CN105851212A - Pear preservative and preparation method thereof - Google Patents

Pear preservative and preparation method thereof Download PDF

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Publication number
CN105851212A
CN105851212A CN201610205895.1A CN201610205895A CN105851212A CN 105851212 A CN105851212 A CN 105851212A CN 201610205895 A CN201610205895 A CN 201610205895A CN 105851212 A CN105851212 A CN 105851212A
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China
Prior art keywords
parts
gained
extract
preparation
antistaling agent
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Pending
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CN201610205895.1A
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Chinese (zh)
Inventor
刘铁铮
李学营
付雅丽
李勇
郝婕
韩彦肖
刘国胜
索相敏
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Shijiazhuang Institute of Fruit Trees of Hebei Academy of Agriculture and ForestrySciences
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Shijiazhuang Institute of Fruit Trees of Hebei Academy of Agriculture and ForestrySciences
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Application filed by Shijiazhuang Institute of Fruit Trees of Hebei Academy of Agriculture and ForestrySciences filed Critical Shijiazhuang Institute of Fruit Trees of Hebei Academy of Agriculture and ForestrySciences
Priority to CN201610205895.1A priority Critical patent/CN105851212A/en
Publication of CN105851212A publication Critical patent/CN105851212A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
    • A23B7/00Preservation or chemical ripening of fruit or vegetables
    • A23B7/14Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10
    • A23B7/153Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10 in the form of liquids or solids
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23BPRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
    • A23B7/00Preservation or chemical ripening of fruit or vegetables
    • A23B7/14Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10
    • A23B7/153Preserving or ripening with chemicals not covered by groups A23B7/08 or A23B7/10 in the form of liquids or solids
    • A23B7/154Organic compounds; Microorganisms; Enzymes
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2400/00Lactic or propionic acid bacteria
    • A23V2400/11Lactobacillus

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Microbiology (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The present invention discloses a pear preservative and a preparation method thereof. The pear preservative is prepared from the following raw materials in parts by weight: 10-20 parts of herb of salsola-like inula extract, 3-7 parts of celery powder, 27-33 parts of grape seed extract, 36-44 parts of lavender extract, 15-25 parts of bamboo leaf flavone, 15-32 parts of sage extract powder, and 2-4 parts of lignin. The pear preservative is long in shelf life, non-toxic and safe, does not bring medicinal harm, and has advantages of inhibiting pathogens, keeping sensory quality, and being convenient in operation in use and long in release period.

