CN105802537A - Tremella polysaccharide and sticky rice protein modified starch-based cigarette lap adhesive and preparation method thereof - Google Patents
Tremella polysaccharide and sticky rice protein modified starch-based cigarette lap adhesive and preparation method thereof Download PDFInfo
- Publication number
- CN105802537A CN105802537A CN201610242192.6A CN201610242192A CN105802537A CN 105802537 A CN105802537 A CN 105802537A CN 201610242192 A CN201610242192 A CN 201610242192A CN 105802537 A CN105802537 A CN 105802537A
- Authority
- CN
- China
- Prior art keywords
- tremella polysaccharide
- cigarette
- adhesive
- oryza glutinosa
- modified starch
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J103/00—Adhesives based on starch, amylose or amylopectin or on their derivatives or degradation products
- C09J103/02—Starch; Degradation products thereof, e.g. dextrin
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/08—Macromolecular additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses a tremella polysaccharide and sticky rice protein modified starch-based cigarette lap adhesive. The adhesive is prepared from, by weight, 30-40 parts of sticky rice starch, 0.5-1 part of lilies, 0.3-0.5 part of radix ophiopogonis, 0.3-0.5 part of honeysuckles, 0.3-0.5 part of sodium polyacrylate, 0.3-0.5 part of tremella polysaccharide, 3-5 parts of sticky rice protein, 0.5-1 part of fructose, 0.05-0.1 part of papain, 1-2 parts of borax, 3-5 parts of glycerin, 3-5 parts of snow pear juice and 0.3-0.5 part of sodium phytate. The cigarette lap adhesive is good in adhesive performance, good in rheological property and stable, is suitable for a high-speed cigarette making machine, can improve the smoking taste of cigarettes, reduces harm of harmful components in the cigarette to human bodies, has the auxiliary effects of clearing away heat and toxin, clearing away the lung-heat and moistening the throat, and is high in use value and high in practicality.
Description
Technical field
The present invention relates to cigarette material technical field, particularly relate to a kind of tremella polysaccharide-Oryza glutinosa protein modified starch base cigarette mouth building adhesive and preparation method thereof.
Background technology
Adhesive is one of raw and auxiliary material important in production of cigarettes manufacture process, all refers to adhesive in a lot of production of cigarettes operations, mainly includes overlapping glue, spigot joint glue, filter stick centre-line glue, packaging glue and aluminum foil composite glue etc..At present, using most common cigarette glue stick is polyvinyl acetate emulsion class adhesive, and it possesses the adhesive property of excellence, rheological property etc., it is possible to adapts to the requirement of high-speed cigarette machine, meets the needs of large-scale production.But the special odor that the residual monomer of synthetic latex and plasticizer etc. have can bring certain impact to Sensory Quality of Cigarette, and affects the biological safety of cigarette product simultaneously.
Starchiness adhesive belongs to natural class adhesive, has environmental protection, cheap, the advantage of wide material sources, has had been subjected to increasing concern as cigarette glue stick.But, the most a lot of starchiness adhesive bonds performance, mobile performance and rate of drying are the most undesirable, the problem such as when there is production, speed is low, viscosity is poor, glue poor stability, it is difficult to adapt to the demand that high-speed cigarette machine mass rapid produces.Simultaneously, owing to overlapping glue stick directly participates in the burning of cigarette, the suction taste of Medicated cigarette can be produced impact, therefore, for making starchiness cigarette mouth building adhesive obtain widely promotion and application, it is necessary to improve its viscosity, mobility and stability, reduces the negative effect to cigarette odor-absorbing simultaneously, promote suction comfortableness.
Summary of the invention
The object of the invention is contemplated to make up the defect of prior art, it is provided that a kind of gumminess is good, stability is high, be suitable for high-speed cigarette machine uses, and tremella polysaccharide-Oryza glutinosa protein modified starch base cigarette mouth building adhesive that cigarette odor-absorbing can be improved and preparation method thereof.
