CN101892028A - Environment-friendly curtain adhesive for hair product and preparation method thereof - Google Patents
Environment-friendly curtain adhesive for hair product and preparation method thereof Download PDFInfo
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- CN101892028A CN101892028A CN 201010219645 CN201010219645A CN101892028A CN 101892028 A CN101892028 A CN 101892028A CN 201010219645 CN201010219645 CN 201010219645 CN 201010219645 A CN201010219645 A CN 201010219645A CN 101892028 A CN101892028 A CN 101892028A
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Abstract
The invention relates to an environmental-friendly curtain adhesive for a hair product and a preparation method thereof. The environmental-friendly curtain adhesive for a hair product is compatibly dissolved and synthesized by the following raw materials in parts by weight: 0.05 part of alcohol-soluble polyurethane adhesive b, 0.04 to 0.15 part of sugar ester, 0.05 to 0.25 part of rosin, 0.05 to 0.4 part of curing agent of alcohol-soluble polyurethane adhesive, 0.01 to 0.08 part of sodium persulfate and 0.15 to 0.75 part of absolute ethyl alcohol. In the preparation method, the thermal decomposition type sodium persulfate is used as the initiator to avoid pollution caused by a decomposition product remained in the adhesive when the organic peroxide is used as the initiator; the high-temperature polymerization replaces the low-temperature polymerization to reduce the energy consumption; the conversion rate of the polymerization reaction is improved and the quantity of the recovered monomer is reduced; the physical degasification and the chemical degasification are combined, so that the degasification time is shortened and the energy consumption is reduced.
Description
Technical field
The invention belongs to chemical technology, the mutual interleaving techniques of biotechnology field, be specifically related to a kind of environment-friendly curtain adhesive for hair product and preparation method thereof.
Background technology
The curtain adhesive of hair products is based on solvent type resin class tackiness agent at present, and it exists the most of curtain adhesive bonding of following defective (1) wig firm inadequately, causes the alopecia phenomenon easily; (2) after wig used curtain adhesive, the curtain limit of wig was harder, and is soft inadequately; (3) moiety of traditional curtain adhesive does not reach environmental requirement.
Summary of the invention
The objective of the invention is to overcome above-mentioned the deficiencies in the prior art and provide that a kind of cohesive force is strong, effect is lasting, and nontoxic, non-stimulated, the simple environment-friendly curtain adhesive for hair product of manufacture craft and preparation method thereof.
The object of the present invention is achieved like this:
A kind of environment-friendly curtain adhesive for hair product is characterized in that: be fused into and get through compatibility according to parts by weight by following raw materials: 0.05～0.5 part in alcohol-soluble polyurethane tackiness agent; 0.04～0.15 part of sucrose ester; 0.05～0.25 part of rosin; 0.05～0.4 part in the solidifying agent of alcohol-soluble polyurethane tackiness agent; 0.01～0.08 part of Sodium Persulfate; 0.15～0.75 part of dehydrated alcohol.
A kind of preparation method of above-mentioned environment-friendly curtain adhesive for hair product is characterized in that: carry out according to following steps:
Solidifying agent with alcohol-soluble polyurethane tackiness agent and alcohol-soluble polyurethane tackiness agent is a raw material, with water-soluble thermolysis type Sodium Persulfate is initiator, with sucrose ester and rosin is additive, with quantitative dehydrated alcohol is solvent, 30-90 ℃ of high temperature letex polymerization, the transformation efficiency 85-98% that is weight percentage, it is 40-80 ℃ that polyreaction finishes final vacuum degassing temperature, vacuum tightness is 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, drying are made solid phase prod, obtain environment-friendly curtain adhesive for hair product.
Environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, and shady and cool place preserves.
The present invention has following advantage: this method is an initiator with thermolysis type Sodium Persulfate, has avoided the use organo-peroxide to make initiator, and its resolvent remains in the pollution that causes in the glue; Replace low temperature polymerization with high temperature polymerization, can reduce energy consumption; Improve polymerization conversion, reduce and reclaim amount of monomer; Physics, the chemistry degassing combine, and shorten the degassing time, save energy consumption.
