CN105838301A - Special sealant for high capacity batteries and preparation process thereof - Google Patents

Special sealant for high capacity batteries and preparation process thereof Download PDF

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Publication number
CN105838301A
CN105838301A CN201610248740.6A CN201610248740A CN105838301A CN 105838301 A CN105838301 A CN 105838301A CN 201610248740 A CN201610248740 A CN 201610248740A CN 105838301 A CN105838301 A CN 105838301A
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Prior art keywords
adds
parts
reactor
mixed
fried
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Chinese (zh)
Inventor
翟恩宏
邱昌炯
陈同吾
官仕朝
李家梅
郑学柱
尹德义
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ANHUI INNOVATION NEW ENERGY Co Ltd
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ANHUI INNOVATION NEW ENERGY Co Ltd
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Priority to CN201610248740.6A priority Critical patent/CN105838301A/en
Publication of CN105838301A publication Critical patent/CN105838301A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J161/00Adhesives based on condensation polymers of aldehydes or ketones; Adhesives based on derivatives of such polymers
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G16/00Condensation polymers of aldehydes or ketones with monomers not provided for in the groups C08G4/00 - C08G14/00
    • C08G16/02Condensation polymers of aldehydes or ketones with monomers not provided for in the groups C08G4/00 - C08G14/00 of aldehydes
    • C08G16/0212Condensation polymers of aldehydes or ketones with monomers not provided for in the groups C08G4/00 - C08G14/00 of aldehydes with acyclic or carbocyclic organic compounds
    • C08G16/0218Condensation polymers of aldehydes or ketones with monomers not provided for in the groups C08G4/00 - C08G14/00 of aldehydes with acyclic or carbocyclic organic compounds containing atoms other than carbon and hydrogen
    • C08G16/0231Condensation polymers of aldehydes or ketones with monomers not provided for in the groups C08G4/00 - C08G14/00 of aldehydes with acyclic or carbocyclic organic compounds containing atoms other than carbon and hydrogen containing nitrogen
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02Non-macromolecular additives
    • C09J11/04Non-macromolecular additives inorganic
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09JADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
    • C09J11/00Features of adhesives not provided for in group C09J9/00, e.g. additives
    • C09J11/02Non-macromolecular additives
    • C09J11/06Non-macromolecular additives organic
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00Specific properties of additives
    • C08K2201/014Additives containing two or more different additives of the same subgroup in C08K
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2203/00Applications
    • C08L2203/20Applications use in electrical or conductive gadgets
    • C08L2203/206Applications use in electrical or conductive gadgets use in coating or encapsulating of electronic parts
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Inorganic Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The invention provides a special sealant for high capacity batteries and a preparation method thereof. The sealant is prepared from the following components: vegetable oil, potassium permanganate, methanol, ethylene glycol, pentaerythritol, sulfolane, alkylphenol ethoxylates, ethanolamine, zinc naphthenate, low grade ether, epoxy organosilicone, a toughening agent, a coupling agent, a curing agent, ethyl cyanoacetate, solid formaldehyde, piperidine, cyclohexane, ethyl acetate, phosphorus pentoxide, sulfur dioxide, hydroquinone, E-42 epoxy resin, a phenolic aldehyde-nitrile-butadiene rubber copolymer, acetone, ethylenediamine, fried common coltsfoot flower, stir-fried platycodon root, fried white silkworm, unibract fritillary bulb, fried opium poppy capsule, fried scorpion and scented tea. When used for sealing plastic surfaces, the sealant has an insulating function on the one hand and a sealing function on the other hand. The sealant prepared by utilizing the method is non-toxic and harmless, furthest ensures leakage of harmful substances of batteries, is also simple in process and low in cost and has excellent properties, a wide range of application, good stability, strong waterproofness, high bonding strength and strong practicability.

Description

High-capacity battery special seal gum and preparation technology thereof
Technical field:
The present invention designs a kind of battery auxiliary material preparation technology, is specifically related to a kind of high-capacity battery Special seal Glue and preparation technology thereof.
Background technology:
Chemical industry is to develop the most rapid mainstay of the national economy industry modern times, and fine chemistry industry tail Gas important component part, has obtained the development advanced by leaps and bounds, the clothing, food, lodging and transportion--basic necessities of life of the unresolved mankind in 20th century And the energy, resource and environment problem make significant contribution;
Needing specialty glue for battery parcel glue, glue is development of modern industry and human living standard's raising Requisite important materials, adhesive and bonding technology are with the incomparable extraordinary work of other connected modes Skill, plays great effect in modern economy, modern national defense, modern science and technology.
