CN105778606A - External wall waterproof putty paste and preparation method thereof - Google Patents
External wall waterproof putty paste and preparation method thereof Download PDFInfo
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- CN105778606A CN105778606A CN201610301821.8A CN201610301821A CN105778606A CN 105778606 A CN105778606 A CN 105778606A CN 201610301821 A CN201610301821 A CN 201610301821A CN 105778606 A CN105778606 A CN 105778606A
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- external wall
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- wall waterproof
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/34—Filling pastes
Abstract
The invention provides external wall waterproof putty paste, which is mainly prepared from the following raw materials in parts by mass: 12 to 16 parts of polyvinyl acetate, 13 to 18 parts of soluble starch, 10 to 15 parts of polyacrylate sodium, 96 to 104 parts of ground limestone, 17 to 23 parts of sodium carboxymethylcellulose, 34 to 42 parts of talcum powder, 9 to 14 parts of polypropylene fiber, 18 to 22 parts of attapulgite, 30 to 50 parts of deionized water, 1 to 2 parts of preservative and 0.5 to 1.5 parts of dispersing agents. The obtained product has the advantages that the construction is convenient; the water resistance performance is good; cracking prevention and powder falling prevention are realized; the bonding strength is high; the comprehensive performance is excellent.
Description
Technical field
The present invention relates to paint field, particularly relate to external wall waterproof putty paste and preparation method thereof.
Background technology
Putty is a kind of material decorating character of smooth surface of wall, is a kind of thick slurry coating material, is before coating paints
Requisite a kind of product.Painting imposes on priming paint or is directly coated with and imposes on object, in order to remove on coated article surface height the most not
Flat defect.The further raising required home decoration along with people, the development of putty also tends to middle and high end, not only wants
Ask and there are good water proofing property, splitting resistance and the more preferable affinity of finish coat etc., its aspect such as safe and environment-friendly is proposed more
High request.
Publication No. CN 105017835 A(application number 201510457993.X) Chinese patent literature disclose outside one
Wall powder of lacquer putty for use on, by modified talc powder 45-60 part, carbonic acid fine particle calcium carbonate 10-40 part, sierozem power 20-30 part, hydroxypropyl methyl cellulose
1.5-2.5 part, nano zine oxide 10-15 part, silica flour 5-10 part, starch alkenyl succinate ester 2-5 part, rubber powder 2-3 part, pigment
0.5-1 part is made.Publication No. CN 102875085 A(application number 201210319039.0) Chinese patent literature disclose and
A kind of waterproof powder of lacquer putty for use on external wall.Described waterproof powder of lacquer putty for use on external wall includes the raw material according to following percetage by weight proportioning: Kaolin
Powder 15-35%, sepiolite powder 10-20%, portland cement 20-40%, Gypsum Fibrosum powder 5-15%, hydroxypropyl methyl cellulose 1-
6%, Semen oryzae sativae gel powder 2-20%, cold melt polyvinyl alcohol rubber powder 0.5-4%.Publication No. CN 103497564 A(application number
Chinese patent literature 201310385713.X) discloses a kind of Dry powder latex paint water resistant putty powder, former by following weight portion
Material composition: dry powder 15-25, sierozem power 30-40, dicalcium powder 10-20, modified talc powder 20-30, hydroxypropyl methyl are fine
Dimension element 0.5-1.5, hydroxypropyl guar gum 0.4-0.6, redispersable latex powder 2-3.
At present major part putty the most on the market, its resistance to water is poor, peeling after making moist, mouldy, affects attractive in appearance, actual application effect
The most bad, it is impossible to meet the demand in market, therefore should strengthen research in this respect, strive for developing a kind of water proof exterior wall putty
Cream.
Summary of the invention
For problem of the prior art, it is an object of the invention to provide a kind of good water-proof effect, use outside safety and stability
Wall water-proof putty cream and preparation method thereof.
The technical scheme is that
External wall waterproof putty paste, is mainly prepared from by following raw materials according, is mass parts: polyvinyl acetate 12-16, solubility
Starch 13-18, sodium polyacrylate 10-15, ground calcium carbonate 96-104, sodium carboxymethyl cellulose 17-23, Pulvis Talci 34-42, poly-
Tacryl 9-14, attapulgite 18-22, deionized water 30-50, preservative 1-2, dispersant 0.5-1.5.
