CN105707647A - Environment-friendly and non-toxic preservative for condiments and preparation method of preservative - Google Patents

Environment-friendly and non-toxic preservative for condiments and preparation method of preservative Download PDF

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Publication number
CN105707647A
CN105707647A CN201610192445.3A CN201610192445A CN105707647A CN 105707647 A CN105707647 A CN 105707647A CN 201610192445 A CN201610192445 A CN 201610192445A CN 105707647 A CN105707647 A CN 105707647A
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extract
parts
thing
ethanol
preservative
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李杰忠
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With Chicken Coop Mountain County Flavouring Co Ltd
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With Chicken Coop Mountain County Flavouring Co Ltd
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/34Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
    • A23L3/3454Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
    • A23L3/3463Organic compounds; Microorganisms; Enzymes
    • A23L3/3526Organic compounds containing nitrogen
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/34Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
    • A23L3/3454Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
    • A23L3/3463Organic compounds; Microorganisms; Enzymes
    • A23L3/3472Compounds of undetermined constitution obtained from animals or plants
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/34Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
    • A23L3/3454Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
    • A23L3/3463Organic compounds; Microorganisms; Enzymes
    • A23L3/3481Organic compounds containing oxygen
    • A23L3/349Organic compounds containing oxygen with singly-bound oxygen
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/34Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
    • A23L3/3454Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
    • A23L3/3463Organic compounds; Microorganisms; Enzymes
    • A23L3/3481Organic compounds containing oxygen
    • A23L3/3499Organic compounds containing oxygen with doubly-bound oxygen
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/34Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
    • A23L3/3454Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
    • A23L3/3463Organic compounds; Microorganisms; Enzymes
    • A23L3/3481Organic compounds containing oxygen
    • A23L3/3508Organic compounds containing oxygen containing carboxyl groups
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/34Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
    • A23L3/3454Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
    • A23L3/3463Organic compounds; Microorganisms; Enzymes
    • A23L3/3562Sugars; Derivatives thereof
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L3/00Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs
    • A23L3/34Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals
    • A23L3/3454Preservation of foods or foodstuffs, in general, e.g. pasteurising, sterilising, specially adapted for foods or foodstuffs by treatment with chemicals in the form of liquids or solids
    • A23L3/3463Organic compounds; Microorganisms; Enzymes
    • A23L3/3571Microorganisms; Enzymes
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2400/00Lactic or propionic acid bacteria
    • A23V2400/21Streptococcus, lactococcus
    • A23V2400/231Lactis

Abstract

The invention provides an environment-friendly and non-toxic preservative for condiments and a preparation method of the preservative and relates to the technical field of food additives. The preservative is prepared from the following raw materials: protamine, chitosan, a tea polyphenol extract, a Chinese herbal medicine extract, trans-cinnamic acid, agaro-oligosaccharides, bacteriocin, nisin, a spice extract, an acidulant, ethanol and water. The prepared preservative is environment-friendly, non-toxic and pure-natural, compounds a plant source, an animal source and a microorganism source, is non-toxic and harmless for a human body, cannot affect human health, can effectively prolong the shelf life of a hot sauce product and has very high sterilization and bacteriostasis capabilities.

Description

A kind of green non-poisonous anticorrisive agent and preparation method thereof for flavouring
Technical field
The present invention relates to technical field of food additives, be specifically related to a kind of green non-poisonous anticorrisive agent and preparation method thereof for flavouring.
Background technology
Food antiseptic is an ancient topic. before the mankind also do not have chemical synthesis food preservative, people have searched out the way that makes in a large number effective period of food quality extend, as high salt is pickled, in high molasses system, acid, wine, sootiness, water, underground deposit etc.
Along with the development of food industry, tradition anti-corrosion method can not meet its anticorrosion needs, people food antiseptic method is had higher requirement, require operation simpler, shelf-life is longer, anticorrosion cost is lower. based on this, chemical products comes into vogue for the way of food antiseptic. early the chemical preservation of phase mainly contains formaldehyde, the contour malicious product of Nitrates, work out again benzene first later acid, Sodium Benzoate, dehydroacetic acid is received, tens of kinds of all kinds of chemical synthesis food of sodium Diacetate etc. anticorrisive agent. at present, anticorrisive agent is the most extensive in the use of food, it can effectively prevent food by the generation of the caused putrid and deteriorated phenomenon of microorganism, thereby extending its storage life. can say, do not have food preservative just can not have modern food industry.
Along with scientific and technical progress, it is right that people progressively find that chemical synthesis food preservative exists so grave danger of health., wide spectrum is all devoted to again in countries in the world, safety, efficiently the research and development of food preservative. in recent years, along with the raising of people's life and the level of consumption, people level of security to food is had higher requirement, food processing enterprises are in order to comply with market change, its product also more and more changes to the direction such as " green " and " natural ", therefore, my god so, the research and development of the functional food anticorrisive agent of safety just necessitate.