Embodiment
Embodiment 1: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 10 gram alcohol-soluble polyurethane tackiness agents and 5 gram alcohol-soluble polyurethane tackiness agents are raw material, with 1 gram Sodium Persulfate is initiator, 4 gram sucrose esters and 5 gram rosin are additive, are solvent with 15 gram dehydrated alcohols.
The making method of this kind environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 10 gram alcohol-soluble polyurethane tackiness agents and 5 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 1 gram is initiator, with 4 gram sucrose esters and 5 gram rosin is additive, with 15 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 2: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 12 gram alcohol-soluble polyurethane tackiness agents and 7 gram alcohol-soluble polyurethane tackiness agents are raw material, with 2 gram Sodium Persulfates is initiator, 6 gram sucrose esters and 7 gram rosin are additive, are solvent with 20 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 12 gram alcohol-soluble polyurethane tackiness agents and 7 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 2 grams is initiator, with 6 gram sucrose esters and 7 gram rosin is additive, with 20 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 3: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 14 gram alcohol-soluble polyurethane tackiness agents and 9 gram alcohol-soluble polyurethane tackiness agents are raw material, with 3 gram Sodium Persulfates is initiator, 5 gram sucrose esters and 8 gram rosin are additive, are solvent with 25 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 14 gram alcohol-soluble polyurethane tackiness agents and 9 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 3 grams is initiator, with 5 gram sucrose esters and 8 rosin is additive, with 25 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 4: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 16 gram alcohol-soluble polyurethane tackiness agents and 11 gram alcohol-soluble polyurethane tackiness agents are raw material, with 4 gram Sodium Persulfates is initiator, 10 gram sucrose esters and 10 gram rosin are additive, are solvent with 35 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 16 gram alcohol-soluble polyurethane tackiness agents and 11 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 4 grams is initiator, with 10 gram sucrose esters and 10 gram rosin is additive, with 35 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 5: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 18 gram alcohol-soluble polyurethane tackiness agents and 12 gram alcohol-soluble polyurethane tackiness agents are raw material, with 5 gram Sodium Persulfates is initiator, 12 gram sucrose esters and 13 gram rosin are additive, are solvent with 40 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 18 gram alcohol-soluble polyurethane tackiness agents and 12 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 5 grams is initiator, with 12 gram sucrose esters and 13 gram rosin is additive, with 40 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 6: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 20 gram alcohol-soluble polyurethane tackiness agents and 14 gram alcohol-soluble polyurethane tackiness agents are raw material, with 5.5 gram Sodium Persulfates is initiator, 14 gram sucrose esters and 15 gram rosin are additive, are solvent with 45 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 20 gram alcohol-soluble polyurethane tackiness agents and 14 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 6 grams is initiator, with 16 gram sucrose esters and 20 gram rosin is additive, with 55 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 7: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 40 gram alcohol-soluble polyurethane tackiness agents are raw material, with 8 gram Sodium Persulfates is initiator, 15 gram sucrose esters and 25 gram rosin are additive, are solvent with 75 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 40 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 8 grams is initiator, with 15 gram sucrose esters and 25 gram rosin is additive, with 75 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 8: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 400 gram alcohol-soluble polyurethane tackiness agents are raw material, with 80 gram Sodium Persulfates is initiator, 150 gram sucrose esters and 250 gram rosin are additive, are solvent with 750 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 400 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 80 grams is initiator, with 150 gram sucrose esters and 250 gram rosin is additive, with 750 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 9: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 500 gram alcohol-soluble polyurethane tackiness agents and 50 gram alcohol-soluble polyurethane tackiness agents are raw material, with 10 gram Sodium Persulfates is initiator, 40 gram sucrose esters and 50 gram rosin are additive, are solvent with 150 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 500 gram alcohol-soluble polyurethane tackiness agents and 50 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 10 grams is initiator, with 40 gram sucrose esters and 50 gram rosin is additive, with 150 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 10: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 400 gram alcohol-soluble polyurethane tackiness agents are raw material, with 10 gram Sodium Persulfates is initiator, 40 gram sucrose esters and 50 gram rosin are additive, are solvent with 150 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 400 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 10 grams is initiator, with 40 gram sucrose esters and 50 gram rosin is additive, with 150 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 11: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 50 gram alcohol-soluble polyurethane tackiness agents are raw material, with 80 gram Sodium Persulfates is initiator, 40 gram sucrose esters and 50 gram rosin are