Description

A kind of pears antistaling agent and preparation method thereof
Technical field
The present invention relates to field of fruit freshness keeping, be specifically related to a kind of pears antistaling agent and preparation method thereof.
Background technology
Anticorrosion is requisite sport technique segment in circulation after fresh fruit of vegetables is adopted, and relies on antisepsis antistaling agent to process, suppress fungus, The microorganism such as antibacterial, yeast morbidity as caused by dye is rotted.Preservative is divided into chemosynthesis agent and two kinds of natural extract preparation Type.For a long time, because chemicals imitates height, long half time, low cost, natural extract stable effective ingredients is poor, partly Phase of declining is short, cost is high, and antiseptic preservation of fruits and vegetables continues to use chemicals, even pesticide always.Along with pollution-free food and environmental protection ideas Universal, safe and efficient crude antistaling agent researchs and develops, it has also become the study hotspot of preserving fruit and vegetable utilizing both at home and abroad.
Summary of the invention
For solving the problems referred to above, the invention provides a kind of pears antistaling agent and preparation method thereof, long fresh-keeping period is nontoxic, safe, no Poisoning can be brought, and there is suppression cause of disease, keep organoleptic quality, easy to operate during use, the advantage of release phase length.
For achieving the above object, the technical scheme that the present invention takes is:
A kind of pears antistaling agent, is prepared from by the raw material of following weight portion:
Herba Inulae Salsoloidis extract 10~20 parts, celery powder 3~7 parts, Proflavanol 27~33 parts, lavandula angustifolia extracting solution 36~ 44 parts, Folium Bambusae pyrite 15~25 parts, sage extract powder 15~32 parts, lignin 2~4 parts.
The preparation method of above-mentioned a kind of pears antistaling agent, comprises the steps:
S1, take dry Herba Inulae Salsoloidis herb, with the 90% aqueous solutions of organic solvent room temperature merceration three times of 5 times of volumes after pulverizing, 18h every time, filters, concentrated filtrate, obtains dark brown paste, and recycling design;Then by the paste of gained with suitable After water-dispersible, successively with dichloromethane, ethyl acetate extracts three times respectively, and the filtering residue part continuation water-cooled of gained is extracted Take three times, each 20h, merge all lixiviating solution, obtain Herba Inulae Salsoloidis extract;
S2, take clean after fresh Herba Apii graveolentis, cutting, be placed in steam-explosion jar, being passed through nitrogen to steam explosion pressure inside the tank is 0.6~1.4MPa, After explosion treatment 7~23min, room temperature is concentrated into relative density 1.10~1.20, is spray-dried, obtains celery powder;
S3, dry lavandula angustifolia flash extracter being processed, gained extracting solution first heats with high heat, heats with slow fire after boiling 1.3~1.5h, hollow fiber ultrafiltration membrane filters, and obtains lavandula angustifolia extracting solution;
S4, by after Salvia japonica Thunb. drying and crushing, add 10~15 parts of room temperature pure water, and even, then according to inoculum concentration 1.3~2.3% Ratio microbe inoculation leaven, keep temperature 32~39 DEG C, ferment 48~52 hours, oven drying at low temperature after fermentation ends, Obtain sage extract powder;
S5, the Herba Inulae Salsoloidis extract 10 weighing step S1 gained~20 parts, the celery powder 3 of step S2 gained~7 parts, step The lavandula angustifolia extracting solution 36 of rapid S3 gained~44 parts, the sage extract powder 15 of step S4 gained~32 parts, Semen Vitis viniferae Elite 27~33 parts, Folium Bambusae pyrite 15~25 parts and lignin 2~4 parts are placed in after being sufficiently mixed in mixing and blending machine, bottling, Obtain finished product.
