CN105725090A - Composite celery powder pickling agent - Google Patents

Composite celery powder pickling agent Download PDF

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Publication number
CN105725090A
CN105725090A CN201610066169.6A CN201610066169A CN105725090A CN 105725090 A CN105725090 A CN 105725090A CN 201610066169 A CN201610066169 A CN 201610066169A CN 105725090 A CN105725090 A CN 105725090A
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CN
China
Prior art keywords
celery powder
pickling agent
powder
celery
organic solvent
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Pending
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CN201610066169.6A
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Chinese (zh)
Inventor
石亚中
伍亚华
袁铭
王改玲
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Bengbu College
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Bengbu College
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Priority to CN201610066169.6A priority Critical patent/CN105725090A/en
Publication of CN105725090A publication Critical patent/CN105725090A/en
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

Abstract

The invention discloses a composite celery powder pickling agent which is prepared from the following components: 100-200mg/kg of pomegranate peel polyphenols, 0.2-0.4% of celery powder, 270-330mg/kg of vitamin C, 360-440mg/kg of tea polyphenol, 150-250mg/kg of bamboo leaf flavonoid and 150-320mg/kg of salvia officinalis extract powder. On premise that the quality of a pickled meat product is ensured, bamboo leaf flavonoid, tea polyphenol, user-made celery powder, user-made salvia officinalis extract powder and pomegranate peel polyphenols are compounded to prepare the pickling agent, then the residual amount of nitrite in the pickled meat product can be effectively reduced, and meanwhile the quality of the pickled meat product can be improved.