Summary of the invention
(1) technical problem solving
Limited for chemical preservative antibacterial ability in above-mentioned prior art, the shortcomings such as large, the antibacterial kind of toxic and side effect is single, poor stability, the invention provides a kind of green non-poisonous anticorrisive agent and preparation method thereof for flavouring, develop efficient, safe, stable natural antiseptic agent. exploitation had both possessed fungistatic effect, there is bactericidal action simultaneously, and low to environment for use requirement, wide spectrum, efficient natural anticorrosion agent producing process.
(2) technical scheme
For realizing above object, the present invention is achieved by the following technical programs:
The green non-poisonous anticorrisive agent of a kind of flavouring, the raw material that it contains following weight portion: Protamine-2 5-40 part, shitosan 25-40 part, Tea Polyphenols extract 60-90 part, Chinese herbal medicine extract 60-90 part, trans-cinnamic acid 20-30 part, agar compound sugar 20-30 part, bacteriocin 50-85 part, nisin 50-85 part, spice extract 60-90 part, acid 20-30 part, ethanol 60-100 part, water 100-200 part.
Preferably, the raw material that described flavouring contains following weight portion with green non-poisonous anticorrisive agent: Protamine-2 7-38 part, shitosan 27-38 part, Tea Polyphenols extract 65-85 part, Chinese herbal medicine extract 65-80 part, trans-cinnamic acid 22-29 part, agar compound sugar 21-28 part, bacteriocin 55-80 part, nisin 55-80 part, spice extract 65-80 part, acid 22-29 part, ethanol 70-95 part, water 110-190 part.
Preferably, the raw material that described flavouring contains following weight portion with green non-poisonous anticorrisive agent: nucleoprotamine 30-36 part, shitosan 30-35 part, Tea Polyphenols extract 70-80 part, Chinese herbal medicine extract 70-78 part, trans-cinnamic acid 25-27 part, agar compound sugar 23-26 part, bacteriocin 60-70 part, nisin 60-75 part, spice extract 70-78 part, acid 24-27 part, ethanol 75-90 part, water 130-170 part.
Preferably, the raw material that described flavouring contains following weight portion with green non-poisonous anticorrisive agent: 33 parts of nucleoprotamine, 32 parts of shitosans, 75 parts of Tea Polyphenols extracts, 74 parts of Chinese herbal medicine extracts, 25 parts of trans-cinnamic acids, 25 parts of agar compound sugar, 65 parts of bacteriocins, 68 parts of nisins, 75 parts of spice extracts, 25 parts of acids, 80 parts of ethanol, 150 parts, water.
Preferably, described Chinese herbal medicine extract is the mixture of licorice, smoked plum extractive, Flos Caryophylli extract, pepper extract, dried orange peel extracts, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract.
A preparation method for green non-poisonous anticorrisive agent for flavouring, comprises the steps:
S1, take raw material according to weight portion, under room temperature, Tea Polyphenols extract, Chinese herbal medicine are carried Get thing and spice extract and mix, then get 25 parts of ethanol and mix with it, make mixed solvent standby With; The extracting method of described Tea Polyphenols extract and spice extract is: by tealeaves and Xin Xiang After cleaning, shredding, mix, then mixture is inserted in multi-function extractor, add 3-4 doubly to mixed The water of compound matter, regulating extractor pressure is that 1.0-1.5MPa, temperature are 35-38 DEG C, extracts 3 Inferior, each 2 hours, obtain Tea Polyphenols extract and spice extract; Described Chinese herbal medicine is carried The extracting method of getting thing is: cloves, Chinese prickly ash, galangal, Radix Glycyrrhizae, dark plum cleaned and pulverized, Soak with ethanol, through Soxhlet extractor extracting, then concentrate residual by rotary evaporator Ethanol, ethanol can recycle, and makes Chinese herbal medicine extract;
S2, Jiang Shui are heated to 40-50 DEG C, then the mixed solvent that step S1 is made is added to the water, Be stirred to completely and dissolve, being cooled to room temperature, to obtain mixed dissolution liquid for subsequent use;
S3, nucleoprotamine, shitosan, trans-cinnamic acid, agar compound sugar, bacteriocin, nisin are joined in the mixed dissolution of step S2, after stirring makes it to dissolve, acidic flavoring agent solution is joined in the mixed solvent having dissolved, stir while adding, make it to mix, stirring and dissolving, passes through flame filter press by solution.
Preferably, described in step S1, the extracting method of Tea Polyphenols extract and spice extract is: after tealeaves and Xin Xiang are cleaned, shredded, mix, again mixture is inserted in multi-function extractor, add 4 times to the water of compounding substances, regulating extractor pressure is that 1.5MPa, temperature are 37 DEG C, extract 3 times, each 2 hours, obtain Tea Polyphenols extract and spice extract.