Wherein, described microbe leaven is mixed gained by lactobacillus, long spore Lip river moral yeast and Corynebacterium glutamicum.
Wherein, described lactobacillus: long spore Lip river moral yeast: the mass ratio of Corynebacterium glutamicum is 1: 5: 1.
Wherein, described organic solvent is the turpentine derivatives of natural origin.
Wherein, described turpentine derivatives is the isomery of pinene, disproportionation products.
The method have the advantages that
Long fresh-keeping period, nontoxic, safe, poisoning will not be brought, and there is suppression cause of disease, keep organoleptic quality, operate during use Convenient, the advantage of release phase length.
Detailed description of the invention
In order to make objects and advantages of the present invention clearer, below in conjunction with embodiment, the present invention is carried out the most specifically Bright.Should be appreciated that specific embodiment described herein, only in order to explain the present invention, is not intended to limit the present invention.
Microbe leaven used in following example is pressed quality by lactobacillus, long spore Lip river moral yeast and Corynebacterium glutamicum Than being 1: 5: 1 mixing gained, the organic solvent used is the turpentine derivatives of natural origin, described turpentine derivatives Isomery, disproportionation products for pinene.
Embodiment 1
S1, take dry Herba Inulae Salsoloidis herb, with the 90% aqueous solutions of organic solvent room temperature merceration three times of 5 times of volumes after pulverizing, 18h every time, filters, concentrated filtrate, obtains dark brown paste, and recycling design;Then by the paste of gained with suitable After water-dispersible, successively with dichloromethane, ethyl acetate extracts three times respectively, and the filtering residue part continuation water-cooled of gained is extracted Take three times, each 20h, merge all lixiviating solution, obtain Herba Inulae Salsoloidis extract;
S2, take clean after fresh Herba Apii graveolentis, cutting, be placed in steam-explosion jar, being passed through nitrogen to steam explosion pressure inside the tank is 0.6MPa, After explosion treatment 23min, room temperature is concentrated into relative density 1.10, is spray-dried, obtains celery powder;
S3, dry lavandula angustifolia flash extracter being processed, gained extracting solution first heats with high heat, heats with slow fire after boiling 1.3h, hollow fiber ultrafiltration membrane filters, obtains lavandula angustifolia extracting solution;
S4, by after Salvia japonica Thunb. drying and crushing, add 10 parts of room temperature pure water, and even, then according to the ratio of inoculum concentration 1.3% Microbe inoculation leaven, keeps temperature 32 DEG C, ferments 52 hours, oven drying at low temperature after fermentation ends, obtains Salvia japonica Thunb. and extracts Thing powder;
S5, weigh the Herba Inulae Salsoloidis extract 10 parts of step S1 gained, the celery powder 3 parts of step S2 gained, step S3 gained Lavandula angustifolia extracting solution 36 parts, 15 parts of the sage extract powder of step S4 gained, Proflavanol 27 parts, Folium Bambusae pyrite 15 Part and lignin 2 parts are placed in after being sufficiently mixed in mixing and blending machine, bottling, obtain finished product.
Embodiment 2
S1, take dry Herba Inulae Salsoloidis herb, with the 90% aqueous solutions of organic solvent room temperature merceration three times of 5 times of volumes after pulverizing, 18h every time, filters, concentrated filtrate, obtains dark brown paste, and recycling design;Then by the paste of gained with suitable After water-dispersible, successively with dichloromethane, ethyl acetate extracts three times respectively, and the filtering residue part continuation water-cooled of gained is extracted Take three times, each 20h, merge all lixiviating solution, obtain Herba Inulae Salsoloidis extract;