additive, are solvent with 150 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 50 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 80 grams is initiator, with 40 gram sucrose esters and 50 gram rosin is additive, with 150 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 12: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 50 gram alcohol-soluble polyurethane tackiness agents are raw material, with 10 gram Sodium Persulfates is initiator, 150 gram sucrose esters and 50 gram rosin are additive, are solvent with 150 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 50 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 10 grams is initiator, with 150 gram sucrose esters and 50 gram rosin is additive, with 150 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 13: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 50 gram alcohol-soluble polyurethane tackiness agents are raw material, with 10 gram Sodium Persulfates is initiator, 40 gram sucrose esters and 250 gram rosin are additive, are solvent with 150 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 50 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 10 grams is initiator, with 40 gram sucrose esters and 250 gram rosin is additive, with 150 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 14: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 50 gram alcohol-soluble polyurethane tackiness agents are raw material, with 10 gram Sodium Persulfates is initiator, 40 gram sucrose esters and 50 gram rosin are additive, are solvent with 750 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 50 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 10 grams is initiator, with 40 gram sucrose esters and 50 gram rosin is additive, with 750 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 15: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 100 gram alcohol-soluble polyurethane tackiness agents and 100 gram alcohol-soluble polyurethane tackiness agents are raw material, with 50 gram Sodium Persulfates is initiator, 100 gram sucrose esters and 100 gram rosin are additive, are solvent with 200 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 50 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 10 grams is initiator, with 40 gram sucrose esters and 50 gram rosin is additive, with 750 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 16: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 300 gram alcohol-soluble polyurethane tackiness agents and 200 gram alcohol-soluble polyurethane tackiness agents are raw material, with 60 gram Sodium Persulfates is initiator, 120 gram sucrose esters and 200 gram rosin are additive, are solvent with 500 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 300 gram alcohol-soluble polyurethane tackiness agents and 200 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 60 grams is initiator, with 120 gram sucrose esters and 200 gram rosin is additive, with 500 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 17: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 500 gram alcohol-soluble polyurethane tackiness agents and 400 gram alcohol-soluble polyurethane tackiness agents are raw material, with 80 gram Sodium Persulfates is initiator, 150 gram sucrose esters and 250 gram rosin are additive, are solvent with 750 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 500 gram alcohol-soluble polyurethane tackiness agents and 400 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 80 grams is initiator, with 150 gram sucrose esters and 250 gram rosin is additive, with 750 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 18: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 150 gram alcohol-soluble polyurethane tackiness agents and 150 gram alcohol-soluble polyurethane tackiness agents are raw material, with 40 gram Sodium Persulfates is initiator, 120 gram sucrose esters and 180 gram rosin are additive, are solvent with 550 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 150 gram alcohol-soluble polyurethane tackiness agents and 150 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 40 grams is initiator, with 120 gram sucrose esters and 180 gram rosin is additive, with 550 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 19: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 5 gram alcohol-soluble polyurethane tackiness agents and 40 gram alcohol-soluble polyurethane tackiness agents are raw material, with 1 gram Sodium Persulfate is initiator, 15 gram sucrose esters and 25 gram rosin are additive, are solvent with 15 gram dehydrated alcohols.
A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 5 gram alcohol-soluble polyurethane tackiness agents and 40 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 1 gram is initiator, with 15 gram sucrose esters and 25 gram rosin is additive, with 15 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Embodiment 20: a kind of environment-friendly curtain adhesive for hair product is that the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 5 gram alcohol-soluble polyurethane tackiness agents are raw material, with 1 gram Sodium Persulfate is initiator, 4 gram sucrose esters and 5 gram rosin are additive, are solvent with 75 gram dehydrated alcohols.A kind of making method of environment-friendly curtain adhesive for hair product is as follows: the solidifying agent with 50 gram alcohol-soluble polyurethane tackiness agents and 5 gram alcohol-soluble polyurethane tackiness agents is a raw material, with the water-soluble thermolysis type Sodium Persulfate of 1 gram is initiator, with 4 gram sucrose esters and 5 gram rosin is additive, with 75 gram dehydrated alcohols is solvent, 30-90 ℃ of high temperature letex polymerization, transformation efficiency 85-98%, polyreaction finishes 40-80 ℃ of final vacuum degassing temperature, vacuum tightness 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, dry, make solid phase prod, obtain environment-friendly curtain adhesive for hair product, environment-friendly curtain adhesive is adorned with blue thick PVC plastic tank sealing, shady and cool place preserves.