Description

A kind of celery powder composite pickling agent
Technical field
The present invention relates to food field of deep, be specifically related to a kind of celery powder composite pickling agent.
Background technology
Butcher's meat is unique due to local flavor, quality, can preserve for a long time again, so deeply being liked by consumer.But being usually added into nitrite in butcher's meat curing process, it can react generation N~nitroso compound with dimethylamine under certain condition and have mutagenesis and carcinogenecity, is excessively used and there is safety issue.Therefore, it is necessary to seek natural materials to replace being directly added into nitrite in meat products, produce natural meat products.Domestic and international many scholars have carried out a large amount of reduction or have removed residue of nitrite in meat products and improve butcher's meat matter quantifier elimination.But its method only discusses different additive to the external elimination effect of nitrite or the experiment of single factor impact on marinated meat product, studies still few on the composite pickling agent of the residual affecting Nitrite in Meat Products and butcher's meat quality at present.
Summary of the invention
For solving the problems referred to above, the invention provides a kind of celery powder composite pickling agent, under the premise taking into account marinated meat product quality, undertaken Folium Bambosae flavone, tea polyphenols, homemade celery powder, self-control sage extract powder and Punica granatum L. polyphenol composite preparing curing agent, can effectively reduce butcher's meat nitrate residue, improve marinated meat product quality simultaneously.
For achieving the above object, the technical scheme that the present invention takes is:
A kind of celery powder composite pickling agent, is prepared from by following components:
Pomegranate peel polyphenol 100~200mg/kg, celery powder 0.2~0.4%, Catergen 70~330mg/kg, tea polyphenols 360~440mg/kg, Folium Bambosae flavone 150~250mg/kg, sage extract powder 150~320mg/kg.
Preferably, described celery powder is prepared from by following steps:
S1, take 60~70 parts clean after fresh Herba Apii graveolentis, cutting, be placed in steam-explosion jar, passing into nitrogen to steam explosion pressure inside the tank is 0.7~1.3MPa, and after explosion treatment 8~25min, room temperature is concentrated into relative density 1.10~1.20, spray drying, obtains powder body;
S2,10~15 parts of room temperature pure water of addition, and even, then according to the ratio microbe inoculation leaven of inoculum concentration 1.5~2.5%, keep temperature 35~41 DEG C, ferment 53 hours, oven drying at low temperature after fermentation ends, obtain celery powder.
Preferably, the composition of described microbe leaven is: according to bacterial strain quantity than lactobacillus: Bacillus licheniformis: Corynebacterium glutamicum is: the proportions of 2: 1: 3: 2 becomes 1.6~1.8 × 107The leaven of bacterial strain/ml.
Preferably, described sage extract powder passes through following steps gained:
Being processed by dry Salvia japonica Thunb. flash extracter, gained extracting solution first heats with high heat, heats 1.3~1.5h with slow fire after boiling, and hollow fiber ultrafiltration membrane filters;Medicinal residues add 10~15 times of soak by water twice, and hollow fiber ultrafiltration membrane filters, and merges three filtrates, is concentrated into 1.5g/ml;It is slowly added to 85~95% organic solvents, until organic solvent concentration is 55~65%, cold preservation 7~9 hours, supernatant is removed after the centrifugal 17~23min of 3000~4000r/min, precipitate with deionized water is dissolved to original volume, with organic solvent deposit 2 times, organic solvent concentration respectively 65~75%, 75~85%;Precipitate with deionized water is dissolved to original volume, adds the solution of trichloroacetic acid of 1/6~1/5 volume 11~13%, fully stands 4~6h after mixing, go to precipitate to obtain supernatant after the centrifugal 16~24min of 3000~4000r/min, by gained supernatant sucking filtration, dry, obtain sage extract.
Preferably, described organic solvent is the turpentine derivatives of natural origin.
Preferably, described turpentine derivatives is the isomery of pinene, disproportionation products.
Preferably, above-mentioned celery powder composite pickling agent, following components it is prepared from:
Pomegranate peel polyphenol 150mg/kg, celery powder 0.3%, vitamin C 300mg/kg, tea polyphenols 400mg/kg, Folium Bambosae flavone 200mg/kg, sage extract powder 235mg/kg.
The method have the advantages that
Under the premise taking into account marinated meat product quality, undertaken Folium Bambosae flavone, tea polyphenols, homemade celery powder, self-control sage extract powder and pomegranate peel polyphenol composite preparing curing agent, can effectively reduce butcher's meat nitrate residue, improve marinated meat product quality simultaneously.
Detailed description of the invention
In order to make objects and advantages of the present invention clearly understand, below in conjunction with embodiment, the present invention is further elaborated.Should be appreciated that specific embodiment described herein is only in order to explain the present invention, is not intended to limit the present invention.
The organic solvent used in following example is the turpentine derivatives of natural origin;Turpentine derivatives is the isomery of pinene, disproportionation products.
Embodiment 1
A kind of celery powder composite pickling agent, is prepared from by following components:
Pomegranate peel polyphenol 100mg/kg, celery powder 0.2%, Catergen 70mg/kg, tea polyphenols 360mg/kg, Folium Bambosae flavone 150mg/kg, sage extract powder 150mg/kg.
Described celery powder is prepared from by following steps:
S1, take 60 parts clean after fresh Herba Apii graveolentis, cutting, be placed in steam-explosion jar, passing into nitrogen to steam explosion pressure inside the tank is 0.7MPa, and after explosion treatment 8min, room temperature is concentrated into relative density 1.10, spray drying, obtains powder body;