Preferred version is, polyvinyl acetate 13-15, soluble starch 14-17, sodium polyacrylate 11-14, heavy carbonic acid
Calcium 98-102, sodium carboxymethyl cellulose 19-21, Pulvis Talci 36-40, polypropylene fibre 10-13, attapulgite 19-21, deionization
Water 35-45, preservative 1.2-1.8, dispersant 0.8-1.2.
It is more preferable that polyvinyl acetate 14, soluble starch 15.5, sodium polyacrylate 12.5, ground calcium carbonate
100, sodium carboxymethyl cellulose 20, Pulvis Talci 38, polypropylene fibre 11.5, attapulgite 20, deionized water 40, preservative 1.5,
Dispersant 1.0.
The preparation method of described external wall waterproof putty paste, step is as follows:
(1) take ground calcium carbonate and attapulgite is placed under hot environment drying 1-3 hour, take out and grind 30-46 minute
(preferably: grind 34-42 minute;More preferably: grind 38 minutes), mixture powder is made;
(2) deionized water is added to agitator, add Pulvis Talci and dispersant, high-speed stirred 20-40 minute, then add successively
Entering polyvinyl acetate, sodium polyacrylate, sodium carboxymethyl cellulose and polypropylene fibre, stirring at low speed 40-60 minute is (preferably
: stirring at low speed 45-55 minute;More preferably: stirring at low speed 50 minutes), mix homogeneously, obtain mixture paste;
(3) take soluble starch to mix with step (1) gained mixture powder, add in step (2) gained mixture paste, stir
Mix 45 minutes, add preservative, continue stirring 15-25 minute, discharging after mix homogeneously, pack and i.e. obtain external wall waterproof putty
Cream.
The preparation method of described external wall waterproof putty paste, step (1) dries 1.5-2.5 hour (preferably: dry 2 little
Time).
The preparation method of described external wall waterproof putty paste, the fineness of step (1) mixture controls below 45 μm.
The preparation method of described external wall waterproof putty paste, step (2) high-speed stirred 25-35 minute is (preferably: high-speed stirring
Mix 30 minutes).
The preparation method of described external wall waterproof putty paste, step (2) high-speed stirred speed is 800-1200 rev/min
(preferably: high-speed stirred speed is 900-1100 rev/min;More preferably: high-speed stirred speed is 1000 revs/min).
The preparation method of described external wall waterproof putty paste, step (2) stirring at low speed speed be 200-300 rev/min (excellent
Choosing: stirring at low speed speed is 220-280 rev/min;More preferably: stirring at low speed speed is 250 revs/min).
The preparation method of described external wall waterproof putty paste, step (3) continues stirring 18-22 minute (preferably: continue to stir
Mix 20 minutes).
The external wall waterproof putty paste preparation science that the present invention provides, technique is simple.In addition, the excellent results of the present invention
Being also manifested by: products obtained therefrom easy construction of the present invention, water-tolerant, crack resistence, anti-dry linting, adhesion strength is high, and combination property is excellent
More.
Detailed description of the invention
Describe technical scheme in detail below in conjunction with embodiment and experimental example, but protection domain is not limited to this.
Embodiment 1 external wall waterproof putty paste, is mainly prepared from (every part of 5kg) by following raw materials according: polyvinyl acetate 12
Part, soluble starch 13 parts, sodium polyacrylate 10 parts, ground calcium carbonate 96 parts, sodium carboxymethyl cellulose 17 parts, Pulvis Talci 34
Part, polypropylene fibre 9 parts, attapulgite 18 parts, deionized water 30 parts, preservative 1 part, dispersant 0.5 part.Above-mentioned external wall waterproof
The preparation method of putty paste is:
(1) take ground calcium carbonate and attapulgite is placed under hot environment drying 1 hour, take out and grind 30 minutes, make
Mixture powder, the fineness of mixture controls below 45 μm;
(2) being added to agitator by deionized water, add Pulvis Talci and dispersant, high-speed stirred 20 minutes, mixing speed is
800 revs/min, sequentially add polyvinyl acetate, sodium polyacrylate, sodium carboxymethyl cellulose and polypropylene fibre, low speed
Stirring 40 minutes, mixing speed is 200 revs/min, and mix homogeneously obtains mixture paste;
(3) take soluble starch to mix with step (1) gained mixture powder, add in step (2) gained mixture paste, stir
Mix 45 minutes, add preservative, continue stirring 15 minutes, discharging after mix homogeneously, pack and i.e. obtain external wall waterproof putty paste.