(3) beneficial effect
The invention provides a kind of green non-poisonous anticorrisive agent and preparation method thereof for flavouring, the present invention The anticorrisive agent making is completely harmless to human body, have the high and low poison of biological safety, efficient, add The advantage that dosage is few, antiseptic property is good, antimicrobial spectrum is wide, bacteriostasis is strong;
Anticorrisive agent of the present invention is degraded to the normal composition of food in alimentary canal, does not affect alimentary canal Flora, does not affect the use of medicinal antibiotic, is decomposed into carbohydrate after the shelf-life, nontoxic Harmless, protection of the environment, sterilization, bacteriostasis are strong. have very strong kill and suppress saccharomycete, Mould, bacterium, aspergillus niger, Penicillium citrinum, Escherichia coli, bacillus subtilis, golden yellow Portugal Grape coccus, bacillus, have a liking for salt bacillus, aflatoxin, proteus vulgaris, cheese milk The effect of bacillus, lactobacillus plantarum, aerobic spore-bearing bacilli, clostridium botulinum etc., especially to drawing The saccharomycete, mould, the bacterial action that play food spoilage are the strongest, the valid density of its mould fungus inhibition For 0.004-0.1%, general usual amounts is 0.09-0.18%, and the valid density of anti-bacteria is 0.001-0.1%;
Anticorrisive agent of the present invention is for being plant source, animal sources and microbial source compound preservative, can effectively strengthen the shelf-life of thick-chilli sauce product, simultaneously under the mating reaction by plant source and creatural preservative, just can be antibacterial under low concentration, can not cause the generation of peculiar smell and the variation of color to product itself, can keep the original local flavor of product, manufacture craft of the present invention is simple, environmental protection, cost are low, be convenient to promote the use of, and has significant economy and social benefit.
Detailed description of the invention
For making object, technical scheme and the advantage of the embodiment of the present invention clearer; below in conjunction with the embodiment of the present invention; technical scheme in the embodiment of the present invention is clearly and completely described; obviously; described embodiment is the present invention's part embodiment; instead of whole embodiment. based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtaining under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment 1:
The green non-poisonous anticorrisive agent of the present embodiment flavouring, the raw material that it contains following weight portion: Protamine-2 5-40 part, shitosan 25-40 part, Tea Polyphenols extract 60-90 part, Chinese herbal medicine Extract 60-90 part, trans-cinnamic acid 20-30 part, agar oligosaccharide 20-30 part, bacteriocin50-85 part, nisin 50-85 part, spice extract 60-90 part, acidic flavoring agent 20-30Part, ethanol 60-100 part, water 100-200 part.
According to each parts by weight of raw materials in the present embodiment raw material, the Processing technology of green non-poisonous anticorrisive agent for flavouring, comprises the steps:
S1, weigh raw material according to weight portion, under room temperature, tea polyphenol extract thing, Chinese herbal medicine are carried Take thing and the mixing of spice extract, then take ethanol 25 parts and be mixed with, make mixed solvent standby With; The extracting method of described tea polyphenol extract thing and spice extract is:by Folium Camelliae sinensis and Xin Xiang Clean, mix after chopping, then mixture is inserted in multi-function extractor, adds 3-4 times mixed The water of compound matter, regulating extractor pressure is that 1.0-1.5MPa, temperature are 35-38 DEG C, extracts 3 Secondary, each 2 hours, it is thus achieved that tea polyphenol extract thing and spice extract; Described Chinese herbal medicine carries The extracting method taking thing is:Flos Caryophylli, Pericarpium Zanthoxyli, Rhizoma Alpiniae Officinarum, Radix Glycyrrhizae, Fructus Mume are cleaned and pulverized Soak with ethanol, extract through Soxhlet extractor, then go residual by rotary evaporator concentration Ethanol, ethanol can recycle, and prepares Chinese herbal medicine extract;
S2, Jiang Shui are heated to 40-50 DEG C, then the mixed solvent that step S1 is made is added to the water, Stirring is to being completely dissolved, and being cooled to room temperature, to obtain mixed dissolution liquid standby;
S3, by nucleoprotamine, shitosan, trans-cinnamic acid, agar compound sugar, bacteriocin, Nisin joins in the mixed dissolution of step S2, after stirring is allowed to dissolve, by tart flavour agent solution joins in the mixed solvent having dissolved, stir while adding, make it to mix, stirring and dissolving, passes through flame filter press by solution.
Embodiment 2:
The green non-poisonous preservative of the present embodiment flavoring agent, it contains the raw material of following weight portion: Protamine-2 5 parts, chitosan 25 parts, tea polyphenol extract thing 60 parts, Chinese herbal medicine extract 60 Part, trans-cinnamic acid 20 parts, agar oligosaccharide 20 parts, bacteriocin 50 parts, streptococcus acidi lactici 50 parts of elements, 60 parts of spice extracts, 20 parts of acids, 60 parts of ethanol, 100 parts, water.
