CN105838282A - Loquat leaf polysaccharide-sesame seed protein modified starch-based cigarette lapping adhesive and preparation method thereof - Google Patents
Loquat leaf polysaccharide-sesame seed protein modified starch-based cigarette lapping adhesive and preparation method thereof Download PDFInfo
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- CN105838282A CN105838282A CN201610242194.5A CN201610242194A CN105838282A CN 105838282 A CN105838282 A CN 105838282A CN 201610242194 A CN201610242194 A CN 201610242194A CN 105838282 A CN105838282 A CN 105838282A
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- China
- Prior art keywords
- cigarette
- polysaccharide
- protein
- modified starch
- folium eriobotryae
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J103/00—Adhesives based on starch, amylose or amylopectin or on their derivatives or degradation products
- C09J103/02—Starch; Degradation products thereof, e.g. dextrin
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses a loquat leaf polysaccharide-sesame seed protein modified starch-based cigarette lapping adhesive which is prepared from the following raw materials in parts by weight: 30-40 parts of cassava starch, 0.5-1 part of southernwood, 0.3-0.5 part of snake gourd peel, 0.3-0.5 part of mint, 0.3-0.5 part of sodium polyacrylate, 0.5-1 part of sesame seed protein, 2-4 parts of soybean protein, 0.5-1 part of fructose, 0.3-0.5 part of loquat leaf polysaccharide, 0.05-0.1 part of papain, 1-2 parts of sodium borate, 0.3-0.5 part of tamarind seed gum and 3-5 parts of glycerol. The cigarette lapping adhesive has the advantages of favorable adhesiveness, favorable rheological behavior and high stability, is suitable for high-speed cigarette making machines, is capable of improving the suction flavor of the cigarette and reducing the hazards of the harmful ingredients in the cigarette for the human body, has the auxiliary effects of clearing away the lungheat, moistening dryness and clearing away heat and toxic material, and has high use value and high practicality.
Description
Technical field
The present invention relates to cigarette material technical field, particularly relate to a kind of Folium Eriobotryae polysaccharide-sesame protein modified starch base cigarette mouth building adhesive and preparation method thereof.
Background technology
Adhesive is one of raw and auxiliary material important in production of cigarettes manufacture process, all refers to adhesive in a lot of production of cigarettes operations, mainly includes overlapping glue, spigot joint glue, filter stick centre-line glue, packaging glue and aluminum foil composite glue etc..At present, using most common cigarette glue stick is polyvinyl acetate emulsion class adhesive, and it possesses the adhesive property of excellence, rheological property etc., it is possible to adapts to the requirement of high-speed cigarette machine, meets the needs of large-scale production.But the special odor that the residual monomer of synthetic latex and plasticizer etc. have can bring certain impact to Sensory Quality of Cigarette, and affects the biological safety of cigarette product simultaneously.
Starchiness adhesive belongs to natural class adhesive, has environmental protection, cheap, the advantage of wide material sources, has had been subjected to increasing concern as cigarette glue stick.But, the most a lot of starchiness adhesive bonds performance, mobile performance and rate of drying are the most undesirable, the problem such as when there is production, speed is low, viscosity is poor, glue poor stability, it is difficult to adapt to the demand that high-speed cigarette machine mass rapid produces.Simultaneously, owing to overlapping glue stick directly participates in the burning of cigarette, the suction taste of Medicated cigarette can be produced impact, therefore, for making starchiness cigarette mouth building adhesive obtain widely promotion and application, it is necessary to improve its viscosity, mobility and stability, reduces the negative effect to cigarette odor-absorbing simultaneously, promote suction comfortableness.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of gumminess is good, stability is high, be suitable for high-speed cigarette machine uses, and Folium Eriobotryae polysaccharide-sesame protein modified starch base cigarette mouth building adhesive that cigarette odor-absorbing can be improved and preparation method thereof.
The present invention is achieved by the following technical solutions:
A kind of Folium Eriobotryae polysaccharide-sesame protein modified starch base cigarette mouth building adhesive, it is to be prepared by the raw material of following weight parts:
Tapioca 30-40, Herba Artemisiae Annuae 0.5-1, Fructus Trichosanthis skin 0.3-0.5, Herba Menthae 0.3-0.5, sodium polyacrylate 0.3-0.5, sesame protein 0.5-1, soybean protein 2-4, fructose 0.5-1, Folium Eriobotryae polysaccharide 0.3-0.5, papain 0.05-0.1, Borax 1-2, tamarind seed glue 0.3-0.5, glycerol 3-5.