Summary of the invention:
The technical problem to be solved is to overcome the defect of prior art, it is provided that a kind of high power capacity Battery special seal gum and preparation technology thereof.
The technical problem to be solved realizes by the following technical solutions.
High-capacity battery special seal gum, it is characterised in that: it is prepared from the following components, vegetable oil 36-44 Part, potassium permanganate 4-6 part, methyl alcohol 9-11 part, ethylene glycol 9-11 part, pentaerythrite 4-6 part, sulfolane 9-11 part, APES 4-6 part, monoethanolamine 9-11 part, zinc naphthenate 19-21 part, rudimentary Ether 6-10 part, epoxy organosilicon 50-60 part, toughener 10-15 part, coupling agent 1-2 part, curing agent 2-3 Part, ethyl cyanoacetate 100-150 part, solid formaldehyde 50-60 part, piperidines 2-3 part, hexamethylene 2-5 part, Ethyl acetate 1-3 part, phosphorus pentoxide 2-5 part, sulfur dioxide 1-2 part, hydroquinones 1-3 part, E-42 Epoxy resin 89-99 part, phenolic aldehyde-nitrile rubber copolymer 89-99 part, acetone 66-75 part, ethylenediamine 10-15 Part, honey-fried FLOS FARFARAE 10-12 part, fry balloonflower root 5-8 part, process stiff silkworm 10-12 part, Bulbus Fritillariae Cirrhosae 3-5 part, process small-mouthed jar Grain shell 3-5 part, process scorpio 1-2 part, jasmine tea 4-5 grain.
High-capacity battery special seal gum comprises the following steps and is prepared from:
1) selection one is with the reactor of agitator, then adds in formula important in reactor Stirring opened by vegetable oil;
2) by the potassium permanganate in raw material, sulfolane, APES, monoethanolamine, aphthenic acids Zinc and rudimentary ether, all add in reactor, after being stirred and heated to 60-80 DEG C, and isothermal reaction 2-4h;
3) after above-mentioned steps reaction terminates, reactor is cooled to 20-25 DEG C, by the Ji Wusi in raw material Alcohol, methyl alcohol and ethylene glycol are added thereto, and stand 5-10h, obtain auxiliary material one after stirring;
4) E-42 epoxy resin and acetone are mixed;
5) mixed solvent and phenolic aldehyde-nitrile rubber copolymer are joined in bottle, stirring;
6) it is heated to 81-86 DEG C, adds MMA, continue stirring 1 hour;
7) intermixture is mixed in the ratio of 30:1 in the environment of ethylenediamine early-60 DEG C to 60 DEG C, Stir;
8) cool to room temperature again, obtain auxiliary material two;
9) take epoxy organosilicon, after toughener, coupling agent mixing be completely dissolved, add curing agent and make half Finished product glue;
10) take solid formaldehyde, piperidines adds in a flask, heating simultaneously, and stirring is dissolved, then will It puts in reactor, and reactor is warming up to 90 DEG C, adds ethyl cyanoacetate, heats 2 hours, then Recycling design methyl alcohol, to temperature 120 DEG C, stops heating, adds hexamethylene, ethyl acetate mixing, backflow Dehydration, temperature rises to 125 DEG C, and discharging obtains condensation polymer;
11) condensation polymer and semi-finished product glue being mixed, proportion is 100:20-50, adds 5-10 part accelerator, Being warming up to 90 DEG C, heating duration i.e. can get copolymerization adhesive in 1 hour;
12) take 1-2 part phosphorus pentoxide and add copolymerization adhesive, be heated to 190 DEG C-200 DEG C, vacuum Crack under 0.1MPa, obtain crude monomer;
13) in crude monomer, remaining phosphorus pentoxide, hydroquinones, sulfur dioxide are added, in reaction Stirring in still, temperature control 80-100 DEG C, vacuum be that to collect cut under 0.1MPa be the product of 70-80 DEG C Product, obtain essence monomer;
14) take essence monomer adding mass fraction is the dioctyl phthalate of 1%-2%, lucite powder Mixture, obtains moment adhesive;
15) by the honey-fried FLOS FARFARAE in constitutive material, fry balloonflower root, process stiff silkworm, Bulbus Fritillariae Cirrhosae, process pappy shell and Processing scorpio, put in cucurbit, add the clear water of 5 times, boiling, the water to cucurbit is evaporated, and collects Steam, steam liquefies again;Being put into by jasmine tea in boiling water simultaneously and soak, the water yield is 300ml, soaks 5-8 minute, cross drainage, obtain jasmine tea water;Again the steam collected is mixed with jasmine tea water, mixed Liquid;
16) taking 20% auxiliary material one to mix with 40% mixed liquor, the moment adhesive taking twice 20% adds mixing, Being heated to 60 DEG C, heating duration 10 minutes, during then cooling is placed in the auxiliary material two of 60%;
17) moment adhesive with 80% mixes the most again, cooling, obtains fluid sealant.