According to each parts by weight of raw materials in the present embodiment raw material, the manufacture craft of green non-poisonous anticorrisive agent for flavouring, comprises the steps:
S1, weigh raw material according to weight portion, under room temperature, tea polyphenol extract thing, Chinese herbal medicine are carried Take thing and the mixing of spice extract, then take ethanol 25 parts and be mixed with, make mixed solvent standby With;The extracting method of described tea polyphenol extract thing and spice extract is: by Folium Camelliae sinensis and Xin Xiang Clean, mix after chopping, then mixture is inserted in multi-function extractor, adds 3 times mixed The water of compound matter, regulation extraction pot pressure is 1.0MPa, temperature is 35 DEG C, extracts 3 times, often Secondary 2 hours, it is thus achieved that tea polyphenol extract thing and spice extract;Described Chinese herbal medicine extract Extracting method is: Flos Caryophylli, Pericarpium Zanthoxyli, Rhizoma Alpiniae Officinarum, Radix Glycyrrhizae, Fructus Mume is cleaned and is pulverized, uses ethanol Soak, extract through Soxhlet extractor, then go residual ethanol by rotary evaporator concentration, Ethanol can recycle, and prepares Chinese herbal medicine extract;
S2, heat the water to 40 DEG C, then the mixed solvent that step S1 prepares is added to the water, stir Mixing to being completely dissolved, being cooled to room temperature, to obtain mixed dissolution liquid standby;
S3, by protamine, chitosan, trans-cinnamic acid, agar oligosaccharide, bacteriocin, Nisin joins in the mixed dissolution of step S2, after stirring is allowed to dissolve, by tart flavour Agent solution joins in the mixed solvent dissolved, and stirs while adding, and is allowed to mix homogeneously, Stirring and dissolving, by solution by flame filter press,.
Embodiment 3:
The green non-poisonous preservative of the present embodiment flavoring agent, it contains the raw material of following weight portion: Protamine 40 parts, chitosan 40 parts, tea polyphenol extract thing 90 parts, Chinese herbal medicine extract 90 Part, trans-cinnamic acid 30 parts, agar oligosaccharide 30 parts, bacteriocin 85 parts, streptococcus acidi lactici Element 85 parts, spice extract 90 parts, acidic flavoring agent 30 parts, ethanol 100 parts, 200 parts of water.
According to parts by weight of raw materials each in the present embodiment raw material, flavoring agent is with green non-poisonous preservative Processing technology, comprises the steps:
S1, weigh raw material according to weight portion, under room temperature, tea polyphenol extract thing, Chinese herbal medicine are carried Take thing and the mixing of spice extract, then take ethanol 25 parts and be mixed with, make mixed solvent standby With;The extracting method of described tea polyphenol extract thing and spice extract is: by Folium Camelliae sinensis and Xin Xiang Clean, mix after chopping, then mixture is inserted in multi-function extractor, adds 4 times mixed The water of compound matter, regulation extraction pot pressure is 1.5MPa, temperature is 38 DEG C, extracts 3 times, often Secondary 2 hours, it is thus achieved that tea polyphenol extract thing and spice extract;Described Chinese herbal medicine extract Extracting method is: Flos Caryophylli, Pericarpium Zanthoxyli, Rhizoma Alpiniae Officinarum, Radix Glycyrrhizae, Fructus Mume is cleaned and is pulverized, uses ethanol Soak, extract through Soxhlet extractor, then go residual ethanol by rotary evaporator concentration, Ethanol can recycle, and prepares Chinese herbal medicine extract;
S2, heat the water to 50 DEG C, then the mixed solvent that step S1 prepares is added to the water, stir Mixing to being completely dissolved, being cooled to room temperature, to obtain mixed dissolution liquid standby;
S3, by protamine, chitosan, trans-cinnamic acid, agar oligosaccharide, bacteriocin, Nisin joins in the mixed dissolution of step S2, after stirring is allowed to dissolve, by tart flavour Agent solution joins in the mixed solvent dissolved, and stirs while adding, and is allowed to mix homogeneously, Stirring and dissolving, by solution by flame filter press,.
Embodiment 4:
The green non-poisonous preservative of the present embodiment flavoring agent, it contains the raw material of following weight portion: Protamine 33 parts, chitosan 32 parts, tea polyphenol extract thing 75 parts, Chinese herbal medicine extract 74 Part, trans-cinnamic acid 25 parts, agar oligosaccharide 25 parts, bacteriocin 65 parts, streptococcus acidi lactici Element 68 parts, spice extract 75 parts, acidic flavoring agent 25 parts, ethanol 80 parts, 150 parts of water.