Embodiment 2 external wall waterproof putty paste, is mainly prepared from (every part of 5kg) by following raw materials according: polyvinyl acetate 16
Part, soluble starch 18 parts, sodium polyacrylate 15 parts, ground calcium carbonate 104 parts, sodium carboxymethyl cellulose 23 parts, Pulvis Talci 42
Part, polypropylene fibre 14 parts, attapulgite 22 parts, deionized water 50 parts, preservative 2 parts, dispersant 1.5 parts.Above-mentioned exterior wall is prevented
The preparation method of water putty paste is:
(1) take ground calcium carbonate and attapulgite is placed under hot environment drying 3 hours, take out and grind 46 minutes, make
Mixture powder, the fineness of mixture controls below 45 μm;
(2) being added to agitator by deionized water, add Pulvis Talci and dispersant, high-speed stirred 40 minutes, mixing speed is
1200 revs/min, sequentially add polyvinyl acetate, sodium polyacrylate, sodium carboxymethyl cellulose and polypropylene fibre, low speed
Stirring 60 minutes, mixing speed is 300 revs/min, and mix homogeneously obtains mixture paste;
(3) take soluble starch to mix with step (1) gained mixture powder, add in step (2) gained mixture paste, stir
Mix 45 minutes, add preservative, continue stirring 25 minutes, discharging after mix homogeneously, pack and i.e. obtain external wall waterproof putty paste.
Embodiment 3 external wall waterproof putty paste, is mainly prepared from (every part of 5kg) by following raw materials according: polyvinyl acetate 13
Part, soluble starch 14 parts, sodium polyacrylate 11 parts, ground calcium carbonate 98 parts, sodium carboxymethyl cellulose 19 parts, Pulvis Talci 36
Part, polypropylene fibre 10 parts, attapulgite 19 parts, deionized water 35 parts, preservative 1.2 parts, dispersant 0.8 part.Above-mentioned exterior wall
The preparation method of water-proof putty cream is:
(1) take ground calcium carbonate and attapulgite is placed under hot environment drying 1.5 hours, take out and grind 34 minutes, system
Resulting mixture powder, the fineness of mixture controls below 45 μm;
(2) being added to agitator by deionized water, add Pulvis Talci and dispersant, high-speed stirred 25 minutes, mixing speed is
900 revs/min, sequentially add polyvinyl acetate, sodium polyacrylate, sodium carboxymethyl cellulose and polypropylene fibre, low speed
Stirring 45 minutes, mixing speed is 220 revs/min, and mix homogeneously obtains mixture paste;
(3) take soluble starch to mix with step (1) gained mixture powder, add in step (2) gained mixture paste, stir
Mix 45 minutes, add preservative, continue stirring 18 minutes, discharging after mix homogeneously, pack and i.e. obtain external wall waterproof putty paste.
Embodiment 4 external wall waterproof putty paste, is mainly prepared from (every part of 5kg) by following raw materials according: polyvinyl acetate 15
Part, soluble starch 17 parts, sodium polyacrylate 14 parts, ground calcium carbonate 102 parts, sodium carboxymethyl cellulose 21 parts, Pulvis Talci 40
Part, polypropylene fibre 13 parts, attapulgite 21 parts, deionized water 45 parts, preservative 1.8 parts, dispersant 1.2 parts.Above-mentioned exterior wall
The preparation method of water-proof putty cream is:
(1) take ground calcium carbonate and attapulgite is placed under hot environment drying 2.5 hours, take out and grind 42 minutes, system
Resulting mixture powder, the fineness of mixture controls below 45 μm;
(2) being added to agitator by deionized water, add Pulvis Talci and dispersant, high-speed stirred 35 minutes, mixing speed is
1100 revs/min, sequentially add polyvinyl acetate, sodium polyacrylate, sodium carboxymethyl cellulose and polypropylene fibre, low speed
Stirring 55 minutes, mixing speed is 280 revs/min, and mix homogeneously obtains mixture paste;
(3) take soluble starch to mix with step (1) gained mixture powder, add in step (2) gained mixture paste, stir
Mix 45 minutes, add preservative, continue stirring 22 minutes, discharging after mix homogeneously, pack and i.e. obtain external wall waterproof putty paste.