The invention has the beneficial effects as follows: the glue of cell sealing, for sealed plastic surface, on the one hand play Insulating effect, another plays the effect of sealing, and the fluid sealant utilizing this law to prepare is nontoxic, maximum journey Degree ensure that the leakage of battery harmful substance, and technique is simple simultaneously, and property favorable rates is honest and clean, of many uses, stable Property good, water-resistance is strong, and adhesion strength is high, practical.
Detailed description of the invention:
For the technological means making the present invention realize, creation characteristic, reach purpose and effect and be readily apparent from Solve, below in conjunction with specific embodiment, the present invention is expanded on further.
Specific embodiment 1: high-capacity battery special seal gum, is prepared from the following components, vegetable oil 36 parts, 4 parts of potassium permanganate, methyl alcohol 9 parts, ethylene glycol 9 parts, pentaerythrite 4 parts, sulfolane 9 parts, alkyl Phenol polyethenoxy ether 4 parts, monoethanolamine 9 parts, zinc naphthenate 19 parts, 6 parts of rudimentary ether, epoxy organosilicon 50 parts, Toughener 10 parts, coupling agent 1 part, 2 parts of curing agent, ethyl cyanoacetate 100 parts, solid formaldehyde 50 parts, piperazine Pyridine 2 parts, hexamethylene 2 parts, 1 part of ethyl acetate, phosphorus pentoxide 2 parts, sulfur dioxide 1 part, hydroquinones 1 part, E-42 epoxy resin 89 parts, phenolic aldehyde-nitrile rubber copolymer 89 parts, 66 parts of acetone, ethylenediamine 10 Part, honey-fried FLOS FARFARAE 10 parts, fry balloonflower root 5 parts, process stiff silkworm 10 parts, Bulbus Fritillariae Cirrhosae 3 parts, process pappy shell 3 parts, process Scorpio 1 part, jasmine tea 4.
Specific embodiment 2: high-capacity battery special seal gum, is prepared from the following components, vegetable oil 44 parts, 6 parts of potassium permanganate, methyl alcohol 11 parts, ethylene glycol 11 parts, pentaerythrite 6 parts, sulfolane 11 parts, APES 6 parts, monoethanolamine 11 parts, zinc naphthenate 21 parts, 10 parts of rudimentary ether, epoxy are organic Silicon 60 parts, toughener 15 parts, coupling agent 2 parts, 3 parts of curing agent, ethyl cyanoacetate 150 parts, solid formaldehyde 60 parts, piperidines 3 parts, hexamethylene 5 parts, 3 parts of ethyl acetate, phosphorus pentoxide 5 parts, sulfur dioxide 2 parts, Hydroquinones 3 parts, E-42 epoxy resin 99 parts, phenolic aldehyde-nitrile rubber copolymer 99 parts, 75 parts of acetone, Ethylenediamine 15 parts, honey-fried FLOS FARFARAE 12 parts, fry balloonflower root 8 parts, process stiff silkworm 12 parts, Bulbus Fritillariae Cirrhosae 5 parts, process opium poppy 5 parts of shell, process scorpio 2 parts, jasmine tea 5.