According to parts by weight of raw materials each in the present embodiment raw material, flavoring agent is with green non-poisonous preservative Processing technology, comprises the steps:
S1, weigh raw material according to weight portion, under room temperature, tea polyphenol extract thing, Chinese herbal medicine are carried Take thing and the mixing of spice extract, then take ethanol 25 parts and be mixed with, make mixed solvent standby With;The extracting method of described tea polyphenol extract thing and spice extract is: by Folium Camelliae sinensis and Xin Xiang Clean, mix after chopping, then mixture is inserted in multi-function extractor, adds 3-4 times mixed The water of compound matter, regulation extraction pot pressure is 1.5MPa, temperature is 37 DEG C, extracts 3 times, often Secondary 2 hours, it is thus achieved that tea polyphenol extract thing and spice extract;Described Chinese herbal medicine extract Extracting method is: Flos Caryophylli, Pericarpium Zanthoxyli, Rhizoma Alpiniae Officinarum, Radix Glycyrrhizae, Fructus Mume is cleaned and is pulverized, uses ethanol Soak, extract through Soxhlet extractor, then go residual ethanol by rotary evaporator concentration, Ethanol can recycle, and prepares Chinese herbal medicine extract;
S2, heat the water to 45 DEG C, then the mixed solvent that step S1 prepares is added to the water, stir Mixing to being completely dissolved, being cooled to room temperature, to obtain mixed dissolution liquid standby;
S3, by protamine, chitosan, trans-cinnamic acid, agar oligosaccharide, bacteriocin, Nisin joins in the mixed dissolution of step S2, after stirring is allowed to dissolve, by tart flavour Agent solution joins in the mixed solvent dissolved, and stirs while adding, and is allowed to mix homogeneously, Stirring and dissolving, by solution by flame filter press,.
Embodiment 5:
The green non-poisonous preservative of the present embodiment flavoring agent, it contains the raw material of following weight portion: Protamine-2 7 parts, chitosan 27 parts, tea polyphenol extract thing 65 parts, Chinese herbal medicine extract 65 Part, trans-cinnamic acid 22 parts, agar oligosaccharide 21 parts, bacteriocin 55 parts, streptococcus acidi lactici Element 55 parts, spice extract 65 parts, acidic flavoring agent 22 parts, ethanol 70 parts, 110 parts of water.
According to parts by weight of raw materials each in the present embodiment raw material, flavoring agent is with green non-poisonous preservative Processing technology, comprises the steps:
S1, weigh raw material according to weight portion, under room temperature, tea polyphenol extract thing, Chinese herbal medicine are carried Take thing and the mixing of spice extract, then take ethanol 25 parts and be mixed with, make mixed solvent standby With;The extracting method of described tea polyphenol extract thing and spice extract is: by Folium Camelliae sinensis and Xin Xiang Clean, mix after chopping, then mixture is inserted in multi-function extractor, adds 3.2 times mixed The water of compound matter, regulation extraction pot pressure is 1.1MPa, temperature is 36 DEG C, extracts 3 times, often Secondary 2 hours, it is thus achieved that tea polyphenol extract thing and spice extract;Described Chinese herbal medicine extract Extracting method is: Flos Caryophylli, Pericarpium Zanthoxyli, Rhizoma Alpiniae Officinarum, Radix Glycyrrhizae, Fructus Mume is cleaned and is pulverized, uses ethanol Soak, extract through Soxhlet extractor, then go residual ethanol by rotary evaporator concentration, Ethanol can recycle, and prepares Chinese herbal medicine extract;
S2, heat the water to 42 DEG C, then the mixed solvent that step S1 prepares is added to the water, stir Mixing to being completely dissolved, being cooled to room temperature, to obtain mixed dissolution liquid standby;
S3, by protamine, chitosan, trans-cinnamic acid, agar oligosaccharide, bacteriocin, Nisin joins in the mixed dissolution of step S2, after stirring is allowed to dissolve, by tart flavour Agent solution joins in the mixed solvent dissolved, and stirs while adding, and is allowed to mix homogeneously, Stirring and dissolving, by solution by flame filter press,.
Embodiment 6:
The green non-poisonous preservative of the present embodiment flavoring agent, it contains the raw material of following weight portion: Protamine 38 parts, chitosan 38 parts, tea polyphenol extract thing 85 parts, Chinese herbal medicine extract 80 Part, trans-cinnamic acid 29 parts, agar oligosaccharide 28 parts, bacteriocin 80 parts, streptococcus acidi lactici Element 80 parts, spice extract 80 parts, acidic flavoring agent 29 parts, alcohol 95 part, 190 parts of water.