The preparation method of a kind of Folium Eriobotryae polysaccharide-sesame protein modified starch base cigarette mouth building adhesive, comprises the following steps:
(1) raw material is weighed by weight, by Herba Artemisiae Annuae, Fructus Trichosanthis skin, Herba Menthae grind into powder and mix with tapioca, mix homogeneously with the sodium hydroxide solution of 3-5% by solid-liquid weight ratio 1:1-1:1.5, it is subsequently adding sodium polyacrylate, 60-70 DEG C of tamarind seed glue stirring 20-30min, after cooling, obtains modified tapioca starch；
(2) soybean protein, sesame protein are added to the water by solid-liquid weight ratio 1:6-1:8 stir, it is subsequently adding papain prior to 40-50 DEG C of stirring 1-2h, add Folium Eriobotryae polysaccharide and stir 5-10min in 90-95 DEG C, be subsequently adding fructose, glycerol stirs 1-2h in 70-80 DEG C, obtains compound protein modifying agent after cooling；
(3) after being mixed with the compound protein modifying agent in (2) by the modified tapioca starch in (1), 50-70 DEG C of stirring 0.5-1h, adds remaining raw material mix homogeneously, obtains Folium Eriobotryae polysaccharide-sesame protein modified starch base cigarette mouth building adhesive after cooling.
The invention have the advantage that
The present invention is utilized respectively Folium Eriobotryae polysaccharide, fructose carries out Maillard reaction with the sesame protein of papain partial hydrolysis, soybean protein makes sugar obtain sugar-albumen composition with albumen grafting, sodium polyacrylate and alkali is utilized to carry out tapioca mixed and modified obtaining modified starch, then both are mixed, under the assosting effect of the raw material such as sodium polyacrylate, Borax, sugar-can form firm network structure between albumen composition and modified starch, is therefore effectively improved adhesion strength and the stability of adhesive；And owing to Maillard reaction produces certain flavor substance, effect of Medicated cigarette flavouring can be played, promote the smoking quality of Medicated cigarette；Simultaneously, utilize Herba Artemisiae Annuae, Fructus Trichosanthis skin, the interpolation of Herba Menthae isoreactivity composition and compound, the cigarette mouth building adhesive obtained is made not only to have good glueability and rheological property, good stability, it is adaptable to high-speed cigarette machine, and cigarette odor-absorbing can be improved, the harm to human body of the harmful components that alleviate in Medicated cigarette, also has clearing away lung-heat and moistening for dryness, auxiliary effect of heat-clearing and toxic substances removing, use value is high, practical.
Detailed description of the invention
A kind of Folium Eriobotryae polysaccharide-sesame protein modified starch base cigarette mouth building adhesive, it is to be prepared by the raw material of following weight parts:
Tapioca 30, Herba Artemisiae Annuae 0.5, Fructus Trichosanthis skin 0.3, Herba Menthae 0.3, sodium polyacrylate 0.3, sesame protein 0.5, soybean protein 2, fructose 0.5, Folium Eriobotryae polysaccharide 0.3, papain 0.05, Borax 1, tamarind seed glue 0.3, glycerol 3.
The preparation method of a kind of Folium Eriobotryae polysaccharide-sesame protein modified starch base cigarette mouth building adhesive, comprises the following steps:
(1) raw material is weighed by weight, by Herba Artemisiae Annuae, Fructus Trichosanthis skin, Herba Menthae grind into powder and mix with tapioca, by solid-liquid weight ratio 1:1 and the sodium hydroxide solution mix homogeneously of 3%, it is subsequently adding sodium polyacrylate, 60 DEG C of tamarind seed glue stirring 20min, after cooling, obtains modified tapioca starch；
(2) soybean protein, sesame protein are added to the water by solid-liquid weight ratio 1:6 stir, it is subsequently adding papain prior to 40 DEG C of stirring 1h, add Folium Eriobotryae polysaccharide in 90 DEG C stir 5min, be subsequently adding fructose, glycerol in 70 DEG C stir 1h, after cooling compound protein modifying agent；
(3) modified tapioca starch in (1) is mixed rear 50 DEG C of stirring 0.5h with the compound protein modifying agent in (2), add remaining raw material mix homogeneously after cooling, obtain Folium Eriobotryae polysaccharide-sesame protein modified starch base cigarette mouth building adhesive.
Above-mentioned prepared cigarette mouth building adhesive has good viscosity and mobility, at normal temperatures, can keep stable within three months.Under the conditions of the cigarette machine of speed of operation 10000/minute uses, equipment normal operation, steadily, it is firmly neat that the even patch of mouth taken by the cigarette sample rolled, and does not has alice phenomenon.Obtained cigarette sample sensory evaluating smoking's result is better than common overlapping glue cigarette sample.