S2, take clean after fresh Herba Apii graveolentis, cutting, be placed in steam-explosion jar, being passed through nitrogen to steam explosion pressure inside the tank is 1.4MPa, After explosion treatment 7min, room temperature is concentrated into relative density 1.20, is spray-dried, obtains celery powder;
S3, dry lavandula angustifolia flash extracter being processed, gained extracting solution first heats with high heat, heats with slow fire after boiling 1.5h, hollow fiber ultrafiltration membrane filters, obtains lavandula angustifolia extracting solution;
S4, by after Salvia japonica Thunb. drying and crushing, add 15 parts of room temperature pure water, and even, then according to the ratio of inoculum concentration 2.3% Microbe inoculation leaven, keeps temperature 39 DEG C, ferments 48 hours, oven drying at low temperature after fermentation ends, obtains Salvia japonica Thunb. and extracts Thing powder;
S5, weigh the Herba Inulae Salsoloidis extract 20 parts of step S1 gained, the celery powder 7 parts of step S2 gained, step S3 gained Lavandula angustifolia extracting solution 44 parts, 32 parts of the sage extract powder of step S4 gained, Proflavanol 33 parts, Folium Bambusae pyrite 25 Part and lignin 4 parts are placed in after being sufficiently mixed in mixing and blending machine, bottling, obtain finished product.
Embodiment 3
S1, take dry Herba Inulae Salsoloidis herb, with the 90% aqueous solutions of organic solvent room temperature merceration three times of 5 times of volumes after pulverizing, 18h every time, filters, concentrated filtrate, obtains dark brown paste, and recycling design;Then by the paste of gained with suitable After water-dispersible, successively with dichloromethane, ethyl acetate extracts three times respectively, and the filtering residue part continuation water-cooled of gained is extracted Take three times, each 20h, merge all lixiviating solution, obtain Herba Inulae Salsoloidis extract;
S2, take clean after fresh Herba Apii graveolentis, cutting, be placed in steam-explosion jar, being passed through nitrogen to steam explosion pressure inside the tank is 1MPa, quick-fried After tear reason 15min, room temperature is concentrated into relative density 1.15, is spray-dried, obtains celery powder;
S3, dry lavandula angustifolia flash extracter being processed, gained extracting solution first heats with high heat, heats with slow fire after boiling 1.4h, hollow fiber ultrafiltration membrane filters, obtains lavandula angustifolia extracting solution;
S4, by after Salvia japonica Thunb. drying and crushing, add 12.5 parts of room temperature pure water, and even, then according to the ratio of inoculum concentration 1.8% Example microbe inoculation leaven, keeps temperature 35.5 DEG C, ferments 50 hours, and oven drying at low temperature after fermentation ends obtains Salvia japonica Thunb. Extract powder;
S5, weigh the Herba Inulae Salsoloidis extract 15 parts of step S1 gained, the celery powder 5 parts of step S2 gained, step S3 gained Lavandula angustifolia extracting solution 40 parts, 23.5 parts of the sage extract powder of step S4 gained, Proflavanol 30 parts, Folium Bambusae pyrite 20 Part and lignin 3 parts are placed in after being sufficiently mixed in mixing and blending machine, bottling, obtain finished product.
The antistaling agent of embodiment 1-3 gained being sprayed at pears surface, stores 90 days (3 months) fruit colors bud green, fruit is new Fresh, without pit, without rust staining, rot on a small quantity;And the pears not sprayed, fruit appearance quality has declined, pit, rust on peel Speckle increases, and rotting rate also reaches 40%.
The above is only the preferred embodiment of the present invention, it is noted that for those skilled in the art, Without departing from the principles of the invention, it is also possible to make some improvements and modifications, these improvements and modifications also should be regarded as the present invention Protection domain.