Embodiment 5 external wall waterproof putty paste, is mainly prepared from (every part of 5kg) by following raw materials according: polyvinyl acetate 14
Part, soluble starch 15.5 parts, sodium polyacrylate 12.5 parts, ground calcium carbonate 100 parts, sodium carboxymethyl cellulose 20 parts, Talcum
38 parts of powder, polypropylene fibre 11.5 parts, attapulgite 20 parts, deionized water 40 parts, preservative 1.5 parts, dispersant 1.0 parts.On
The preparation method stating external wall waterproof putty paste is:
(1) take ground calcium carbonate (purchased from Hubei Bang Sheng Chemical Co., Ltd.) and attapulgite (has purchased from Australia of Shenzhen perseverance science and technology
Limit company) it is placed under hot environment drying 2 hours, take out and grind 38 minutes, make mixture powder, the fineness of mixture
Control below 45 μm;
(2) deionized water is added to agitator, add Pulvis Talci (grinding Industrial Co., Ltd. purchased from upper sea valley) and dispersant
(purchased from Shandong, Weifang one Chemical Co., Ltd.), high-speed stirred 30 minutes, mixing speed is 1000 revs/min, sequentially adds poly-
Vinylacetate (grinding Science and Technology Ltd. purchased from upper sea valley), sodium polyacrylate are (purchased from the Henan limited public affairs of grand good chemical products
Department), sodium carboxymethyl cellulose (purchased from oasis, Zhejiang Bioisystech Co., Ltd) and polypropylene fibre (contain chemical purchased from sky, Henan
Industrial Co., Ltd), stirring at low speed 50 minutes, mixing speed is 250 revs/min, and mix homogeneously obtains mixture paste;
(3) take soluble starch (purchased from Shanghai Bang Jing cause company limited) to mix with step (1) gained mixture powder, add
In step (2) gained mixture paste, stir 45 minutes, add preservative (purchased from Yiwu City De Rui Chemical Co., Ltd.),
Continue stirring 20 minutes, discharging after mix homogeneously, pack and i.e. obtain external wall waterproof putty paste.
Primary raw material used by the present invention:
Polyvinyl acetate: be the polymer of vinyl acetate (vinylacetate).For colourless viscous fluid or pale yellow transparent glass
Glass shape granule, odorless, tasteless, flexible and plasticity.Can not dissolve each other with fat and water, can be with ethanol, acetic acid, acetone, acetic acid second
Ester dissolves each other.Purposes: chewing gum base material can be made;Can be used as coating, adhesive, paper, chewing gum base and fabric finishing agent, it is possible to
As polyvinyl alcohol and the raw material of Pioloform, polyvinyl acetal.
Soluble starch: be a kind of white or off-white powder, odorless, tasteless, 100 mesh percent of pass 100%.Soluble starch
Insoluble in cold water, it is dissolved in boiling water.
Sodium polyacrylate: a kind of new functional macromolecule material, plays peptizaiton, in textile auxiliary in water paint
Play slurry peptizaiton, Ceramic manufacturing auxiliary agent rises peptizaiton, as washing assisant in detergent, play peptizaiton, antifouling
Dirt resedimentation and thickening power etc..
Ground calcium carbonate: be called for short triple superphosphate, be to be ground formed by natural carbonate mineral such as calcite, marble, limestone.
Have chemical purity height, inertia is big, be difficult to chemical reaction, Heat stability is good, will not decompose below 400 DEG C, whiteness is high, oil suction
Rate is low, index of refraction is low, matter is soft, dry, without water of crystallization, the low wearing valve of hardness is little, nontoxic, tasteless, odorless, good dispersion etc. are excellent
Point, is mainly used as powdery inorganic filler.