Claims (2)
1. Folium Eriobotryae polysaccharide-sesame protein modified starch base cigarette mouth building adhesive, it is characterised in that it is to be prepared by the raw material of following weight parts:
Tapioca 30-40, Herba Artemisiae Annuae 0.5-1, Fructus Trichosanthis skin 0.3-0.5, Herba Menthae 0.3-0.5, sodium polyacrylate 0.3-0.5, sesame protein 0.5-1, soybean protein 2-4, fructose 0.5-1, Folium Eriobotryae polysaccharide 0.3-0.5, papain 0.05-0.1, Borax 1-2, tamarind seed glue 0.3-0.5, glycerol 3-5.
The preparation method of a kind of Folium Eriobotryae polysaccharide the most according to claim 1-sesame protein modified starch base cigarette mouth building adhesive, it is characterised in that comprise the following steps:
(1) raw material is weighed by weight, by Herba Artemisiae Annuae, Fructus Trichosanthis skin, Herba Menthae grind into powder and mix with tapioca, mix homogeneously with the sodium hydroxide solution of 3-5% by solid-liquid weight ratio 1:1-1:1.5, it is subsequently adding sodium polyacrylate, 60-70 DEG C of tamarind seed glue stirring 20-30min, after cooling, obtains modified tapioca starch；
(2) soybean protein, sesame protein are added to the water by solid-liquid weight ratio 1:6-1:8 stir, it is subsequently adding papain prior to 40-50 DEG C of stirring 1-2h, add Folium Eriobotryae polysaccharide and stir 5-10min in 90-95 DEG C, be subsequently adding fructose, glycerol stirs 1-2h in 70-80 DEG C, obtains compound protein modifying agent after cooling；
(3) after being mixed with the compound protein modifying agent in (2) by the modified tapioca starch in (1), 50-70 DEG C of stirring 0.5-1h, adds remaining raw material mix homogeneously, obtains Folium Eriobotryae polysaccharide-sesame protein modified starch base cigarette mouth building adhesive after cooling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610242194.5A CN105838282A (en) | 2016-04-19 | 2016-04-19 | Loquat leaf polysaccharide-sesame seed protein modified starch-based cigarette lapping adhesive and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610242194.5A CN105838282A (en) | 2016-04-19 | 2016-04-19 | Loquat leaf polysaccharide-sesame seed protein modified starch-based cigarette lapping adhesive and preparation method thereof |
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| CN105838282A true CN105838282A (en) | 2016-08-10 |
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| CN201610242194.5A Pending CN105838282A (en) | 2016-04-19 | 2016-04-19 | Loquat leaf polysaccharide-sesame seed protein modified starch-based cigarette lapping adhesive and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111231424A (en) * | 2020-02-20 | 2020-06-05 | 上海乐盈纸业有限公司 | Corrugated board and production process thereof |
| CN114271527A (en) * | 2022-01-07 | 2022-04-05 | 云南猫哆哩集团食品有限责任公司 | Adhesive for special reconstituted tobacco for heating non-combustible cigarettes and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1586339A (en) * | 2004-09-13 | 2005-03-02 | 南阳卷烟厂 | Cigarette product containing Chinese herbal medicine |
| CN103773276A (en) * | 2014-01-16 | 2014-05-07 | 常州大学 | Preparation method for environment-friendly starch cigarette adhesive |
| CN103773269A (en) * | 2012-10-20 | 2014-05-07 | 中国烟草总公司郑州烟草研究院 | Novel amyloid cigarette adhesive containing synthetic polymer |
| CN103865645A (en) * | 2012-12-11 | 2014-06-18 | 爱普香料集团股份有限公司 | Preparation method of fruit concentrate Maillard reaction product, and application of product in tobacco perfuming |
-
2016
- 2016-04-19 CN CN201610242194.5A patent/CN105838282A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1586339A (en) * | 2004-09-13 | 2005-03-02 | 南阳卷烟厂 | Cigarette product containing Chinese herbal medicine |
| CN103773269A (en) * | 2012-10-20 | 2014-05-07 | 中国烟草总公司郑州烟草研究院 | Novel amyloid cigarette adhesive containing synthetic polymer |
| CN103865645A (en) * | 2012-12-11 | 2014-06-18 | 爱普香料集团股份有限公司 | Preparation method of fruit concentrate Maillard reaction product, and application of product in tobacco perfuming |
| CN103773276A (en) * | 2014-01-16 | 2014-05-07 | 常州大学 | Preparation method for environment-friendly starch cigarette adhesive |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111231424A (en) * | 2020-02-20 | 2020-06-05 | 上海乐盈纸业有限公司 | Corrugated board and production process thereof |
| CN114271527A (en) * | 2022-01-07 | 2022-04-05 | 云南猫哆哩集团食品有限责任公司 | Adhesive for special reconstituted tobacco for heating non-combustible cigarettes and preparation method thereof |
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Application publication date: 20160810 |
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