S2,10 parts of room temperature pure water of addition, and even, then according to the ratio microbe inoculation leaven of inoculum concentration 1.5%, keep temperature 35 DEG C, ferment 53 hours, oven drying at low temperature after fermentation ends, obtain celery powder;The composition of described microbe leaven is: according to bacterial strain quantity than lactobacillus: Bacillus licheniformis: Corynebacterium glutamicum is: the proportions of 2: 1: 3: 2 becomes 1.6 × 107The leaven of bacterial strain/ml.
Described sage extract powder passes through following steps gained:
Being processed by dry Salvia japonica Thunb. flash extracter, gained extracting solution first heats with high heat, heats 1.3h with slow fire after boiling, and hollow fiber ultrafiltration membrane filters;Medicinal residues add 10 times of soak by water twice, and hollow fiber ultrafiltration membrane filters, and merges three filtrates, is concentrated into 1.5g/ml;It is slowly added to 85% organic solvent, until organic solvent concentration is 55%, cold preservation 7 hours, remove supernatant after the centrifugal 17min of 3000r/min, precipitate with deionized water is dissolved to original volume, with organic solvent deposit 2 times, organic solvent concentration respectively 65%, 75%;Precipitate with deionized water is dissolved to original volume, adds the solution of trichloroacetic acid of 1/6 volume 11%, goes to precipitate to obtain supernatant, by gained supernatant sucking filtration, dry, obtain sage extract after fully standing the centrifugal 16min of 4h, 3000r/min after mixing.
Embodiment 2
A kind of celery powder composite pickling agent, is prepared from by following components:
Pomegranate peel polyphenol 200mg/kg, celery powder 0.4%, vitamin C 330mg/kg, tea polyphenols 440mg/kg, Folium Bambosae flavone 250mg/kg, sage extract powder 320mg/kg.
Described celery powder is prepared from by following steps:
S1, take 70 parts clean after fresh Herba Apii graveolentis, cutting, be placed in steam-explosion jar, passing into nitrogen to steam explosion pressure inside the tank is 1.3MPa, and after explosion treatment 25min, room temperature is concentrated into relative density 1.20, spray drying, obtains powder body;
S2,15 parts of room temperature pure water of addition, and even, then according to the ratio microbe inoculation leaven of inoculum concentration 2.5%, keep temperature 41 DEG C, ferment 53 hours, oven drying at low temperature after fermentation ends, obtain celery powder;The composition of described microbe leaven is: according to bacterial strain quantity than lactobacillus: Bacillus licheniformis: Corynebacterium glutamicum is: the proportions of 2: 1: 3: 2 becomes 1.8 × 107The leaven of bacterial strain/ml.
Described sage extract powder passes through following steps gained:
Being processed by dry Salvia japonica Thunb. flash extracter, gained extracting solution first heats with high heat, heats 1.5h with slow fire after boiling, and hollow fiber ultrafiltration membrane filters;Medicinal residues add 15 times of soak by water twice, and hollow fiber ultrafiltration membrane filters, and merges three filtrates, is concentrated into 1.5g/ml;It is slowly added to 95% organic solvent, until organic solvent concentration is 65%, cold preservation 9 hours, remove supernatant after the centrifugal 23min of 4000r/min, precipitate with deionized water is dissolved to original volume, with organic solvent deposit 2 times, organic solvent concentration respectively 75%, 85%;Precipitate with deionized water is dissolved to original volume, adds the solution of trichloroacetic acid of 1/5 volume 13%, goes to precipitate to obtain supernatant, by gained supernatant sucking filtration, dry, obtain sage extract after fully standing the centrifugal 24min of 6h, 4000r/min after mixing.
Embodiment 3
A kind of celery powder composite pickling agent, is prepared from by following components:
Pomegranate peel polyphenol 150mg/kg, celery powder 0.3%, vitamin C 300mg/kg, tea polyphenols 400mg/kg, Folium Bambosae flavone 200mg/kg, sage extract powder 235mg/kg.
Described celery powder is prepared from by following steps:
S1, take 65 parts clean after fresh Herba Apii graveolentis, cutting, be placed in steam-explosion jar, passing into nitrogen to steam explosion pressure inside the tank is 1MPa, and after explosion treatment 16.5min, room temperature is concentrated into relative density 1.15, spray drying, obtains powder body;
S2,12.5 parts of room temperature pure water of addition, and even, then according to the ratio microbe inoculation leaven of inoculum concentration 2%, keep temperature 36 DEG C, ferment 53 hours, oven drying at low temperature after fermentation ends, obtain celery powder;The composition of described microbe leaven is: according to bacterial strain quantity than lactobacillus: Bacillus licheniformis: Corynebacterium glutamicum is: the proportions of 2: 1: 3: 2 becomes 1.7 × 107The leaven of bacterial strain/ml.
Described sage extract powder passes through following steps gained:
Being processed by dry Salvia japonica Thunb. flash extracter, gained extracting solution first heats with high heat, heats 1.4h with slow fire after boiling, and hollow fiber ultrafiltration membrane filters;Medicinal residues add 12.5 times of soak by water twice, and hollow fiber ultrafiltration membrane filters, and merges three filtrates, is concentrated into 1.5g/ml;It is slowly added to 90% organic solvent, until organic solvent concentration is 55~65%, cold preservation 7~9 hours, supernatant is removed after the centrifugal 20min of 3500r/min, precipitate with deionized water is dissolved to original volume, with organic solvent deposit 2 times, and organic solvent concentration respectively 70%, 80%;Precipitate with deionized water is dissolved to original volume, adds the solution of trichloroacetic acid of 11/60 volume 12%, goes to precipitate to obtain supernatant, by gained supernatant sucking filtration, dry, obtain sage extract after fully standing the centrifugal 20min of 5h, 3500r/min after mixing.
The above is only the preferred embodiment of the present invention; it should be pointed out that, for those skilled in the art, under the premise without departing from the principles of the invention; can also making some improvements and modifications, these improvements and modifications also should be regarded as protection scope of the present invention.