The present invention is achieved by the following technical solutions:
A kind of tremella polysaccharide-Oryza glutinosa protein modified starch base cigarette mouth building adhesive, it is to be prepared by the raw material of following weight parts:
Glutinous rice starch 30-40, Bulbus Lilii 0.5-1, Radix Ophiopogonis 0.3-0.5, Flos Lonicerae 0.3-0.5, sodium polyacrylate 0.3-0.5, tremella polysaccharide 0.3-0.5, Oryza glutinosa albumen 3-5, fructose 0.5-1, papain 0.05-0.1, Borax 1-2, glycerol 3-5, snow pear juice 3-5, sodium phytate 0.3-0.5.
The preparation method of a kind of tremella polysaccharide-Oryza glutinosa protein modified starch base cigarette mouth building adhesive, comprises the following steps:
(1) raw material is weighed by weight, by Bulbus Lilii, Radix Ophiopogonis, Flos Lonicerae grind into powder and mix with glutinous rice starch, mix homogeneously with the sodium hydroxide solution of 3-5% by solid-liquid weight ratio 1:1-1:1.5, be subsequently adding sodium polyacrylate 60-70 DEG C stirring 20-30min, after cooling, obtain modified glutinous rice starch；
(2) Oryza glutinosa albumen is added to the water by solid-liquid weight ratio 1:6-1:8 stirs, it is subsequently adding papain prior to 40-50 DEG C of stirring 1-2h, add tremella polysaccharide and stir 5-10min in 90-95 DEG C, be subsequently adding fructose, glycerol stirs 1-2h in 70-80 DEG C, obtains compound protein modifying agent after cooling；
(3) after being mixed with the compound protein modifying agent in (2) by the modified glutinous rice starch in (1), 50-70 DEG C of stirring 0.5-1h, adds remaining raw material mix homogeneously, obtains tremella polysaccharide-Oryza glutinosa protein modified starch base cigarette mouth building adhesive after cooling.
The invention have the advantage that
The present invention is utilized respectively tremella polysaccharide, the Oryza glutinosa albumen of fructose and papain partial hydrolysis carries out Maillard reaction makes sugar obtain sugar-albumen composition with albumen grafting, sodium polyacrylate and alkali is utilized to carry out glutinous rice starch mixed and modified obtaining modified starch, then both are mixed, under the assosting effect of the raw material such as sodium polyacrylate, Borax, sugar-can form firm network structure between albumen composition and modified starch, is therefore effectively improved adhesion strength and the stability of adhesive；And owing to Maillard reaction produces certain flavor substance, effect of Medicated cigarette flavouring can be played, promote the smoking quality of Medicated cigarette；Simultaneously, utilize Bulbus Lilii, Radix Ophiopogonis, the interpolation of Flos Lonicerae isoreactivity composition and compound, the cigarette mouth building adhesive obtained is made not only to have good glueability and rheological property, good stability, be applicable to high-speed cigarette machine, and cigarette odor-absorbing can be improved, the harm to human body of the harmful components that alleviate in Medicated cigarette, auxiliary effect that also heat-clearing and toxic substances removing, lung heat clearing wet one's whistle, use value is high, practical.
Detailed description of the invention
A kind of tremella polysaccharide-Oryza glutinosa protein modified starch base cigarette mouth building adhesive, it is to be prepared by the raw material of following weight parts:
Glutinous rice starch 30, Bulbus Lilii 0.5, Radix Ophiopogonis 0.3, Flos Lonicerae 0.3, sodium polyacrylate 0.3, tremella polysaccharide 0.3, Oryza glutinosa albumen 3, fructose 0.5, papain 0.05, Borax 1, glycerol 3, snow pear juice 3, sodium phytate 0.3.
The preparation method of a kind of tremella polysaccharide-Oryza glutinosa protein modified starch base cigarette mouth building adhesive, comprises the following steps:
(1) raw material is weighed by weight, by Bulbus Lilii, Radix Ophiopogonis, Flos Lonicerae grind into powder and mix with glutinous rice starch, by solid-liquid weight ratio 1:1 and the sodium hydroxide solution mix homogeneously of 3%, it is subsequently adding sodium polyacrylate 60 DEG C stirring 20min, after cooling, obtains modified glutinous rice starch；
(2) Oryza glutinosa albumen is added to the water by solid-liquid weight ratio 1:6 stirs, it is subsequently adding papain prior to 40 DEG C of stirring 1h, add tremella polysaccharide in 90 DEG C stir 5min, be subsequently adding fructose, glycerol in 70 DEG C stir 1h, after cooling compound protein modifying agent；
(3) the modified glutinous rice starch in (1) is mixed rear 50 DEG C of stirring 0.5h with the compound protein modifying agent in (2), add remaining raw material mix homogeneously after cooling, obtain tremella polysaccharide-Oryza glutinosa protein modified starch base cigarette mouth building adhesive.