Claims (3)
1. an environment-friendly curtain adhesive for hair product is characterized in that: be fused into and get through compatibility according to parts by weight by following raw materials: 0.05～0.5 part in alcohol-soluble polyurethane tackiness agent; 0.04～0.15 part of sucrose ester; 0.05～0.25 part of rosin; 0.05～0.4 part in the solidifying agent of alcohol-soluble polyurethane tackiness agent; 0.01～0.08 part of Sodium Persulfate; 0.15～0.75 part of dehydrated alcohol.
2. the preparation method of an environment-friendly curtain adhesive for hair product as claimed in claim 1 is characterized in that: carry out according to following steps:
Solidifying agent with alcohol-soluble polyurethane tackiness agent and alcohol-soluble polyurethane tackiness agent is a raw material, with water-soluble thermolysis type Sodium Persulfate is initiator, with sucrose ester and rosin is additive, with quantitative dehydrated alcohol is solvent, 30-90 ℃ of high temperature letex polymerization, the transformation efficiency 85-98% that is weight percentage, it is 40-80 ℃ that polyreaction finishes final vacuum degassing temperature, vacuum tightness is 0.06-0.09MPa, degassing back residue alcohol-soluble polyurethane binder content is at 0-5ppm, cohesion, drying are made solid phase prod, obtain environment-friendly curtain adhesive for hair product.
3. the preparation method of environment-friendly curtain adhesive for hair product according to claim 2 is characterized in that: environment-friendly curtain adhesive is adorned the preservation of shady and cool place with blue thick PVC plastic tank sealing.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201010219645A CN101892028B (en) | 2010-07-07 | 2010-07-07 | Environment-friendly curtain adhesive for hair product and preparation method thereof |
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| CN201010219645A CN101892028B (en) | 2010-07-07 | 2010-07-07 | Environment-friendly curtain adhesive for hair product and preparation method thereof |
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| CN101892028A true CN101892028A (en) | 2010-11-24 |
| CN101892028B CN101892028B (en) | 2012-10-03 |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105614973A (en) * | 2015-12-25 | 2016-06-01 | 广东宏杰内衣实业有限公司 | Hemming technology for brassiere with no frame |
| CN106010418A (en) * | 2016-06-20 | 2016-10-12 | 郑州大学 | Environment-friendly high-strength polyurethane adhesive for wig hair weft glue and preparation method of polyurethane adhesive |
| CN113382834A (en) * | 2018-11-21 | 2021-09-10 | 绿色科技全球私人有限公司 | Novel aqueous binder using sugar fatty acid ester |
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| CN1077625A (en) * | 1993-04-07 | 1993-10-27 | 徐景辉 | Mousse rubber cement and manufacture method thereof |
| CN1590425A (en) * | 2003-04-04 | 2005-03-09 | 中国石油天然气集团公司 | Synthesis method of high conversion food grade styrene butadiene rubber |
| JP2009221445A (en) * | 2008-03-19 | 2009-10-01 | Nippon Fuirin Kk | Rubber adhesive for wig |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105614973A (en) * | 2015-12-25 | 2016-06-01 | 广东宏杰内衣实业有限公司 | Hemming technology for brassiere with no frame |
| CN106010418A (en) * | 2016-06-20 | 2016-10-12 | 郑州大学 | Environment-friendly high-strength polyurethane adhesive for wig hair weft glue and preparation method of polyurethane adhesive |
| CN106010418B (en) * | 2016-06-20 | 2019-08-23 | 郑州大学 | Environment protection type high-strength wig curtain adhesive polyurethane adhesive and preparation method thereof |
| CN113382834A (en) * | 2018-11-21 | 2021-09-10 | 绿色科技全球私人有限公司 | Novel aqueous binder using sugar fatty acid ester |
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| CN101892028B (en) | 2012-10-03 |
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