Claims (7)

1. a celery powder composite pickling agent, it is characterised in that be prepared from by following components:
Pomegranate peel polyphenol 100~200mg/kg, celery powder 0.2~0.4%, Catergen 70~330mg/kg, tea polyphenols 360~440mg/kg, Folium Bambosae flavone 150~250mg/kg, sage extract powder 150~320mg/kg.
2. a kind of celery powder composite pickling agent according to claim 1, it is characterised in that described celery powder is prepared from by following steps:
S1, take 60~70 parts clean after fresh Herba Apii graveolentis, cutting, be placed in steam-explosion jar, passing into nitrogen to steam explosion pressure inside the tank is 0.7~1.3MPa, and after explosion treatment 8~25min, room temperature is concentrated into relative density 1.10~1.20, spray drying, obtains powder body;
S2,10~15 parts of room temperature pure water of addition, and even, then according to the ratio microbe inoculation leaven of inoculum concentration 1.5~2.5%, keep temperature 35~41 DEG C, ferment 53 hours, oven drying at low temperature after fermentation ends, obtain celery powder.
3. a kind of celery powder composite pickling agent according to claim 2, it is characterized in that, the composition of described microbe leaven is: according to bacterial strain quantity than lactobacillus: Bacillus licheniformis: Corynebacterium glutamicum is: the proportions of 2: 1: 3: 2 becomes 1.6~1.8 × 107The leaven of bacterial strain/ml.
4. a kind of celery powder composite pickling agent according to claim 1, it is characterised in that described sage extract powder passes through following steps gained:
Being processed by dry Salvia japonica Thunb. flash extracter, gained extracting solution first heats with high heat, heats 1.3~1.5h with slow fire after boiling, and hollow fiber ultrafiltration membrane filters;Medicinal residues add 10~15 times of soak by water twice, and hollow fiber ultrafiltration membrane filters, and merges three filtrates, is concentrated into 1.5g/ml;It is slowly added to 85~95% organic solvents, until organic solvent concentration is 55~65%, cold preservation 7~9 hours, supernatant is removed after the centrifugal 17~23min of 3000~4000r/min, precipitate with deionized water is dissolved to original volume, with organic solvent deposit 2 times, organic solvent concentration respectively 65~75%, 75~85%;Precipitate with deionized water is dissolved to original volume, adds the solution of trichloroacetic acid of 1/6~1/5 volume 11~13%, fully stands 4~6h after mixing, go to precipitate to obtain supernatant after the centrifugal 16~24min of 3000~4000r/min, by gained supernatant sucking filtration, dry, obtain sage extract.
5. a kind of celery powder composite pickling agent according to claim 1, it is characterised in that described organic solvent is the turpentine derivatives of natural origin.
6. a kind of celery powder composite pickling agent according to claim 1, it is characterised in that described turpentine derivatives is the isomery of pinene, disproportionation products.
7. a kind of celery powder composite pickling agent according to claim 1, it is characterised in that be prepared from by following components:
Pomegranate peel polyphenol 150mg/kg, celery powder 0.3%, vitamin C 300mg/kg, tea polyphenols 400mg/kg, Folium Bambusae pyrite 200mg/kg, sage extract powder 235mg/kg.
CN201610066169.6A 2016-01-25 2016-01-25 Composite celery powder pickling agent Pending CN105725090A (en)

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106262668A (en) * 2016-08-10 2017-01-04 中盐新干盐化有限公司 A kind of preparation method of bacon salt
CN106722722A (en) * 2016-12-30 2017-05-31 重庆汤嫂食品有限公司 The processing technology of Pickling Powder
CN107950979A (en) * 2017-12-26 2018-04-24 山东龙盛食品股份有限公司 A kind of spices cure and preparation method thereof
CN108041547A (en) * 2017-12-08 2018-05-18 定远县南德调味品加工厂 A kind of vegetables element fresh seasoning and preparation method thereof
CN111317106A (en) * 2020-03-25 2020-06-23 吉林大学 Preparation method for improving quality of low-nitrite western-style smoked and cooked ham
CN113080388A (en) * 2021-05-19 2021-07-09 吉林大学 Method for making low-nitrite western-style smoked and cooked ham
CN114098013A (en) * 2021-10-21 2022-03-01 湖南省嘉品嘉味生物科技有限公司 Pickling process for reducing nitrite content of meat product

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CN101406296A (en) * 2008-10-13 2009-04-15 江苏迈斯克食品有限公司 Green composite additive agent for sauced beef
CN104082699A (en) * 2014-06-16 2014-10-08 天津农学院 Preparation method of fermented celery powder based on natural preserving

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106262668A (en) * 2016-08-10 2017-01-04 中盐新干盐化有限公司 A kind of preparation method of bacon salt
CN106722722A (en) * 2016-12-30 2017-05-31 重庆汤嫂食品有限公司 The processing technology of Pickling Powder
CN108041547A (en) * 2017-12-08 2018-05-18 定远县南德调味品加工厂 A kind of vegetables element fresh seasoning and preparation method thereof
CN107950979A (en) * 2017-12-26 2018-04-24 山东龙盛食品股份有限公司 A kind of spices cure and preparation method thereof
CN111317106A (en) * 2020-03-25 2020-06-23 吉林大学 Preparation method for improving quality of low-nitrite western-style smoked and cooked ham
CN113080388A (en) * 2021-05-19 2021-07-09 吉林大学 Method for making low-nitrite western-style smoked and cooked ham
CN114098013A (en) * 2021-10-21 2022-03-01 湖南省嘉品嘉味生物科技有限公司 Pickling process for reducing nitrite content of meat product

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