Its preparation method includes:
1) selection one is with the reactor of agitator, then adds in formula important in reactor Stirring opened by vegetable oil;
2) by the potassium permanganate in raw material, sulfolane, APES, monoethanolamine, aphthenic acids Zinc and rudimentary ether, all add in reactor, after being stirred and heated to 60-80 DEG C, and isothermal reaction 2-4h;
3) until above-mentioned steps reaction terminate after, reactor is cooled to 20-25 DEG C, by the pentaerythrite in raw material, Methyl alcohol and ethylene glycol are added thereto, and stand 5-10h, obtain auxiliary material one after stirring;
4) E-42 epoxy resin and acetone are mixed;
5) mixed solvent and phenolic aldehyde-nitrile rubber copolymer are joined in bottle, stirring;
6) it is heated to 81-86 DEG C, adds MMA, continue stirring 1 hour;
7) intermixture is mixed in the ratio of 30:1 in the environment of ethylenediamine early-60 DEG C to 60 DEG C, fill Divide and stir;
8) cool to room temperature again, obtain auxiliary material two;
9) take epoxy organosilicon, after toughener, coupling agent mixing be completely dissolved, add curing agent and make half Finished product glue;
10) take solid formaldehyde, piperidines adds in a flask, heating simultaneously, and stirring is dissolved, then by it Put in reactor, reactor is warming up to 90 DEG C, add ethyl cyanoacetate, heat 2 hours, so Rear recycling design methyl alcohol, to temperature 120 DEG C, stops heating, adds hexamethylene, ethyl acetate mixing, Reflux dewatering, temperature rises to 125 DEG C, and discharging obtains condensation polymer;
11) condensation polymer and semi-finished product glue being mixed, proportion is 100:20-50, adds 5-10 part accelerator, Being warming up to 90 DEG C, heating duration i.e. can get copolymerization adhesive in 1 hour;
12) take 1-2 part phosphorus pentoxide and add copolymerization adhesive, be heated to 190 DEG C-200 DEG C, vacuum Crack under 0.1MPa, obtain crude monomer;
13) in crude monomer, remaining phosphorus pentoxide, hydroquinones, sulfur dioxide are added, at reactor Interior stirring, temperature control 80-100 DEG C, vacuum be under 0.1MPa collect cut be 70-80 DEG C Product, obtains essence monomer;
14) take essence monomer adding mass fraction is the dioctyl phthalate of 1%-2%, lucite powder Mixture, obtains moment adhesive;
15) by the honey-fried FLOS FARFARAE in constitutive material, fry balloonflower root, process stiff silkworm, Bulbus Fritillariae Cirrhosae, process pappy shell and process Scorpio, puts in cucurbit, adds the clear water of 5 times, boiling, and the water to cucurbit is evaporated, and receives Collection steam, steam liquefies again;Being put into by jasmine tea in boiling water simultaneously and soak, the water yield is 300ml, Soak 5-8 minute, cross drainage, obtain jasmine tea water;Again the steam collected is mixed with jasmine tea water, Obtain mixed liquor;
16) taking 20% auxiliary material one to mix with 40% mixed liquor, the moment adhesive taking twice 20% adds mixing, Being heated to 60 DEG C, heating duration 10 minutes, during then cooling is placed in the auxiliary material two of 60%;
17) moment adhesive with 80% mixes the most again, cooling, obtains fluid sealant.
The general principle of the present invention, principal character and advantages of the present invention have more than been shown and described.One's own profession Skilled person will appreciate that of industry, the present invention is not restricted to the described embodiments, above-described embodiment and explanation The principle that the present invention is simply described described in book, without departing from the spirit and scope of the present invention, The present invention also has various changes and modifications, and these changes and improvements both fall within claimed invention model In enclosing.Claimed scope is defined by appending claims and equivalent thereof.

Claims (2)

1. high-capacity battery special seal gum, it is characterised in that: it is prepared from the following components, vegetable oil 36-44 part, potassium permanganate 4-6 part, methyl alcohol 9-11 part, ethylene glycol 9-11 part, pentaerythrite 4-6 part, ring Fourth sulfone 9-11 part, APES 4-6 part, monoethanolamine 9-11 part, zinc naphthenate 19-21 part, Rudimentary ether 6-10 part, epoxy organosilicon 50-60 part, toughener 10-15 part, coupling agent 1-2 part, curing agent 2-3 part, ethyl cyanoacetate 100-150 part, solid formaldehyde 50-60 part, piperidines 2-3 part, hexamethylene 2-5 part, Ethyl acetate 1-3 part, phosphorus pentoxide 2-5 part, sulfur dioxide 1-2 part, hydroquinones 1-3 part, E-42 Epoxy resin 89-99 part, phenolic aldehyde-nitrile rubber copolymer 89-99 part, acetone 66-75 part, ethylenediamine 10-15 Part, honey-fried FLOS FARFARAE 10-12 part, fry balloonflower root 5-8 part, process stiff silkworm 10-12 part, Bulbus Fritillariae Cirrhosae 3-5 part, process small-mouthed jar Grain shell 3-5 part, process scorpio 1-2 part, jasmine tea 4-5 grain.
