料有限公司 | Wear-resisting interior wall coating of one kind insulation and preparation method thereof |
| CN110655821A (en) * | 2019-10-31 | 2020-01-07 | 浙江壁灵宝建材科技有限公司 | Waterproof interior wall putty powder and preparation method thereof |
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| CN103059192A (en) * | 2012-12-26 | 2013-04-24 | 海南必凯水性涂料有限公司 | Polyvinyl dichloride (PVDC) latex used for interior and exterior wall coating materials and preparation method thereof and application thereof |
| CN104073104A (en) * | 2014-06-24 | 2014-10-01 | 哈尔滨佳饰达科技开发有限公司 | Basal screeding material with capability of preventing indoor decorative cracking |
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| AU2003236666A1 (en) * | 2002-05-17 | 2003-12-02 | Suyesa Compania Suiza- Espanola De Yesos, S.A | Method and system for forming butt joints of plaster fibre-board |
| DE202004011761U1 (en) * | 2004-07-23 | 2004-12-16 | Sicc Gmbh | An elastic putty composition comprising a filler, soft vacuumized glass ceramic microhollow bodies and a binder consisting of a synthetic plastic dispersion useful as a fabric-free intermediate coating |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106634140A (en) * | 2016-10-08 | 2017-05-10 | 深圳市富粤新材料有限公司 | Outer wall natural stone paint coating and preparation technology thereof |
| CN107189516A (en) * | 2017-07-14 | 2017-09-22 | 合肥威斯伏新材料有限公司 | Wear-resisting interior wall coating of one kind insulation and preparation method thereof |
| CN110655821A (en) * | 2019-10-31 | 2020-01-07 | 浙江壁灵宝建材科技有限公司 | Waterproof interior wall putty powder and preparation method thereof |
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