Claims (6)

1. a pears antistaling agent, it is characterised in that be prepared from by the raw material of following weight portion:
Herba Inulae Salsoloidis extract 10~20 parts, celery powder 3~7 parts, Proflavanol 27~33 parts, lavandula angustifolia extracting solution 36~ 44 parts, Folium Bambusae pyrite 15~25 parts, sage extract powder 15~32 parts, lignin 2~4 parts.
The preparation method of a kind of pears antistaling agent the most as claimed in claim 1, is characterised by, comprises the steps:
S1, take dry Herba Inulae Salsoloidis herb, with the 90% aqueous solutions of organic solvent room temperature merceration three times of 5 times of volumes after pulverizing, 18h every time, filters, concentrated filtrate, obtains dark brown paste, and recycling design;Then by the paste of gained with suitable After water-dispersible, successively with dichloromethane, ethyl acetate extracts three times respectively, and the filtering residue part continuation water-cooled of gained is extracted Take three times, each 20h, merge all lixiviating solution, obtain Herba Inulae Salsoloidis extract;
S2, take clean after fresh Herba Apii graveolentis, cutting, be placed in steam-explosion jar, being passed through nitrogen to steam explosion pressure inside the tank is 0.6~1.4MPa, After explosion treatment 7~23min, room temperature is concentrated into relative density 1.10~1.20, is spray-dried, obtains celery powder;
S3, dry lavandula angustifolia flash extracter being processed, gained extracting solution first heats with high heat, heats with slow fire after boiling 1.3~1.5h, hollow fiber ultrafiltration membrane filters, and obtains lavandula angustifolia extracting solution;
S4, by after Salvia japonica Thunb. drying and crushing, add 10~15 parts of room temperature pure water, and even, then according to inoculum concentration 1.3~2.3% Ratio microbe inoculation leaven, keep temperature 32~39 DEG C, ferment 48~52 hours, oven drying at low temperature after fermentation ends, Obtain sage extract powder;
S5, the Herba Inulae Salsoloidis extract 10 weighing step S1 gained~20 parts, the celery powder 3 of step S2 gained~7 parts, step The lavandula angustifolia extracting solution 36 of rapid S3 gained~44 parts, the sage extract powder 15 of step S4 gained~32 parts, Semen Vitis viniferae Elite 27~33 parts, Folium Bambusae pyrite 15~25 parts and lignin 2~4 parts are placed in after being sufficiently mixed in mixing and blending machine, bottling, Obtain finished product.
The preparation method of a kind of pears antistaling agent the most as claimed in claim 2, it is characterised in that described microbe leaven is by breast Acidfast bacilli, long spore Lip river moral yeast and Corynebacterium glutamicum mixing gained.
The preparation method of a kind of pears antistaling agent the most as claimed in claim 3, it is characterised in that described lactobacillus: long spore Lip river Moral yeast: the mass ratio of Corynebacterium glutamicum is 1: 5: 1.
The preparation method of a kind of pears antistaling agent the most as claimed in claim 2, it is characterised in that described organic solvent is natural next The turpentine derivatives in source.
The preparation method of a kind of pears antistaling agent the most as claimed in claim 2, it is characterised in that described turpentine derivatives is pinene Isomery, disproportionation products.
CN201610205895.1A 2016-03-28 2016-03-28 Pear preservative and preparation method thereof Pending CN105851212A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106942360A (en) * 2017-03-17 2017-07-14 运城学院 A kind of antistaling agent fresh-keeping for sweet cherry and preparation method thereof
CN107149080A (en) * 2017-05-11 2017-09-12 郑州科技学院 A kind of microcapsule food preservative and preparation method thereof
CN107232291A (en) * 2017-05-17 2017-10-10 安徽禾泉农庄生态农业有限公司 A kind of fresh-keeping treating method of bamboo shoots
CN107535587A (en) * 2017-09-28 2018-01-05 广西吉朋投资有限公司 A kind of antistaling agent for grape and preparation method thereof
CN109645114A (en) * 2019-01-06 2019-04-19 浙江大学 Method based on Pidolidone/beta-aminobutyric acid and bio-control yeast prevention and treatment fruit postharvest diseases
CN110089561A (en) * 2019-06-04 2019-08-06 塔里木大学 A kind of bergamot pear antistaling agent and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1450861A (en) * 2000-03-03 2003-10-22 桔感有限公司 Fruit and vegetable preservative agent
CN101366412A (en) * 2008-09-26 2009-02-18 中国农业大学 Natural fruit and vegetables disinfection antistaling agent, preparation and process of using
CN102524373A (en) * 2010-12-15 2012-07-04 戚冬梅 Fruit preservative
CN104982511A (en) * 2015-06-12 2015-10-21 高孝军 Bergamot pear preservative and manufacturing method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1450861A (en) * 2000-03-03 2003-10-22 桔感有限公司 Fruit and vegetable preservative agent
CN101366412A (en) * 2008-09-26 2009-02-18 中国农业大学 Natural fruit and vegetables disinfection antistaling agent, preparation and process of using
CN102524373A (en) * 2010-12-15 2012-07-04 戚冬梅 Fruit preservative
CN104982511A (en) * 2015-06-12 2015-10-21 高孝军 Bergamot pear preservative and manufacturing method thereof

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* Cited by examiner, † Cited by third party
Title
张兴主编: "《中国农药概览》", 30 April 2011, 中国农业出版社 *

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106942360A (en) * 2017-03-17 2017-07-14 运城学院 A kind of antistaling agent fresh-keeping for sweet cherry and preparation method thereof
CN106942360B (en) * 2017-03-17 2020-09-08 运城学院 Preparation method of preservative for preserving sweet cherries
CN107149080A (en) * 2017-05-11 2017-09-12 郑州科技学院 A kind of microcapsule food preservative and preparation method thereof
CN107232291A (en) * 2017-05-17 2017-10-10 安徽禾泉农庄生态农业有限公司 A kind of fresh-keeping treating method of bamboo shoots
CN107535587A (en) * 2017-09-28 2018-01-05 广西吉朋投资有限公司 A kind of antistaling agent for grape and preparation method thereof
CN109645114A (en) * 2019-01-06 2019-04-19 浙江大学 Method based on Pidolidone/beta-aminobutyric acid and bio-control yeast prevention and treatment fruit postharvest diseases
CN110089561A (en) * 2019-06-04 2019-08-06 塔里木大学 A kind of bergamot pear antistaling agent and preparation method thereof

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Application publication date: 20160817