2. according to the high-capacity battery special seal gum described in claim 1, it is characterised in that: include Following steps are prepared from:
1) selection one is with the reactor of agitator, then adds in formula important in reactor Stirring opened by vegetable oil;
2) by the potassium permanganate in raw material, sulfolane, APES, monoethanolamine, aphthenic acids Zinc and rudimentary ether, all add in reactor, after being stirred and heated to 60-80 DEG C, and isothermal reaction 2-4h;
3) after above-mentioned steps reaction terminates, reactor is cooled to 20-25 DEG C, by the Ji Wusi in raw material Alcohol, methyl alcohol and ethylene glycol are added thereto, and stand 5-10h, obtain auxiliary material one after stirring;
4) E-42 epoxy resin and acetone are mixed;
5) mixed solvent and phenolic aldehyde-nitrile rubber copolymer are joined in bottle, stirring;
6) it is heated to 81-86 DEG C, adds MMA, continue stirring 1 hour;
7) intermixture is mixed in the ratio of 30:1 in the environment of ethylenediamine early-60 DEG C to 60 DEG C, Stir;
8) cool to room temperature again, obtain auxiliary material two;
9) take epoxy organosilicon, after toughener, coupling agent mixing be completely dissolved, add curing agent and make half Finished product glue;
10) take solid formaldehyde, piperidines adds in a flask, heating simultaneously, and stirring is dissolved, then will It puts in reactor, and reactor is warming up to 90 DEG C, adds ethyl cyanoacetate, heats 2 hours, then Recycling design methyl alcohol, to temperature 120 DEG C, stops heating, adds hexamethylene, ethyl acetate mixing, backflow Dehydration, temperature rises to 125 DEG C, and discharging obtains condensation polymer;
11) condensation polymer and semi-finished product glue being mixed, proportion is 100:20-50, adds 5-10 part accelerator, Being warming up to 90 DEG C, heating duration i.e. can get copolymerization adhesive in 1 hour;
12) take 1-2 part phosphorus pentoxide and add copolymerization adhesive, be heated to 190 DEG C-200 DEG C, vacuum Crack under 0.1MPa, obtain crude monomer;
13) in crude monomer, remaining phosphorus pentoxide, hydroquinones, sulfur dioxide are added, in reaction Stirring in still, temperature control 80-100 DEG C, vacuum be that to collect cut under 0.1MPa be the product of 70-80 DEG C Product, obtain essence monomer;
14) take essence monomer adding mass fraction is the dioctyl phthalate of 1%-2%, lucite powder Mixture, obtains moment adhesive;
15) by the honey-fried FLOS FARFARAE in constitutive material, fry balloonflower root, process stiff silkworm, Bulbus Fritillariae Cirrhosae, process pappy shell and Processing scorpio, put in cucurbit, add the clear water of 5 times, boiling, the water to cucurbit is evaporated, and collects Steam, steam liquefies again;Being put into by jasmine tea in boiling water simultaneously and soak, the water yield is 300ml, soaks 5-8 minute, cross drainage, obtain jasmine tea water;Again the steam collected is mixed with jasmine tea water, mixed Liquid;
16) taking 20% auxiliary material one to mix with 40% mixed liquor, the moment adhesive taking twice 20% adds mixing, Being heated to 60 DEG C, heating duration 10 minutes, during then cooling is placed in the auxiliary material two of 60%;
17) moment adhesive with 80% mixes the most again, cooling, obtains fluid sealant.
CN201610248740.6A 2016-04-19 2016-04-19 Special sealant for high capacity batteries and preparation process thereof Pending CN105838301A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103947793A (en) * 2014-04-09 2014-07-30 郎溪县黄香茶叶有限公司 Tea drink formula beneficial to wind dispelling and phlegm relief and preparation method thereof
CN104073198A (en) * 2014-06-26 2014-10-01 安徽神舟飞船胶业有限公司 Formula and preparation process of non-toxic epoxy resin adhesive
CN104194715A (en) * 2014-08-26 2014-12-10 安徽神舟飞船胶业有限公司 Formula and preparation process of instant organic silicon adhesive
CN104711043A (en) * 2015-01-30 2015-06-17 安徽海德石油化工有限公司 Novel burner plant oil and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103947793A (en) * 2014-04-09 2014-07-30 郎溪县黄香茶叶有限公司 Tea drink formula beneficial to wind dispelling and phlegm relief and preparation method thereof
CN104073198A (en) * 2014-06-26 2014-10-01 安徽神舟飞船胶业有限公司 Formula and preparation process of non-toxic epoxy resin adhesive
CN104194715A (en) * 2014-08-26 2014-12-10 安徽神舟飞船胶业有限公司 Formula and preparation process of instant organic silicon adhesive
CN104711043A (en) * 2015-01-30 2015-06-17 安徽海德石油化工有限公司 Novel burner plant oil and preparation method thereof

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Application publication date: 20160810