Sodium carboxymethyl cellulose: for the sodium salt of carboxymethyl cellulose ether, belong to anionic cellulose ether, for white or milky white
Color fibre sprills or granule, odorless, tasteless, tasteless, there is hygroscopicity, it is easy to be dispersed in water into clear gum solution, insoluble
In organic solvent.Purposes: be used as thickening agent in food industry, is used as pharmaceutical carrier in medical industry, use in daily chemical industry
Make adhesive, resist the most dignified dose.Printing and dyeing industry is used as the protecting colloid etc. of sizing agent and printing gum.Can in petrochemical industry
As oil recovery fracturing fluid composition.
Pulvis Talci: main component is the magnesium silicate that Talcum is aqueous, for white or off-white color, fine, powder without grittiness, has
Have that lubricity, anti-glutinous, fluidizer, fire resistance, acid-resisting, insulating properties, fusing point height, chemical torpescence, covering power be good, softness,
The excellent Wuli-Shili-Renli system approach such as good luster, absorption affinity are strong.Purposes: can be used for the chemical industry conducts such as rubber, plastics, paint
Strengthening modification filler.
Polypropylene fibre: be that the synthesis that the isotactic polypropylene obtained with propylene polymerization spins for raw material is fine, there is matter
Gently, intensity height, good springiness, the feature such as wear-resisting, corrosion-resistant and heat-resisting, impermeability can be improved, be that a kind of effective rigidity is from anti-
Water material.
Attapulgite: be a kind of have chain layer structure containing Shuifu County's zeopan clay mineral.Its structure exists
Crystal lattice, containing variable amount of Na in side crystal+、Ca2+、Fe3+、Al3+, crystal is needle-like, threadiness or fiber collection shape,
Because of special crystal structure, thermal stability is good, at high temperature without flocks, additionally attapulgite also have good plasticity,
Rheological characteristic and chemical inertness, have certain bonding force, and dried contraction is little, is not easily cracked.
The performance test of test example 1 gained of the present invention external wall waterproof putty paste (embodiment 5):
1. choose gained external wall waterproof putty paste of the present invention, scratch;And carry out according to the requirement of JG/T157-2009 R type
Basic property is tested, and its testing standard is as shown in table 1:
Table 1 testing standard
Understand after tested, product of the present invention state in a reservoir, application property, grinability, alkali resistance, initial dry cracking resistance and low
The temperature equal conformance with standard of bin stability, and surface drying time is 0.8h, under standard state, adhesion strength is 0.90 MPa, freeze-thaw cycle
Adhesion strength after (5 times) is 0.58 MPa, hence it is evident that be better than standard.
2. choose gained external wall waterproof putty paste of the present invention and commercial exterior wall putty cream, carry out water resistance test respectively.
Result of the test: the water absorption of products obtained therefrom of the present invention is 0.2g/min, the water resistance test in 114h, without losing in vain,
The phenomenon such as bubble, come off, and the state that easily restores to the original state after stopping test;And the water absorption of commercial products is 1.7g/min, in 98h
Water resistance test, without lose white, bubble, the phenomenon such as come off, and stops more difficult reinstatement state after test, and gained of the present invention is described
The water-fast effect of product is more notable.
It should be pointed out that, the detailed description of the invention more representational example that is the present invention, it is clear that the skill of the present invention
Art scheme is not limited to above-described embodiment, it is also possible to have many variations.Those of ordinary skill in the art, the most public with present invention institute
What what that open or according to file written description was undoubted obtained, all it is considered as this patent scope of the claimed.