Above-mentioned prepared cigarette mouth building adhesive has good viscosity and mobility, at normal temperatures, can keep stable within three months.Under the conditions of the cigarette machine of speed of operation 10000/minute uses, equipment normal operation, steadily, it is firmly neat that the even patch of mouth taken by the cigarette sample rolled, and does not has alice phenomenon.Obtained cigarette sample sensory evaluating smoking's result is better than common overlapping glue cigarette sample.
Claims (2)
1. tremella polysaccharide-Oryza glutinosa protein modified starch base cigarette mouth building adhesive, it is characterised in that it is to be prepared by the raw material of following weight parts:
Glutinous rice starch 30-40, Bulbus Lilii 0.5-1, Radix Ophiopogonis 0.3-0.5, Flos Lonicerae 0.3-0.5, sodium polyacrylate 0.3-0.5, tremella polysaccharide 0.3-0.5, Oryza glutinosa albumen 3-5, fructose 0.5-1, papain 0.05-0.1, Borax 1-2, glycerol 3-5, snow pear juice 3-5, sodium phytate 0.3-0.5.
The preparation method of a kind of tremella polysaccharide-Oryza glutinosa the most according to claim 1 protein modified starch base cigarette mouth building adhesive, it is characterised in that comprise the following steps:
(1) raw material is weighed by weight, by Bulbus Lilii, Radix Ophiopogonis, Flos Lonicerae grind into powder and mix with glutinous rice starch, mix homogeneously with the sodium hydroxide solution of 3-5% by solid-liquid weight ratio 1:1-1:1.5, be subsequently adding sodium polyacrylate 60-70 DEG C stirring 20-30min, after cooling, obtain modified glutinous rice starch；
(2) Oryza glutinosa albumen is added to the water by solid-liquid weight ratio 1:6-1:8 stirs, it is subsequently adding papain prior to 40-50 DEG C of stirring 1-2h, add tremella polysaccharide and stir 5-10min in 90-95 DEG C, be subsequently adding fructose, glycerol stirs 1-2h in 70-80 DEG C, obtains compound protein modifying agent after cooling；
(3) after being mixed with the compound protein modifying agent in (2) by the modified glutinous rice starch in (1), 50-70 DEG C of stirring 0.5-1h, adds remaining raw material mix homogeneously, obtains tremella polysaccharide-Oryza glutinosa protein modified starch base cigarette mouth building adhesive after cooling.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610242192.6A CN105802537A (en) | 2016-04-19 | 2016-04-19 | Tremella polysaccharide and sticky rice protein modified starch-based cigarette lap adhesive and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610242192.6A CN105802537A (en) | 2016-04-19 | 2016-04-19 | Tremella polysaccharide and sticky rice protein modified starch-based cigarette lap adhesive and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105802537A true CN105802537A (en) | 2016-07-27 |
Family
ID=56458175
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610242192.6A Pending CN105802537A (en) | 2016-04-19 | 2016-04-19 | Tremella polysaccharide and sticky rice protein modified starch-based cigarette lap adhesive and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105802537A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101629019A (en) * | 2009-01-21 | 2010-01-20 | 郑州佰沃生物质材料有限公司 | Basic biomass synthetic resin and preparation method and application thereof |
| CN103773269A (en) * | 2012-10-20 | 2014-05-07 | 中国烟草总公司郑州烟草研究院 | Novel amyloid cigarette adhesive containing synthetic polymer |
| CN103773276A (en) * | 2014-01-16 | 2014-05-07 | 常州大学 | Preparation method for environment-friendly starch cigarette adhesive |
| CN103865645A (en) * | 2012-12-11 | 2014-06-18 | 爱普香料集团股份有限公司 | Preparation method of fruit concentrate Maillard reaction product, and application of product in tobacco perfuming |
-
2016
- 2016-04-19 CN CN201610242192.6A patent/CN105802537A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101629019A (en) * | 2009-01-21 | 2010-01-20 | 郑州佰沃生物质材料有限公司 | Basic biomass synthetic resin and preparation method and application thereof |