According to parts by weight of raw materials each in the present embodiment raw material, flavoring agent is with green non-poisonous preservative Processing technology, comprises the steps:
S1, weigh raw material according to weight portion, under room temperature, tea polyphenol extract thing, Chinese herbal medicine are carried Take thing and the mixing of spice extract, then take ethanol 25 parts and be mixed with, make mixed solvent standby With;The extracting method of described tea polyphenol extract thing and spice extract is: by Folium Camelliae sinensis and Xin Xiang Clean, mix after chopping, then mixture is inserted in multi-function extractor, adds 3.5 times mixed The water of compound matter, regulation extraction pot pressure is 1.3MPa, temperature is 37 DEG C, extracts 3 times, often Secondary 2 hours, it is thus achieved that tea polyphenol extract thing and spice extract;Described Chinese herbal medicine extract Extracting method is: Flos Caryophylli, Pericarpium Zanthoxyli, Rhizoma Alpiniae Officinarum, Radix Glycyrrhizae, Fructus Mume is cleaned and is pulverized, uses ethanol Soak, extract through Soxhlet extractor, then go residual ethanol by rotary evaporator concentration, Ethanol can recycle, and prepares Chinese herbal medicine extract;
S2, heat the water to 44 DEG C, then the mixed solvent that step S1 prepares is added to the water, stir Mixing to being completely dissolved, being cooled to room temperature, to obtain mixed dissolution liquid standby;
S3, by protamine, chitosan, trans-cinnamic acid, agar oligosaccharide, bacteriocin, Nisin joins in the mixed dissolution of step S2, after stirring is allowed to dissolve, by tart flavour Agent solution joins in the mixed solvent dissolved, and stirs while adding, and is allowed to mix homogeneously, Stirring and dissolving, by solution by flame filter press,.
Embodiment 7:
The green non-poisonous preservative of the present embodiment flavoring agent, it contains the raw material of following weight portion: Protamine 30 parts, chitosan 30 parts, tea polyphenol extract thing 70 parts, Chinese herbal medicine extract 70 Part, trans-cinnamic acid 25 parts, agar oligosaccharide 23 parts, bacteriocin 60 parts, streptococcus acidi lactici Element 60 parts, spice extract 70 parts, acidic flavoring agent 24 parts, ethanol 75 parts, 130 parts of water.
According to parts by weight of raw materials each in the present embodiment raw material, flavoring agent is with green non-poisonous preservative Processing technology, comprises the steps:
S1, weigh raw material according to weight portion, under room temperature, tea polyphenol extract thing, Chinese herbal medicine are carried Take thing and the mixing of spice extract, then take ethanol 25 parts and be mixed with, make mixed solvent standby With;The extracting method of described tea polyphenol extract thing and spice extract is: by Folium Camelliae sinensis and Xin Xiang Clean, mix after chopping, then mixture is inserted in multi-function extractor, adds 3.6 times mixed The water of compound matter, regulation extraction pot pressure is 1.2MPa, temperature is 36 DEG C, extracts 3 times, often Secondary 2 hours, it is thus achieved that tea polyphenol extract thing and spice extract;Described Chinese herbal medicine extract Extracting method is: Flos Caryophylli, Pericarpium Zanthoxyli, Rhizoma Alpiniae Officinarum, Radix Glycyrrhizae, Fructus Mume is cleaned and is pulverized, uses ethanol Soak, extract through Soxhlet extractor, then go residual ethanol by rotary evaporator concentration, Ethanol can recycle, and prepares Chinese herbal medicine extract;
S2, heat the water to 46 DEG C, then the mixed solvent that step S1 prepares is added to the water, stir Mixing to being completely dissolved, being cooled to room temperature, to obtain mixed dissolution liquid standby;
S3, by protamine, chitosan, trans-cinnamic acid, agar oligosaccharide, bacteriocin, Nisin joins in the mixed dissolution of step S2, after stirring is allowed to dissolve, by tart flavour Agent solution joins in the mixed solvent dissolved, and stirs while adding, and is allowed to mix homogeneously, Stirring and dissolving, by solution by flame filter press,.
Embodiment 8:
The green non-poisonous preservative of the present embodiment flavoring agent, it contains the raw material of following weight portion: Protamine 36 parts, chitosan 35 parts, tea polyphenol extract thing 80 parts, Chinese herbal medicine extract 78 Part, trans-cinnamic acid 27 parts, agar oligosaccharide 26 parts, bacteriocin 70 parts, streptococcus acidi lactici Element 75 parts, spice extract 78 parts, acidic flavoring agent 27 parts, ethanol 90 parts, 170 parts of water.