Claims (10)
1. external wall waterproof putty paste, it is characterised in that be mainly prepared from by following raw materials according, be mass parts: polyvinyl acetate
Ester 12-16, soluble starch 13-18, sodium polyacrylate 10-15, ground calcium carbonate 96-104, sodium carboxymethyl cellulose 17-23,
Pulvis Talci 34-42, polypropylene fibre 9-14, attapulgite 18-22, deionized water 30-50, preservative 1-2, dispersant 0.5-
1.5。
2. external wall waterproof putty paste as claimed in claim 1, it is characterised in that polyvinyl acetate 13-15, soluble starch
14-17, sodium polyacrylate 11-14, ground calcium carbonate 98-102, sodium carboxymethyl cellulose 19-21, Pulvis Talci 36-40, polypropylene
Fiber 10-13, attapulgite 19-21, deionized water 35-45, preservative 1.2-1.8, dispersant 0.8-1.2.
3. external wall waterproof putty paste as claimed in claim 1, it is characterised in that polyvinyl acetate 14, soluble starch
15.5, sodium polyacrylate 12.5, ground calcium carbonate 100, sodium carboxymethyl cellulose 20, Pulvis Talci 38, polypropylene fibre 11.5, recessed
Convex rod soil 20, deionized water 40, preservative 1.5, dispersant 1.0.
4. the preparation method of the external wall waterproof putty paste as described in claim 1-3 is arbitrary, it is characterised in that step is as follows:
(1) take ground calcium carbonate and attapulgite is placed under hot environment drying 1-3 hour, take out and grind 30-46 minute
(preferably: grind 34-42 minute;More preferably: grind 38 minutes), mixture powder is made;
(2) deionized water is added to agitator, add Pulvis Talci and dispersant, high-speed stirred 20-40 minute, then add successively
Entering polyvinyl acetate, sodium polyacrylate, sodium carboxymethyl cellulose and polypropylene fibre, stirring at low speed 40-60 minute is (preferably
: stirring at low speed 45-55 minute;More preferably: stirring at low speed 50 minutes), mix homogeneously, obtain mixture paste;
(3) take soluble starch to mix with step (1) gained mixture powder, add in step (2) gained mixture paste, stir
Mix 45 minutes, add preservative, continue stirring 15-25 minute, discharging after mix homogeneously, pack and i.e. obtain external wall waterproof putty
Cream.
5. the preparation method of external wall waterproof putty paste as claimed in claim 4, it is characterised in that step (1) dries 1.5-2.5
Hour (preferably: dry 2 hours).
6. the preparation method of external wall waterproof putty paste as claimed in claim 4, it is characterised in that step (1) mixture thin
Degree controls below 45 μm.
7. the preparation method of external wall waterproof putty paste as claimed in claim 4, it is characterised in that step (2) high-speed stirred 25-
35 minutes (preferably: high-speed stirred 30 minutes).
8. the preparation method of external wall waterproof putty paste as claimed in claim 4, it is characterised in that step (2) high-speed stirred speed
Degree is for 800-1200 rev/min (preferably: high-speed stirred speed is 900-1100 rev/min;More preferably: high-speed stirred
Speed is 1000 revs/min).
9. the preparation method of external wall waterproof putty paste as claimed in claim 4, it is characterised in that step (2) stirring at low speed speed
Degree is for 200-300 rev/min (preferably: stirring at low speed speed is 220-280 rev/min;More preferably: stirring at low speed speed
Degree is 250 revs/min).
10. the preparation method of external wall waterproof putty paste as claimed in claim 4, it is characterised in that step (3) continues stirring
18-22 minute (preferably: continue stirring 20 minutes).
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CN107010881A (en) * | 2017-04-11 | 2017-08-04 | 安徽省明美矿物化工有限公司 | A kind of new calcimine containing attapulgite and preparation method thereof |
CN107383990A (en) * | 2017-09-22 | 2017-11-24 | 苏州振振好新型建材科技有限公司 | A kind of alkali resistant high adhesion force external wall waterproof putty and preparation method thereof |
CN108559405A (en) * | 2018-05-16 | 2018-09-21 | 唐世群 | A kind of preparation method of weathering resistance vehicle polishing cream |
CN109849548A (en) * | 2019-04-10 | 2019-06-07 | 温州市童小戒文化用品有限公司 | A kind of manufacturing method of washable color in sheet and its single page that colors in |
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CN109849548A (en) * | 2019-04-10 | 2019-06-07 | 温州市童小戒文化用品有限公司 | A kind of manufacturing method of washable color in sheet and its single page that colors in |
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