| CN103773269A (en) * | 2012-10-20 | 2014-05-07 | 中国烟草总公司郑州烟草研究院 | Novel amyloid cigarette adhesive containing synthetic polymer |
| CN103865645A (en) * | 2012-12-11 | 2014-06-18 | 爱普香料集团股份有限公司 | Preparation method of fruit concentrate Maillard reaction product, and application of product in tobacco perfuming |
| CN103773276A (en) * | 2014-01-16 | 2014-05-07 | 常州大学 | Preparation method for environment-friendly starch cigarette adhesive |
Non-Patent Citations (1)
| Title |
|---|
| 曾晓鹰 等: "《卷烟调香体系构建 以云烟品牌为例》", 28 February 2013, 西南交通大学出版社 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102181247B (en) | Water-based superspeed cigarette lap adhesive and preparation method thereof | |
| CN105838282A (en) | Loquat leaf polysaccharide-sesame seed protein modified starch-based cigarette lapping adhesive and preparation method thereof | |
| CN105907331A (en) | A cigarette mouth building adhesive based on mulberry leaf polysaccharide-soybean protein modified starch and a preparing method thereof | |
| CN103393008A (en) | Nutrition-equalized purple crystal composite rice and preparation method thereof | |
| CN105802536A (en) | High-toughness and waterproof modified starch-base cigarette lapping adhesive and preparing method thereof | |
| CN105802537A (en) | Tremella polysaccharide and sticky rice protein modified starch-based cigarette lap adhesive and preparation method thereof | |
| CN105802540A (en) | Pumpkin polysaccharide-soybean protein modified starch based cigarette mouth building adhesive and preparation method thereof | |
| CN103360985B (en) | A kind of natural rubber packaging adhesive and preparation method thereof | |
| CN1927075B (en) | Cigarette lamina adhesive additive and preparation method thereof | |
| CN105802539A (en) | Astragalus polysaccharide-wheat protein modified starch based cigarette lap joint adhesion agent and preparation method thereof | |
| CN105907330A (en) | A cigarette mouth building adhesive based on shiitake polysaccharide-peanut protein modified starch and a preparing method thereof | |
| CN105838281A (en) | Aloe polysaccharide-rice protein modified starch-based cigarette lap adhesive and preparation method thereof | |
| CN105802538A (en) | Isatis root polysaccharide-wheat protein modified starch-based cigarette lap opening adhesive and preparation method thereof | |
| CN105747265A (en) | Fresh-scent type tobacco sheet tobacco shreds and preparing method thereof | |
| CN105802535A (en) | Nanocarbon-containing modified starch-based cigarette lap adhesive and preparation method thereof | |
| CN105802534A (en) | Low-temperature-resistant modified-starch-based cigarette holder adhesive and preparation method thereof | |
| CN105820773A (en) | Ginkgo biloba polysaccharide and soybean protein modified starch-base cigarette lap adhesive and preparation method thereof | |
| CN105907332A (en) | A cigarette mouth building adhesive based on Chinese date polysaccharide-soybean protein modified starch and a preparing method thereof | |
| CN105860874A (en) | Sophora japonica polysaccharide-wheat protein modified starch-based cigarette lap adhesive and preparation method thereof | |
| CN105768188A (en) | Sheet tobacco shred containing pine bark and preparation method thereof | |
| CN105768196A (en) | Sheet tobacco shred containing water chestnut hull and preparation method thereof | |
| CN105768183A (en) | Tobacco flakes capable of soothing the nerves and aiding sleep and production method thereof | |
| CN105860875A (en) | Eucommia polysaccharide-soy protein modified starch based cigarette lap joint adhesive and preparation method thereof | |
| CN104946163B (en) | High-speed cigarette machine modified starch base adhesive | |
| CN105111972B (en) | Preparation method of adhesive for cigarette packaging |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20160727 |