According to parts by weight of raw materials each in the present embodiment raw material, flavoring agent is with green non-poisonous preservative Processing technology, comprises the steps:
S1, weigh raw material according to weight portion, under room temperature, tea polyphenol extract thing, Chinese herbal medicine are carried Take thing and the mixing of spice extract, then take ethanol 25 parts and be mixed with, make mixed solvent standby With;The extracting method of described tea polyphenol extract thing and spice extract is: by Folium Camelliae sinensis and Xin Xiang Clean, mix after chopping, then mixture is inserted in multi-function extractor, adds 3.8 times mixed The water of compound matter, regulation extraction pot pressure is 1.4MPa, temperature is 37 DEG C, extracts 3 times, often Secondary 2 hours, it is thus achieved that tea polyphenol extract thing and spice extract;Described Chinese herbal medicine extract Extracting method is: Flos Caryophylli, Pericarpium Zanthoxyli, Rhizoma Alpiniae Officinarum, Radix Glycyrrhizae, Fructus Mume is cleaned and is pulverized, uses ethanol Soak, extract through Soxhlet extractor, then go residual ethanol by rotary evaporator concentration, Ethanol can recycle, and prepares Chinese herbal medicine extract;
S2, heat the water to 48 DEG C, then the mixed solvent that step S1 prepares is added to the water, stir Mixing to being completely dissolved, being cooled to room temperature, to obtain mixed dissolution liquid standby;
S3, by protamine, chitosan, trans-cinnamic acid, agar oligosaccharide, bacteriocin, Nisin joins in the mixed dissolution of step S2, after stirring is allowed to dissolve, by tart flavour Agent solution joins in the mixed solvent dissolved, and stirs while adding, and is allowed to mix homogeneously, Stirring and dissolving, by solution by flame filter press,.
The green non-poisonous preservative of flavoring agent of the present invention, can effectively strengthen the guarantor of thick-chilli sauce product The matter phase, while the feature that himself is safe and harmless, easy to use, more lossless product special flavour, Be greatly saved production cost, according to preliminary estimation, this project put into serial production the year after next can be enterprise increase newly Income from sales more than 1,500 ten thousand yuan, the new profit about 1,300,000 yuan.Simultaneously by biological antiseptic skill The application of art, will be greatly enhanced the enterprise product market competitiveness, expand production scale of enterprise, from And drive the development of kind thick area pepper planting industry, it is contemplated that pepper planting area 2500 can be increased newly Mu, more than 500 families of bringing along farmers, year is Increase Income of Peasant Households more than 1,000 ten thousand yuan, economic and social benefit Substantially.
It should be noted that in this article, the relational terms of such as first and second or the like is only Only it is used for separating an entity or operation with another entity or operating space, and not necessarily Require or imply and there is the relation of any this reality or suitable between these entities or operation Sequence.And, term " includes ", " comprising " or its any other variant are intended to nonexcludability Comprise, so that include the process of a series of key element, method, article or equipment not only Including those key elements, but also include other key elements being not expressly set out, or also include The key element intrinsic for this process, method, article or equipment.There is no more restriction In the case of, statement " including ... " key element limited, it is not excluded that including described wanting Process, method, article or the equipment of element there is also other identical element.
Above example only in order to technical scheme to be described, is not intended to limit, although With reference to previous embodiment, the present invention is described in detail, those of ordinary skill in the art It is understood that the technical scheme described in foregoing embodiments still can be modified by it, Or wherein portion of techniques feature is carried out equivalent;And these amendments or replacement, not The essence making appropriate technical solution departs from the spirit and scope of various embodiments of the present invention technical scheme.

Claims (7)

1. the green non-poisonous preservative of flavoring agent, it is characterised in that it contains following weight The raw material of part: Protamine-2 5-40 part, chitosan 25-40 part, tea polyphenol extract thing 60-90 Part, Chinese herbal medicine extract 60-90 part, trans-cinnamic acid 20-30 part, agar oligosaccharide 20-30 Part, bacteriocin 50-85 part, nisin 50-85 part, spice extract 60-90 part, Acidic flavoring agent 20-30 part, ethanol 60-100 part, water 100-200 part.
2. the green non-poisonous preservative of flavoring agent as claimed in claim 1, it is characterised in that It contains the raw material of following weight portion: Protamine-2 7-38 part, chitosan 27-38 part, tea are many Phenol extraction thing 65-85 part, Chinese herbal medicine extract 65-80 part, trans-cinnamic acid 22-29 part, fine jade Lipooligosaccharide 21-28 part, bacteriocin 55-80 part, nisin 55-80 part, spice Extract 65-80 part, acidic flavoring agent 22-29 part, ethanol 70-95 part, water 110-190 part.
3. the green non-poisonous preservative of flavoring agent as claimed in claim 1, it is characterised in that It contains the raw material of following weight portion: protamine 30-36 part, chitosan 30-35 part, tea are many Phenol extraction thing 70-80 part, Chinese herbal medicine extract 70-78 part, trans-cinnamic acid 25-27 part, fine jade Lipooligosaccharide 23-26 part, bacteriocin 60-70 part, nisin 60-75 part, spice Extract 70-78 part, acidic flavoring agent 24-27 part, ethanol 75-90 part, water 130-170 part.
4. the green non-poisonous preservative of flavoring agent as claimed in claim 1, it is characterised in that Its raw material containing following weight portion: protamine 33 parts, chitosan 32 parts, tea polyphenols carry Take thing 75 parts, Chinese herbal medicine extract 74 parts, trans-cinnamic acid 25 parts, agar oligosaccharide 25 Part, bacteriocin 65 parts, nisin 68 parts, spice extract 75 parts, acidic flavoring agent 25 parts, ethanol 80 parts, 150 parts of water.
5. the green non-poisonous preservative of flavoring agent as claimed in claim 1, it is characterised in that Described Chinese herbal medicine extract is that Radix Glycyrrhizae extract, Fructus Mume extract, Flos Caryophylli extract, Pericarpium Zanthoxyli carry Take the mixture of thing, Pericarpium Citri Reticulatae extract, Cortex cinnamomi japonici (Ramulus Cinnamomi) extract.
6. the flavoring agent preparation method of green non-poisonous preservative, it is characterised in that include Following steps:
S1, weigh raw material according to weight portion, under room temperature, tea polyphenol extract thing, Chinese herbal medicine are carried Take thing and the mixing of spice extract, then take ethanol 25 parts and be mixed with, make mixed solvent standby With;The extracting method of described tea polyphenol extract thing and spice extract is: by Folium Camelliae sinensis and Xin Xiang Clean, mix after chopping, then mixture is inserted in multi-function extractor, adds 3-4 times mixed The water of compound matter, regulation extraction pot pressure is 1.0-1.5MPa, temperature is 35-38 DEG C, extracts 3 Secondary, each 2 hours, it is thus achieved that tea polyphenol extract thing and spice extract;Described Chinese herbal medicine carries The extracting method taking thing is: Flos Caryophylli, Pericarpium Zanthoxyli, Rhizoma Alpiniae Officinarum, Radix Glycyrrhizae, Fructus Mume are cleaned and pulverized, Soak with ethanol, extract through Soxhlet extractor, then go residual by rotary evaporator concentration Ethanol, ethanol can recycle, and prepares Chinese herbal medicine extract;
S2, heat the water to 40-50 DEG C, then the mixed solvent that step S1 prepares be added to the water, Stirring is to being completely dissolved, and being cooled to room temperature, to obtain mixed dissolution liquid standby;
S3, by protamine, chitosan, trans-cinnamic acid, agar oligosaccharide, bacteriocin, Nisin joins in the mixed dissolution of step S2, after stirring is allowed to dissolve, by tart flavour Agent solution joins in the mixed solvent dissolved, and stirs while adding, and is allowed to mix homogeneously, Stirring and dissolving, by solution by flame filter press,.
7. the preparation method of Oleum Sesami Fructus Capsici sauce preservative as claimed in claim 6, its feature Being, described in step S1, the extracting method of tea polyphenol extract thing and spice extract is: by tea Leaf and Xin Xiang clean, mix after chopping, then are inserted by mixture in multi-function extractor, add 4 The water of times compounding substances, regulation extraction pot pressure is 1.5MPa, temperature is 37 DEG C, extracts 3 Secondary, each 2 hours, it is thus achieved that tea polyphenol extract thing and spice extract.
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CN107594379A (en) * 2017-11-01 2018-01-19 张国栋 A kind of preparation method of roasting milk chicken
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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106107413A (en) * 2016-08-01 2016-11-16 河南牧业经济学院 A kind of biological preservative and preparation method thereof
CN106212634A (en) * 2016-08-06 2016-12-14 灏规旦 A kind of cold fresh pork natural antiseptic agent and preparation method thereof
CN108185264A (en) * 2017-03-02 2018-06-22 安徽键合科技有限公司 A kind of natural environmental-protective preservative and preparation method thereof
CN107279674A (en) * 2017-07-20 2017-10-24 太仓市荣德生物技术研究所 A kind of biological food preservative
CN107594379A (en) * 2017-11-01 2018-01-19 张国栋 A kind of preparation method of roasting milk chicken
CN109566720A (en) * 2019-01-21 2019-04-05 山东元泰生物工程有限公司 A kind of special anti-corrosion agent and preparation method thereof and application
CN110037227A (en) * 2019-05-13 2019-07-23 芜湖职业技术学院 Biological source food preservative material compositions, biological source food preservative and preparation method thereof
CN110313572A (en) * 2019-08-08 2019-10-11 启东晋盛大公化工有限公司 It is a kind of using butyl hydroxybenzoate as the preservative of major ingredient and its preparation process
CN110692985A (en) * 2019-11-06 2020-01-17 四川旅游学院 Formula and preparation process of bean soup Sichuan-style sauce added with composite biological preservative
CN115486478A (en) * 2022-10-09 2022-12-20 江苏天美健大自然生物工程有限公司 Preservative composition for protein beverage and preparation method thereof

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Application publication date: 20160629